SCIENTIFIC ABSTRACT A.V. DOLGOPOLOVA - I.M. DOLGOPOLSKIY

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• Collection: Scientific Abstracts
• Document Number (FOIA) /ESDN (CREST): CIA-RDP86-00513R000410810020-5
• Release Decision: RIF
• Original Classification: S
• Document Page Count: 100
• Document Creation Date: November 2, 2016
• Document Release Date: June 13, 2000
• Sequence Number: 20
• Publication Date: December 31, 1967
• Content Type: SCIENTIFIC ABSTRACT

DOLGOFOLOVAr A.V., doktor mod.nat4c; MAKSAID)VAp
Ye.N., kand.med.nauk
1. . --- I ~ .- ~ , , , , - - ... i.,
"Meimatic fever in children". Reviewed by
A.V.Dolgopolova,
E.N.Makoakova. Vop.revm. 3 no.ls89-92 Ja-Mr 163.
(MM 16:4)
(RHEUMATIC VEVER)

DOILOPOLOV,A,_ Aj, ,,prof.
State and development of research on the problem
of rheumatic
fever and diseases of the joints in childhood
throughout, the
flussian Federation. Vop. rovm. 3 no.4t67-71 O-D
163.
(MIRA 17:2)
1. Predsedatell Problemnoy komissil po revmatizmu
i bolfiznyam
sustavov pri Uchenom meditainskom Sovete
Ministerstva zdravo-
okhraneniya RSFSR* '

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00
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C4wd

UGMEOV, V.M., prof., otv. red.; BEHIMMA, 11J., doktor
red. nauk,
,red.; VOLKOV) Adn,, re(j.;
B.M.,, red.; RAPHKOV, BAC, red.; HASTORGUYEV, A.V.,, red.;
TELEGINA, A.A., red.; YATSUK, S.L.,, red.; LEVIN, N.V.,
takhn.
red.
[Proceedings of the Fourth Joint Scientific Conference of
Young
Neurosurgeons) Chetvertaia ob"edinemaia nauchnaia
konferentslia
molodykh meirokhirargov, trudy. Leningrad. Medgiz. 1961.
414 p.
(MI&'l 15:6)
1. Ob"yed-Inennaya nauchnaya konferentsiya molodykh
neyrokhirurgov,
4tbo 2. lAiningradskiy neyrokhlrurgicheskiy inatitut in.
prof. A.L.
Polenova (for Volkov, Dokzopolova,
YatsW-,,Hachkowl3.Iaboratoriya opera-
ti,4noy neyrokhirurgli LeningrOqkogo noyrokhirargichask
Insti-
.1 Molo 4
tuta imcni prof. A.L.Po' enorva (for Rikiforov,, Telegi .
. Ka-
fedra operativnoy khirurgli poulatricheakogo
11-aditsinakogo institutap
Leningrad (for Miliforov, Telegina) Yatsuk). 5. Direktor
Leningrad-
skogo nauchno-issledovatellskego neMkhirargicheskogo
instituta
im. prof. A.L.Polenova (for Uerywov).
(NE- RVOUS SYSTal ... SURGMY)

5/196/61/000/009/013/052
B194/E155
AUTHORS: Ddi~opolov, V.I., Dolgopolova, L.N., and
Kamayeval G6F,
TITLEs Fluorescent silicate enamel
PERIODICALI Referatiirnyy zhurnal, Elektrotekhnika i
energetika,
no.9, 1961, 12, abstract 9V 94. (Svetotekhnika, no-3,
1961j 18-21)
TEXT: A fluorencent silicate enamel has been developed which
has a brightness and duration of after-glow similar to
those of
the fluorescent plastics now used but which is superior in
respect
of stability of physical and chemical properties and
resistance to
moisture and atmosphere. The consumption of fluorescent
materials
in the silicate fluorescent enamel is half that in plastics.
According to preliminary calculations the cost of one m2 of
silicate fluorescent enamel is a fifth of that of
fluorescent
plastic. The silicate fluorescent enamel can be used for
--aking
fluorescent signs.
4 figures, 2 literature references,
(Abstractor,s notes Complete translation.]
Card 1/1

DOLGOPOLOV, V.I., in:sh.;. DOLGOPOLOVA L.N.v inzh.;
PETROVA, N.G., Jnzh.
-1-- -
Principal characteristics of materials used in
manufacturing
light fixtures. Svetotekhnika 9 no.11:18-22 N 163.
(MIRA l6tl2)
1. Vaesoyuznyy evetotekhnicheskly institut.

