SCIENTIFIC ABSTRACT DUFEK, O - DUGACHEVA, G.M.

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SCIENTIFIC ABSTRACT
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COUNTRY I Czechoslovakia L-2 CATEGORY i ABS, JOUR. AMIM. i LiOs 1959, .1o. 86228 AUTHOR Dufek, 0.1 Tumal H. TIMS. Rapid Concurrent Patent iornetric Determinatior of Chromium, Vanadium and Iron in Carbides by Leans of Trivalent Titanium Chloride. oRn. PUB. i Hutn. 11StYj 155~j 141 110 39 24-247 ABSTRACT It was found that on ote.-ftiometric titration' of a mixture of Crt -(+), V(5+), Ko((+~ and Fe(3+) with TiC13 solution, in a medium of 1-.ClO,, and FICI the lst Jump of U r o t c n 'C'.116al corresnonds to reduction of dr(W to ur(3+) and f 'I, to V(I++), the 2nd -- to conversion of Fe(3+) to 0 ~ :,eL'2+), and the 3rd -- to conversion of Yo((+) to I,o(5+). 1-1 ti-x presence of I ''a-tortrate or c! 'trate t1- Ere is obscrved aI so -a 1+th iumi) of potential corresponding to convcrslon of 7(4~ ) to VZ3+). Or. analysis cf carbides 1so"ated from steel IC-50 mg sample is dissolyed in 3-5 ml (Q6 1'. C10,,, evaporated ,41th several drop.,, conctritrated 1111103 to evolution of dense ,.Zies (0.5 hour), residue combined with sevLral drops of ki.ARD: 112 CZECH/34-59-7-15/22 AUTHORS:-Dufek Rudolf, InS. and Kopa, Lubog, In6. TITLE: Determination o lulginium Oxide in Aluminium Bronze (Stanoveni kyslidnfku hlinit(fho v hlinikove'm bronzu) PERIODICAL: Hutnick~ Listy, 1959, Nr 7, pp 620-622 (Czechoslovakia) ABSTIUCT: It is stated that,so far,methods for determining the oxygen content in aluminium bronze have not been described. In the Metal Research InstituteofPanenskd Br"eiany two methods are applied. In the first instance chemical determination, which is easier to ixtroduce into the manufacturing process, in the second instance the vacuum extraction method is applied. The execution of both methods is described. For some specimens both methods were applied and the results are compared in Table 5. The results obtained by the brom-methanol method, so far used exclusively for determining oxygen in aliminium, is in good agreement with the results obtained by vacuum extraction. The smelting in vacuum is affected at 1.650'JC directly in a graphite crucible without Card 1/2 a steel bath. The obtained values were between the limits 1;1~ CZECH/34-59-7-15/22 Determination of Aluminium Oxide in Aluminium Bronze of 0.0005 to 0.0030% 020 There are 5 tables and 7 references, 5 of which are German, 1 English and 1 Czech. ASSOCIATION: Vizkuani ldstav kovu, Panenskg Br%etany (Metals Research Institute, Panenske, Brezany) V/ Card 2/2 DUMI stantelay AsseaW beAm for constrwUon of large Kodels. Slovarenstvi n no.lolb-17 Ja 163. 1. Cookoolo"nake savoll naftovych motcru, Praha. Seving an whip-stitch aw-bg rAchines. p.46. (Textil.-Praha, Vol, 9, no. 2, M. 1954) SO: Monthly list of East European Accemione (SEAL), LC Vol 4, no. 6. June 1955, Uncl DUFEIL" V. Crimped Silon.Maments, p, 337. TESTIL (Kinisteratvo lahkaho pruxyalu) Prah%, Czechoslovakia, Vol. 1.1+,, no. 9, Sept. 1959. Manthly List of East Europwm Accessims (EFAI), Vole 9, no, 1, Jan. 1960 Uncl. DU?Xgj, YU4W!j !ns.1 PICRAg Wilk Pbtal-ftivaic friation materials for the automobile industry. Automobil Cz 7 no,dt233-236 Ag 163, L Vyskumy uotav pro pnekoven notalurgil, Sumperk. SAMMOZ.1 RATMU#I-; =W,#]Ll MCHIA.1 WMTt,, of nitral dsfecU Plosb. chiro 42 nowUt759-764 W63. 1e lo vnitrul oddeleni UIN v Pmut nacelnik doc.dr. V.Wfek. FUCH 9 A, I FABUN,. J.; POKOMp Jo; FOCTA g J. I ~V, IrAomption of -prol*Apd ventrioulgr tachycoxdia with an eleatrical cbarge. Cas. lek. cesk. 102 no.01330-1331 29 N 163. 1. Iltermi a antatAtiologicko oddeleni UVII, Praha-Stresorviae# vedcraci doc. dre V. Duf9k; C.Sc.,, a MMra Ja Pokorny, Me* I i U-E- ---, 4--- --. L .1 - 1.4 1- DUK77r7y. Contribution to the fractography of sintered carbides. p. V6. (Strojirenstvi. Vol. 7p no. 9., Sept. 1957. Praha, Cze-hoslovakia) YonUily Index of East Buropean Accessions (MI) 1C. Vol. 7j, no. 2,, February 1958 Vol 7 1 Dctarwir-Wap 1,44 V,L AlLry L~f;t&M'Wl btf4rXi" e~ou zii~ 4--f (A .-1 57 r4w ur~~j rtfit m .. kna qi- 4 -t- '#T ZO al ~.%71,'Alilll) h- -4 It t, 'I W-4 ATOM CZECII/34-59-9-8/22 AU 11 AUTHORS: Potrdlik, Miroslav, Engineer sad Dufek. Vladimir, Engineer TITI TITLE: Contribution to the Study of the Sintering phas_e~"*r Cemented Carbides f 7V th~L autMra_de"v~Lhaf- tu OAS'04' it v ailitooring phitsw~ And: ~Vie -propor.U ik's 0*0 ant 0 ~Mer seen ~,Gv ai a-.