SCIENTIFIC ABSTRACT BERAK, J. - BERAN, J.

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BEW, Jozef, dr.Inz.; WCZAI,:')KI, Romuald, mgr.; 'WOjCIK, Jerzv, rrr.; Stufar, mgr. Bontonlif.,s. Wlad chem 14 rcl.11:693-716 1 160. 1. Klerownik Laboratorlum Syntezy 1,11oncmi-row, Zaklad ll'aukovc- Badawczip, Zaklady Chemii Orpanicznej, O!3wiecim (for Berak)P 2. Starai inzynierowie Laboratorlum Syntezy Monomerow, Zaklad l(aukowo-Badawczy, Zaklady Chemli Crp,,sAnlcznej, Cswieclt (for Guczalski and WoJoik) 3. Kierowrik Fracownl badan Struktu-alnych, Laboratorlum 3yntezy ~bnomerow, Zaklady Ohemii 0rF,,anlc-,;,nejl, Oswiecim. (for Zalwert). t44 1,4 qt, -9r'. BERAK, Jozef, :11.; GUCZALSKI, Romuald; WOJCIK, J.-ray; ZALWERT, Stefen Urp,rading of Polish made bentonite by acid treatment. Pr-,,.em rhem 39-no.1):573-575 S 160. 1. Zak:lad vaukowo-Badawazy, Zaklady C;h,gmiczne, Oswiecim. BERAK, Josef On possibilities of substituting fluorine by oxyger. in apatite. Chemia stosaw 5 no.4:565-57) 161. 1. Katedra Chemii Meorganinnej 1, Politechnika ', Wrcclaw Katedra Chemii, Wydzial !nzynieryjno-bk(:,nomiczny, Wyzsza Szkola lk)nomicznap Wroclaw. MUREA, Larisa; WERMESCHER, B.1 BMUL, H. Applying amperometric titration with Ueo eleotrode indicators in drug control. II. Bromination reaction by substitution as applied to reaorcin. Rev chimie Min petr 12 no.12:723-726 D 162. 1. Institutul pentru Controlul do Stat al Medicamentului al Cercetari Farmaceutice. (Drugs) (Broadnaticn) (Romoroinol) EF"K, Jozef Phase eqvdUbaria in the system CaO-F2Oi--CaF2. III. The uystar C 3 4 -C&(PO3)2CaF2,1 Rocz chomii :). -41 -S2* a (PO )2 36 no.3z4O3 9 1 1. DerAtrtment of Inorlan' - "iemistry 1, Institute of Tochnolcgy, Wroclaw, and Department of Chenintry, Faculty of .-,"ngineering and Economics, Hi-.h Schot '11 .~- r-.L.; I I..' ~ .,j & MRAK, Jozef; A=UROVSKI, Edward Phase equilibria in the systems UO.-P205 arld U03-P205. Rocz ch3mii 36 noo3:553-556 162. . 1. Katedra, Chemii Nicorganicznoj I, Politechnika, ~~oclaw. BERAK, Jozef Basic principles of the phases of thermophosphates be,sed oln calcium metaphosphate. Przam chem 41 nci.~:74-77 F 6,'.!. 1. Katedra Chemii. !qieorganlcznej I, Politechnika, Wroclaw i Katedre. ^~hemii, Wydzial Inzynieryjno-Mcvnomiczny, Wvzsza Szkola Ekonominma, Wroclaw P/0 1 62/0it 110021'Jo 1100 1 D204~D303 AUTHORS Berak, J6zef. BI, , Guczalski, Romuaid, 1100cik. Jerty anti Zalwer7779-fefan TITLE: Synthesis of butadiene from eThyl alcolic." lain, thermodynamics and catalysllz- FERIODICAL~ Przemysl chemIcznyj v. 41, no 2, 1962,. 810 321 'iintoric.,l account, based on boviet and Weszl!rn work vt~Z-' )f %i',c Lebed-v :31ngle-iitaga proceE5,,:; :,or the i3ynth,~- z; i. s-)f ',u'A-,adiena: 2C 2H, OH ---+ C 4 H6 "' H 2H -,;j (Eq s tv r e:3 s I ng 2 C the :.mportance -.)f the choice of catalyst, :)n the yield, Earl:ier Stu- d.-Les of the compiex mechanism of this re;i:tii;n arE. -.hen des-ribed. acce ting the ccnciusions of Gorin (Ref 11. Trudy iNIT-SK, 1, -~,r 1 94,9~ The firsi stage is thought To be -t1he dehydrojrenat---~n CH"~ - 2 OH -> CH-~ ' CHO +- H 2 (Eq, 2),, followed by condensation of 'the a,~etakdehyde- 2CH [CH CP~)I! Clio CF.71 CH Clio 'lard 1 /7~ P/01 4/'c.2,/ 041/ 002/301 /0,01 'iynrnesis of uutadiene from ethyl D204/D-503 Off - CHO - H,,) (Eq, 3 ), -i,he t~ -- u group In crotonaldcOlyl-- A -hen hydro,:enated w.ith H-) removec from the et'ianol. CH, - Cil, "H,-.jH -.