REPORT ON MONAZITE PROPERTIES OF FOOTE MINERIOS INDUSTRIALIZADOS LIMITADA (FOMIL)

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CIA-RDP80-00926A000600040002-1
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RIPPUB
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R
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37
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December 15, 2016
Document Release Date: 
December 14, 2001
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2
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Publication Date: 
October 26, 1948
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REPORT
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COUNTRY SUBJECT PLACE ACQUIRED 25X1A DATE ACQUIRED CLASS1F ICA ION Approved For ReovispRi 0 INFOR Bras ii ack1,11,926A0006RM:RA0?,1 PORT 25X1A 1 P&P 376 DATE DISTR. 26 Oct 1948 Report on Monastte Properties of Foote Minerios NO. OF PAGES 1 Zadustrialisados Limited& (FOUM) *DOE Review Completed* NO. OF ENCLS. (LISTED BELOW) *DO SUPPLEMENT TO ? 25X1X REPORT NO. SOURCE Documentar7 Awallable on leen from the CIA Library is a Report on Monasite Properties of Foote Minerles indestrielisaies Limited& (FOAW, dated 27 Sep 49, and prepared by NW lichal. Urger and Reward R Xremers, Vice.President and Director of Research, respectively, of Lindsay Iightlt Chemical Ce, manufacturers of rare earth chemicals. Dr tremere is a graituate geologist and holds a PhD in chemical.engineeri3g, The report includes 17 pictures of the monazite properties end processing operations and also three pictures and brief comment on POMLLeis beryl mine at Sepacia4 Also included in the report are Dr Kremerst comments on The Foote Mineral Co Report on Foote Minerios Indsetrialisados, Ltd 25X1A ? end CLASSIFICATION ReSTRECTED/IIS OFFICIALS ONLY STATE X NAVY X AIR x NSRO AEC DISTRIBUTION ARMYIi J RESTRICTED Approved For Release 2003/10/02 : CIA-RDP80-00926A000600040002-1 LA .;SSII-IGAIION / , '- 'Approved For Relamig 3i 1NFOR COUNTRY Brazil SUBJECT Report on Monazite Properties of Foote Minerlos Industrialized?, Limitada (70MIL) fiet,26A0006ofwef2ilo PORT PLACE ACQUIRED DATE ACQUIRED 25X1A 25X1A DATE DISTR. 26 Oct 1948 NO. OF PAGES 1 NO. OF ENCS. (LISTED BELOW) SUPPLEMENT TO REPORT NO. 25X1X SOURCE Documentary awailAble on lonn froA the CLA Library is a Report on Monazite Propertila Or Ioo.e Mlneries Industrializaios dated 27 Sep 48, and nreper,i 4 NW Mchel berger and Howard II Kremars, Vice-President and Director of research, raip)otively, of Lindsay Light A Chemical Co. manufacturers of rare earth chemicals. ;Jr tremers is a graduate geologist and holds a PhD in chemical engineering. The report includes 17 pictures of the monazite properties and processing operatic-41e end also three pictures and brief comment on YOMILes beryl mins at Sapacia. Also included in the report are Dr Krenerst c mmants on The Foote Mineral Co report on Foote Minerios Industrializados, Ltd 25X1A STATE ARMY ? R fiLt end . UMRABY 25X1A CLASSIFICATION 10.18TRICTED/u3 orincIALs CHU NAVY Ix MP N$RB AEC DISTRISUTION TI ; RESTRICTED Approved For Release 2003/10/02: CIA-RDP80-00926A000600040002-1 25X1X Approved For Release 2003/10/02 : CIA-RDP80-00926A000600040002-1 Next 1 Page(s) In Document Exempt Approved For Release 2003/10/02 : CIA-RDP80-00926A000600040002-1 ;STANDARD FORM VICPIC 6 4Akfroved For Release 20 ? ITORIDP80-00926A000600040002-1 -Office Memorandum ? UNITED STATES GOVERNMENT TO .Liaison Branch, 1318 "M" Building FROM Chief, Graphics Register, OCD SUBJECT: Enclosures - DATE: 28 October 1948 25X1A 1. We have the reports, but we do not have the enclosures to these reports. Please send us the enclosures so we may include them in our files. I ? //t.44,.//e i?itc74,14(1 #44, agzr rte/tel,74 iit 4/? Approved For Release 2003/10/02 80-00926A000600040002-1 25X1A 25X1A 3 )/ .1" 11111 11111111E111E11111 111 1 III 111111111111111111111E111 11111111111111111?1?11?1111.1111?MIIIIMME1111?111111111111 1 111111111111111111111111111?1111111111111111111111111.11111111 11111111111111 1111111111111111111111111111E11111111 1111111111111111111111 Approved For Release 2003/10/02 : CIA-RDP80-00926A000600040002-1 RESUMED Liaison Branch, 1318 "8. Building Chief, Graphics Register* 9CD linclosures 28 October 1948 25X1A 1. We have the repcits, but we do not have the enclosures to these ?north. Please send us the enclosures so we msy include thee in our files. Approved For OSTRICH) elease 200 1 ; ? 2 L i nomg ciAi-RbP8v-o0926Agoo6000Ll000z-i -4 1 ilt, 25X1A Approved ForReleardOMUM 80-00926A000600040002-1 Lie RESTRIaksay Light 4 Chemical CampAqy WOOS ON momarE normus OF FOOTE MINIMS INDUSTMALIZADOS =ITALIA (roma) Vitoria, E. L, Unto', Brazil liehelberger and RemOroll Z. Kreger September 27, 1948 3.. Introduction 2, Field testing equient 3 Monsaite deposits controlled by 1 1 2 Capiba - . - - . . . . 6 emplommk 6 Poedsda Futa - - . e MilAla a. U. IF .0.. AI or 10 +0 es. ea, ? at ex Of a* 9 Ube -?? 