SCIENTIFIC ABSTRACT KLETCHENKOV, I.I. - KLETS, E.I.

• Document Type: CREST
• Collection: Scientific Abstracts
• Document Number (FOIA) /ESDN (CREST): CIA-RDP86-00513R000723020015-1
• Release Decision: RIF
• Original Classification: S
• Document Page Count: 100
• Document Creation Date: December 30, 2016
• Document Release Date: June 19, 2000
• Sequence Number: 15
• Publication Date: December 31, 1967
• Content Type: SCIENTIFIC ABSTRACT

XWWSOT, Mikhail Makaroviche 4otsent, kand, tokho. vauk; ILICMMO. Nikolay
Somenoviah# dotsent# kand, tokhn, cook; XLBTCIMKff. ly" lvmvich,
aspirant.
Inavel-lacquar for conductors xmdo from modiflod Isauers. Xxv.
,rye., uahob, sav,,t slektromakh. 2 no.603-95 159.
(MIRA 12-.U)
loZavedu)rushchly kafooiroy dleloktrlkov I poloprovodnlkov Xlyovskop
politakhnichookogo Institute, (for Nakrasov), 2.rafedra dislektrikov
I poluprovodultoy Ayovskogo politakhnicheekogo Institute, (for
11'ahank0o 3#11yovskly politekhnichaskly institut (for Kletchonkov)..
(Blectrio Insulators and Insulation)
R ~R; 13A

SOV/144-59-5-11/14
AU'i1HMW: Nek-Lasov M#Mo# Candidate of Technical Scienceog Docent,
Kletcheaov I*, Aspirant
M ed Silicone Insulation
PA~IaODIGALs Izvestiya ashikh.uchebnykh zavedeni Elektro-
mekhanika, 1919# Yr 5, pp 98 - 100 (Us
A)
ABSTRACT! Insulating materials based on orsunic polymeric resins
modified by polyorganosiloxanes are of considerable int-
erest* These materials have good.adhesion to metals a
resistance to heat which is nearly as pod as that ok
ordinary silicone resins and high drying-speeds. Resins
that may be modified in;lude polyesters, epoxidest poly-
vinylacetylat phonolformaldehydos and others. Moreover
the process of combined pol7merisation of certain organic
polymers (oils and resins) with monomers or polyorgano-
siloxanes can also give technically valuable products*
By this process of co olymerisation, the authors devel-
oped a series of modMed silicones and in particular a
combination of silicone -and tung oii desim=tcd SK-3*
They also used polyorganosiloxane fluids Vrs 2, 39 4 and
9 (of thd All-Union Electro-Tochnical Institute nomen-
Cald 113 clature),, Insulation baood on modified silicones has a

SOV/144-50 5-12/24
Lodified Silicone Insulation
good resistance to moisture and oil, is flexible and of
good inculating properties,, For examplej samples of cable
paper (K-12) of 100 x 100 = were impregnated, with silicone
fluid.Nr 29 pure silicone varnish BF-3 and co-polymer SK-3a
The samples were heat-treated at a tompoisture of 150 -
16&C, which did not impair tho mechanical properties of
tho paperl they were then weighed and naintained in a wet
atmosphere for 40 hours. '11he results of the tests axe
Civen in Figure 1 and it will be seen that treatment with
co-polymer SK-3 gives the least water absorption the
weiShL increase bein6 only 1.4%. 2lectric strength tests
results on the material after exposure to zoiLt atmosphere
are recorded in Figure 21 it will be seen th-A co-polymer
SK-3 givos tho best recult6o Varni3h SK-3 vae also used
to impregnate the annular windings of a tran:'former used
in vieldinG lar pipes It o rates undor particularly
Card 2/3 difficult condrtionsl ;n piperinee its Primrtry winding is