-P Cfl., - CH -= CH - CH 019 - CH~ ' C11C) Y, 5 2 d~;'!I' ~nd isomerism yields biitadlene, C11, - 1,:.i "if C-H M 2 -4 H-0 OR CH , CH -- CH, (Eq The Present a~t-crs r,, rl a~ 2 c: b,) i --n ~onsi-3t~i of cair;uiatine, ccnotan-~' 1 5; for 300 7001. 800 ::.nd )000')F- Kp r 400, 5W bOo P'Jc~- 2 were cal-~,,alated by the melhod of Uli,:h (Ref. Ka rape tyans, Kh1micheskaya termodinamika 1~r~w~ 194qt,, from the heate of reu~:t--,n .-Lr.a eciropy .uplq- f.~r Eq. 5 - 5 were computed ty ,he .'Re f fr,,m T-ht, mas (. - 36~ Trane Far, Soc 44, 230. 1948), mi: potentlal3 The val'iies are tabuiatea~ the the choice of the optimum temperature for the pro-ess -nd on kAnet!~ factors. In the remainder of the T view the work done outside the USSR, son(erned viith ---t3 ly it is -oncluded that the beat choice would be MG0 an:i *he Card 21 3 37 -, ', I A)1,1162104 1/0,"2,/ Go 1/001 Synthesis of butadiene from ethyl -3204ID5(~f exact properties depending on the method of prepara,.:~.on and i)-,n ad- ditives. A high activity catal st, B-4, developed at the Zak*'Ead natzkovo-badawczy ZCh 06wiecim ~Scientlfiz, -Researzh InstIt-a-le i~f ,h,-- Chemical Works O~wipcim) will be described in Pt, iI of thi3 work. There are I `4ure, 1 taule and ~?7 references; )7 Srirjet-'O'.~(, an.: 20 non-Soviet-bloc. The 4 most recent references to ;he E~IgL-.oh- language pub!ications read as follows. J. Bremner and G.. Minas, Trans. Far Soo., 44, 23u, 1948; H, Jones, E., STan.,.y and B, Cvrp-~,rj J . Am, ljhe, Joc-,- M 1822, 1949~ B.B. Uu:7son. H.E- Jone,3, (,,E- Welling, ffincx1ey and E-W. Sianly, InI.. Eng CnF,r,,., 42' -;~r)q' 195CI- G.S,, Synthetic Rubber, New Y.:)rkl, 1954, AS30CIATION; Zak~"ad naukovo-oadawcyz ZCh 0,!)%&ir-cim ~Sclent--'..c Rp-- search Institute of the Chemj-::aI Wozk-3. OwiVc--m) Card 3/15 ,BIMK', Jozef.14.; GUCLUSKI, RomLald; WOJCIX, jerzy; Z:;Ik?F.!iT,, Stefan Synthesis of butadlene from ettohyl al,:oh:)l. II.z Inivatigettion of the activity of the B-4 catalyst. Przom chism 41 no.3:13-C-133 Mr 162. 1. Zaldad Ilaukowo-Badawcz)r ZCb Osvieclin a BFZ=, Jozef M.; GUCZALZKI, Romald; WOJCIK, ~'erz7 Synthesis of butadionie from etbyl alcohol. Pt. I, Ialuence of betonite upon the vality of the cataA:rzer. Przem chem 41 no.4:190-191 Ap 62. 1. Zeklad Ilaukawo-Badavesy Zakladow (:,hemicznych,, 1),3wiveim. LERAK, Jozef M.; 'JULA16KI. 'A',~CIK, Zerzy Synthesis of butedinne frax, ethyi alcol-jol. It. 4. of SiO2upon tba decmposition temperature cf - l,.y-,l::-Gxl*de. Frzem ch6m a no.5s271-274. Eu 162, BERAK, Jozef M.; GUCZALSKI, Ramuald; WOJCIK, Jerzy A new basis of testing the activity oJ' butadiene catalysts. Frzem chem 41 no.61300-302 Je 162. 1. Zaklad Haukowo-Badawczy, Zaklady Chemicans, Oswiecim. BERAK, Josef, 9.1 GUCZALSKI, Romuald; WOJCIK, Jerzy Influence of carbonate upon the properties of the M9(0H)2-Si02 system. Prsem chem 41 no.7:38(~-392 Jl 162. 1. Zaklad Naukowo-Badawczy, Zaklady Chemiczne, Oswiecim. BERAK, Jozef H.; GUCZALSKI, Romaald; WOJCIK, Jerzy; ZALWERT, Stefan Cation exchange and thermal treatment and their influence upon the rehydration property of montmorIllonite from Xielce. PrZem chem 41 no.l2t692-695 D 162. 1. Laboratorium Katalizy Zakladu Naukawo-Badaweaego, Zaklady Chemicine, Oswiecim. BERAKI Jozef.M.. Refining conditions and the acidity of bentonite from Keilt!e. Przem chem 42 no.1:28-31 Ja 163. 1. LAboratorium Katalizy Zakladu Nau,kowo-Badawcz(jgo, btkln-ly Chemiczne, Oswiecim. Oil Ap CUCHOSLOVAKIP./tnalytical Chemistry - Analysis of Inori,,ttnic E-2 Subotancos libs jour Rr-f - Kbimiya~ No 41 19581 No 10973 Auttor Lub~c-iir Dera!