12 0 12 Paysti Patramenio Caju Itapotanga ? Ylra ,Olb olo 13 13 4. Magmatic Separttion Plant 14 Labor 6. Comments on Foote Mineral Company report on FOMIL Brasil Monazite Estimate e. Photographs S cc: Sts. De rtment A *mission X CoaPani G. E Lindsey III James S. Murray Research file Intelligence service 3 extras 19 20 21 24 par 13; OFFICIALS OILY Approved For Release 2003/10/02 : CIA-RDP80-00926A000600040002-1 Approved For Release 2003110/02: CIA-RDP80-00926A000600040002-1 Lindsay I.iht & (ram) E. 3, Sento, Brasil 11. if ? Sisbalbarear and Havaard 11. trimers 3404111ther 27, 1948 Bering the period August 15 to September 1.2, 1% tm made a brief surnor of the monesite properties at present centre L. The surrey was made to determine the monetite potential of POKILts orsoorties and the actual and potentitil m*it?it:Auction of FOWL. All inspections of Pam. peOperitel were made with the guldanve of di*rdBruit (general managler and dames Crawford (superintendent). A]themi certain other phasing of MIL were inspected, such as their Sapacia bent mine (20 he. from 3. Tem*, Minos Gerais), only brief repDrts an the.. activities are given here. Soh of the informatiOn on the arl extent of the mines ws obtained Iran. impoosible to bring large samples to the United of the telt* herein reported were made in the field. The tooting pment consietellef (1) a portable beta-gamma Geiger-Mueller surrey meter (Beckman model NO, ABC model 9(W 15A Serial No. 1106), (2) hand spectroscope, magnifying glass, etc., Approved For Release 2003/10/02: CIA-RDP80-00926A000600040002-1 or t Approved For Release 2003/10/02 : CIA-RDP80-00926A000600040002-1 OL andards for monazite sand consisting of mixture itionst \Monazite nmenite Zircon Silica 1 35 35 9 Compoa tion 25 55 10 10 50 35 10 5 .041. 010.11P?lio 2.5. 55 35 7.5 5 55 35 5 10 55 20 15 The sand mixtures re glued on ctrdboards and the cards thus obtained were covered h celluloid for protection. The standarde were carri. ecl in two.piece cigaret case which was used as a volumetric measure in panning touts. The standards were extremely helpfNill but they should have included the range 50 to 100%, Volumetric measurements were made of panned oon entrates, and were based on a bulk value for heavy mineral sand of 2.14 to 2.43 g./cc. Where analyses are reported with an analysis malber (AN the assays 'Ari"C made at our laboratories. Mineral analyses were mad* by magnetic separati )r_ (Operation Manual, art 20 C, .200), and chemical analyses were made by oqx. standard monazite analysis method (operatton anual, ?art 2, C R-1). ITS CONTROLIE:a 3Y FOND, At present, the principal 3razil monazite deposits consist of modern Aro recent marine beaches along the Atlantic coast in the states of Rio de Janiero; Espirito Santo, and 3ahia. These beach deposits vary both in the content d. the composition of their heavy sands. The heavy mineral concentrates cons int predominantly of ilmenites monasite, and zircon. In addition to beach san nearly all of the rocks and clay derived therefrom contain monazite. It, i3 entirely probable that nazite-bearine rocks extend at least 100 miles inkTid Approved For Release 2003/10/02 : CIA-RDP80-00926A000600040002-1 Approved For Release 2003/10/02 : CIA-RDP80-00926A000600040002-1 along much of the Atlantic coast bordered by the states of Rio de Janiero, Espirito Santo, and Bahia. As a matter of fact, panning tests of clays derived from the country rock in many parts of Espirito Santo showed appreciable amounts of monazite. The Brazil beach deposits are oftwo types, recent and modern, represented schematically in Figures 1 and 2. FOMIL monazite deposits are in Espirito Santo and are named as follows (see map for location): Name Former owner or Lessor Capuba Carspebus No. 1 Carapebus No. 2 Ponta da Fruta Parsti Patremonio Caju du Pont du Pont du Pont du Pont Torres Torres Torres Torres In addition MIL has first rights to mineItapotanga, when such rights are granted by the DNPM. FOMIL is also considering the prqchase of the U b ix mine which, is awned by a farmer at Ubu, E. E. Santo. The Torres properties were leased to FOMIL for a three year period beginning Jan. 1, 1947 on a royalty basis of Cr$600 per metric ton refined monazite produced. The du Pont properties are now in FOMIL's name and ere obtained from du Pont when the latter ceased ilmenite prospecting in Dra '1. FOMIL has pronpected all of their properties. Their prospecting method consisted of taking samples with a pat hole digger until clay or eater NTS reached (up to 6 meters deep). The overburden sample was discarded, and a representative sample of the concentrate sand layer (if present) was made by quartering. Concentrate sand lenses were thus outlined and the depths noted. Sampling was usually done every 30 meters. The samples were taken to the Vitoria office, and after washing, grain counts were made. We consider the sample taking method as being adequate, but we do not believe that the grain- count azi*PoivsedtgotMelielMANOIE :ta-0151gOlebirk0618 to grain size. ono_1with respect at IAPprned Fur Release 200 ? SA-KiA TERESA 1101Q2 IA g RD P80 009i26A00060001nn02-1 3.?f e'es AR ACRUZ i ? ? a.' if. t I ? , ? i ? ! i , "ON ? ? r SAtATA .EOPOLDJILA ? ? DOMIKL405 MARTtNs S% ? .? ? FUNDA?-,\ CARIACICA ? ? ? ? SE R RA ? 40G CAPUEIA. ..1.4LAtru_2pe iwarepe6us , _CARAPE8a5 No.1 -VCARAPEBus N..2 V IT O RI A ?JABALT54 E,. r ? ? , ? ALFREoo C14/0/C5/- ? ? a 55%. ? p. ? ? p. tCoNtox ANCI-tiETA 15.5 S ITAP ? J -207GuARApARi Jc? PONTA OA FRI1TA No. PONTA OA PRVTA 44.2 4/M.' IM/E3RAL MEA/PE (MI 48 RA ? 44I- BA ureic; PARATt PATRAM ONIb CAJLI TAPorl IN4r SCALE - 500,00o Approved For Release 20(0/*OW : CIA-RDP80-00926A000600D4000211 40" Approved For Release 2003/10/02 : CIA-RDP80-00926A000600040002-1 - RECENT bE.AC.1-1 SAN. HEAVY NA 4ERAI. 0C ILA N SAND LAV:` - V:/ I- LI, I rie di -- -No , I I ? ? Ng- 1 / I / I \ ".1 fy. 1.? ? ? ? -, z ? _ e ?-? e ?-? / \???? .... I - ? I ."*./ 167. "" riGuRE., 2 - MODEPN PiEs.kc Approved For Release 2003/10/02 : CIA-RDP80-00926A000600040002-1 Approved For Release 2003/10/02 : CIA-RDP80-00926A000600040002-1 At the time of our visit, Fain had not completed assays of many of their amples. CA PUBA This is a recent beach deposit about 2 km. lonc situated about 30 km.. NNE of Vitoria and about 300?500 meters from the present beach. Du Pont formerly considered working the area for ilmenite. We did not see much ci this property; no good mining areas were visited. FOMIL is doing no mining at Capubal but intends to mine it for sir )r sand, Du Pont reported the average composition of the sand in the mine is follows: Ilmenite 1-1?30 ..... Seeand_class ilmenite ----- Nemasite. 