SOV/144-59-5-11/14
Uodif ied 'O"ilicone Insulation
very near the selds and is exposed to high temperatures,
steam nnd bad weather, Me coils impregnated with SK-3
were compared with other types@ including the standard
product imprepated with varnish Nr 460, and the best
results are tabulated The rformance of the coils
impreGnated with co-p;rr was particularly good*
It is concluded that a tied licone insulatibn is very
useful for electrical equipment ex osed to high tempez,-
aturas and humiditys,* Modified silicone insulation has
the advantage that it is only'a,quatter of the'cost of
insulation based on pure silicone compositions* The
reoistanco to heat of the modifi-od silicones is not ggive
an good as that of the straight silicones, but the acLnes-
ion, elasticity and mechanical proportion are usmlly
much bettors
There aim 2 figures 1 table and 2 Soviet raforencoas
AS6WIATIONs Kafodra dielektRkov i poluprovodnikov TAyovsklypolit-
ekhnichaskiy institut (Ohair of Dielectrics and BOMI-
conductors, Xiyov.Polytechnicai, Institute)
SUBLITTLD: April 28tho 1959a
Car d

9 1 BOOK EXPL4DITATION SOV/16229
Alentlyev, Aleksandr Aleksandrovich,, Xvan lianovieh Kletchenkov
and Aleksandr Alskeandrovloh Pashchenko ------
Kremnlyorganichesk#@ g1drofobizatory (Hydrophobic Organosilicons).
Kipv* Ciostakhizdat USSRO 1962. 109 V. boo oopies printed.
Ed,: V, N, Oavrllovj Tech, Ed,: K, F, Guearov,
PURPOSEs This book let is Intended for technical and scientific
personnel concerned with the development of processes of water-
.proofing materials,
COVEMOIN The bo oklet deals with hydrophobic organosilloons. The
use of organosilicon compounds for waterprooflng glass,, honey-
comb concrete, porous silicate cement, and cellulose materials
is discussed. The technology of waterproofing materials and
methods for determining their waterproofness are described In,
detail, The chemistry and development of organosilloon compounds
Is reviewed, The booklet Is based on the works of K. A. Andrlanovp
card 1/4

Hydrophobic Organosilioons- SOV/5229
A, P, Krashkovo B, N. Dolgov, S. A. Yaxanovr and M. 0. Voronkov.
There are 85 referenoess 31 Soviet, 33 Englishp 15 Germans
4 French,, and 2 Ukrainian.
TABIS OF CONTENTS:
Foreword 3
Ch. 1. Chemistry of Organosilloon Compounds 6
1, Main stages in the development of the chemistry of
organosilloon compounds 6
2. Organosilioon compounds and their properties
3. Principal methods of producing monomeric organosilloon
compounds
40 Production of polymeric organomilloon compounds 36
5. Basic organosilicon compounds used in waterproofing 37
Ch. 11. Wetting Processes 46
Card 2/4

ACCESSION XR1 AP4020294 5/0239/800WOM/WWOMS
AUTHDRSt Makramovil Me Mel Xletobeakov, Is 1,1 21*evlabs Re As
TITL& Low voltage nonlinear resistance In doped silicon carbide
swress iwz, naika, 1$640- 23-0
TOPMUOSt reavistances Im vclUge roxistencop low valtage uoh)lmar revistamep
silicon carbide# doped silicon *&M4*s volt upere che geristics chromim
borldes silicon# silica, berjUlus ad
SAA
ABSTRACTs Nonlinear resistance has been measured for the "as 3iC-CrO2-ft(--
BOO)j that iss SO with additions of C 'Sim Crh'"029 And CrB24kO,
with contents of Is 20 50 100 Aud 29 012 were Obtairisidi and It was towd thA
with incre"a of CrM2 come" above 2$ nciMnearlty of the volt-ampere cheractus-
istics declined, We is Wobably duo to formation of ocadmitive bridges at 041,
The intro&wtion of Si., Si%O or W Along with Or% inereastid the e2actriml
resistance And made it possible to obtain nonlinear resistance with a
of nodunearity as bigh 4 (in &&Vles that are mah' mixture resistant am
beat resistant Aid that are "r7 StAbU under operating oonditiou)s Us SGAWSL
Card 1/2

