GLYCOL ESTERS OF PYROPHOSPHOROUS ACID.

Document Type: 
Collection: 
Document Number (FOIA) /ESDN (CREST): 
CIA-RDP83-00423R001200820003-5
Release Decision: 
RIPPUB
Original Classification: 
K
Document Page Count: 
1
Document Creation Date: 
November 9, 2016
Document Release Date: 
March 5, 1999
Sequence Number: 
3
Case Number: 
Content Type: 
MISC
File: 
AttachmentSize
PDF icon CIA-RDP83-00423R001200820003-5.pdf133.48 KB
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Approved For Release 1999/09/10 : CIA-RDP83-00423R001200820003-5 Glycol estsrz of pyropbosphorous acid. addn. fa Dot 1ad.y &JQ d . !Tauk . `. ; . S CPYRGHT cunt of 0 and a base pv'rid: t e 40r (CH20 and dietn, of the n20 l>4903. + i .1ar1y v e e0,, b.,, 00 b144-5", d2O L"[e0 b2 e obtained.- 20 . 8201 and ; they r .I ikonorov, 0.U. 'edo rova, C . -Vlnokrova and .0. Shi- buz ?Oa with 0 dild. with 2-3 parts ed by 3 bra. at room temp. gave after filtration 44, 5% OCTeC.OPOPOC es M: e2N'fPh, or about -50 801.46281 44` OCR(CHVC1) CH. oPOPoCH20-11- apt '"1.5180; 34.8% NiINJ 29, n 111.41745. Theme e readily add t violently with H20. Treatment. of 001H 0 i1 01101 oo? ing, in Et 0 gave after sepn. of pptd. sC1 orreepondl 8201.156 cue led. b 293-40, dzo .1.446, '1.4600; bS90.10# dZ01.l592, 1.4515; di-Bu. 10.2%, 3-4 0, d 1.1405 530;- di-iso-'r 201.4557; di-Pr, b,104-5?1 Similarly were tormadr 68,1% 0CIteCHaOPCP(C t)2, 201.4520; di. analo ,, 33.so , b.1100, 82.:i...1090, analog, 24.5 , b888_81J, 8281.1070, nr` 1.45300 20 b3120-1 0 j d .0300 x 1.4554; 58.8% 0C McCH,01f P(O; t b4110-1 8201. 064 00H(O: 0 1,4563; 81-Pr analog- 8201.1368,, n 201o4460; 40.1% dt..Bu analog, b, 152-.6?, d20l.0865, z 01, 4580 H OPOP(OEt)2, b112110 P01-1 { 0CH1 0 #3, %100-la, dD.fl1 4295, d20l.2,00, d Z01.198 phoe,)bit nn01.473. These esters possess s. The ;die 801.1990, n -1,4 b0,98~-102?, Gr di-Bu analog, b3147-50?, usual properties of the of the higher unsym. esters are reduced by the (It shown)di--. , 6D , b284-50, 2X1.4660; 2 di-Pr A~ppro mid or'ke e sea19 /%1V L N&3?db'423R001200820003-5