DOWOPMOV, V.I., insh.;,j)%G
. inzh.1 PEMOVA, N.G., inzh.;
BELOGLOVSKAYAR T.I., insh.
Blectroluminea cant idide flowsheets and aignal
registerc for
control bDarda. Elsk. sta. 34 no.7s72-73 n 163.
(MIRA 16t8)

DOLGOPOLOVA, N. N.
Dolp!)olovp, IN. N. - "Physical nnd n..,,-rochpr,-lcnl
chjrxct#-r1st4cs of tl,~~ -,!' r,
wooded tteprpe contour under conditions of the
Centrsl-chrmo2er. forert nrPserve."
Tm,dy Tsentr--Cherno7em. e,06. 7Ppovednika, Issue 2, 1948
n. q-',17, - Biblloi;:
1b5 items
SO: U-A355, 11 August 53, (letoPis 'Zhurnpl Invkh Ststey.
No. 15, 19LQ)

S/139/60/000/03/028/o45
.1314
AUTHORS: Stolov, A.L. and
Dol o olova
TITLE: The-Infra-red Specj:r~_j7f, a -Glow Discharje~\
PERIODICAL: Izvestiya vyxslxikh uc:hebnykh zavedenly,
Fizika,
1960, No 3, pp 154 - 157' (USSR)
ABSTRACT: The infra-red spectrum in the region 650 - 6 500
cm-1
was obtained with the ald of the IKS-1.1 spectrometer
incorporating NaCl and LiF crystals. The detector
was a vacuum thermocouple, having a sonsitivity of
I V/W. The source of radiation was the positive
column 6f a DC glow discharge. The use of DC discharges
-led to a considerable reduction in the noise level
and the pressure in thei discharge vessel could be
increased right up to the atmospheric pressure, thus
increasing the intensity of the source. The discharge
was excited in a metal tube with a NaCl window and
water-cooled copper el,Bctrodes. The discharge was
operated at 1 000 V, 150 mA. The spectrum of a glow
discharge in carbon dioxide is shown in Figure I and
is identical with the flame spectrum of CO + 02
Cardl/3 (Refs 6,7). The upper trace was obtained with LiF
and
k--,-

S/139/6o/ooO/03/028/045
EOJ2/E314
The Infra-red Spectrum of a Glow Dischar e
the lower with NaCl. The slit widths were; 1 - 0.4;
2 - 0.3; 3 - 0.19 and 4 - 1.0 mm, respectively.
Figure 2 shows the spectrum of the glow discharge in
air. The arrows show No, NO 2 and N.04 bands. These
1
occur at 1945, 1585 and 1815 cm- respectively. In
absorption, the corresponding wave numbers are 1878,
1621, 1749 cm-1, respectively. A study was #1so made
of the intensity of the CO band at 234( _'L
2 .) cm as a
function of presswre. It was found that the behaviour
of the curve depends both on the re-absorption of the
radiation and on the distance of the particular section
of the discharge from the axis. At greater distances
from the axis saturation of the curve occurs at lower
pressures. Re-absorption has a similar effect and tends
to accelerate the saturation of the curve as the pressure
is increased. A ~:;ixlculation was made of the probability
of transfer of a vibrational quantum on coll6sion
Card2/3 between C02 molecules. The result is 0.2 x 10 which

S/139/60/000/03/028/045
The Infra-red Spectrum of a Glow Discharge B032/9314
is smaller by an order of magnitude than that obtained
by Terenin and Neuvmin (Ref 2). The discrepancy may be
ascribed to the fact that reabsorption and peripheral
regions of the discharge were not taken into account in
Ref 2. The above results ror the probabIlity, on the
other hand, were obtained by investLgating the CO 2 band
at 4.6 IL, where reabsorption Is practically absent#
There are 4 figures, 1 table and 14 references, 12 of
which are Soviet and 2 English.
ASSOCIATION: Kazanskiy gosumiyersitst (Kazan State University)
SUBMITTED: Muly 17, 1959 k-111"
Card 5/5

DOUIOPOLOVA, N.R.; )WKIZIR# P.T.1 WARTS, VA
Effect of development conditions on the shape of
the spectral
sensitivity curve or ungensitizaA pbotogravhIc
lavers. Zhur.
nauch. i prikl. fot. A kin. 8 no.3:185-189 My--Je
1153.
(MIRA 16:6)
1. Filial Vessoyuznogo
nauchno-iseledovatelle):ogo kLnofoto-
instituta, YAzan'.
(hotogmphlc seneitometry)

NIKISHKINAq F,I.; DOLGOPOLOVAs R*V,
f%nil conditions for %he effectiveness of borort
fertilizers.
Thchvo,edenie no.11&70-78 N 164 (MIR& 18 il)
1, Pbehvennyy institut imeni V.V. Dokuchayeva
P14 S S3Rp
Moskva.

