SCIENTIFIC ABSTRACT FR:HAIDEGGER, E. TO:HAHN, S.

• Document Type: CREST
• Collection: Scientific Abstracts
• Document Number (FOIA) /ESDN (CREST): CIA-RDP86-00513R000617800036-6
• Release Decision: RIF
• Original Classification: U
• Document Page Count: 99
• Document Creation Date: November 2, 2016
• Sequence Number: 36
• Publication Date: December 31, 1967
• Content Type: SCIENTIFIC ABSTR

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Ir ie obtained, yield 44;x, melt. p. 129 to 129.5`'
(from e~lcohol) . 3.5 g of sl is added to a cooled
solution of 2.03 g of Te in 12 ml of 10,E-ual
Card ; 6~7
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XUGOSLAVIA~Orgar-j. c Chemi atry . Synthetic 4rge~ni c Chemi. stry . G
Aba Jour: RQf Zht~r-Kbimiyft, P1o 22, 1959, 74038
benzene: + petroleum eater), ITIf, 2, 52, 198 to
200/9, 66 to 67 (from benzene ~~--petroleum ~;ther),
5, ~-, :ll, 40, A, 88, M, 85 tq E15.5 (from bcAn zenc
+ petnl~leum ether); IITg; 5, -, 86 to 87, a,
A ~ ~7, .~ 46 , ~ to 47 (from dilute CHa01i)
I~p 22,
j TIIh,
~
10, y, 1~8 to 109, 20, ~.~~, 1~5~ A, ~a, -, ~f~ t~~ 89
(from 'eenzen + petroleum ~;therl; IIIl., 1, -, 150 to
152, 7.1, 120, A, 84, �, 129.5 to 130 (from dilute
alochol); III, 2.17, -, 144 to 105, 5, o �9, 40,
A, 91, ��, 129 to 1.30 (f rora CH � ()K ); II Tk, l0, -,
129 to 130, 20, 7.2, 90, A, 9~, -, ~ to 81
benze~ae ~� petroleum ether); II:[L, 1.2,131} bn {from
1.36/18,
-i Y40, B; 8~, 158~to 163/.15yi 1~~3;to 141+/5, - (Liquid,
Card S/7
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YUGOSLAVIA/Organ:t~~ Chemistry, $ynthet~:~e Orgnnic Chemir~tz�y. (',
Abs Jour: Ref Zhy~�-Khimiya, No 22, 1~;iE3, '~'40~9.
initiaA TTT~�e, their amounts in g, boil. p. in r C/
mm, melt , p , in ' C, amounts of C , ~ -I~ in m1 and of
pigs. in g, reaction duxation in min., purification
method, yield of I in i;`,;, ite boiling point :fin `1 (:/
mm and j:ts melting point in. '' C axe enumerated: IIIa,
3, -, ].~El to 142, 15, 5.7, 40, P~, 84, 160 to 12/15,
13p to ].31 (from benzene + alcohol); IIIb, 4, -, 62.
to 64, E3, 7.1, 1+0, -, 153 to 157 f 18, 7o to r~1 (from
benzene: + petroleum ether); IITc, 17, 136 to 138/15,
34 to 31E, 45, 13.6, 45, ,B, 84, l55 to 160/16 148
to 1~~~'].1, - (liquid, n" dD = 1.6236rr d~ ~~
1.1629 );. IIId, 5, 111, -, l5, 2.8, 45, ~, 98, -,
49 to G;U (from petroleum ether); ITIe, 10, ~, 123
to 124, 20, 7.2, 60, A, 86, -, 147 to 10$ (frets
Card ; 4/7
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' YUGOSLAVIA~Orgatlie Chemistry. Synthetic Organic Chemistry. G
Abs Jour: Ref ~?,l1ur-Khirrdya, P1o 22, 1958, 74038
alco;h~ol) . 6 g of VI is E~ddPd to 4.2 g of benzyl-
anili~ne in 30 ml of C, HrIJ, thn mixture ie r~eaeaned
12 hours, after which 40 ml of water is added, tree
mixture is filtered and 'IIIdi'lutebalcohol)yiTIla9to~~
melt . p. 111 to 112 ' (fr~am cnc~leci
zxlq are bailed with F,~94 in water-.free C, H` N, ,
poured out into a > to l~~-fold amount of water heated
to 5C~ or 60'~, seasoned l2. hours and filtered, and Ia
to a:cl are ct~tained. If ~7eceasary, 7a to :tq ara pre-
liminarixy disao].ved i.n 8 to lOr,�ual Na(`I~I at hQatiug
and filtered, and Za to lc~ are separated with ~.0~-uaJ,
HCl (,method A), or the reaeticn mass is extraete
with ether, the extract is washednw~he f~1low~n~lthed
dist:tlled in vacuo (r~ethod R~ .