- I ts fact - t arIng--phas Lat a &:--Zo rw--vi-thwu t-- of the main carbide framework which could be produced by a somewhat different method of crystalliza- tion and which would quite definitely manifest itself in the final properties of the cemented carbide components. Therefore, the arrived at conclusions should be verified on aIntered carbides produced by ordinary methods using sintoring media which proved most suitable in the here described tests. In these, the authors investigated the properties of an "artificial sintering substance", i.e. a Need cobalt alloy, the composition of which was Card 1/3 chosen to correspond with the ideas of the author on the, CZECH/34-59-9-8/29 Contribution to the Study of the Siritering Phase of Cemented Carbide& desired composition of the sintering phase in sintered carbidsis currently used in machining and fabricating. Such tests can also be applied for studying the effect of certain additional carbide admixtures, which have a pr--o-n-o-u--n-cod-influenco-on-the-proptrties of -the--sintering------ phase. As examples, the authors describe the application of this method to the study of crystallization of Co-WC- systems-with various CO/VC ratios (50, 33, 45% WC) and Co-WC systems, some containing additionally TiC, TaC, Cr C2 and VC. On the basis of the obtained results, thl authors conclude that the composition and the crystallization of the sintering phase cannot be allowed to be governed by random manufacturing conditions and that it in necessary to study systematically the phenomena occurring in these three ranges, which are diagrammatically outlined in Fig-10, P 789- This is a sketch-reprtsenting the crystallization of the sintering phase in the cavity of a carbide and consists of intrazonal, monozonal and Card 2/3 p*lyzonal ranges of crystallization. The authors believe CZECH/34-59-9-8/22 Cont.ribution to the Study of the Sintering Phase of Cemented Carbides that systematic study of the relevant phenomena could lead to a substantial improvement in the properties of commorciully important cemented carbides, to advantages in alloying with substances which dissolve in the ointering phase, thereby ensuring better mechanical properties. That success can be achieved in this way is proved by the favourable results obtained with the Czech produced universal sintered carbide, which is alloyed with a small quantity of Cr C ich,during the process of sinteringtpassos inta i.'ecobalt sinter- ing phase. There are 11 figures (including 10 micro- photographs), 2 tables and 36 references, 12 of which are Czech, 9 Gorman, 8 Soviet and 7 English. ASSOCIATIO14: V*"Zkunny 6stay pro pr9lkovou mttalurgii, Vestec u Prahy (Research Institute for Powder Metallurgy, V*stec, Nr Prague) SUBMITTID: January 13, 1959 Card 3/3 CZECH/34-59-9-9/22 AUTHORS 8 r _g4, gnsineer and Like', Ji'f, Engineer TITLZs Analysis of the Influence of Addition Carbides on the Properties of High Cobalt Content Sintered Carbides of the System WC-Co Using Mathematical Statistics Methods PERIODICAL: Kutuickeo listyl 1959% Nr 9, PP 791-796 ABSTRACT: the authors carried out experiments aimed at elucidating the influence of TaC and Cr C 2 additions on the properties of WC-Co systems with coball contents of 15 to 30% (types G3 and G6). To prevent incorrect interpretation, the authors made, use, of mathematical statistics taking into consideration differences in the criginal raw materials-ine4dition-to- differences in the quantities or TaG and Cr3C26 The quantity of Cr 3C2 in the main tests (0-75%) w&n based on results of preliminary tests. The authors emphasizo that the application of mathematical statistics in useful for workinc, put the-plans-or the experimints. For 9arrying out the full factorial experi- ment of the type 2 , 64 tests would have been necessary. However, the authors used a shortened series of tests nvolving only sixteen combinations. The pilot plant Card 1/2 iscale tests showed that the favourable influence of TaC CZECH/34-59-9-9/22 An.'AlYsix of the Influence of Addition Carbides on the Proportion of High Cobalt Content Sintered Carbides of the System WC-Co Using Mathematical Statistics Methods observed earlier for S and G-1 type carbides also pertains -to, Q type carbides in the case of higher cobalt contents. There are 3 figures, 3 tables and 15 references, 8 of which are Czech, I Soviet and 6 English. ASSOCIATIONSt VUPM and VUHZ SUBMITTEDi February 21, 1959 Card 2/2 22686 Z/013/60/000/002/001/0011 D007/D102 21 $V AUTHORS: Dufek, Vl., Engineer, and Petrdlik, M., Engineer TITLE. Hot-pressed asaiconductive ignitron ignitors TEXT: -The-article deecribes-a~method of boron-c,arbide-ignitron- ignitors production which combines pressing of the powered semicon- ductive material, and subsequent firing in a non-oxidizing medium, with simultaneous bonding or the ceramic body to the metal stems This pressure-sinteringi or hot-pressing method, so far onl seldom used in the OSSR, was applied by the V~zkuW "tav ro pr3kovou metalurgii (Research Institute for Powder Metaliurgy~ in Vestec to the production of an ignitron to be lnst~lled in an electronic weld- ing apparatus developed by the Vftkumn;t ustav zvAra6sk~ (Welding Research Institute) in Bratislava. The boron carbide ignitor (Fig.1) consists of a ceramic body vhich extends into a mercury pool and a molybdanim stem for current admission. In production tests the two conventional methods, i. e., pressing aaid firing, were combined into Card 1/7 a single process by using a resistance-heated graphite die (Fig. 2). The heating