L 0
,.72~L-67 , D~(d)_
AIL(_ NKt AP6018636
SOURCE CODEt Ui-/-6-i(i8-i-~6-ibb76-/00-3/-05-7-0-/-O--5-7-6--~
AUTHOR: DolgopolovaL-T-. F. (Sverdlovsk); Ivanov,_Y,
K._S5yerdlovek)
ORG: none
TITLE: Numerical differentiation
SOURCE: Zhurnal vychislitellnoy matenatiki i matematicheskoy
fiziki, V. 6, no. 3,
1966, 570-576
TOPIC TAGS: numeric solution, differentiation error,
approximation calculation,
approximation error
ABSTRACT: Various articles dealing with numerical
differentiation substitute the
function f(x), which is -to be differentiated, by &r.
approximatlon polynomial p(x)t
and this is followed by an estimate of the lfl(x) - PIWI error.
However, unlike
integration, numerical differentiation belongs to inaccurate
problemil: one can always,
find cases where for an arbitrarily small deviation of the known
approximate function
fa(x) from the exact one fW their derivatives may differ by an
arbitrarily large
amount. Consequently, there is a need for a theory of inaccurate
problems. The pre-
sent authors use a modification of the regularizing method due
to A. N. Tikhonov
(Dokl. AN SSSR, 1963, 151, no. 3, 501-504) which permits the
establishment of a polyL
nomial pa(x), uniformly approaching E'(x), from the function
f6(x). Tn this modifica-I
tion, an operator equation of the M'st kind is solved in which
instead of requiring
UDC; 518;517.949.12

L 07257-67
that the operator be cont-inuous, one demands only that it be
cloised. The basic re-
sults are presented in the form of five theorems. Orig. art.
haus: 43 formulas.
SUB CODE; 121 SUBH DATE: O3Jul6S/ ORIG REF-. 006/ OTH REF, 005

TKACHEVO I.G.; DOLO:)POLOVA,, T.I.
Influence of the consistency of the overburden soils
on the
occurrence of clay inrush in the mines of Kumetsic
PAsin,
F12.-ta)dl. probl. rasrab. pol. iskop. no.105-89 165.
(MIRA 18110)
1. Vasso),uznyy nauchno-iseledovatel'skiy institut
gornoy
geomekharilki i markshwjdarskogo dela, Leningrad.

V-1
V.Ye.; VASILZNKO, R.I.; VELLRR, R.L.; VMLOVSKIT, A.M.;
VJIRM, B.F.; VOYDAWVSXATA, Ye.N., VOLOSKIT, A(U.; GLAZKOVSKIT, A.A.;
GRANOVSKrT, B.L.; GMffM. N.S.; GUDrMA, N.V.; ffOl"Gh"A,
KARCHIVSlff, V.A.; KOVACHWA, Te.B.; KU.DRYAVTSIT, P.S.; L I.;
LISOVSKIT, D.I.; LI)MITSKATA. Z.P.; MATVEYEV, N.I.; MEWNITSKIT,
A.N.;
MIRONOV, A.A.; MIKHMVA, A.A.; MURACH, N.N.; OKU51, A.B.;
OLIKROV,N.P.;
OSIPOVA, T.13.,- PAVLOV, V.P., ROTINTAN, A.L.; SAWIN, N.P.;
SMTUKOV,N.N.;
SIMOV, P.H.; SOBOW. S.I.; MTMS, IT.L.; TSITM, V.M.-,
SHAMMAzAR01r, A.K.; SHEYN, Ta.P.; SHEMCUITZV, S.D.; SHXbtAN, B.P.;
SHISHKIN, N.H.; SHLOPOV, A.P.
Goorgli Ivanoviah Blinov. TSY~t.met. 213 no.6:62 N-D 155.
(MIRA 10:11)
(Blinov, Georgii Ivanovich, 1911-1955)