Accmiom NRi Apho2o294
range of the nonlinear factor with these additions was 2 to 3,5, Bed results
were obtained bgr adding about U% of this bondl% matwial to $106 Oriss art*
hut 3 figures
AMICION i X
VeysIdy ordens, Lonlas polit Institut (Slav polytech.
i nical Institute)
SUBMn'TZD# 030ot62 DA219 ACQs 32Kard4 XWLS 001
SUB CODSo PH HD RV BM 000 Onm 0001

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ACC HAS AR6017159 SOURCE CODSo UR/02f5/66/0OO/bOl/BO39/BO39
AUTHORt Xletohonkovp Is Ill
. -Kz~
TITLEs A now method of_obtaining a point-oontoot P-n unotIOA In 00
n-type silicon
OVI
SOURCE: Ref, sh, Elaktronika I yeye primeneniyep Abe. 1B317
REP SOURCEt Vestne MZevsk. 2olitekhnA In-tag Ser. avtomatlido
no, 1,9
slaktropriborostr, I rad 1964# 161-265
TOPIC TAGSatvijunotionj n type silicon aluminum wire
Etc, a n-type sill oon wafer
ABSTRACTs A fine aluminum wire is welded on
by passing single sawtooth pulses thim-ug the contact with the wafer,
ONO"
I* B. (Translation of abstract) tAKj
SUB CODE: .70)Lst SVM1=5A29==mantL
ic

ARG03200f BOURCX COD191 tJR/0271/GS/000/007/B027/D021
AUTHOR'Joifthonk2ya
TITtZt OR-# AND-~j and INHIMTOR-typs diode logic circuits of mfcrominiaturv~,`
design
C,
'SOURCEt ReL sh. Avtomatika, tolemakhaniks t vychislitelInar tekhnikag Abe'
7B197
~REF SOURCE: Vesta. -ftmk. g2lite" in-ta. Ser. radioelektron., no, 2, 5~1
1985, 127-131
TOPIC TAGS. logic circuit,, logic design, silicon diode, pn junction, AND circuicv,4
OR circuit, INHIBITOR circuit,, microminiature design, n type silicon
A13STRACT: A method of producing OR-, AND-, and INMBITOR-type diode logic
circuits with three microminiature inputs Is described. It Is based on a now me"
of obtaining point-contact p-n junctions on n-type silicon. The p-n junction is
is
produced by fusing a thin aluminum wire to an a-type silicon crystal, while a sing
pulse of sawtooth current to transmitted through the contact between the wire and
the silicon. To microminiturise the OR circuit, all Its elemonts,,utillse one Swoon2
card 1/ 2 UDQ 681. 142. 67

5
-crYstaL Inmicrominiaturitteg AND wWINMMTOR circuitse all the circuit
diodes utilize Vne silicon crystal,, while the 0th
resistances 0: or elements of the circui
ts L 0.
r6 microminiature Volutn* resistorse, Orig ark WWI 6 Ulust
mtiog4,,
(Translation of ah#tr&Qtj
'SUB CODE
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Awd 212
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K-L E re c it 9 4
L , J.; MOMUM, J.; ZIMWX19, P-; TOMIDUT. S.;R6HLtKG. S.
Affect of pentammothylenstetrasolo on thyroid incorporation of ra&IOWIM
in mts. Ceske fY~Iol, 8 no.2sl33-236 Vlar 59.
1, Ustay pro pool 0 matim a dits, TykIW ustav ondokrinolOSIG49 Prahm.
produesquo nn "oslu o ucluoich ionisacniho sareni dw 26.10. 1958 v
Prasee
(PMYIJMMTAVWOLN. off.
on thyroid radloiodins Incorporation (Cs))
(TMOID Game off* of drup on I
pentylonototmole on md1olodlue incorporation (02))
(IMM, radioactive,
thyroid incorporation, off. of pentylowtstrasolo (02))