current-was a_pplied-to the grap4ito electrodes-of the die thru water-cooled copper terminals from a 15 M variable-voltage transformer, with the secondary voltage adjustablts in 0.1 V inter- vals within a range of 3 - 12 V. The boron carbide body was heated and simultaneoixely pressed by a double-sidea hydraulic press, with the pressure applied to both the male and female dies. To avoid short circuits within the press frame, at least one die mustbe insulated by a porcelain plate* The temperature of the graphite die was measured externally with an optical pyrometer When the desired temperature was reached, it was kept constant wit4n + 500 for a certain time by adjusting the transformer voltage. AYter this timeq- the current was cut-off and the pressure released. The sample war left in the die to cool off. As the last operation of the press.4ng process, the pressure on the female die was increased to achievj a complete filling of the die cavity resulting in a perfect shapr of the ceramle body requiring no additional grinding. Temperatures if 2,500'C and more can be achieved with the equipment used, but pres- Card 21? 226% --:,Y/013/4W/4=/002/001/001------- Hot-pressed semiconductiveoo* D007/DI02 sures, are limited by the strength of the graphite dies and should not exceed 10 kg/c!2 at surfaces perpendicular to the pressing direction. ressures were precisely measured with gaSes installed on both cylinders. Production tests were performed with semiconduct- ing materials containing boron carbide (of last-German and Soviet origin, both of similar quality) mixed with aluminum silicate Al;A~-3SiOp (a product of Merck). Optimum composition was found to W - be 55%B4C, 35 - 40% A1203' 3S102 $ and 5 - 10% ZrO2; optimum sinter- ing temperatiLge (measured on the surface of the graphite die) was 1.320 - 1,340 C to be maintained for 2 minutes. To test the qualit;r of the ignitors, ignitrons were ignited-by the discharge of a 1 - J.L. --=I arof arad- -of-, igni~ors-for-use-,-witli,--- ivdtrons waslestabl.shed by-measuring-the dependence of ignition voltage on electrode immersion in-mercury. The re'gularity of igni- tion was checked bycomparison on an o'scillogTaph. The ignition voltage, adjusted to the limit of dependable ignition at each immersion, was measured with a peak voltmeter. Measuring data, as Card 3/7 7- 22686 -Z/013/60/000/002/001/001~ Hot-prassed semiconduc-tivev-0-0 D007/DlO2 obtalned with these ignitrons, are listed in Table IL The pro.. perties of the Czechoslovak ignitrons are similar to those of a Phillips Ignitron. In conclusion' the author states that pressure sintering proved a suitable method of producing intricate ceramic bodies. The products proved successful in tests and enabled the building of an operational., all-metal welder ignitron at the VfJS in Bratislava. There are 3 figures, 2 tables and 2 references: one from the Soviet bloc. The reference to the English-language publica- tion reads as follows: USA, pat. 2, 456.891, December 1948. ASSOCIATION: V~zkumnf u6stav pro prAikovou metalurgii, Vek;tee (Research Institute for Powder Metallurgy, Vestec). Card 4/7 Cross-sLection of boron car- bide ignitor (actual size).- Legend: (1) Mo-stem; (2) 1 - Ret bortarbldovim WPOZOPO&M lskvt#eW ceramic body. velikaji) ft-slopka, vlaint tommkki Mike Card Hot-pressed semiconductive.';. 226% Z/013/60/000/002/001/001 DOO?/DI02 Fig. 2- VIO, Graphite die for the production ofignitron ignitors. Legend: 1. Vale diet 2. upper graphite-electrode; 3. Mo-stem; 4. boron carbide ignitor, 5. graphite lining; 6. power graphite electrode; 7. stebl female die.- 0&. 2 - Oftiffaq wk. PO vjmw UPS- gvW Wodal, I - homl "X#Vk. 2 - haml #WHOW 3 - mo-nopte" #Mingo WOU1. U. del- amort SPW M41L Card 6/? Hot-pressed semiconductive... __ineno -spec 2. composition E I': Geight 151~) - 2a B 0 USOR 2b. A B A 3illica" i Is a Zgl SZG; 30. 'l te;.2d. . I istance; 3a. at' 3 Re s we to .4" con~alct; 3b, at full immersion; '4w* 4. Ignition voltage M; 5. 1* 0 t4 average current (mk). . Crard 7/7 Z/034/60/000/04/010/028 9073/E535 AUTHORS: Hampl, Vlad1m1r, Doctor and Dufek, Vladimir, Engineer TITLE: Spectral Determination of Tantalum in Sintered Carbides --PZRIODICAI;-: ABSTRACT: The experiments of the authors can be sub-divided Into two parts, namely, determination of the tantalum content by means of an a.c. are and determination by meAns of a condensed spark. - The operating conditions in both- casfis- are described. It was found that the results of the spectral determination differ for the two methods. In the case of determination by, means of an arc, the characteristic of the current intensity depends on the shape of the specimen which manifests itself also by a considerable scattering in the values. The condensed spark showed a more regular characteristic of the current intensity and the results are more reproducible and nearer to reality in spite of the fact that the specimen shape also exerts an influence. For some of the specimens a parallel chemical analysis was