-.-- 1-1st 1% L GiVC1, Title Direct C',ji.iplexorionettical DeterrAnatiori of MagneGikn in lairninuri lklloy3 with Erio Chrome B3.ac',,-. T. Orig Pub llutniche listYi .1957, 12, No 5., 434-343 Abstract 1" Licthud of 1.1t; d,-.te-.TAmtion in Al rilt)y.3 without ar~~ prelininary suparatiin of other ulcrx~n-~s, which can b(-~ concualad, by FCU and and triathanolruAne, wnE; developed. 1 r.-LUt. o)~ 96%-ual MN aclution cuid 10 rlit of thiethal-, conceal 100 ng of 'd, 2 mg of Fe, 5 !ig of Cu, 1 no of --~ti and 5 rig of Ni in 130 to 150 31it of a so:-uti,:r. at 15 � 20 and pH of about 10 in prt;sence of ML;,Oll,. ca and Ti in usunl. anounts (under 0.05%) do not inlf-,rferc with the doternination. I g of the alloy (--0.4% of Mg, is dissol-~ed in 20 ,.11it of HP,1 (1 : 1): the solutior, Is Card 1/2 L CZECHOSLOVAKIPt/Analytical Chenistry - Arwalyais of Inorgt~!dc Substan,.Q3 Abs Jour : Pj2f 22iur - Khiiaiya) No 4j 1958p No 10973 Card evaporated to about 2 to 3 allt and cUlutcd with wr-'-.cr to 200 nlit. 80 mlit of water, 10 mlit of' triQtbanolruainc and 10 --LUt of the buffer solution (11 g of t4114Cl ~'Tr, Wit C)f concuntrated MI),011+water up to 200 ri.*U.t) are add~ad to M ralit of the obtained solution) it is kcpt in a wat~--:.r bath at 150 untll tho solution baccmcs trancparent cr a littlu cloud,v, 10 rLlit of frostily prepared 104,11-uaal YCN solution and a little of Eri(D Chrome black T (mixed with NaC1, 1 : 1:! arc! added, and 5 minutes latur it is tl.tratcd with :i O.ol 1-1 coriplexona III solution until a lig)it-bluc colorati-Dr. appoars (until grcenish coloration, it Fe was present). 2/2 BERAK) L.; KLIK, F.; KOVAIJC , P. Some reoults of nuclear research In Czechoslovnkia. Vestnik CSAV 73 no. 1: 60-64 164. DERAK, I.ubomir Activated barium sulfate as microstrontium, sorbent. jaderna enorgie 9 no. 12:392 D 163. 1. batav jadeTmeho vyzkumu, Ceskosloveriska akadeirde ved, Rez. :.nalytical Cho-mistry. 1.nalysio cf E-',,, InorCmic Substanoos. "bs Jour aRof Zhur - Khim., No 10, 1958, N,) 321.7-1. ,',u Qior tbiborir Dorak Inst I Titlo :Rap! I ComploxonomAric Dotorminationo f Zn in Cop]:cr ;,Iloys Orig Pub iHutnicko li3ty, 1957, 12, No 9, 817-EI18 i;, mothol of Zn dotonninatiun is d oso ribu~l. it~ is bascl, on bindim,, Zn (Cu and Ni as vroll) in. cy-mido c,-,.IpLoxcs (ot;hz)r intorforing clumunts ara traneforrod into complox)natcs), tho follov,in,,, dissocirticr. of tho Zn cyL-::.idc complux -v-ith fDrr:ij-l- 2+ - dohidu and tho titration of soparatod Zn -.-;ith a ccnplfxc.n) III solution (1). 0.5 g of tho ftlloy is Jissolvcl in 10 mlit of concintrntod FD103, tho solutim iii ovauor%tod Lntil t-h-: N oxidus aro oliminatcA, dilutod with -vattor to 100 nlit and filtorod. 20 mlit of tho filtrato Ui dilutol vriti vrator to Card 1/2 CZECIIOSLOV,KI:, / '.jlalytical Chonittry. ..mlysis Df E-2 Inorlanic Substrnoos. ,bs Jour Rof ,hur - Khim., No 10t l9SB, No 3217,11 NO T'lit. 0.L05 ~, of ?J'12011.11CI i-q ftJd:A, suirrod (I Qioro was than 0.5"~11 of Fo, 2 g of' K-111:i tartrato is t0dod), 30 m-'it of buffer solution (5,.' g aru diosolvor.1 in wa- tor, mixod with 350 mlit of conciaitnttod Nlf...Olf anI dilutol Yrith -.