Card 3/7
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YUG4SLAVTA~Grganic Chemistry. Syntk~si~ic Organic Chemistry. G
Abs Jour: Ref Zhur-Khimiya, No 22, 1~~58, 74038.
R' ~ i+-C~H,4C~H~f (Ilt)j R a li' ~ C,~H~- (T1); R
n R' H,~C(CH~);CH,~ (Im); ~1~; a Cli3, R' ~ C~H�; (In);
R = C, Hoc, R I ~ C G~`_ (To) j ~i ~ Cr, HS CH,~ , R'
C~H- (Ip)3 R '~7R' ~ C,Hc ~:Cq), ~~nd R ~ CGH~, R' ffi
C~OC~HS (Ix) ; and S-methyl-iea-thioanilide of
thiapyxomueic acid (II) were synlthetized with a
view to study their biological properties. _
Ia to Tg, were prepared of ~~orxespond:Lng C~-G~f~Ha
GCONRR'-s (IITa to ITIc~) and P 5 , and Ir and TI were
prepared by the action of C H COCI (IV) and (CH) SO
(V) an Ie. 22.0 g of bCH~CHCH~~C4C1 (VI) is added
to 23 . ~; g of phenetidine in 204 ml of 5; ~ual Na4H
in 20 n~in.j 1 hour later it ie filtered and IIIk is
obtained, yield 81L;~, melt , p . 130 to 131 � (from dilute
Card 2~7
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..f,
1
YUGOSLAVTA~Orgf~riic Chemistry� Synthetic Organic Cherr~istry. Cr
Abs Jour: Ref ?blur-Khimiya, No 22, 1958, 74038.
Author V.. a~'an Z. Sto~anac, 0. Shchedrov, N. Prs,vdich-
Sla ovich, S. Tomashich~ A� Ever.
Tnst
Title :Amides of Thiopyron~ucic Acid. Thiaamides. Report I.
Orig Pub: Croat. Chem. acta, 195'Tr ~`~, plc 3�t~, 3i9`:~~7~
Abstract: bCH~C;HCH~CCSNRR' ~ Ta to Ir, in which R = R' ~ H
a ' ~ CIi~ Tb ; R ~ H, R' = C:H.S (Ic);
(Ta), R H, R (
I ( )~
R H, R' ~ Ci.H;CH,. (Td); R � H, R ~ C~;,H�~ Te ,
R = Ii R' ~ 2-CH;C4Iiy. (If): R m H, R' n :S-CHjC~ Iiy
(ia) ~ ~ R ~ H, R' ~ 4-Cti CbH~. (~); R ~ ii, .R' ~ .~- r
CmH,~ '(~~-); R ~ H, R' ~~ ~��CH3OC~~.H(~(Z~); ~Tt = H, R
Card 1/7
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YUC~()SL~l.~i~:I.A./Or fra;r i ~^ C~iez~ri s t r~y .. ~;~nthet:i ; ~?r~ ~;a,rxi~~: ~'~t~?tni st r ti' a ..,r
Abs Jour R ~ f Zhur K,s~ ? .m~ yam,, ado 7, 1..98, 2:i!~"j2
at 2~0 to 2~Oo, diswilled with steam and. 1 is extra~::ted
with wat.e~7� from tre residue, yield 63~, meltirl~ point 184
t~o '850 ~,i'rom. a1.^o~ao.l). 10 mmoles of P2S~ is s.dded to 10
rQrrlp? F:~ ~.~}' I: in 10 1Ti1.i.t. of anhydrous C5H5N, al.l i:~ poux�ed
out into `i0 mlit. of wa,tex~ and III is separated. ;at about
0~', 12 hours ?, yield 84~, melting point. 199 to 2000
;'f'rom berirene l � II: wa,s pr. opexed of anhydrous V and
n~..r~l(."~H4N02 similarly t,o I, yiF~ld 50~, 1ltelt,i.~~t; pc~.i.ni. 1.88
to 189� ~ i�xor~ A,l.~:ohol.~; ~1; was prepared simila~�1�)T to lTI,
yield ?3,6 , mpl~t ing point 1 ~ 4 to 1'j5� from. '~4r>z?ne ~ .