carried out,- in spita of Card 1/2 analysing a greater number of specimens, the results obtained differed from those which had been anticipa ted. It is voint*d out that in the c ont:Lro-a-pecison-and,--th*refore, -variations may occur- due to imperfect houtogensity of the tested specimens. If the tantalum carbide concentration is below 1%, the intensity of blackening of the an&lytical tantalum line is so weak that the influence of the background intensity mAnifests itself. The resulting calibration curve (Fig 8),which is based on the evaluation of the tantalum line 2685.1 A, permits direct reading off of the percentual content of tantalum carbide. There are 8 figures and 6 references, I of which is Czech, 2 Soviet, 2 German and 3 English. ASSOCIATIONt Vy'zkumny' U"stav pro pros's'kovou metalurgii, Vestee u Prahy (Power-MetallurSy Research Institute, Vestec Nr.Prague) card-2/2 Z/034/6i/ooo/003/006/011 2073/2535 AUTHORt Duf*k, V., Zngineer TITLEt D*YoXopment of a Universal Sintered Carbide PERIODICALt Hutnicko listyt 1961, No,3, p.208 TZM . The rang: of sintortd zarbides of both the two basia systems WC-C.o 4G **rite) and WC-TIC-Co 418 series) has been extended during recent years by further series (G4-G6 and s4-s6). Although the fields of application of those now grades of vintered carbides arenot accurately delimited, they do overlap. This has advantages but it also has considerable disadvantages. Therefore, the requirement arose for a so-called "universal" sintered carbide which would replace carbides currently used. The universal carbide of the composition 86.5% WC, 5% TiC. 1% TaC, 0.5% Cr3C2 and 7% Co is suitable particularly for machining of austenitic manganese steels for which A 100% increase in the machining performance was obtained. A further reason for introducing the manufacture of universal carbides is to increase exports, since this carbide is ---la.great--demand---in-a~-numbor-of- Report No,. Z-714/57. Card 1/2 Development of a Universal Z/034/61/000/003/006/011 1073/S535 ASSOCIATIONi Vy~zkumny' u'stav pro priikovou astalurgii (Powder Metallurgy Research Institute) [Abstractor's Notet This is a complete translation] Card 2/2 35232 Z/034/62/000/003/003/004 Sq073/E535 AUTIHOR: Duf 1c, V~, Engineer TITLEt 'Nethod of joining carmet sintered layers to a meta,L base Patent Application Class 40 b/2, PV 3990-61, June 26. 1961 !LRIUDICAL: Hutnicki listy. no.3, 1962, 212 T"T: The invention dispenses with the shortcomings of the hitherto available methods which do not produce sufficiently strolls joints. '.he method consists of rnughinz--up-the-t -~~--e of--thve--bas-e- ate7ly-modified, rol-1a--6f--- th olling- stand, after preliminary annealing in a reduction atmosphere at 600 to 1100*C, in such a way that t!.%e surface is covered vith a regular relief of a total depLh of 0.1 to 20 iams the indentations being spaced at 20 mm from each other. Ste^1 sheet coated with a layer of nickel, bronze or copper deposited by plating or by metallizing is used as a base material. The cermet layer consists of iron, copper or bronze powder and contains further metallic, alloy and nonmetallic ndditions or mixtures. Card 1/1 Mital-4avala frictIm mtvAal Diatr:Urt -'a now Cwchoo2oYakl-* produato Spravy pras setal ftmpork no,4JVI~ 262 10 Vyz~y ustay pro praercom metalurgiij &=perk. DUFU P.- v 0 1 I= # Us* d brom-ba&W oormete for friction linings. Straillreutwi-12-n*4Ot7W49---30-0~16Z-.,- -- 1., Vy%kumy ustav pm praakcvm motalurgii, Sumpez*, DMK..11jAUAr, ins. CSc.j ICKES, Frantisek some recent metal-ceramic friction materials. Stroj vyr 13 no.4:260-263 Ap 165. 1. Rese"ch InsUtute of Powder Yatallurgy. limperk (for Dufak). 2. Zavod prvni patiletky National Entorprism, Potstejn (for Kokes). 4; DUMI T. Porbogenic polydnmiao Actly. very. grup. (Pmba) 7 no.2s191-192 165 1, lot Intemal Departmeat * Centml KUItwT Hospital, Preps. 2. JoYablan's addreseWraha 7p Sabnirchoys 17. FARMp J.1 DUnK. T. Payabogealc pololpsUe Cis* lek, cesk. 104 no.27/28:754-761 . 9 il 165. Is Is vnitrui oddel"I UstreW vojonsko newenica v Prate (nacolnik do** dr, To Dufsk, Me,). I iv %P-1 Logo t tior R q 3UBM DATE., MM, T. Pavlovian theory sxA digestive treat. Voj, zdrav. listy 20 C1005:232-236 Sept-Oct 1931, (CUM 21:1) 1 1. Vladimir lhfel-, W.D..X&Jor, Medical Corps. Infootious hepatitis* hekt. lok., ftshm, 31 nao]68323-325 3 Aug 193L (CM 21t I) t Daynt 'treatment of Infectious hepatitis in Soviet literature, Cas, lek, asek, 92 no.9224&2" 2? IPA 1953, (CIML 24-.3) problem ri prelouption at SM, effect at F'On-laillis. cesk. 92 no.3ltl392-13" ll_Doc 1953, 1. Of the Central Killt&ry Rospital. Nagme. WMTO antonum-jo- 49110 MM T- SM STJWCAR J. 0 late WmYsnost& a apllkac~ perecilinovich tablet, Our "perionao of Me use of peroallin tablet* CALLMUS. 