Mrpothermia following the administration of pentamethylonetstr*2014 and
corebrocortical oxygen requirement. Cook. fysiol. 8 no-3:238-239 Apr 59.
1. Ustay pro o matku a dito, Praba. Prodnessno na M. fyolologickyah
dnech v Brno dne 14. 1. 1959.
(PUTT off,
b o4y tompeft dooreaso, off. on oerebrocortical oxygen
roqtarsmont (as))
(MM TAGMATWo, off. of drugs on,
pentylowtatrasolog corebrooortical oxygou reqalromont ro-
quiroment rwation (Cs))
(MMIDAL 00IMs motabe
oxygen requirement in pentylonststrasolo-Inftood hypothermis.

PRUL, Aris NUMIA, Frardmil
I --------------
Awleptlas In hypoxic trodyaardia. Cook. gyn. 24[38] no.3:190-191
Mar 39.
I* Ustav pro poci o matku a dits v Praset roditol prof. dr. J. Traplo
IRMOMIA. exper.
byposto fetal in rabbits, off. of maternal admin. of
(Gs))
("PMIA IMOIRTOMI expert
blypoxio fetal bradyeardia In rabbits# off, of vatornal
admin. of analoptics In progm (Cs))
(AXAWTXCP,, offeatog
on exper, bypoxia fetal bradyaphrdia in rabbits,, maternal
admin. inprogs. (Cs))

DTXDVA, H. I PFML, Jo nd. Isk. ved#:POSPISIL, J.; XLVWXA, P,, Toohniaks
spolupraost IW,~nal A,s Tatlaova, B&
Ussue renotions to oortain types of suture vaterial in rats. Cook.
cm. 24C381 no.gt?%-722 Nov. 1939.
1. Ustay pro pool o vatim a dito v Prate-Podoll, roditel prof. dr.
J. TrapI (SUMM)
7 --7777

PML$Jlrl-.
Phanobarbital and the effect of estrogens on the adrenal cortex
in rats. Case Isk. cask. " no.2?t83&442 I Jl 160.
2. Ustay pro pact o mtku a dite v Prass# reditel doo. Mr. X.
Vojta,
a
MIMEN COAM pbarmadol.
%FHmuzmwlUm pnarftdol. )
(D Islum"016 warms"I.

PML, Arit MMOD, Praideall
Poutwiethylemotetragole and wqgou reqmIrevent In the cerebral
aortas. d"Asksoeske" so.)911235-1238 23 S 1 60.
ustal Via a matta a Mte T prazetraditel doe'dr, NToStA,
pharmacol)
WSIM COM metab)

on tbg problou of the . ,effect or bromine on the estrus cycle In rato.
Cook. gyn. 27(411 "oMM-249 mr 162.
is Ustay pro "a' tku a dits v Pnsa, red. doe. MDr. H-Vojta,
$*$louslly lokar C:X
(ESUM pbamool) (BROWN phameol)