1.47 0.68 .. ? Nonmagnetic 8,47 ............... 77.99 quartz --------- and estimated the mine to contain 11,500 letric tons of ilmenite. 3ased on this, the mine contains 680 metric tons of monazite. However, graft says that the du Pont prospecting did not take into account the generally accepted rule .in such deposits that monazite tends to concentrate in the deeper Irarts of the deposits; the du Pent prospecting was shallow, and test holes were not made to clay or water. We have heard that du Pont now admits that their d ati on the monazite contents of their Brazil prospects are too low. CARAPEBUSN05.lafld2 These mines are located about 20 km. NE of Vitoria and are of the rccnt type. The mines total about 4 km. in length and the mineable areas weru re- ported to be up to 30 meters Ade. The heavy sands consist of limonite, zircon and noziazite, Approved For Release 2003/10/02: CIA-RDP80-00926A000600040002-1 Approved For Release 2003/10/02 : CIA-RDP80-00926A000600040002-1 Du Pont reported that the average composition of the sand on Carapebus No. I was as follows: Ilmenite - - -- - - --.--------- 10.18% Second class ilmenite 5.55 Monazite -- 0.47 Nonmagnetic 6.33 Quartz - 82,45 ? Du Pont estimated that a 10 cm. thick layer of imncentrate contained on the property would contain 401480 metric tons of ilmenite. On this basis, the same layer would contain 1,850 tons of monazite. POMIL's test holes showed rich lens of sand on Carapebus No. 1 which was missed in the du Pont prospect Only a small portion of one ore body on Carapebus No. I was visited. Three ore bodies on Carapebus No. 2were confirmed with the Geiger meter. Neter read- ings of 0,05-0.15 mrihr. were observed (background 0.02 mrihr.). at points indicated by Kraft to contain lenses of. heavy sands. Confirmations of ore bodies disclosed by FOMIL was satisfactory with the Geiger meter provided the ore layers were not too deeply buried. The three ore bodies on Carapebus No. I were reported to have average thicknesses of one meter, widths piot1ng 10 m?ters, and lengths of about 300 meters. Panning tests of mined concentrat showed about 50% heavy sands and 2,5% monazite (about 5% monazite in th heavy mineral concentrate). Panning tests of "barren" sande showed about 0,5% monazite. Considerations of du Pont's surveys indicate that Carapebus No. uay contain 2,000-3,000 tone monazite. Including the "barren" sands, it estimated by us that the mine contains at least 25,(O0 tons monazite. FOMIL's surveys indicate five ore bodies, and Kraft estimates t five deposits contain 2,500 to 3,000 tons of monazite not considering barren sands. Approved For Release 2003/10/02 : CIA-RDP80-00926A000600040002-1 base Approved For Release 2003/10/02: CIA-RDP80-00926A000600040002-1 At the north end of Bsperito Santo Bay,we saw a small beach of modern type (Fig. 2) which consisted of black sand containing about 5,10% momeite, Clay from the cliffs near by showed approximately 0.1-0.5% monazite on panning. Part of Carapebus No. 2 was worked about 20 years ago by the French. Two stockpiles of unwashed beach ooncentratesvere left on the property. Geier meter readings on the two piles were 0,1 to 0.15 mr/hr., and panning tostf showed that the material in the piles contained about 50% heavy sands and 2.5% mnazite (or 5% monazite in the heavy mineral concentrate). The two piles were estimated to contain about 500 to 1,000 tons of heavy minerals. PONTA DA FRUTA The Ponta da Fruta mines Nos. 1 and 2 are located near the vi1iae of Ponta da Fruta, about 35 km. S'of Vitoria and about 20 km. NE of Quarapari. The deposit is of the recent type. The No. 1 mine is 4 km. long and the adjacent No.2 mine is 2 km. long. The thickness of the natural concentrate layer vAe reported by FORM tote 1-3 meters and About 20-30 meters wide. Du Pont's estimation of the average composition of the sand at Ponta da Fruta No. I was as follows: Ilmenite ----------- 12.65% Second Claes ilmenite -- 4.11 Monate 043 Nonmagnetic 14.96 67.85 Quutz They estimated that the ne contained 61,000 metric tons of limonite; on this basis it should contain 1,500 metric tons of monazite. More monazite than this is present because the du Pont surveys did not include the lower natural concentrate layer where the monazite content of the heavy mineral snnd iszre er. FOMIL had not completed calculations of their prospecting test holes at the time of our visit. Geiger meter prospects by us shoved that the mine contained eonsiderable monazite. Approved For Release 2003/10/02: CIA-RDP80-00926A000600040002-1 Approved For Release 2003/10/02 : CIA-RDP80-00926A000600040002-1 -9. &MIL started Tining at Ponta da Fruta 1 in 1948, intending to ship a sircon-ilmenite mixture to the Foote Mineral Co. of Philadelphia. However, when mining was started it was found that the amount of monazite in the ricen- trate was so high that shipment of the concentrate was impossible. ining was done by washing off approltimately 3 ft. of overburden sand with a ira.i11.c run, and then the underlying 6.10 ft. of natural concentrate layer was pumped with water over six roughertables and four cleaner tables. The table tai] tags were pumped to the beach. The heavy mineral concentrate thus produced was tote loaded onto a barge at the beach (100 ton capacity) and was to be shipped to Vitoria. Mining operations were suspended pending the installation of separation evti?iiient at Vitoria. Production from the tables averaged 0.5 ton heavy minerals per