1933, 92131 (1398-13") 0 raphs 1 Orea aAministration of tabletir (Operocillat) containing 2000000 units penicillin 0 and Oo2 to 0*3 go "Iderifte revalts I& &a effective blood level of tho antiblWo which lasts 12 to 16 bro 0.03 units In I al. eorum)o They wore given twice a day In 123 cases balf an hour before seals; there we" no sideeffects. Bloch - Amsterdam (ZX,6,2) SO: 1kaorpta Itedica. Section H. Tel 7. No 9 nidlilr Lt Col, Urs- Obt-re-w- v 0--Jda--" nomomioa Cmtral muua somAtal)p CowA*cc,, idth Capt Ir :arudr WW of arUoloo Olotasstlag Ilectra- aandopww in Cam of Myosardial InflamUmgO do&Ung Ath the reasms far electroasnUagrm Wmaps In lathmUcs, (TZLO Oft 54) $0, On. 4361 30 Wank 1955 Valk, voclarkoff notw of themw of tubotes multus. Cam. Uk. colt. so*48tU32 26 Sw 54. (DUMM XUJIM, theraW wooofts's moth") DUrz, Vladimir, Pplk. Dr. Increasing number ofanicterle forms of Infectious hepatitis. Cask. gastrcqnter. 9 no.2:110-112 June 55. 1. Ustrodnt vojenoka nevacnics, Praha. (RWATITIS. III IOUS anteterlo, Increased numUr of forms) Dunic. nd gir. bike pr rAta2 and otNr Wor ocoltestlons after novooals blftko Case leit#ceske 94_nool8t472-480 29 Apr 55. nerve ~loqk witi procaine; compl.) (PROCAUSO injurious off*ottt In urveblook) IICRA. K.; STIUCAR. J. ftrtbar arperiences with application of penicillin witb ~p#cIal reference to prevention of rhematic fever. C". take cook* 94 no. 5W413-1417 16 Dw 53. (NIMMIC YNW4 "'Ontion MA control, - P441411112.) (PUICILLIT. theraVeatic use. rhm. favor pm.;) _VAU/2 IntmiA Med. Feb-57 CA Sec. 6 $47. _R2FE Kardial. Spolecaosil, Pram. *FKG pti zutem levfho 111niho T_P dot . Cd In m It ral stonosl s VNTTft.LEX. 1956. 214 J397-305) Tables I Illus. 11 The author compared ECG changes with post-mortem findtags in 93 patients *ith mitral stenosts. Signs of right veMricl* hypertrophy in cheitt leads (small Q and high R wave in V1.1 . small R and deep S wave in V4.4 I occu-red in &.11 27 pa- tients with pure mitral, atenosis. tn 5 other patients a complete right bundle- branch block vras found. Hypertrophy of both ventricles was found in the ECG of all 16 patients with rottral stanosts combined with mitral Incompetence: a con- siderably hi&h R and small S wave In dweat leads from both sides. Less advanced m1tral ctemsia combined with mitrat &W matually aortic incompetence in the rest of th* patlents inanifeated Itself by afgas of hyperuophic changes in left precordial leads fth R wavo wMalyl, with dilatation of th,~ right ventricle axW with auricular fibrillation. DUM T Ysoaardial bdarats is yaws &&It*. Toj. sdrav. lmikovua no.34t 1-187 195 ?. (MYOUZOILL in 'YD'IAS &&ate (08)) tar'-_. i DUYU, Vladimir Wfoot of vitamin 0, Iodine and Ober footors on experimontal athero- matos is a Cas w Iske cosk. -97 no,27-28 %868 - 4 July 58. 1. US Prabis. VI. D., Praha-Stresovice, M. (ADMIOSCUMN. experimental, df. of lodho, vitamin 0 & otber drvgs (Cx)) (IODWSI, *ffoots& on "r, artorlosclerosis (Gs)) (vrum c, effsats,- $ame JAMT, M.; SUU. No I PODMIL. N.1 RUA. 7.1 M17 , T. dh ......... Oa the tr*atneut of acuto loukasola by massive wbolo body irradiation combined with subsequent bons marrow transfusion. A ose* report. NeoPladvaAratiel. 7 no.33295-304 160. 1. X111tary Institute of ftlese, Spidealology and Niorobioloa, Central Military Vospltal, Prague, Coechoslovakta. 9012 KAMM trux"I DUM, Vladial I RASAD J=; u4mv FW* Q-T sm in rhe=atic fe"r. Cas.lak.eask. 99 no.20/21044-W 20 P4 960. 1. 1 vnitmi addeloni Mp naaobdk plk. C.Sa.doc. XUDr. Dufok Vladlair - 3:1. wdtrai addol*ni UU9 nacelnA gen. MDr. Daft a Ari s KI) (RHMUTIC I-XV dUg) U E. major Ocou'le1mv nW, $n4mate, pbysicias (time t lehav), U Cot Jo"t NAVPAM 0, Cot ArULDAVLMk&l%Jff Jift Un We Col. Bluest no nW a-vartme-i at istermai swictmo im4 xedw"y 60rafte'ut I cement Military borital M vaiml 0401601 4 Sam"attoo) NV474 of O"Sm"Las Went beelliGis"760 Proviel, Y#]4ds%2 Uftygiattka Ultv Yet 31, 06 It JIM 631 PP IW114- Iftalleb mommaq w4ltiod]o Uvim of pubtlebod literecure &*A of 46i& Is It ptlestaf Moe phem"ardLwaft" histdr3p.Uktal, I-n7l oloatroklmeWpbli, afitkAtAlfilltift 954- alfs,"Malreol M17 *sm altral awsory is 4426140feds Us Moe r other 10"Us"I graphal amli*cardlearm wltb "Plamster? drawtall : to club A" 13 W11,624111 gaws~4"0 f LA 02CHOSLOYAKIA D Xt V., Docent MD.# Cand. of Science First Internal Kedicine-Ward-of the Geneml Military Hospital (is interni oddelen! Ustredni vojenske no- mocnice), Prague Prague# Prakticky lekar, No 7. 19639 pp 2,15-247 "Mondor$s Disease$* TABUN,, JO; -nik ~ Nephrogonic diabetes insipidue. Cao. lak. cask. 103 no.39tlM8-1094 25 S 164. 1. 1 Interot oddelenA Wrodni vajonake nemocnice v Pra$3 (yedouci doe. dr. V. Dafek). DDMI zo 'RecArks on Prep&rations for this Year4 71-xeshing.0p. 104. (INIRGETIU, Vol. No. 3.. Ylarch 1953, Prsh&, Ciochoslovakia.) SO Ycnthly List of East European keessions, IC, Vol. 3, No. 5, YAy 1954, Uncla3sifted. Doolping -tho)atavecawade oontroi mtm. &a Eou noasu-w 162o DLT?.M, Josef, do*, W. CS*. Dynamics of photosynthesis in sot* vegetables depends on their water regime. Rost vyroys 11 no.ls3-16 Ja 165. 1. Chair of ClardenIng of the Higher School of Agriculture, Prague 6, Toohnicka 3. OubKittod September 12, 1964. DtTrTsEs T. I SO: - Monttay List of East European Accession (MM,) LG, Vol. 6, no. 7, -*-,I-y 1957. Uncl. -.