-titcr to 1 lit) and 30 mlit of ~',,-ual XCII :-~ )luti,-,n aro iritrc,ducod; all i s cooled to 150, Brio Chrrmo blacks I (a mixt,,;ro with NaCl, I 1 100) is addol until tht; colcr b~.conos viol,, t ir wino-rod and tho solution i a ti Izated id th 0.01 M solution of I until the color chringos int:) blue. 10~-ual solution of CH 20 (1 to 3 mlit) is aildcl t, the -ti--.r.-.tod sclu- tior until the color changes into vrino-rod arid 2 or 3 drop aro addod and tha titration Yrith 0.01. M solution of I is rosumod addinC tho CH20 solution -at tho samo time until tho color mmains distinctl, bluo. Tho crmr cf Zn dc;torrdn~.ti)n is P1.18/minus 0.1',. Tho mothod is applicabl- t3 tho analysir. of a series of alloys containin6 Sb Mn, Ni, F and Sn. Cr~rd 2/2 B~L.j MURICH, J. 'gijififttion of strontium from calcium by selective procipitatIon of strontium sulfate. Coll Cz chem 26 no.I.i Ja 161. 1. Institut fur 4mforachung, Tache chof lovaki ache Akademie de'r Willaensfgten, Prag. (Strontium) (Calcium) (Precipitation(Chem!;rtry)) (Precipitation(Chemistry)) BAKALEYNIK, Ta.M.; BERAX, L.A. The VP-350 air distributai. Sbor.rat.po avtom.pro!zv.prVt3.!. disp. no.5slIB-121 160, (MBA 11;: 4) 1. Konstruktorakoys byuro "TSvetmetavtmatika." (Fneumatic control) MEIKSWIMIA BERAK, L.; WINIECII, J. Inistituto of Nuclear Research, Czechoslovak Academy of liciences, hez near PrNpe (for both) Prague, 11ollection of Czechoslovak Chemical Communications, No 2, Feb 1966, pp 881-901 "Barium jTulfate activated for sorption of istrontium by heat trew.,nent with caicium sulfate*" BERAKDWA, A.; TOKARZEWSKA, M. I A conference on prob1nma of 'progress In the field of obta!.ning and processing polyvinyl chloride. Przem chem 4L no.7sl,00- 401 J1 162. MMAKOWA I A. Conference on Prograss in Preparation aud Processing of Polyvinyl =aride. Polimery tworz wielk 7 no.7,/P:233-234 Jllg t62. IA t 1 101. A y. Ch~jrrllcnl rrrdurtr., rel he, (,-A 4. on. Iirf, A~:i Jour 14, 1?5-, .',uthnr Bor-1 I r.- t - ............ 7itle In-mprtibl-a ~'rscs nf ,' * . - r~ r :, :ub a r e. 'n y c. i i n i a i i i !i N, IL I 5'~~ N ",m-tro-ot-ii F. t, 41 i c c it Prepi.ra LJ n n -7 11.1t rrIF1 C. i 1~ ROM n ?I N() 'i ~..i c. t Tp k t! ri p t, )fit) of .9everal and r a T) i ~.eter-- m j. naf j r n methoils- for wt,jou-, T)L,~T-;;IFcpuL,j c a I v, i x t -,: r v:s and proprirntionn that 4o not rr,(virc tilflot; atl(-. eollld br in t-it"I of 3ctlvr~nt. 'ryo-geni,e(i ---.P deter i a niLti n r. in e t h od n v f,-.r ih#! lollowing mixtures: and pyra-ii'nji; phenace- Line. ctsr);.ri., and raffeirip; phenacciirp, an- ne , Filitt llirrinc urctropine, sF.Inl Grin-,.escu, T'. rl c,,j n L ry 'I-L7 V-in-,ry ~cory H47; U'7ur 1959, ,~I:th- r -.i rr, CHIOOOLTI..G.; BAMp ^.; VASILIM. P.; FOWTICH. N.; MSHIN, Azimi; HADZRMIU, K.; TAMB, A.; LArATOSH, L.; DIAKU, D.; PArRASEM, S. Determination of bismuth in Razanian &M99 by means 5f AM titration. Apt.del-o 8 no.6:67-67 N-D 159. (KM 13 tO 1. Is Instituta po lintrolyu kachostva madikamentov Winisterstva zdravookhrananlya Ramynakoy NiLrodnoy %topubliki, DWenarest. (BISMUTH-ANALT31:3) SUX,Al-'-7, Given Na:wa COUntrYI Rumania 1112 Academic Dogreess Affiliations SOurcOs Bucharest 9 Parnagla 9 Vol L- 9 No .7 P Jul 1961, lip 403-411- Data$ "Study on the Conservatiol of Vitapd.ns Al B 11 and 0 in Vipl6x 19 2 and Folyvitamin Products.' Authors: -BERAL.,_Ii. 9 larisae Mmsu C I IA-00 B A. Work performed under the auspices oj'.' the InAti1tute rar th St t, Control of _ stigatioffy 2118C.ItUM-L .LDMW_a and Pharmaceutical Inve - -T -1~-oifi-fr~uc~n-tro-I-uY--d-o stat &I FwdTO-wi)-nwjuj al Carbetari Parmaco, SURNAIM., Given Namas Countryt Rumania Acidemic Degreest LffiliatA=S Ins I of Dru a and ~Pharmac nagkit --71nuestioWsw Institutul pentruT55tara"Ta do -Stat 2x== ~entului si. Geroetari Farmaoeutios). Source: Bucharest, Patmaglas Vol IX, No 89 Aug 19619 pp 501-504. Data: "Study on the, Conservation of Vitamins 111, B29 B6 and pp-" Authors; BERA j_t;~ -?hermaciat.