I b.e.
I . ~ t t. lfi! ~J ti~ I ..-
iI
I i -,

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nk,
do
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32409
Z/014/62/000/(14) I /OUA/Ul I
19-1151 40110 9073/ES35
AUTIUMS.- Koutxkf. Jaroplev, Docent Engineer. Candidate of
SCIP1100, Xlojetkii, Zdontk, Engineer, VPtfAka,.jtmniWnv
TI.F.- invitionce or moittng in vacuum on the oroimertlex or
forritic heitaeststa"t xteP1P*1*Cr containinS host
resistarit a a a
m.or(MICAL'. Hutnickd listy nol. 1962, 31-17
TPXT The authors have investigated the inflisence or
melting In vacuum an the properties of hoot t-rest * tant attretiq at
orpsent looing produced or.developed in CzechontovAkiii, [he r1rat
metiritfoat were made an inoculated 12% Cr stfbel (type CrI2*2VI, rh e,
,otudy w4%s mitile sising a 300 kg ingot from a i-ton heat "roduerd In
an electric nrr riornace and having the rollowing compo"ition-
().114;* C. 0.741:t", Mn. o.42% Si, 0,0104 It, 0.018% S, 0,110-~ Ni.
I 1. %4 c1-, 2.()r)% w, 0.16% V, O.lr)~4 Cit. 0.01#)6 N. rrnm thits inwat
2:1 mm dinmeter radio and 14 x A on T%rimms were forged and used
as trit qvectmonx. Furthoirmare. 100 ime diameter electrorie* were
forged and machined down to 80 so diameter anti toned ror Pubooquent
re-melting in vacuumin a furnace, produced by He"ors. lbaratiest
(west Germany), of 30 kX capacity, Three electrodes were
Card 1/3

31409
Influence of melting in vacuum /,/o 34 /6 21ou(;I(X I I /Oo ';/o I I
re-melted At A VACUSIM Of 10- 3 am Ng and !Yother throe Plertrodes
were re-welled at a premsiore or About W MM H Vrom each
serion of' the thus re-melted ingots one wa" Inventirstted in the
ns-cant state, Anti another after forging, A port or the miteri at
from tire original 100 kit ingot was ro-walted in a 40 kor indiortion
furnace in A normal atmosphere and deoxtdtzvl with CnSt Awnin A
part of the material was subjected to toootp in the a-%-roitt "tole.,
another part. after forging. The results, which are describool In
somne detnil. showed that *xcept for a certain increase 4":erpop
resistance, which still has to be verified by meana or Jonfewrion
tpstx, the re-metting In vacuum did not have &ny pronounced
inflifenco on ilia mechanical proportion, The, hydrnxPu content
which wAn very low in this steel, remained virtunity URIVIIA111tod
acter re -irltinc in va"um- The content of other olemontr
did not drop appreciably by the rr-melttnX in vacuum *.xcppt
for trip stiLrogets content, which was 0.042~4 In the I. t nduc t ion
meltq-d xtrel, 4),021.4 in the steel pioduepil at 10- mar M( and
0.01819" 111 the stool produced at 10- MR 110t. rhe Aitthor"
emphasize that the described results Are the firot or A Peries
and were obtained for specimens from a mingle basic heat.
Cord 2/~

324W
Influence of melting in vacuum Z/034/WOOO/001/003/011
Therefore, the validity of the conclusions for other types of
12% Cr steels has still to be verified. There are 22 figures,
5 tables and 5 referencent 3 Soviet-bloc and 2 non-Soviet-blac.
The English-language referent* roads as follows# Ref.5t
K.J.Irvine. D.J.Crowe, F.B.Pickering, J.1ron Steel Inst. 195,
1960, P-386.
ASSOCIATIONt Zdvody V, to Lenina. Plzo'nA
(V, 1. LeniW,.WOrks, Pilsen)
SUBMITEUt Sep-t*nbrr 8, iq6i
Card 3/3

DMERS Zdo insom DroSool IMMUs Mop I=#
Tacuin arc furnace wIting In a vnit of 2&boratcz7 size* Part 2&
bVerl ftas vith W funws tica, M 31st7 27 uo,9t617-426 3
162,
U Zavodr Vol* Imnimp nap*, Mon*
If

EWNM, Zdozwkp DrSo.1 WMU.4 Idenaki, ins.
WtIng less of sms Olss4ntm during the vacuum arc w1ting of
s*lsoted stools and alloys. Rut listy 19 noo8t539-544 Ag 164.
I, Zavody V*I* Lenins, National Enterprise,, Plzen*