- --- Coutimous in=*aw of officiewy in tochideal developmnt, Drevo 18 no.6t2M.J* 163s 19 KWaterstya spatrobvibo prumplu (for Dufka). 2* Ustradni vybor Odborovoho ayum samatnamu spotrebniho WUW lu (for za1vtoo1q). FInZ,, Mdriabo Ins. ((bU-ov%)j DMI, ;omoft ins. (Oatrava)j IUZ M-IX.# Josof ($way). High pmesav liquid fuel burner* 1hargetika Cs 14 no.2# 99-200 P64. --------------------- MiDICA __3*c*_3 VoloU/4 &id~xrinolonr Apr _37- 10 7 S1. VYSKOCIL J. afld I)UF'KA Z. (Md. Chor6h r Privol. Fak, Nemocnice. l1rnol Pathol. -Anal. Ust.-MT-Wr-no. " Ifistologirk6 zmt!ny v endakrinn(ch IlStdcls u kr<k4 po dioutiodoWni pnddvlnf ACTU. insulinu. jejich komloinavi a salicylu. Histological changes of endocrine glands in rabbits after prolonged administration of ACTIL insulin. combinations of tsoth and salicylates SCH. MED. -113rno) 1956, 29/1- 2 (53- 59) Tables I Illus. 3 ACIII was administered to female bits for 6 months JO. 1 -0.2 mg. jkS. /day) alone. in combination with insulin .25 1. U. /kg. /day), then Insulin alone (0.25 1. U. Jkg. /days and sodium salicylate alone (0, 135-0.25 g. jkg. Jday). Important histological changes were found with Insulin alone (signs of adrenal medullary exhaustion, atrophy of the islets of Langerhans. decreased number of eosinophils in adenohypophysia). After ACTIll alotte and In a teaser degree after salicylate, adrer"t h*Tiertrophy was found, but the changes after combination of ACTII with Insulin wore similar to t1mee observed after insulin alaae. Schreiber - Praguo (1,11. S) - - M czIC" SLOVI%Xilk -I J. INOLCIX, 'OMt. Psychiatry Clinic-and First _A4_JH1Z&QYA. and H- JA:' Internal Hedicine Clinic (I. Interns klinika) Medical F.ctilty of Conentus University, Bratislava. "Effects of Psycborharmacologic nrugs on Thyroid Gland in raychiatric ratients." Pra,uo, ActiVita3 "'cryosa Surcrior. Vol 5, No 2, Hay 63i rp 190-191. LY Alostract: Studies in 16 rsychotic and 13 neurotic women whose thyroid .unction wis carefully studied by 6 tests: then treated 4 weeks with either 2400 m3- merrobwmte or 600 m-. chlorrromazine daily. 11. decreased thyroid function In 4, increased it in 2; c. decreased it in 2, increased in 4. In rsychosis, increase was more frequent; in neurosis, decrease. Table. L2 20 L-51*li d Pow* MW ftmift w4mvsku A (j Ar,vti~, Isal ilt, lggw mr P11-1 SIR NNW 76-10-6/34 Thermodynamics of Rare Metals. VII. The Equilibrium of Nickel Tangstate, with Hydrogen Vot the reaction NiTO4 1 Ki + W + 202 following equation is obtained# 0 2_ 1.622 000 Az TI(oal) - 276 o6o - OtO24 TLlg T + 0,0 33 T. - 629363 T. There are 2 figures, 2 tables, 8 Slavic refersuces. ASSOCILATIONi Moscow State Thivervity imeni H.V. Lomonosoy (Roskovskiy cosudaretwennyy universitet imeni N.V. Lomonosova) SUBMITTED# June 25, 1956 AVAILLBLIs Library of Oongres!3 Card 2/2 AUTHORS1 Anikin,A.G.t Dugachova0G.K., Nollnikoy,A.A. SOT/55-58-1-31/33 and Plat*,A.P. TITLICt On the Question -About the Production of Pure Organio'Preparations (I Yoprosu o poluohenii ohintykh organicheekikh preparatoy) MIODICALs Yestnik Mookovskago universitets, Seriya fisikoonatematiahookikh I yestestvsnnykh n&uk, 195a, Ir 1, pp 227-232 (USSR) ABSTRAM During the production of organic preparations defiling adbixturos can be avoided only 'then if not only the final preparation but. also the Intermediate al'.oys are ol*anod. The degree of purity can be oontroled best by the determination of the crystallizing ourveso, since the cry*ltallising temperature in much nor* sensitive with respect to defilement# than e.g. the specific weight or opt I dal-chars-at-orlat Leal value s-. -Tho _&uthors_-d4*so-rit_*th*__ application of this method for the synthesis of the trans.- 1.2 &I - n - butyleyolopentane obtained for the first time. -There- are- 4--Toferences,--2--of -which -are- Sovivt V and -2 -Ansrican~----- ASSOCIATIONiKafedra khinii nefti (Chair of Petroleum Chemistry) lafodra fisich*skoy khiaii (Chair of Physical Chtnistry) SUBMITTEDs March 5, 1957 Card 1/1 ANITIN, A.G.t DUUCW.AO G.K. Determination of purity and crystallization temperature of cortaln, hydrocarbons In suall wasples (I - 2 al). Dokl. AN SSSR 119 no.5; 939-01 Ap - 138. WRA iu-6) IsMosko,"Idy CosuWst"u" lomonosove, Predstavleso, Vo akedeadkou BJ. lazansidso (Sydrocarbous) (ftermaherAstry) DMACEM,, 0, M,,, carAldiRts of Men Sol (dies) -- "fhe or7ottocypic method of do- tormining the piritq of the lov-asIUM orqudc eempounds (Tn small quantities)". MOSOOvi 1959o 17 VP (NO90aw St&to U In X* Ve L4c=onosovp Chan Facultq, Clair of Pbys Chem), 120 ooples (XL, No 21s 19590 nil PRTAMSMMTA~ X-Aq -Tom"ratures of cristallisation of blarleo[2.2.11-2.5-hopUdl end, crolophoptatritas and their sixtures. Vckl.AX SSSR 132 uQ.4: 8374160 Je 60. (MBA 1315) 1. lastitut organichaskoy khiall In. NeD.Zellaskogo Akademll tank SSSR I Moskovskly gosuftrotvemp walveraltst In. Mov*l'ONODGIQTS* Pr*dlt"l**'* akadealken BOASUSSUIldme (BloplohaptsAisus) Oyel4heptatrieta) 8W16 s/o2q/6o/i35/OO3/G32/O59 ,5-, il-)00 ('1..2-)3 oh~r) BOO4/BO6O AUTHORS: Lnikint A. 0. and Dugacheval G. M. TITLE: Determination of small 7=6rxaM1Effs`cts by the Thermographic Method at Temperatures Below ZeroA PERIODICAL: Doklady Akadsaii nauk SSSR, 1960, Vol. 135, No. 3p pp. 634 - 637 TEIT: The authors tried to approach the accuracy of a simple and rapid thermographic method to that of the calorimetric method. The system used fer the purpose is illustrated In Fig.l. Th " measuring device consisted of a-copper-constantan thermocouple, a 41MC-4611PUS-48) potentiometerp and an )7T 49 EPP-09) ricording -potent Lome to - as zero - instruM*1.1t.