/ 0 1)/p 0 /c, A-'q , fie-,
AUTHORt Yefimov, As, ani
TITLE: The FZU Schools
promyshlennosti,
PERIODICAL: Professionallno
p 27 (USSR)
D.olgopolova, Ye. 27-11-19/31
to the Foodstuffs Industry (Shkoly FZU
prodovollatyennykh tovarov)
- Tekhnicheskoye Obrazovaniye, 1957,1# 11,
ABSTRACT: The basic source for training qualified workmen are
the edu-
cational institutions of the Labor Reserves, except for some
branches of industry where the training is supplied by the FZU
schools, (Fabrichno-navodskoye uchenichestvo- Industrial Train-
ing) where every year about 10,000 young workmen of various
food specialities are trained. Thus, 25 to 50 % of the labor-
ers in the bread and confectionery factories are former pupils
of FZU schools. Many FZU` school graduates of the Uzbekkonserv-
treat occupy positions of acting technologists, acting chemists
and instructors of practical training. The article mentions
two men who have distinguished themselves, one working in the
Pervukhin Sugar Plant (Pervukhinukiy eakharnyy zavod) and the
other in the Kupyansk Sugar Plant (Kupyanskiy sakharnyy zav0d).
At a conference of the FZU school directors attached to the
food industry, it was proved that during the last few years
Card 112 the instruotional-pedagogical work at these schools
has con-

UMAWIcIne Strettococci Noy/Doe 48
Medicine Puerperal Infection
"Biological Proportion and Psotore
Controlling
the-Pycavoption of Pyogenlc Microbes in
PuerDeral
Diseases," A. M. Dolgopoltalmya, A.' A.
Sinitakiyo
Ucterlol Iab, arma for Puqr
peral Diseases,
Con Inat of Obstat am Gyne~LLl -a&--
"Akvaher I Ginekoi" io 6
lbvlwn existing data on sub4ect. Presents
rumdto
of bacteriological Investigation of 48 cases.
CMCIUdes that existing laboratory tests for
deter-
Tr-opertiaw- %-A& wthowao alwCus
do not permit d;t;13Ad evaluation of their
22A 6
MM/Xedlcine -- Streptocoool(Coutd) fti/Dee 48
virulence and pathogenicity. Viralence of
"P ;r. - -%
estwi most clearly by determination of
activity of the propagation factor.- Test on
ao&Lmlase In conj%wetlon vith ef
activity of propagation factor is most
comploU
1n the detAmLination of pathogenic and
virulent
it oper lee of stapbylocooci of puerpea~al
origin.
..22

DOI"OLISUTI, A.M.
Bacteriological features of poll tpartal and postabortion
disessex
due to the use of antibiotics [with summary in Yhglishl.
Akush.
gin. 34 no.1:46-49 Ja-Y 158, (MMA 11:4)
1. Iz Instituts almsherstva i ginekologii (dir. -- prof.
P.As
Beloshapka.) ANN SSSR.
(PUINUItAl. IHMTION. ther.
antibiotics, eff. an microbiol. features of blood &
vaginal secretions (Rua))
(JMRTION, compl.
Infect., microbiol, features of blood. & vaginal
secretions after antibiotic ther. (Rus))
(AIMBICTICS, ther. use
pomrperal & pastabortion infect., eff. an microbiol.
features of blood & vaginal secretions (Rue))

OLGOn'SWA. A
Sew epidemiological characteri sties of paerperal
mmatitis
under current conditions. Akuab. i gin. no
2:26-29 162.
iMIRA 15-6)
1, Is baktariologiclaakoy laboratorii (ta*. -
kandidat mdi-
tainskikh nauk A. P. Tegorova) i otdoloniya
Toolarodoirykh
zabolevmty (aam. - prof. S. G. Khaskin) Inatituta
almaherstva
i ginekologii (dir. - chlon-korre"ndent AM SSM
mif.
P. A. Beloalutpko[doceasedl) ANN SSSR.
(BRYAST-DISUMS) (PUIRPMU04)

DOLGOPOLISKAYA, A.M., kand. med. raixk
Ant.1toxIc antistapkdococcal immunIty In
puerperant..-i anti new-
born Infant-9 1- comiectlon with their imunization
with staphy-
lococcal amLttxin, Akusb. i gin. 40 no,-',:27-31
Ja-F 164.
(MIRA 17%8)
1. Bakteriologicheskaya laboratorlya (zav. - kand.
mad. muk
A.P. Yegorova) i 2--ye akasherskoye otdolonlye
(zav. - pnof.
9,G. Khaskin) Instituta akjaheratva i
ginekolog'All (dlr. - prof.
M,A. Petrov-41'e,Blakcv) W WZR, Leningrad.