L 225?8.66
ACC ?As AM012975 Com: UR/0094/65/000/007/004i/6043"
doo, .4
ljollaNam, Ya. No$ Vinograday, A. A.-, Vnlobrinsk , So D-; ylers L.
jy
crudinskiyp P.-G.1 Dolgihov, A. 1.1 Ziltberman, R. I.; Kazak, No A.;
Vny.mevskiy, B.-A-1 Uvehitej 0, S.1 Maltnikov, No A.1 Minint G. Pot MukoseyeV9
Yu. L.; Rayfalld, No Rol ~Petrov, 1. Jol Havint V. 1.1 Samvert M. 1-.j Serbinovskiyp
G. V.; Syromyatnikovo I#'IA@
ORG: none
TITLM Lev VeniAminovich Utvak (on the occasion of his 60th birthday)
SWUM 11romiyahlennaya energettkap not 9# 1765# 43
TOPIC TAGSs electric engineering personnel, electric power engineering
AMTRAM The noted spa6lallst of industrial power production,
Candidate of Technical Sciencesi Docent of the Correspondents
Power Institute Lev Venlaminovich LITVAK.begon his engineering
activity at the Mosoow Assoolation of State Eleatria Stations In
1929o Later he become one of tho coauthors or all the "Directives
for the Increase of ths,power factor" Issued In 19340 1955, wA
1961o He published 70 scientific, papsrs. For his successful
aotivitles In defense Industries during World War 11 he was deoo-
rated by *Znak Pooheta," After the war he concentrated on sol-
entiflo-podagooloal work and In recent years worked actively in

.7 1:,
L 22578-66
ACC NIj
the Toaching449thodologioal Commission of the Ministry of Kigher And
Intermediate Special Education USS14 for the specialty "Electrical tupply
to industrial anterorfass mid cities*" Orig, art# hast 1 figure. JMSJ
SUB COMI 050 100 09 SMN DATZs none

lXL'SHAM, TA.X.; VINOWAM,, A.A.$ VOLOBRr=Xrr, S.D.$ GZnM, L.B.; GRUDlWKIT#
P.G.1 DMINOTO A.I., znfmmNp R.I.; KAZAX, N.A.; XWV3AULJjJ.;.
KNUMSMV B.A.1 LIVSKITS,, D.S.S MZLIXIXOV, X.A.j M3311N, O.P;;
mm"
MCSRM,p Yu.L.1 ATMUID X.R.1 PMOVg 1.1.1 RAVINS V.1.1 SAXOM,
H.L.1 AMn=gKyt O.Y., inommimt I.A.
UY Vanisminamdeb# 1905j, 0*4ils 60th birthday. Proca. norg. 20
no,943 8 #65s .1 - (MIRA 18 s9)

kl 327 Do litkotorye ob lzlozhenii te-oril dvo7rakh Lategradow
vo vtuzakh. Uspekhi matem. Nakhk, Vyp. 3,
i"0: letoplat LburnallnyUh Statey, fi-r. 2c , i~'CAV&, 1949-

ummx, D. V.
Sbornik *&ch Po inaliticheskol geo'MtriiCdollection of problem in amIrtical
goomtrz/O Moskva, Gostekhizdat# 1930o 220 pe
SO: don= hut at Vol. 6 No. 8 Novataber 1953

KIATIVIK D.To [authorh, SAWTSXIY. L.Te. Crevieverl; XYMOV. I.T.Ersdaktor].
"Collection of problems In analytical geometry.0 D.T.Kletenik. Reviewed
by L.B.Sadovskil. ttsp.mat.nauk. 8 no.4:208-210 A-Ag 053. (XLRA 6t8)
((kometry. Analytic) (Klotonik. D.T.)