- The 0 A, divite was housed in a cryostat. The substance whose thermal effects- were studied was either frosen as a drop onto the thermocouple Junction, or filled into a copper foil cup (Fig.1, II). The container of the appa- ratus was cooled in liquid nitrogen, and evaousted to (1-5)-10-2 am Hg. A zurrent of 0.15 a was then passed through the heating coil, whereby a steady radiative heating was attained without direct contaot b9tween Card 1/3 86046 Determination of Small Thormal--Eff*cts by S/020/60/155/003/032/039 the Themographic Method at Temperatures B004/BO6O Below Zero beater and substancos'The-livice, was oaj~jtratod by means of.substanots with-known thermal-of foot*.-: The -amount of-liberttod or aboorbed hoat-as a function of the length L x (am) of the recorded platform was determined. The effect AH . (cal/g) for the substance concerned was calculated from the equatinn: AH, a AL (1/gx). is the weighed portion, A (cal/sm) was deierminAd by valibration. Experiments with cyclohexane (weighed yor- tiony 0-009-0-045 9) showed that this devic# makes it possible to sea- -4ata agreement with available in literature within the error limits. There are i figure, 3 tables, and 8 references: 5 Soviet, 4 US, and I British. ASSOCIATION: Mookovskiy gosudarstvtnnyy universitat im. X.Y. Lomonosova (Moscow State University tm*ni X.V. Lomonesor) PRESENTED: June 20, 1960, by P. A. Rebinder, Acadealf.,lan SUBMITTED: June 15, 1960 Card 2/5 ~14 AND, As --DOUrldrat Loa- of -the-puriwa*L-Orys tallinat ton tergaratures -of.-pu"- hydrocarlbons in amounts of I to 1o5 al. lost. Xosk. un. Ser. 2s Khts. 13 no*3:31-35 S-0 I" (MIRA 13111) 1. Noskovskly Comdaroftem" univoreltot, kafedra ftsichaskoy khislis OWmarbous) (Crystallization) S/076/62/036/009/009/011 8101/BI02 U 7 1'. :);4.3 Inikin, G., Tmp..,ichcv%, G. Prezryakova, V-L.., and T I 1`~ E: aeltint of methyl methacrylate' PERIOUIOALt Zaurn3l finicheakoy khimiis V- 36g no. qt 1962,-20741- 2075 TNA J" % 'Ahe uge of zone melting to purify lo,;-melting orranic substances is A e s. c ri b ':,y the exnmple of methyl methacrylate (crystallizatio n temi)era- t"Ire - 10. ~,Ath an Initi-A plirity of 99.2~. The zone meltinf uas per- fort,-.cl ir. a tinplInte bdth OW .-m lone-inal(le n imwarflnek contakninfr liquid nitroren, ',.) ril~ntinv P rici,rome s,)iral of 0.5 6m diameter, heatinr current i,:-,j) -o-Lt,-~ -i zhift of 1 Vn/mln. A lorrac of purity Rzoiintinr, to "Bias attni:m,l A tor rive pasr-ires, qn.-I 9,1.051~ -if ter ton pausafen. The crire- co Ac fi z~ f purity of tite 3n:rploa has bpen describci earlier !N 1 kIrms, It'is established th-it orf-anic sulistancec cr,rstall". bclo! 0 cn!i be purified by zone meltinr. There ire 2 tibles. Card I/.- 6" -76i O-ei 0.36,1009/0~9,10 I I Zorc of iloljBI02 A6Z~O','IATI Tia33',%OV3'.Ay COCUdaratvanny~ universitat im. 2. V. Lomo-is-)va (.':ozicor Stite Ur-tvaraity imeni V. Lommnosov) 6UB".IT",."J3 Yebruarj 1,)$ 1~62 C-ard 2/2 S/191/62/000/012/002/015 BiOl/B186, AUTHORS: Anikint A. 0.9'Gerasinov, Ta* lop Dugachavap Go Met Preanyakovap V. Me TITLE: Purification of organic monomers-by zone refining PERIODICAL: Plasticheskiye macay, no. 12, 1962, 13-17 TEXT : A general survey is:given on the theoretical principles of zone refining, based predominantly on non-Soviet papers. The applicability of this refining aethod to low-melting organic substances is discussed and the practical results are given that were obfained in the zone melting of methyl methacrylate and styrene. Zone refining was performed in an 80 mm tin pla,te ttrough immersed in liquia nitrogen. The sample was heated with a 0.5 mm nichrome coil (amperMe 4 a), the molten zone- being_-____-_ i+.T--*U" 4AM Ai by remelting it 10 times. In styrenei-the triAial-dogroo-of-puri-ty-of-ga.85-aole- 4 -tieso e Working-at low:!--,--.,~-Z Card 1/2 b/191 62/000/012/002/015 Purification of organic mofioiers ... t Yale temperatures requires the caietul exclusion of atmospheric moisture. There are 5 figures and 2 461*se The most iup~6rtant English-language references are: J. Its 3*yAofis R. A. Saunderaq Brit. J. Appl. Phys.# 119 126 (ig6o), John S. Ballp A.!V* Holm, C. R, F*rrinj Petr. Engr.9 30# no. 13, C-36 (1958)- Card 2/2 Zone malting of methIl methacrylatee Zhur. Alit. k)-jm. 36 no.912074-21,M 3 t62* (HIPA 17t6) 1, Wakovskly grcsud&r3tvenVy utiversitet I mrd lzrxnesova. ANIKIN, Alsksey Gorasimovichl DUGACHETA, G4LUna Kikhaylovnal GEWDUT9 laslot pie.