DOLGOPOL'SKATA, LA.
MWAM-04 IN
Some special prolvlrms in tho work of cutting
shops abroad.
Shvein,pron, no.!:26-29 my-To 1.59. (JOW1219)
(Garment cutting)

kv,
L
DOWOPOL' SXATA, N.A.
the formittion of overpXowths in the sea;
preliminary communication on the firot year of research.
Trudy
SBS 8s 157-173 ',,~4. (MIRA Ilil)
(Marine biologr)

N-) t-. I --~ ut vi. I , IS W h'i il-Y1 %V% .
D0140POLISMA. HOL,
-
Or
,a more Calie of unomplated Immigration from the
Mediterranean
Sea Into Mack Sea. Trudy SB3 8:174-177 154. (KIRA 11:1)
(Sevastopol, BV of-Cirripedia)

DOMPOLI SXkTA H
Metamorphosis of decapods of the Black Sea. TrAr SBS
8:178-213
154* (min na)
(Black Sea-Decapoda (Crustaces.)

t.4
DOWOi~~ I SXATA. MA.'~
,%Qwm&tiw
of the decapode of thet Black Sea for the nutrition
of fishes and 4.olphins. Trudy SBS 8:21b-219 154.
(Black Sea-Decapods.)
(Fishes-Food)
(Dolphins)

D01"PoLga
ft" A#i"
Cladocors, of the Black Sea. 1~!udy SW 10:27-75
(31mck Sea-Vater f loan)
158.
(MIRA 12:9)

soy/89-6-6-i6/27
AUTHORSg Dolgopollskaya, IL A., Illin, L. A., Puzanov, I. A.,
Tsenevi, V. A.
TITLEs The Application of Raddoactive Isotopes in Fighting
Fouling at Sea (11-rimeneniVe radloaktivnykh izotopov v bor;be
a
obrastaniyami v atore)
PERIODICALs Atomnaya energiya, IqIjq, Vol 6, Nr 6, pp 674-676
(USSR)
ABSTRACT: The present "Letter to the Editor" deals with the
experimental
verification of the possibility of protecting ships and other
objects exposed to, sea water by a coating which contains
radio-
active ingrediento against being overgrown by marine micro.-
organisms and ple.nts, Already in 1955 V. A. Tsenev suggested
the. use of A-aotive isotopes for this purpose. For their
experiments the a,uthars used the A-active isotope Y 91
(dissolved in 3N IICI) the fl-particles of which have a range
of " 8 mm in water. k 120-40 mm large and 2.5 mm thick glass
9!
ple,te was coated irith a film of the radioactive solution (Y
vii;h water of diluted polyvinyl acetate emulsion). After
hes6ting to 600 with subsequent cooling to 200 the surface of
Card 1/3 thei plate was covered by three layers of ethinol
varnish and

The Application of Radioactive 'Leotopes in soy/69-6-6-i6/27
Fighting Fouling at Sea
PKh7-70 varnish (Pig 1). The entire thickness of the coatings
2
was 35�3 mg/cm . The results of the surface activity measure..
ments of 4 test plates are listed in a table. The plates as
well as the oontrol plates were lowered into the sea to a
depth
of I m 40 m off nhore (at that place the sea was 3 m deep).
Figure I shows suoh a plate before the lowering into the sea
water and figure 2 shows a plate with neutral surface (a) and
another one with activated surface (b) which w,---
qlAh.4-c-ted to
the action of the sea water for 10 daye. BeLrzyLnles v-a-.e
cl-
served on both plates. A further experiment was carried out
for
61 days. The control plate and the neutral parts of the test
plates were coverod with a layer of a thickneas of 25 mm, the
active surface renained uncovered. A third experiment which
(November 16, 1957) lasted for 102 days, and in the course of
which the surface activity decreased to less than one third,
showed that the activated surface was still free from
Card 2/3

The Ayplioation oit Radioactive Itotopen in
Fighting ... Fouling at Sea -
SUBMITTED:
BOV/89-6-6-16/27
overgrowths. Figure 3 shows the photographs of three plates
(sem Table) after 102 days in sea water. Far the application
Of 13uch protective coatings above all long lived Pemitters
are suggested; besides Y 91 mainly Tl 204(T - 2.7 a), Ru!06 -
Rh 106 (360 d)~ Ce14.4 _ Pr 144 (288 d). There are 3 figures
and
I table.
AuVist 19, 1958
Card 3/3

D0140POLISKAYA, N.A.; GURIVICH, Ye.,S.; SFrKINAo
O.W.; AKOROCEOVA, A.F.
Mechaniam of the action of antifouling paints. Trudy
SBS 11:
254-261. '59. (MIRA 13:5)
(Ships-Painting) (Copper--Toxicology) (Cirripedia)

DOLGOPOLISKAYA, M.A.
Development of fouling aa affected by the depth of sulmrsion
in offshore
waters of the Bl"k Sea in the region of the Crimea. Trudy
SBS .12:
192-206 159. (MIRA 14:10)
(BLACK 8U-4tWHE BIOLOGY)