Card 2~2
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Y?TGOLII,,A.L`I,~,/0r~xli~ C'hFrr:istr;f S;n-:'~.Pt�i.. Qr~.ni~ ('~I�rT?.istr~,. G-2
A.bs ~f~ cur R~: (' Z!>>xr Kl~ itri vr;,, Prc~ t , 1. `if' , ?J ~''%
Aut~hc>r� ~~'o ~t~hn, ~~!� Pr�e�d.i~ ~~57_e,do~~~! ,
I n s t ~ _d.~..~._,_.~..~.,...
TitlFR i'h>= i'! ~=z~�:rat~ian cf Scm.~ 1� `~~!it~ror,~r~r~~i ~..~ pti-r:i~1~~r;=, ~.r~~
-�t.hic~p;rr idorA~:s .~
Orin Pub C.'raat. ~ ~�~~m~ s.~_t�,~., 195`?, 4'~-), No ~', _l~7 ~.~9
~,bst1`tx~:t, 1 ,z ~'~ nit ophony].;. ?..pyx�.icf,j,c: N x? t~.r~cl 1 ~~L' ~n,ii~rap?,.rnyl:)..
-�2�~~ryridon~ ,T.II w~Y~e; syn.tl~.~;l;iz!~d a.nd f.h~: :ar�z�:;.~ponding
2 ,thiop~x idonFs ITI: and It' ,~ wzz`P abtairzed fr c~rr '~~ ~:~..
P~vr~idone .~ is pr~par~~~d of 0.1. rr?ol~a of ~ ~;~.mi.no~:~yrid.:i.r~.~ in
100 ml.it of ~0`~i~�u.~1 ~I`S0~ ~>> the ~x.~tian of O.LC~a mnl~ of
N~NO~, y:iF:ld ?5~, -a..r~c1 it: i; txa.r?.sb.r~ir;~~~~ ir"�o t.ru K ciQr�i
vative tV 1 a:~::nx�ciill~ t,a B.in.z� Fuld Fts~,�tli E~L:ieL~i~,s As!?:.
Chem,, :1~~1, !~9, 1.0'7,1; ~~ i:a a mc~z~ot;.,YcLx�a.t.~:, ~rlYltln~~
point 2b~ to 4:'(3~ . 45 rrrcr!al ~~;~ of i~I~.~iyd.~~uu!3 `J, 1f`Q :nrns~l.e
of m: ~B.rC~~~~NO~ a!ld 0.3 ~ o~; c:'u powder ~r~ t?.a~atPd ~+ Yiolirs
Ca~r~d 1./2
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A~~s Jour Rc:i `L.?:,ur ~ .310.1.�, Na 3, 1~~)`~j.3, J.~'(l~i
Author 5t;orri, P. , Ma.:~ir:li jo, A., iie~~i~., V.
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APPROVED FOR RELEASE. 06/23/11 CIA-RDP86-005138000617800036-6

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