- -SUR a_1 isat -Pharmacist.- tguU, G:f -Pharmacist.- IAOOBj A I -Pharmaoiste- Cal L., (J,-. ct,7-jT, GIven Names co'Intnf: Rumani a Alia,dv"-Ic Affiliation- Source: Bucharest, EarmSgiat Vol IXI No lOv Oct 1961, pp 661-668. Data: "Methods for the Determination of Water In Drugs." Aut)-ors: 4TIERAL, H., -PhRrTnaciet.- SMICESCU, Viorica, -Pharmacist.- GRINTESCU, Poulim, -Pharmacist.- 1.13rk performed under the auspices of the Institute for the State Control of Drugs and Pharmacctutital Research (Institutul pentru Controlul de Stat al Medlearientului sl Cercetari Farmaceutice). SERAI., H.; POPESC-9, D.; CONSTANTIMCU, T. Determination of 5,6-dimethylbenzimidazo'le. 'Rev chimle Min petr 13 no.1:54 Ja 162. NWESOMR, B.1 MURU, Larioa; - BERAL) H I - Methods of amperometric titration with two indicating electrodes, applied to dmg control. --11. Determination of sonw) sulfamides with potassium brM:k!LtO. Re-r chimie Hin poix 13 no.2:105-107 F 162. 1. Inatitutul pentru Controlul do stat al modicamentulul ai cori.,etari farmacoutice. WERMSCHER, B.1; MUREA, L.1 BERAL, H. ApplIcation of* the method of amperowitric determination iclth Wo electrode indicators in the cont,!-ol of medicaments. I'1. Rev chimis Kin petr 13 no.3j172-17.3 Mr 162. ildj.'.~Ldl-. lr,L;titut,p- of estate Gontrol of 'A,~dicinr!:.; r~nu ilh:-Ta(~7~.uttcal -,,!rCil (Irrtitlltlll Pentru control'.'. de ,;Irlt ---I Mf ~ al cdcamont(,lor si Cerceturi famw cm-~.Jce) - ~for - A) ~,lucharf'..'t, FLMacilk, No -tr "Application of A.MI)L-I'mc-tric 1.1trt.-UGn -Nitn tivo acc~rouer in thr~ Control ol o:.' thf: Con(ii'dons of Ampermetric ii'u-&-,don c.L' u(,~rt;.in L-IL.font.- -.-,,ith u Ulver Hitrate '-oiutiozi.11 (5) BERALS Hq MUREA, L.; WMESCHER, B. Application of the amperemeter method vVI two indicator olectrodes in controlling medicaments. IF. Rev chimbt b1in petr 13 no,4t239-240 Ap 162, BERLL, H.; WFMIZCHER, B.; MUREA, L.; MADGEARU, M.; CUCIUREANIJ, E. Wokwa-ft ~w it MW -Ampwremetric study of the oddition react-ion of br6mine to double bonds illuatzated by the determination of phancxIorn and evipan. Rev chimie Min petr 14 no.1:49-50 Ja 16,1. 1. Instit-atul pentru, controlul do stat at medicamentelor si cercetari farmaccuticeo w H.; MURZA, L.; WMESCIER, B.; MADGEARU, 1l.; CUCIURF.ANJ, E. .!!!2 - Study of the amperemetrio titration corxlJ.tions of somw sulfonamides with sodium nitrate solution. Rev chimio Mit pett 14 no.1:50 Ja 063. 1. Institutul pentru controlul do stat Ut medi came nte Lor ai cercetari farmaceutice. EML) H.; CONSTANTINESCU, T. Determitation of p-axypropiophe none in 5-365 phrenarythol tableta. Rey chimia Min potr 14 no-4.2.15-06 Ap 16.3. 1. Institutul pentru controlul de stat sl modicawnt4-lor al cercetari farmacoutice. LIM A L H A RPES',: I E::', i, kmperame tri i al -~ 7,1 :-,g IX.-; I t r~r gar, ~761. D 6, I n9 u fo~ n ~ntrf)l Ci I MY i ei C B"FIALP 11, ; W:RW.XHF:R, B, j MUREA, L. ; GUCIUJC-,ANU, E 1 - ; M. Stlidy of the amppromatric dosing method iising corlum sulfate its a titrAtion agnnt with npplirittlon to the prowthfusino datermlnRtlon. Rev chimim !~ir, petr 16 no.2, 10 5 F '0 5. 