DOLGOPOLISKAYA, M.A.
Biological method for tooting the effectivenoBs of
&ntifouling
coatings. Trud SBS 321209-218 159. (KIRA 14:10)
ROTECTIVE COATINGS-TOXICOLOGY)

DOLGOPOLISKAYAv M.A.; OMVICHt U.S.1 SILAPIROt Ts.Z.
Effect of a bacterial fibm on the leaching "of poisons
from a coat
of -antifoulUg jwint, Trudy SBS 131309-314 160. (MIRA
14:3)
(Paint-Toxiciology) (Marine microbiolo.F)
(Fouling of ship bottome

-DDIAOPOLISKAXA M. A.; GUREVIGHt 761S.
Toxicity of different poisons used in antifouling paints.
Tru 13:315-
321* 160. (MIRA 14:31
(Paint .. Joxicology) (Fouling of ship bottoms)

DOLGOPOLISKAYA, M.A.; SHAPIRO,. A.Z.; GORBENK0, Yu.A.
--- Destruction of the film-forming matrix of antifouling
paints by
14003-308 161. - (MMA 15W
marine or aniaw. 7)ru4 SBS
Wne foullng) (Protective coatings)

DOILOPOOSKAYA) AKSELIBAIII), A.M.
Fffect cf ultrasonic Oro Alations on tbe crganiv:rs
o", marine
fouling and the process of fouling. Trudy SBS
17:309-324 t64.
(MIR-A 18:6)

VODYANITSKIY, V.A., otv. red.; MIZILIOLISKAYA, m. kand., biol.
p
nauk. r--A.: GREZE, V.N., doktor red.; IVLEV,
V.S.., doktor biol. tauk, red.[da vrm, G.K.,
kand, biolo nauk# rod,; SHAFLPIU), L.D.p red.
(Studies of plmkton in the Illaak ard Azc)v 31oasl lss.le-
dovamiia planktona Chernogo i Assovskogo moroi' Kiev
tlaukova dumkas 1965. 115 P. (14111A 18-:131
. . Akademiya nauk-URSR, :Kieve'.2#. Chlen-korrespondent
AN Uk-..SSR (for Vodyanitskiy).

VODYANITSKIY, V.A.t otv, rediel DOLGOPDLISKAYA,
M.A., kand. biol.
nauk, red.; VINOGROa)r KX,'-iMOWttt)-L-~--bauk,
red*-
GREZE., V.N., doktor bi,51. nauk., red.; 1VLEV,
V.S., doktor
biol. nauk-, red.[deceased); KIOMLIVA, kand.
blol.
nauk, red.; SHARPILO, I.D.,, nut.
(Benthos) Bentos. Kiev,, Naukwra dumka,, 1965.
13r4? P.
(MIRA 18-7)
1. Akadeudya nauk SSSR. 2. Mien-korrespondent
AN Ukr.SSR
(for Vodyanitskiy).

1,1190 62/004/007/004/009
B145' 160
AUTHORS: Milovs'kaya, . Ye. B., Dolgvpol I skaya, P. 1.
TITLE: Role of amines in the polymerization with Ziegler
catalysts
PLRIOLICAL: Vysokomolekul3~arnyye soyedineniya, v. 4, no. 7,
1962,
1049-1052
TEXT: To investigate the effect of the presence of complexing
compounds
on the molecular weicht of the reaction products obtained by
polymerization
with Ziegler catalysts, triethyl. Evnine i(as made to react
with P-TiCl 39
and with a mixture of 5-TiCl 3 with diethyl aluminum ch-loride
in benzene
and octane. 81 % amine was-found in the filtrate from the
reaction
product obtained by 5-hr shaking of triethyl amine with P-TiCl
3
(molecular ratio - 0.46 : 1) in benzene at 200C. If there is
more TiCl 3
than anine, the am'LnL in the filtrate deareases, to'27 % at
Tidi 3 : amine
a 4 : 1 for instanea. Octane is a less active solvent than
benzene
Card 1/3