hour pert able for six tables. Only a small stock of concentrate was made and this is at the mine. A sample of the heavy mineral concentrate produced by the tables had the following analysis (AN 485129): Ilmenite - 46.0% Monazite -------------- 13.4 Nonmagnetic - 40.6 (largely zircon 7:15n Assuming that the mined sands contained 50% heavy minerals of the above composition, the mine aould contain 110,000 tons heavy mineral concentrate or 50,600 tons ilmenite, 14,700 tons monazite and approximately 45,000 tons ziron, exclusive of these minerals contained in the overburden and "barren" 3T.:-.nea;. M A 1-B A The Mai-Ba mine is a modern beach deposit located on the present ocaf n beach adjacent to Lake Mat-Ba about 10 kr, from Anchieta. It is about 2,000 meters long and the mineable area is about 10.15 rioters wide adjacent to k brut lay cliffs which are about 20 to 30 meters high. This is the only FOMIL beach mine being worked. Operations were startet on May 13. 194$._ Approved For Release 2003/10/02 : CIA-RDP80-00926A000600040002-1 Approved For Release 2003/10/02 : CIA-RDP80-00926A000600040002-1 Mining is done by r emoving approximately 10 ft. of overburden sand near the cliff base. The thusly exposed layers of monazite and black sand are shoveled out selectively. The monazite bearing veins vary from 1 cm. to 1 meter thick the average of those seen was about 10 mt.; and the total vein thickness reacved is about 0,5-1 meter. The natural concentrate they removed is supposed tots roughly adjusted At the mine to contain about 20% heavy Minerals. It is trans- ported by truck to the mill located about 100 meters front the mine. After storms, considerable monazite concentrates are found on the beach, and these are scraped up and t emporarily stored in piles on the beach for transportation to the mill. The monazite-rich veins exposed in the mines often consist locally of 70- monazite, and occasionally, cemented monazite sandstones are found adjacent to the cliff. At the mill, a reserve stock of about 4,000 tons of mined sand is kert on hand for t abling in case of inclement conditions on the b each which prevent raining. This stockpile was sarnpled and analyzed as follows (AN 4,85126): +20 mesh ......----.. -- -- I1PAnite (plus garnet) 27.4 Monazite 12.3 -- Nonmagnetic -------- ------- 1.2 .0 The mined sand- at this mill is shoveled into a launder and the sand slurry flows by gravity onto t wo Deister tables having 4 ft. X 1.0 ft. decks. The tables aere somewhat overloaded and a concentrate containing about 55-702; monazite was produced at the rate of approximately 1-1.5 ton per hour pe r t able. The mama- cite recovery was estimated to be about &V. Tailings from the tables flow by gravity to a pump where they are presently pumped to a pile located between the mill and beach. FOMIL eventually contemplates pumping the tailings directly to the beach, a distance of about 100 meters, whea pipe can be secured. Approved For Release 2003/10/02 : CIA-RDP80-00926A000600040002-1 Approved For Release 2003/10/02 : CIA-RDP80-00926A000600040002-1 Analysis of a sample of tailings taken Aug. 18,1948 showed (AN 4851 28.7% lime:lite 3.5% monazite 67.8% nonmagnetic sands Monazite concentrate from the tables flows into boxes (2 mt. meter cap*ca where the excess water is drained off. From these boxes, the concentrate is shoveled to a temporary stockpile which is trucked to a warehouse on the wharf at Anchieta. There it is bagged for barge transportation to the ma7tetic separa- tion plant at Vitoria. Production of tabled monazite concentrate averages 1.0-1.5 ton per hour per table. For a 20 hour day, 26 day month, the production from two tables could therefore be over 1,000 tons of concentrate per month. The actual average produc- tion rate has been about 200 tons per month on account of stoppages one shift operation. A sample of tabled concentrate such as is shipped to Ancl e (t /mg. 18, 1948) analyzed (AN 483121) as follows: Ilmenits (+garnet) 38?2% Monazite 40.0 Nonmagnetic 2.1?8 Tao On Sept. 23, 1948 we received a sample of Mai-Ba table concentrate fr which analyzed (AN 485140): limonite monasita Nonmagnetic 19% 70 11 (largely zircon -Tam From panning teats we estimated that the "barren" sand on the beach surface contained about 2% heavy minerals and 0.05-0.1% monazite. The entire mine may contain 20,000-30,000 tons of monazite in the high grade veins now beir.k; mined and it may contain an equal amount in the overburden "barren" sands. Kraft believes that any estimate of the amount of monazite in the mine is impo ' because he reports that mined-out holes canbe re-worked after storms; Approved For Release 2003/10/02 : CIA-RDP80-00926A000600040002-1 Approved For Release 2003/10/02 : CIA-RDP80-00926A000600040002-1 in fact he reported that one bole has been mined four times to date. It is our opinion that additional tables should be installed at the nill to give greater monazite recoveries. FIDMIL plans to install a third table to wash he tailings from the present bo tables to recover additional monazite and. ar ilmenite fraction which will ie stockpiled at the mine and returned. to Torres ownership. The quality of the monazite produced by us at our laboratory by Lagnetic separation was satisfactory. Analysis of such separated monazite obtained from various Mai-Ba samples during the course of their mineral analyses were follows: Analysis Number 485114 485116 %Mu]. % Th0 CIlel 8,25 69.2 7.1 68.2 7.2 A "clean" monazite produced on t .NIL magnetic separator from -Pa concentrates analyzed (AN 485132) 66,2% total oxides and 6,2% TWa. UBU The Ubu deposit is of the recent type and is located at the fishing village of Ubu. It is about 2 an. long and is just