1. in3tti.11t5 for C)tata Control of Mwile-i!ie anti FharmacautLcal 11pnearch, Bucharest. T-1VT t /I I T r T(c ) jr)/-Iff-, - - . ~ - - 1. - I .. 166ol[65101610021010510105 I ACC NR: AP6C23VI-1 SOURCe' CODEt R~ am, 11. 'hiren L.; CiicluronEu of' DriiCp m0j'harmacoutical losearch (IrwtitutU:L PC) I Itru I- 1 "11 J-!1(,xioAo1or vi covcc,tarl farmacouiAco to as i 11,~ -f doterni-ration using cerium su-1pha titration 'I 'r-1-1-1 1-1 la-L app.1 i'-:11,1011 to U10 doterrdnation of promthazine 16, no. 2, 06 1 -, 5, 105 L t,10--atdr)-1, coriii co n rTpoulxj t-mi~yl that, ai-q,-.-tromotric titrction u3ing ~i!rAjuj sulfate is a oat!,; 1 Vor t.i~o il-t,:wizination of prom,liazino with an applied curront of 10 to "'J 1111-:At, ~ ',i'intinw-i i-loctrodes and tho vulfuric acid concentration ma --: nt, I. orrnr of Um mthod Is v.1i:hin +0-70 percent. Orig. art. has: i I alvi I Z)Ui") 0'/ 0,11! 1;i-:F: oW ard i/I L -C., 0 'tVs,- _L,_3_49c)0-66 r6MR-,X!16c~i66~6 SOURCI~ CODE '-ffu-[666j-[6510:.- 1665-162W0203 F 6 / AUTHORt Baral, if.; Igmt, V. arc ORG: Inatituto for the State Control of jrua3 and Phari! coutical Ross) h (Institutul pontru controlu do stat, RF modicamontelor si corcotarl farmaceutico) TITLE: Determination of p-acetaminobanzaldohyde -isordcoti-noyl-bydra zone in 11M tablets SOURC?.: Reviata do chinie, v. 16, no- 5, 1965, 293 TOPIC TAGS: bromide, b::-omate, quantitative amlysis, pharmacology, drug AB37-vICT: The authors describe a brononetric nothod for the direct doterr-dnation of of tha active substance from the powdered 11-HIA tablets. The nothod !involves troatmont! of the porwder with an oxcoss of a bromate-bromide rzdsturo in dilute ]Vdrochloric acid modium, followed by ret1tration of the excess brordne. The method !.;s silvle and pm- cise, with an error of 2.32 percent* Orige art. hats: 1 table* ~JPRg SUB CODE: 07, 06 SUB14 DATE& none ORIG RE;F: (101 O-17f RIJFt 005 Card 1; 3o773-66 1 ACC NR, AF66-10261 SOURCE COEE: RU/0003/65/6i6 1.'-/C600/(D601 AUTHOR: M'urea, L.; Beralt..H.; Cuciureanu, E.; Madgearu, M. ORG: Institute for the State Control of Drugs and Pharmaceutical Research .L. (Institutul Pentru Controlul do Stat al Medicamentulu.1 si Cercetari rarrna6leutice) TITLE: Determination of methoxy-3(dimthylamino 3-niethyl-2-propyl.)-l.C,-phenothiazine (Nozinan) in pharmace-.iticals SOURCE: Revista de c:-iimie, v. 16, no. 11-12, 1965, 600-601 TOPIC TAGS: amperometuric titration, pharmacology ABSTRACT: The authors describe the amporometric deterr.-dnation of Nozin-in t*IF~tc' and liquid. The methDd elaborated requires approximatelY 30 minute5 F-r de-.erndna1',-.oA and is more specific, more exact and sim ler than the gravizietric wthod u;:ed Orig. art. has: 1 fij~ure and 1 table. Fit-Tis] SUB CODE: 07, 06 / SUBM DATE: none Card L 39125-M WMNR. AP6030354 SOURCE CODE: RU/OO()3A,-;/Ol6/OO3/O16q/O169 AUTHOR: Beral, H.; C Dumitrescu E.- Orintescu -L. .2? -_==== ___ &Lifeteanu.- Ij -----L B CRG: Institute for the State Control of Drugs and Pharmaceutical Research (Institutul pentru-c-o-nrr=5ur-Ue--5T-a'*,, &I medicamentelor sl carcet I rarmaceuticilr- TITLE: Quantitative determination of 7-chloro-2-mothylwuino-5-phenyl-3H-1, 4-benzodiazepin-4-oxide from libri= pills p SOURCE: Revista de chimLle, v. 16, no. 3, 1965, 169 TOPIC TAGS: dioxane, chloroform, perchloric acid, tranquilizer, pharmacologr ASS-LRACT: The authors tested several methods for the w-..alysis of LiDrium pills. Beet *esults were ubtaired by titration with perchloric acid in dioxane as titrating agent, of the ground pills dissolved in ch1wroform. Methyl red was the most effective indicator. Orig. art. has: 1 table. [JPRS) SUB CODE: 07, 06 / SUBM DATE: none / OTH REF: 00~'i "7 64--' Card 1/1 T, 31,90-1-66 ACC NR, AP6026622 06;'Ji-~:--vu /dboj)i;~/o WO 0-96~Wla-�~' AUTIMI. 