GLYCOL ESTERS OF PYROPHOSPHOROUS ACID.

• Document Type: CREST
• Collection: General CIA Records
• Document Number (FOIA) /ESDN (CREST): CIA-RDP83-00423R001200820003-5
• Release Decision: RIPPUB
• Original Classification: K
• Document Page Count: 1
• Document Creation Date: November 9, 2016
• Document Release Date: March 5, 1999
• Sequence Number: 3
• Content Type: MISC

Approved For Release 1999/09/10 : CIA-RDP83-00423R001200820003-5
Glycol estsrz of pyropbosphorous acid.
addn.
fa
Dot 1ad.y &JQ d . !Tauk . `. ; . S
CPYRGHT
cunt of 0 and a base pv'rid:
t e 40r (CH20
and dietn, of the
n20
l>4903. + i .1ar1y
v e
e0,, b.,,
00 b144-5", d2O
L"[e0 b2
e obtained.-
20 . 8201
and ; they r
.I ikonorov, 0.U. 'edo rova, C . -Vlnokrova and .0. Shi-
buz
?Oa with
0 dild. with 2-3 parts
ed by 3 bra. at room temp. gave after filtration
44, 5% OCTeC.OPOPOC
es M: e2N'fPh, or
about -50
801.46281 44` OCR(CHVC1) CH. oPOPoCH20-11-
apt '"1.5180; 34.8% NiINJ
29, n 111.41745. Theme e
readily add
t violently with H20. Treatment. of 001H 0 i1 01101
oo? ing, in Et 0 gave after sepn. of pptd. sC1
orreepondl
8201.156
cue led.
b 293-40, dzo .1.446, '1.4600;
bS90.10# dZ01.l592, 1.4515; di-Bu. 10.2%,
3-4 0, d 1.1405
530;- di-iso-'r
201.4557; di-Pr,
b,104-5?1
Similarly were tormadr 68,1% 0CIteCHaOPCP(C t)2,
201.4520; di. analo ,, 33.so , b.1100, 82.:i...1090,
analog, 24.5 , b888_81J, 8281.1070, nr` 1.45300
20
b3120-1 0 j d .0300 x
1.4554; 58.8% 0C McCH,01f
P(O; t
b4110-1
8201. 064
00H(O:
0
1,4563; 81-Pr analog-
8201.1368,, n
201o4460; 40.1% dt..Bu analog, b, 152-.6?, d20l.0865, z 01, 4580
H OPOP(OEt)2, b112110
P01-1 { 0CH1 0 #3, %100-la, dD.fl1 4295,
d20l.2,00,
d Z01.198
phoe,)bit
nn01.473. These esters possess
s. The ;die
801.1990, n -1,4
b0,98~-102?,
Gr
di-Bu analog, b3147-50?,
usual properties of the
of the higher unsym. esters are reduced by the
(It shown)di--. , 6D , b284-50,
2X1.4660; 2 di-Pr
A~ppro mid or'ke e sea19 /%1V L N&3?db'423R001200820003-5