south of Yatiaa. The deposit is similar to the Parati deposit. It 10..5 partially worked for monazite in 1928 by Societe Franco Brasileiro (the old KIM company). it is at present ovned by a Brazilian fisherman living at Ubu. POMIL has no mining rights to the property but is considering obtaining them, P A-R A T I The Parati deposit is of the recent type and is located just south of Ubu. It is about 2 km. long It has been partially mined by Torres, and at preert the mine sands belonging to Torres are being washed by him in "dollies" pd the concentrate containing about 507") monczite is sold to NIBRA for cr4600 er .on of contained monazite. FOHIL estimates tat the dolly operation will be com- pietedqPinegnFerofeiwo 2003/10/02 : CIA-RDP80-00926A000600040002-1 Approved For Release 2003/10/02 : CIA-RDP80-00926A000600040002-1 FOMIL eventually plans to loork the mine In mach the same manner thqt Tja.13,71 is being worked. 'Monazite concentrates from Parati probably will be aiailr to those obtained from Kai-Ba. PATRAMON 1 0 The Patramonia deposit is of the recent type and is located just south of the village of Piuma. The mineable area is abut 2,000 meters long .z.rld consists of surface layer of concentrate about .1 meter thick and 15 meters wide. A sample of the concentrate analysed (AN 485130) as follows: limonite 63.0 Monazite 3.4 Nonmagnetic ---------- .b according to this, the concentrate vein contains 42,000 tons ilmeni e and 2,200 tons monazite. CAJU ? The Caju deposit is of the zscent type and is located about 2 ha. sonth of Pima. It is reached by canoe from the costal road. Portions of it 1-ave b eon worked by Torres, and there are several stockpiles of washed sand at the mine. At Pima, a stockpile of 740 tons of Hilmenite sand" (washed sand from Caju) is being considered for purchase by Kraft. According to his analysis it conta ins 15.4% monazite. Our analysis of the material showed 70,V 7.9% monazite, and 21..2% noravagnetic (.A.N 485131). The Caju deposit is about 4 los, long and is situated near an a-1-71e alurce of fresh water. ITAPOTANGA The Itapotanga deposit is of the recent type and is located about 7 :cz south of Piurna. RAUL has no mining rights to the property, but has a. protecol on its claim. The mineable area la about 3.5 kn. long and 5..10 meters wide. Approved For Release 2003/10/02 : CIA-RDP80-00926A000600040002-1 Approved For Release 2003/10/02 : CIA-RDP80-00926A000600040002-1 or a sang* or tke isavy stirtortil yelp at4.,,ww$ (Ab win) V ohla. P t '741 tLe Lri Ok. Ltor. ? lioilkatase 2003/10/02 : CIA-RDP80-00926A000600040002-1 Approved For Release 2003/ t*RDP80-00926A000600040002-1 To: Charles R. Lindsay, III From: Howard E. Kremers 3eptemLer 5, Subject; IfEMCO-HOrE MAGNETIC bEPARATO% AT THE FOMIL "n" PLANT. Following is. a summary of my observations and opinions on the performance of the Fomil magnetic separator. Alltests were made in the presence of either J. rawford or Ed Kraft. Mai-Ba concentrates containing about 60 to 72% monazite were used. When first seen, the machine was adjusted by the M personnel and was giving an iImenite-garnet mixture on the first three poles, and a clean monazite on the las three poles. The maChine. was operating at maximum amperage at 230 volts, was producing .cleaned monazite at the rate of approx. 25 Kg. per hour (005 ton y,er day). Slight adjustments to decrease the air gaps between the main and cross belts gave a slightly better yield. With the air gaps as small as possible (less than 1/8 inch) time tests at varying amperages indicated that the last three poles were operating very close to maximum magnetic flux. After various adjustments had been made we were able to increase the yield of monazite to approx. 100 Ke. per hour. The following data were t aken after a. two- hour "warm rup" period; Feed rate: 424 Kg,/hr, (maximum possible) Belt speed: approx. 50-60 ftimin. (slowestpossible; increase in belt speed gave poorer results) Air gap:. less than 1/8 in. (as all as possible) Volt 270 volts (the machine is rated at 230 volts) Pole Amps % removed Composition of sand 1 . 7.0 15.3 ilmenite-garnet 2 64 7.3 ilmenite.garnet 3 6.5 8.2 90-95% monazite 4 8,2 7.8 90^.95% monazite 5 1108 2,9 90-95% monazite 6 Nonmagnetic 12.8 4.7 l 90.95% monazite approx. 60% monazite Yield: Approx. 100 Kg. monazite per hour from pole3p4,5, and 6. Approx. 24% of the head feed was removed as monazite.. Approx. 35-40% of the monaazite present in the head, feed was removed in one pass. The machine was being overloaded by operation at 270 volts. The coils had an outside temperature of approx. 53*C. The 7.*otor driving the ac-dc converter was running at about a 45,0 C. temper-All-re rise. Continuous operations under such conditions would be inadvisable. Further attempts were then made to obtain monazite.ilmenite fractions poles 2.6 which could be separated into ilmenite middlings and clean monazite by splitting the two streams of 'and as they came off the cross belts. the machine operating at 250 volts, and after a two hour warm.aup, the best monazite ybld was obtained. The recovery of cleaned monazite on one pass was found Analysis of the sand showed the actual monazite content to be about 56%. 41* We undeglarttacr INRolfiiM411W0iokziifk-aiR8219042611/490ifitififl4609831 eo this temperature is not excessive. -16- mew 1elipictri1,IF91.