11 ; lyanC Stoicoscli, V. WG: Inq=uto fox! ;ho State Contr-QLo.L.Drurc and Pliarmacoutical Research (Inatititul pontru controlul do atat al modicanontolor si cercetari farnacoutice) Dote rrr1nat-1on of 11-mothyl-3-1)on,-,oyl-4-hydrcocy-4-phark7l-pi.poridine hydrochloride and procaino hydrocUoride in injectable A.L.U. SOURCE: Roviota do dUrdo, v9 16, no* 5, 1965, 2-94-295 TOPIC TAGSt quantitative ana2ysis, chloroform, porchloric acid, dioxane, pharma- coloC.y, drue., AES,-7U,CT: Tho authors describe a method for the datorrdnation Jii nor.-aqueous modium of 11ds anesthetic substance, either pure or as tho injectable solution. 111he method involV03 titration in chloroform solution vith a solution of porehlorio 8-cid in diw:ane, using ratanil yellow as indicator; it in simple and acmiyate an(i is oug- gested for uso in quality controls Orig. art, has: 2 tables* LjPR-E,7 SUB CODEz 07, 06 / SUBH DATEs none / ORIG FZ-Ft 002 / OTH REF: 002 227-66 WCC"916-AP6031575 SaWE CODE: RU/0003/66/017/0()1/0046/0( AUTEOR: Mures, L.: Beral. H.1 Cuclureanu, E. MacLqe.!ulu, M. 9 ORG i -Institute for the State Control of Drugiq~ and,_!)!.ologic 1 Product3 (Inititutul, pentrix controlul de etat al madicawntelor si cercetari far-micouticeT TITIE: Amperometric determination of some barbituri(~- derivatives by mean3 of silv,3r nitrate solution SOURCE: Revista de chimiep ve 17, no. 1, 1966, 46-4'? TOPIC TAGS: amperometric titration, drug, silver nitrate ABSTRACT: The authors determined the optimal conditd.ons for the amperometric titration with two indicator electrodes of luminal, reronal and anital with silver nitrate solution. Quantities of 0.03 to 0.1 grams can be determined with an errcr of :tO.23 to :LO-32 percent. Orig. art. hast 1 figure and 1 table. IMS: 36t0021 SUB CODE: (Y1,, 06 SUBM DATEt none SOV REF: 004 / OTH 'W: 009 Card 1/1 7-WJ& MM Cox# W1M*31&VQL?1WW50A" I Mi now TMXs Deten&nation in non-equeow imedim of I-ethyl:& 7-wtM1--1dV-n4VhtiriUw0 4--on, 3-c L12 Add SOURCEt Rovistal do chdLideg T. 170 no* 1. 1966# 50 TOPIC TAGS: qutntitative analysist organic solvent ABSTRACT: After teetir4j dimethy1foramidep ethylene& aminop mothanolp bensew ad mixtures of these asi solvents for the determination of the product$ the authorm determined that best retmlts are obtained vith othylwe diamine, using aso-v6let an indicatort ce with a 122 mixture of dimethyl-farmsmikle and wthwol, using thymol blue as indiostore Origo &A. has: 1 table. [.JPRSt 36,,0021 WDICe 07 SM 1ATES' none / MIG MWo 001 / OTH FdWs 002 7 A- 7" 7 1 7 C..-t t-,- ri BE kh. 1Bqr4L-X6j (Bukharost); DFIIEN:SKU :re.(Bukharei,t); STUIC'II-JKU,V. KALAFEULIJU0 I. (Bukhaz-oa'.-,I;GRINT3MKL', P. Methods for controlling pharrraceutic pr-:1parations. Apt. delo 10 no.4: 82-85 Jl-Ag 161. OALU 14:12) 1. Inatitutul do Corcetari Fannacoutico si Sontrolul Modic&mantelor, Bucuresti. (DRUGS-STANDAIC)S) 71- .,I. . I ~ 1. - I ... . 'at.-. -- - deep Jr-Illinj w~,!"' 1'. 23-1 V,)I. 4, 71C. t'2, Jurle- 1).'17, "~,; ""- L- .. - )~q .- '7 :;-. 1, Jd'%". 1.)