S/190/62/004/007/004/009
Role of amines in the... B145/B180
(76 and 77 ~4 amino in the filtrate at a ratio of 1 : 1).
Triethyl amine
and diethyl aluminum, chloride yfeld a stable complex: Gaseous
products did
not form when a C.61 molar solution of the complax was kept at
115cC
for ;..' rrs. In one axparimen-., triethyl Emine was added to a
mixture of
P-TiC14 and diethyl aluminum chloride. In a second, the amine
was caused
to re,::t with TiCl3 for 5 hrs before addir,g the diethyl
aluaiinum chloride.
The raction was then continued for another 2 hra. In the first
case
.0,01
H ) AM : T~Cl : amine - 1.44-2.1 : 1 : 1, more
with -.-.e molar ratio (-2 5 2 2 3
than ;;~, Yo amine was found in -.he complex containing the
organoaluminum
compound. In the second, with the moiar ratio 2.2-3.6 : 1 : 1,
a6 %
amine was found. The results confirm~that the activity of the
organo-
aluminum compound is higher than that)of TiCl They show that the
3*
molecular weight is increased by polym 'erization with Ziegler
catalysts in
the iresence of amines, owing to the 'formation of a complex.
This reduces
the concentration of active oxganoaluminum compounds which
could expel
the polymer chain from the catalyst surface. B. A.' Dolgoplosk
is
thanked for his assiatance. There are 3 tables. The most
important
/7
CtLr,l 21 ,#

3/190/62/004/007/004/009
Role of amines in the... B145/B18O
.1
.Z.nglish-language references are: K. Vesely, J. Polymer Sci.,
34, 46,
1959; Z. Badin, J. Amer. Chem. Soo., 80, 6549, 19581 G. Natta,
J. Pasquon, E. Giachetti, Makromol. Chem. , 24, 258, 1957; 11.
Antler,
A. Leubengauer, J. Amer. Chem. Soc., 77, 5250, 19055-
ASSOCIATION: TnS~,tUt vysokomolekulyarnykh isoyedineniy AN
SSSR (Institute
bf High-molecular Compounds AS USSR)
SUBMITTED: April 21, 1961
Card 3/3

S/'190/62/004/010/007/010
B1414/BI86
AUTHORS i Milovskaya, Ye. B. I Dolgoplosk, B. A. I R2.~o olLgLk
~a, P~.I.
TITL'S': Interaction of organoaluminum ccmpounds with ethyl
chloride
in connection with the polymerization process
PERIODICALt Vysokomolekulyarny:re soyedineniya,.v. 4, no. 10,
1962,
1503-15o6
TEXTt A quantitative study of the interaction between
triethylaluminum
(I) or diethylaluminum chloride (It) with ethyl chloride in
octane showed
that hardly any reaction takes place below 8000. On addition of
benzene
the reaction with I was 3carcel.,r affected, but the reaction
with II
became very.iiitensive; it-resulted in the initially ablorleS13
solution
becoming a yellow, and in demixing. The organoaluminum compound
wa*s
completely decomposed and EC1 separated. Without ethyl chloride
no
reaction occurred in the presence of aromatic aolvAnts. Maximum
reactions were observed at 20 - 50 OC with mola:~ fa~tios of 3
end 12
between xylene and -III uni of 2 between naphthalene and III,
the ratio
Card 1/2

5/15,OJ62/004/010/0,37/010
interaction bf organoalumitium ... B144/Bl(86
between C H I and .11 beilng in both cases 28. The prod-icts
obtained,
2 5~ . .1
C2H 5AlCl 2 kimdl AM 31 are Liationic catalysts. Tertiary
amine prevented
any reaction' of this kind,3 since it is & strongeP-complexing
agent than
the organoaluminum compou-nd. Introduction of Oj~mole of I per
mole of
11 into the.system complqjt~sly suppressed the renption, since
the
R3Al + RAM 2TIR2AlCl equigibrium was shifted towgrd R 2AIM,
resulting
in a reduction of cationic activity. This effe,-,t can be used
to
eliminate cationic processles when polymerization'ta conducted
in the
presence of Ziegler ciatalybts, ethyl chloride, and aromatic
hydrocarbons.
There are 2 tables. 11
ASWCIATION, Institut vyso*comolekulyarnylch soyedineniy AN SSSR
(Institute of High-molecular Compounds AS USSR)
SUBMITTEDI June 12, 1961
Card 2/2

S/1913J63/005/001/019/020
B1171B186
AUTHORS: Milovokaya, Ye. Bol Dolgopollskaya, Ps Is
TITLE: Initiation of' radical polynerization by peroxide
derivatives
of organoaluminum compounds
PERIODICAL: Vysokomalekulyarnyye soyedineniya., v. 5, no- 1,
1963, 151
TEXT: The polymerization of vinyl acetate up to -25 0C can be
efficiently
initiated by systems based on aluminum alkyl derivatives with
cresol
peroxide or oxygen. At low temperatures, a polymer with '-j- -
1.26 is
formed with Al(C2 H5)5 - C)2 . The hitherto unused system Ak(b
2H 5)3 -
benzoyl peroxide proved highly active. With. a. concentration
P'.
Al (C 11 ) 1 mole~4 of the monomer, and IL i-1 ratio of the
components,
2 5 3
the yield of polymer with 1'1 0.47 was 27% af ter 8 hrs at -25
0C. At
the same ratio but at 200C the reaction rate is hard to
.regulate. The
initiation in the system Al(C211 03 - benzoyl peroxide is
apparently due
to a reaction of the orianoaluminum compound with ihe carbonyl
group of
Card 1/2