-At?!se 2003/10/02 : CIA-RDP80-00926A000600040002-1 -2- to be not more than 50-60 Kg. per hour. Tho yield 'could not be improved becmse the shading on the first pole VE.5 out of alignment with the other -oeles; et-hioh feed rates 6 ridge of ilmenite was left on the croeebelt-discharge siee cf tne t so, that It interfered with the r emoval of :3nd trm the subsequelt cl0005 elts At high feed rates, the monazite fractions were badly contaminated with thir . Attempts to correct this conation by changing the position of the Ta_in be not successful. The only c,rrection is to retap the first pole tIci re- locate the brass shoes. With such correction, the caoacity undoubteely cem be in- creased. The sand plltters on the cross belts are poorly designed. It it iajosible to male satisfactory adjustments with the present equipment. The sard r-.3eeivers should be modified so that control can be made by adjusting vanes to split the monazite and ilmenite sano streams. Repassing the nonmagnetic tailings which contain approx. 3o-.60 :nn .aite aoes not give a satisfactory recovery of clear monazite. Apparently the J-7-!gh,4s are strong enough to pick up the 3pre weakly magnetic monazite sands. It has been consistently observed that a slightly better separation as obtained With warm feed sand. However, at the last operation of the separator usulo warm ? sand (approx. 45?00, trouble was encountered with the main belt. Alttoyooh it was not stretched too tight, the joint in the belt began to loosen resulting in a troublesome bow in the middle of the belt. Before farther operation, theelt will have to be repaired. The belt joint should be vlacanized. It is possible to completely remove il without removing monazite. This gives a mo ing at the rate of 0.5.1 ton per hour. It satisfactory monazite product by screening set up at the M.S plant to inveotigate this lienite from the sand on 411 six poles nazite; zircon) quartz nonmagnetic tali- may be possible to obtain a fairly these tailings. ?A screen is now beinz possibility. . All of the suggestions offered by Foote in thier cables of the past week have been tried. With appropriate alterations of the machine, it be possible, to produce 75 K. cleaned monazite per hour (450 metric tons per year at 20 hours )er day and 300 day year operations). In my opinion, the separator is poorly designed in the following ways: 1. The magnets are too weak. 2. The first pole is out of alignment. 3. Th, cross belts are too thick. 4.. The main belt is not vulcanized and is slightly irreuler. 5. The sand splitters on the cross belt receivers are poorl:,, ,ye*7ned, 6. The rheostats for pole control are too small one has b,::cn. burned out to date). Cost estimates: The diesel generator and crier each consume about 15 liters of oil pe r hour. The oil costs Fomil C$1.35 per liter. For 20 hour day operation, the, oil (c)sA, is approx. US$40.00. Labor costs at the 113 plant are approx. US$15.00 per ;i y. For a daily 20 hour operation with a recovery of 100 K. cleaned monazite per (2 metric tons per day), the separation cost would be about US$27.50, exclulNu of overhead, maintenance, mining costs, etc. Is! H. E. KremerF- cc: Foote Mineral Co. Edward Kraft Richard P. Nor.ssen, Jr. H ? priSMeIrtgr Release 2003/10/02 : CIA-RDP80-00926A000600040002-1 C. 1. Lindsay III Approved For Release 2003/10/02 : CIA-RDP80-00926A000600040002-1 Analyses of MaiJa nonmagnetic tailings obtained by removing ilmenite on all six poles of the Memco-Hope separator were as follows (AN 485112): The sample represented approximately 2 tons of material Mesh +20 40 6086 100 Screen analysis Chemical analysis 0.2 6,4 1/.0 .4 0 % monazite 69 63 46 Total oxides Th02 Mineral analysis Ilmenite Monazite ........ -76 Nonmagnetic --------- -17. Since the removal of Limonite alone could be easily done with the separator, it was thought that screening this material through a 60 mesh screen ihoule give a +60 mesh material which might be acceptable monazite, or could be blended with refined monazite to give an acceptable monazite! If practical, such a tvcedure might increase the ?OMIT, output of refined monazite. An experintal mile of ilmenite-free tailings produced by the separator and containing (AN 485l2F!) 2.1% ilmenite, 72.5% monazite, and 24.4% nonmegnetic sands was screened or a 60 mesh screen. 4)4rcalmate1y 60% of the sample Nes retained on the screen and 4,h5s material analyzed (AN 485110) 58.6% total oxides and -642% Th02 equivalent to 86% monazite. Consideration of the screen analysis above shows that screeniT:, the material on a 60 mesh screen would give a +60 mesh fraction containing 83 monazite. On Sept. 27, 1948 we received from Kraft a sample of MM-Ha material from which the ilmenite had been removed on the MIL separator and which was screened at the MS plant; it analysed (AN 485156) B14 monazite, 44 iltenite and 15% zircon. Approved For Release 2003/10/02 : CIA-RDP80-00926A000600040002-1 Approved For Release 2003/10/02 : CIA-RDP80-00926A000600040002-1 In order to fortify this to 95% monczite, one part of the a5z would have to be blended with two parts of 100% monazite. In order the 85% material to 90% monazite, Iwo parts of the 03% material would blended with one part of 100% monazite. When last seen in the early part of Slixtember, 1948, it was estiinat FOMIL separator had an annual capacity of 450-600 tons refined monazite t 55% Mai-Ba concentrate (20 hours per day, 300 day year operation), o of 4,500 tons per year of Limonite-free B5% material, to be screened. TN t-] order to produce onazite, the capacity would be based on the otenti.,.1 monazite production, and the total yearly production of 90% monazite would 1-)e approximately 1,300 tone. Improvements in the design and operation of the separator would improve the yield. rial increa3e v-D to b BONDED 3 Approximately 420 tons of monazite concentrate are bonded at the IT ELL draws against a letter of credit t)ed on t his sand containing 86;.1 monazite. Analysis of core s amples of this stockpile a re a s follows: Core Qample AN 4 ilmenite % monazite 1 485119 24.9 57.1 18.0 2 485120 25.3 57.3 17.4 3 483121 26.8 53.7 19.5 4 485122 27.5 10.7 18.8 5 48512, 25.9 55.6 18.5 AMAGE3 26.0 55.5 18.5 Approved For Release 2003/10/02 : CIA-RDP80-00926A000600040002-1 Approved For Release 2003/10/02 : CIA-RDP80-00926A000600040002-1 , LABOR. As of September 4, 1948, the following breakdown of reonnel appliad to FoYaL. Non-..supervisory labor costs are figured at C415 percay per person for a 26.day month; at U3.1.0.05 per cruserio this cost is US519.50 per mxIth. Mechanics and mine bosses receive Cr$2.500,60 to Cr$3.500 00 p5r month. 