- - I- . - . - . , . " I BEFUN p A. "New working methols and improvement suggestions in the Prumst..v Natioral Enterprise in flarlubice.11 p. 147 POZE2,91I STA1111Y. Praha, Czechoslovakia, Vol. 7, fle. 3, March, 1.959 Monthly Ust of East European Accessions (EEAI), I.C, Vol. 8, No. 9, Septmber 1959 Uncl. NtUVI, Antonin, inz, , A high-wall frelght car for ore nnd fuel trrinnportntion. ZpI rlop tech 10 no. 2: 58-55, '6) 1 MAN, Antonin Fallwmy cArn for tranmportatien of pov,!,,!r and Frjlr, raterlmlff. ale I (lop to-rh W nr. It7o. 162. BERAN, Antonin Special railroad car.9 for transportation of powdered and granular materials of the Czechoslove,k Ra-ilraods. Inz stavDy 10 no.ll:Suppl.:Mechenizace no.lltl;'7-130 162. 1. Vyzkumnv ustav kolejovych vozidel, Frralha. BERAN, Antonin A new tne oeries Ra tank car. Zel dop tech 10 no.10:3017 f62. CUCHOSLOVAKIA/Chemical Technology. Chemical P:t-oducts and Tbeir Application. Part 2. - Ceramicii. Glass. Binders. Concretes. - Glass. If Abs Jcur: Referat. Zhurwa Khimiya, No 21p 1955~!) 71550. Author C.M. Baran. Inst Title Glass Containing Above 96% Of S102 - Production Methol and Utilization. V Orig Pub: "r a keramik, 1958, 8, No 1, 10. Abstract- The production method of glass (G) containing more than 96~ of S102, and the peculiarity of which is the separation of fus ad S1021 consistij in the fol- lowirq;: first glass correspone-ing to the molecular compooition M20-B203-=2 is melted; its peculiar- ity is the splitting into two differe.-,,it phases at Card 1/3 CZECHOISLOVAKIA/Chemical Technology. Chemical h,oducts and Their Application. Pait 2. - Ceramice.. Glass. Binders. Concretes. - Glass. H Abs Jour: Referat. Zhunral Xhimiya) No 21, 1958, 71550. the temperature close to the softening point of G. One of these phases, the rich one in S102, producce the skeleton of the future porcus glass, and the other, in which B203 and NagO prevailt is soluble in mineral acids; tEe dissolution rate is about I (of the thickness) per 8 hours. Glass treated with acids possesses minute co-inicating pores, dimen- sions of which are 30 to 50 A; its specific surface is 200 sq.m per cub.cm. Such a poroui3 glass lets water through (0.001 ml per sq. cm x hour under 1 atm pressure), its absorption of air moisture is 25% and it can be used for making bacteriological, monochromatic and catalytic filters. If the porous Card 2/3 CZECHOSLOIIAKIA/Chemical Technology. Chemical Products a Their Application. Part 2. - Ceramic3. Glass. Bindors. Concretes. - Glass. Abs Jour: Referat. Zhurnal Kbimiya, No 2-1, 1958, 71550- G was heated to 1000 - 11000, the pores become sealed and glans with following properties is obtained: S102 content - from 96 to 98~, thermal expansion factor - 7.5 - 10-7, softening point - 15000, transformation temperature - 9000, tangent of the argle of dielectric losses at 1 megacycle and 2DO - -5 - 10-4, Opecifte resist!vity - a little less than that of fused q7,mrtz, high acid and alkali resistivity, As far as its Iro- perties are concerned, "Vycor" glass is but little inferior to funed SiO2 and its produ..,tion is easier and cheaper. Prcduction of tubea and little crucibles with W&118 UP to 3 Em thick of that glass was started in Czechoslovakia. Card 3/3 P31W.1, F. Coal defrosting in steam electric-power plant:j. p. 293. -21 ERG 7 CL , IKA. 'raha, Czechoslova; a,, Vol. 9, no. 6, June 1959 Monthly list cf East European Accessions, (M- J) LC, Vol. 13x No. 10, Oct- 1959 Uncl. F. Operating ex,.:~erierces with doulle-draft ~-