-,, OTT-*i;J.-; FLATS, A.Y.,, prof., oty. red.; ZOROBMVA,, N.A., red.1 YERWOV, N.S.9 tekhn. red. (Determination of the parltr of organic substances) Opre- delode chistoty organl"kikh veshchoetv. Oty. red. I.A.I. Gersaimov, A.P.Plate. Wakva, Isd-vo Mosk. univ. 1963. L47 P. (MIRA 16:10) 1. Chlon-korrespondent AN SWR (for Gerasimov). I (Organic compounds) (Chemistry, Amlytical) TOPIC TAGS: =etl7lmetbacrylatej, sulfurio acidy radiolysts, purification, pol~rmerlzationx crycacopic analysis ABSMLC7-i The pure met17;pathaMlate (12,A) necesaftary for eleetrochemicauq- Itiated Terization'jean be obt&ined S.-CM ca-z-ercial 99*8% KIM stabilized with 4r poD ,qd,roT,U.none by treating vith 25% cauntic solution to remove percaides,, and then with F '~~ to renove, carborql conpounds and fir-illy by distilling at rectaxed P.ress~~2e bmm H&) under oVeen-free nitrogene The 92.99" M11A thus obtained has less than 10- mole per liter of acids* An apparatum was constructed for the erfoscopic am%vais of 11QMA* Crystallization ntrvoa for cormercial and the purified 1.11k are givme 0riY,# art. heat 2 figurose Card 1/8/ DUGACHLTAO G.,X.j ANIKINt A.0, Zonal melting and oontral of the degree of purity of dim thy1dichlarosilano. Plast.massy no.10121-24 163. (MM 16olo) 0 SNYAXOVA, T-M- L&; PRL Purification of triaxans ty zone malting. Zhur.fiz.khIm. 37 noolot2363- 2364 0 163. (MIRA 17o2) 1. Moskovskly gosudaretyennyy univeraltst iman-I Lomenosova. AMIXINp A.00 Zone mltlng of organic substance crystallising -at temperature -a UP to 106P C. Zhur, fis, khim. 38 no.lt208-210 Ja'64. (KMk 17 12) 1. Moskovskly gosudareViennyy universitet imeni Lomonosova, ACCESSION MR: AP4039625. S/0076/64/038/005/1372/1374 AUTHORS: Anikinj A.G. (Moscow); _!,_G.X. (Moscow) TITLE: Methods and technique of physico-chomical investigation. Determining -the purit7 of organic monomers in a hermetically - closed Vessel by the cryoscojic mathod #_1`181 A610-51 1964t-1372- 374. TOPIC TAGSt cheniul p4rity.-erganic monomer purity, cryoscopic purity determination# crystallization curve, malting point curve, trioxanso methylaothaerriatel disethyldichlorosilane, octomethyl- tatracyclosiloxanel low melting organic monomer, high malting organic monomer ABSTRACT; The equipment used for detemining such jurity for solids or liquids at room temperatures is figured (see an osure). For low melting compound* an outor jacket is sealed to the equipment where vacuum for regulating the cooling rate is created. The monomer is kept under inert gas. The selection of the coQIing agent do ends upon the crystall1vatLon temperature of the given monomer, the goat- ing agent upon the melting point. Purity was determined according 84,dt, 113 :1,ACCESSICH MR: AP4039625 to the crystallization or malting curves. :Crystallization curves were determined with a SOlf-3cribing potentiometer for 0.07, 0.03 and 0 5 grad/mm,3eqsitivity. Purity was determined for trioxans (99 6jo)O, metqlmethaerylate (99.") dimethyldichlorosilans (".01) and octomethy tetracyclosiloxans (0.5%) with crystallization too- peratures between 60-'and -80C. The cryoscopic constants for Cal- culating purity weredetermined experimentally by lowering the temperature with an artificial a&aiture- Orig. art. has: 2 fi4x~res and 1 table.- ASSOCIATICK: Xo3kovskiy gosudarstvanny*y universite't in. N.V. Lomon03ova (Moscow State Vniversity) 'SUBMITTED: 04jun63 SNMI 01 SUB CME OCS cc MR RSF SOW: 005 Orml 005, 2/3 C*r ACCUSION NItAP4039625 4 INCLOSM t Ol OP Figure I Vessel for determining the purity of solid organic compounds at room temperature: I --jacket for--tk4t-tb-erinocougo~,-2~-stirre-r -___3___oute__tube._ 4--glass outlet for introducing r -and removing Inert gas, 5- thermocouple, ~4. 6 - tube for the core, 7 - core, 8 - electro- 'S magnetic coil. t rl h;.11, ion imp'l ri tas; tt es kJoy "-),tat ,4 IN -*,s Lccx% 7 -e t engjy of 0 t 5 t av c o w I I he I a r - r-a -4 -4 r -e ~i A a r f A is m d 17. h ri K* v, r i v t ha T-'Fx~.j yt%&M i c 4'z fl :r'. % : , , K- -'. ~ A, I ,,, :, wuski 1 an* ud*rv tv-er,.ryv univi-t %I ~, - - . (Koic,r-d 1 4 I , - cy, , , , ~, ~l - Ch- I I ~ iF f, -1,17M : k" . W2 A-Wirli, A,n AD ~m thp i..f t a0 ej Alt~ :."o r4grung of~p -i~)Idag v-&3 carriod -na cm di-nett,.' on - l1qtal ,-oi)dlL!*na and havirg an .,,~rutporsOur- grudienta and ".4 -th :>( the WaA ~mtf;jrlr, w-gi In !'-Ir.- the uppew ' ruMA~m f 'i tr imUll thr. ImpurR- _f ctm t tin w a '41i J3 thA i*ao mAting w,&s evt ! v 0 uts d = tvrd a t 0 ~ 15 !.,,p If tho bta r cii d! rn ethy 1w --4 metbriql is that thiv i,~a, 11--ttom fama gcne must tr) fram gv, M 4k Tvr-kiy gr-!4x)r,6rqi-viN:":nyy tmjvpr-a ~r- F.14 C 1, 0o "DI ANDaNs A.G. . RAMENK00 N. V, ~ _p;,,Av Z0r-6 maltW Of Octa"Usyl tet.-arreloolloxene, Plast, masoy no,1:20-23 165. (MIRA 3.8t4) r Ind t~tls r 1; up n a T I xi -Yf 1, till t.T ~ , - ~ ~. 4 ?,;, .1 ~, , ., k , 'V I '. - . , ! I ~..j . ~ ~ A% "'i, ~ , , - t , :1~ ~% , 1 1. 11 YT14 MI , :)', .1 r A r w r 6 law T ons alit 9 -.1 ilf Witter