014I Edward Krat ?nerai Manager) J. Crawford kulerintendent) Phillip Meddewar (Office Manager) A. Cabral (Purchasing, Procurement) Joseph Graf (Geologist) Office boy 3 Office girls (typing, filing, assay, etc. AIMS MAI-BA 30 - laborers (419.50 x 30) Chauffeur - ????411tainrina? ???? ....... ???????????,??????? MI?4/I? Mechanic (043.000,00 per month) ----- Fiscal -- Foreman (Cr$3.000,00 per month) - HMV! p laborers (319,50 x 8) - mechanics (Cr$3.000,00 per month) PONTA DA RUTA Watchman BAPACIA BERYL MINE ...... mom& we Us$ Mont iv Salary 250.00 300.00 150.00 100.00 200.00 10,00 -19 Totals 585.00 50.00 150.00 125.00 150.00 Kurt Volmer (Foreman) 17 - laborers (19.50 x 17) 156.00 300.00 1?.50 1,0.00 ,331.50 a51.00 ?T19.515 ;?af.50 TCTAL $3085.50 Approved For Release 2003/10/02 : CIA-RDP80-00926A000600040002-1 Approved For Release 2003/10/02 : CIA-RDP80-00926A000600040002-1 6. COMMENTS ON DIE FOOTE MINERAL CONANT REPORT ON FOOTE MINERIO3 INDU3TRIALIZADOS, LTD., (GORDON CHAMBHRS, 4-20-48), Page 2. B. Although one of the types.of FCMIL's business is the buying of cres from small prospectors and miners (in particular, beryl ore), this activit decreased markedly due to a lack of working capital. C, D. The importation of materials for resale in Brazil has been limited. We do not believe that FOKIL at present has an adequate distribution prograia. Although opportunities for resale may exist in Brazil, it m)uld avear beet to investigate the actual market in Brazil before undertaking a resale program. Page 3 MINING RESLIVES. According to Kraft, the mines Capuba, Carepebus No. 1 and 2 and Ponta da Fruta are now permanently owned by F)MIL. Also according to Kraft, there is little possibility of Vincent Torres extending the leases on Iai-Ba, Parati, Patramonia, and Caju. Page 4 MINING METHODS. Hydraulic mining of beach sands was practiced for only a short period at the Ponta da Fruta mine; this mine is at present closed down. Only MaiaBa is being mined, and the sand is dug by hand and trucked to the mill. This mining is primarily for monazite; ilaenite eventually may be an irlportant product the zircon is reported to of poor quality. Only one beryl mine at Sa?aria is being worked; mica is being mined A this mine on a contract basis, Page 5 EQUIPHONA, A sand concentrating plant consisting of six rougher Deistert,,blas and four cleaning tables was erected at Ponta da Fruta; this is now shut kiouri. The sand plant at Mai-Ba has two Deister tables, Approved For Release 2003/10/02 : CIA-RDP80-00926A000600040002-1 Approved For Release 2003/10/02 : CIA-RDP80-00926A000600040002-1 The magnetic equipment at present consists of a rotary drier, CrOSF- belt magnetic separator, conveyers, and a Diesel generator. The installation of an electrostatic separator et this time is not recommended. Laboratory equipment at the FOMIL office is very limited. It consists of quartz crystal inspection equipment, a microscope, and surveying equipment. The analytical equipment and Geiger counter are inadequate. Page 5 WATER PND FUEL. Sea water is plentiful at the sand mines. The only miries with adequate fresh water are Mai-Ba and Caju. Page 6 SAND MINING The FOMIL beach surveys at present are incomplete, although it is reported that all the necessary samples have been taken, The FD MIL grain-count method of 'assaying the samples leaves much to be desired, and it is our opinion that such tests should be made by more accurate methods. Page 8 :PERSONNEL. In the opinion of Kraft and Crawford, the geologist Joseph is not suitable because he is not dependable. He should be used to make surveys, etc. but instead he has been doing non-geological work. It is our opinion that the salary rates for the supervisors and engineers should be increased. FOMIL will not show a profit for several years, ant to prevent discouragement, certain of the salaries should be increased. BRAZILMONAZITE ESTIT4ATE. An accurate estimate of the amount of mineable monazite in Brazil Ir impossible to make because there are no adequate surveys. It is a fact th,t the potential production of Brasil monazite is tremendous. Approved For Release 2003/10/02 : CIA-RDP80-00926A000600040002-1 Approved For Release 2003/10/02 : CIA-RDP80-00926A000600040002-1 The Brazilian PK estimat a he menazite resaurces of Brazil are ale.:ut 200,000 tons. Such an estimate undoubteely accounts only for monazite contained in the rich natural concentrett sand lenses on the modern beaches. We believe the 200,000 ton estiaate is low for the followie (1). Brazil mining practice is to "high grade" a aine mith crude dedeg aethode. The low grade material is discarded. In all of the beach mines, the amount of monazite contained in the "low grade"- and "barren" sande at least approximates or is considerab - greater than the amountcontin in the high grade veins. Abandoned mints such as the Mane Ltru mine which is oonsideree worked-out, could be profitably worked to recover additional monazite. (2), Sore mines, such Mai-Ba? are continually depositing mortazite. pef'ience of MIL is being able to rine mined.