S/190/63/005/001/019/020
Initiation of radical polymerization B117/Ble6
the peroxide, and subsequent decomposition via the 0-0 bond. This
assumption is confirmed by the,,fact that no polymerization
occurs in the
substitution of azyl petroxide by the peroxide of tertiary butyl.
Similar
systeEs-~i-an b4' pr6*d-u"Be-a-on* 'the- basis - -a-1-y" knd
halogen alkyl.
derivatives of aluminum. Abstracter's note: Esisentially oomplete
tranalation.1
-SUBMITTED: April 7, 1962
Card 2/2

'AGGESSION )Ms APhO303.52 S/0190/ii4/006/003/0412/0416
Vesolova;
AUTHORS% Milovakayaj Yei, B61 ZIAwwrleval T. 0,; Dolgopolisk", P,
TME: Radical polymerimation of polar monomers bducod by AIR 3 -
bonsoyl peroxide
SOME: Vy*sokomolekulyi%rrq* ye soyedinfiniya., v. 6, no. 3., 1964.,
412-la6
TOPIC TAGS: polymerization, radical polymi)rizatioa, polymerization
initiator,
alkylaluminum compound, triethylalum4num., triisobutylaluminum,
polar monomer,,
vinylacetate, methylmothaerylate, acryloidtrile, bensoyl porOX~Ldo
ABSTRACT: Polymerization of -','he polar monomers vinylacetate,
iftethylmethaerylate,
and acrylonitrile was conducted in the presence ofthe systems Al(C
H5)3 - benzoyl
2
peroxide or Al(iso-Cog)3 - banzoyl, peroxide as initiator, The
polymerization of
-vinylacetate,was condueted in 84mole/liter solutions in benzene,
It was found
that the opti.mal conditJ.ons yielding polymers with specific
vii3cosities of 0.68
and 0.85 were 1 mole/% of A.1(C2H5)_3 (on the basis of the
polyiwar), a. 110.25 ratio
of Al(C2HS)3 to benzoyl peroxide, and teuq)eratur03 Of -25 and QG*
The polymeriza-
.,,Card 1/2

',;;..,':ACCESSION NRt AP4030352
tion of methylmethacr7late took place in a 3 mo.LeAitor volution in
dimethy1formam-
ide at -.2C and in a 7--~jl mole/liter solution in :qr1ana at -200
(the polymerization.
in xyleno proceeding at a wch faster rats). The polymerization ot
acrylonitrile
was conduc-~ed in 2-3.5 zmole,,~iter solutions in
(limethy1formamide. Satisfactory
~results were obtained only ct 200. It was observed that here the
molecular weight
.:reached a high value within a few hours and retiained practically
unchanged there-
','.after. The authors ehirwr altio that polymerization does not
occur in the absence
-of benzoyl peroxide arul that It is essential to bring the
&U:y1a3mrdnum portion
of the initiator systait in oontact with the monomor before adding
'the benzoyl,
:peroxide, Orig. art, hast 2 charts awl 2 tablose
ASSOCIMON: Institut v,"~sokomolekulvarny*kh soyedineniy AN SSSR
(Institute of
H
41olecular Compounis AN SSSR)
igh
SUBMUTSD s O4Feb63 DATS AGQs O7MAy64 ENGLt 00
SUB CODEt CH NO REF 601's 006 OTHERs 004

, Yo. 13. ; d"lflrRAVIJ,:VA . T. G.. ;
D01.60POLISIMA , I . 1.
"-V,%tf
P-groxy &wivat.ivas ct orj;anoalumin,,xm tmnpounds
ne Ini t ia tora
of radicnI po:,merJ--ation. Roport No. 1: Systf-ir,
organoulurrinum
1
'OM
. pound - ox-.,;-iren or isopropylben-,eno
hvilropci-coxidu. Izv AN
3SSR Ser h'him no. 4:720-726 AP 164. (MIM 17: 5)
lo vysokoiro'Aeki;lyarnykh coyedilnenly, AN SSSR6

DOLGOPOL'SKIY, A. B. (Moscow)
"The Theory of Probability and the Development of a
Language Relationship."
Theses - Conference on Machine Translations, 15 - 21 May
195B, Moscow.

DOLCOPOL'SI-M, A. B.
r- ------
"Gipoteza