-out areas storms is an example of this. (3). No surveys have been made of the monazite resources of beach sands lying law the water level. It is Brazilian practice not ta ne below the water table because proper equiament is not used. The igneous country rock along the aonaziteeproducing coast i the aouree of the nonaiite on the beaches. Nearly ell samples of clay (derived from this rack) will show 7ionazite on panning. If zuch clu were available in this country, serious consideration mould be ivur to mining them for monazite. It was reported to us that clays tis far 100 miles inlaad from the coast will show monazite. on panning. In clay Cliffs at Mat-Ba, manazite is etsily visible atcertain avots st random samples of the clay will Show at least small amounts site an panning. Approved For Release 2003/10/02 : CIA-RDP80-00926A000600040002-1 Approved For Release 2003/10/02 : CIA-RDP80-00926A000600040002-1 The amount of such clays in Brazil is unlimited insofar as monazite firoo ctiGn is concerned. From our observations, mr estimate that the monazite resyirces of Brazil anount to m,,ny millions of tons. Approved For Release 2003/10/02 : CIA-RDP80-00926A000600040002-1 25X1A 25X1A Approved For Release 2003/10/02 : CIA-RDP80-00926A000600040002-1 A small monazite beach at Carapsbus. AREA 23314 BRAZIL ESPIRITO SANTO OARAPEBUS 20 16 8 40 12 0 (AC 1265). Small monazite beach. 1948. Restricted Ubu, E. Espirito Santo AREA 233H BRAZIL E. ESPIRITO SANTO UBU (wac 163) 1940. Restricted 20 49 S 40 37 W Approved For Release 2003/10/02 : CIA-RDP80-00926A000600040002-1 25X1A 25X1A 25X1A 25X1A 25X1A 25X1A Approved For Release 2003/10/02 : CIA-RDP80-00926A000600040002-1 ARCA 23511 BRAZIL ESPIRITO SANTO POITA.DE FRUTA (RAO 1263) Monazite mine controlled by BOWL. 1? I Restricted 20 32 8 40 43 W 1 94 8 . AREA 23314 BRAZIL ESPIRITO SANTO PARATI 20 50 40 38 A (MAO 1263) Monazite mining controlled by FOMIL. Sand is mined from ridge immediately left of the beach. 1948. Restricted AREA 23314 BRAZIL ESPIRITO SANTO PONTA DE FRUTA 20 32 S 40 23 W (WAG 1263). Monazite mine control Pal by FoMIL. The buildinem house pump and tabling e ui 1948. Restricted AREA 23314 BRAZIL ESPIRITO SANTO PONTA DE FRUTA 20 32 8 40 23 N AC Beach mined for monazite. 1948. Restricted Approved For Release 2003/10/02 : CIA-RDP80-00926A000600040002-1 25X1A 25X1A 25X1A 25X1A 25X1A 25X1A Approved For Release 2003/10/02 : CIA-RDP80-00926A000600040002-1 AREA 23311 BRAZIL ESPIRITO SANTO MAI-BA 20 36 S 40 36 I (WAC 1263) Beach mined for monazite. 1)48. Restricted AREA 233H BRAZIL ESPIRITO SANTO MAlz.BA 20 36 S 40 36 I (WAC 1263) Temporary piles of sand scraped from the beach au-face after storms. (Monazite mining). Restricted Approved For Release 2003/10/02 : CIA-RDP80-00926A000600040002-1 25X1A 25X1A Approved For Release 2003/10/02 : CIA-RDP80-00926A000600040002-1 Approved For Release 2003110102: AREA 255H (WAG 1265) Itstreaseino. Woe sr* dug hy sad Um view A.40, rieh *and veins (dart ItrOa,er 410, 1-410-1. Te mined ami in transported to it Till truck Creed apaiest the cliff), *bore *1). asaa is avsilable, 'be *and isinaspartaid itzt temporary stores* piles* 25X1A BRAZIL ESPIRITO SANTO MAI-BA 20 36 S 40 56 N Monazite mine controlled by FOMIL. 1948. Restricted 25X1A 1A AREA 235H BRAZIL ESPIRITO SANTO MAI-BA 20 36 s 402356XW Figgc,_ufali Monazite mining controlled Restricted t TPA. 1948. 25X1A 23311 BRAZIL ESP1i1TO SANTO MAI-BA 20 56 B 40 56 N 126 Monazite mining controlled by RAIL. 1948. Restricted 0926A000600040002-1 25X1A 25X1A Approved For Release 2003/10/02: CIA-RDP80-00926A000600040002-1 AREA 2554 BRAZIL ESPIRITO SANTO PARATI O 50 S 40 58 (MAC 1A,5) Monazite mining controlled by FOMIL. Torres dolly operations. Restricted k&riti booth Lismisa,7), '34/nd is tie ridge immediately left of the act. Approved For Release 2003/10/02 : CIA-RDP80-00926A000600040002-1 25X1A 25X1A 25X1A Approved For Release 2003/10/02: CIA-RDP80-00926A000600040002-1 Mai- Ba mill. The anicentrat?kng tables are in th( thatched building, and pumps and power equipment are in the building to the left. The mined sand stock- pile is at the extreme upper right. AREA 2.5311 BRAZIL ESPIRITO SANTO MA1-8A 20 36 S 40 36W L2 Monazite mining controlled by FOM1L. 1948. Restricted AREA 235H BRAZIL ESPIRITO SANTO MAI-BA 20 36 S 40 36 W (WAC 1263) Monazite mining controlled by FOMIL. View of II from the beach. Restricted 1)48. Approved For Release 2003/10/02 : CIA-RDP80-00926A000600040002-1 25X1A 25X1A Approved For Release 2003/10/02 : CIA-RDP80-00926A000600040002-1 25X1A 25X1A ARIA (*AC drier 1948. 2338 BRAZIL LSPIRITO SANT3 VITORIA 20 I) 1263) Monazite mining controlled by FOMIL. at the rear of Magnetic separator plant near S 40 21 Rotary ra.' VITORIA 20 19 near Vitoria. S 40 21 A 1948. 25X1A 25X1A Restricted AREA 233H BRAZIL ESP131TO (*AC 1263) Macnetic separator SANTO plant Restricted 25X1A gno lent, c drier at the rear of the tic separator, prd rotary ARIA 233H BRAZIL ESP131TO SANTO VITORIA 20 1) S 40 21 N (WAC 1263) Monazite mining controlled by FOMIL. Cross?belt magnetic separator. 1948. Restricted Approved For Release 2003/10/02 : CIA-RDP80-00926A000600040002-1 25X1A 25X1A 25X1A 25X1A AREA 5351.1 BRAZIL RIO OE JANEIRO SAPUCAIA 22 02 S 42 50 W Artmeve d aRtIt tEte)i ease. 0 3d GA422,-b Geht-IRDRalhO 0 Restricted 000600040002-1 AREA 553H BRAZIL RIO OE JANEIRO SAPUCAIA 22 02 S 42 50 W (Times Gazetteer) Beryl mine controlled by FOMI" Restricted Sapacia beryl mine. The blasted pegmatite rock is hand picked for beryl as it is shoveled illAP a glory hole from which it is conveyed to the mine dump. AREA 53511 BRAZIL RIO DE JANEIRO SAPUCAIA 22 02 S 42 50 W (Times Gazetteer) Beryl mine controlled by FOM Restricted Approved For Release 2003/10/02 : CIA-RDP80-00926A000600040002-1 25X1A 25X1A 25X1A