- KUMIX, D. 1.
Ccollsotion of problem In analytical posetry] Sbornlk sadsch
po ausliticheskoi geoutril* Isd* 2-e. Nookwa, Gost4kbIsdat,
19540 240 Ps (MM a$ ZD)

XLVTUIIjA;jll jlktgrorloh-tlM!jW# 1#1o6 professor, red*tor: 80liCOM, Teikot
rea"Orl TvvuLWuF*--N&A4# zekhacbeskly redairtor
EcoUsotion of Proxonslu evalytical geometry] lbormtk sadaah pa,
sualitichaskat geoustril, Pod red6 N.T.Iflum. hd4 4-ase sterso-
tipaod. wolkV80 Gass Isd-va takMiko-teorst, lit-ry, 1956, 240
(NM 10121
("Oestry,, #Wulytio-Pro'bless. siterateose stae)

Di stro 4s4i
Ixfow no"All of tdlf, gad
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X% I cn~v - oft-W L4
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4~i, t aira. ~ Ou w . i z3z, i 'Ma, a fu 14 1 Ad
I UU, 0 0" 124 41 2 "A 1 4311, 0 101 ~ (13 it 2 1~
4 A.; 0 ~013r~, M 2 2 1 _f I 4~ f. 7. f 40 7 0 PU . 0, a Q -, 4.
2 2W, 1 004, 0 0022VU, 2 115. 1 NZO, 0.00-63M, 2 263~
f 40re: 1) f. 0 13 7 V, ! -U 5. , , -.% %F 4 1 ,, iv 106 At I rl" I
tlM d4nfWAtkf"J
5(
CC- eft. f-tv
UN LiCl., 44.33. 173. a 04. lei.. 40 M. 291 3 4A, nd
ZfRir, A2.33. ". C&S. I imfic&U"n fr-nm ttegw d.t4
~k-4t th4 "Its kwm etmgA-~%el ith the W4,~tul %," ~
A-IMO-A he th-T frV!h4$!S 44 ght f4~-WWC QCW COG.-eJ6.1
ZfO,,-JrCJfA, whit# upt- hydrtj!ytn in dr, m vr~Gui
likil; Acrqsf#vllYLq)o-A criv-M, 182*, AAdzea-.0-
CIIIA, m. M . The stsWity J th4ne typ" 4 cAm k-1"
li~r.ncd by letraMMem Imm the rkmwato of (Woup R~ T
cream wtih iw-,rftw is the mv4"t radi4s of th* -irtl
rdermem A P xggL~-6-
JA

AUTHM Osipovp Os A,j " Kletenik, ru. B. 79-11-3/56
TITIZ: Dipole Xoments of the Complex Compounds of Zirconium Chloride with
Compound Leters of Monobasic Acids XII (Dipollnyyo momenty kompleks-
nyklj soyedineniy tetrakhlorida tsirkoniya a sloshnymi efIrami. odno.
onnoynykh kislot XII)e
MIODICAL: Zhurnal Obohchey Khinii r U. pp. 272L.2927 (M)
1957,p Vol. 27P N
AW7RACT: The interaction of the tetrachlorides of tin and titanium with vas
rious or(;antc compounds containing nitro&en and wqGan 3eads to the
formation of complex molecules with high dipole-coments 1-3. Such a
high polarity of tho complex compounds with arM, and TiC14 cannot,
alone be explainW by a polarization-interaction ard indicates the
occurrence of a strongly polarized donor-acceptor-birAing. In this
raper the authors give the rtsults which they obtained in the deter*
minAtion of the dipole-nonents of the complox conpoarxb of sirconium
chloridep ethyl. and i3opropyWormate.9 atryl.,, Isopropyl..,p Isobutyl.
and bonsylo-acetate with the ethyl ester of butyric acid* Thus it is
shown that the interaction between zirconium chloride and the compound
asters of monobasic acids leads to the formation or complex compounds
Card 1/2 of high polarity. The dipole moments of the resulting compounds were

Dipole koments of the Complex Compounds of Zirconium Chloride -i'lith 77-11-3/56
Compound Lsters of Monobasic Acids III,
measured (in benzens)e The change of the alcohol radical in the estor
has no influence upon the height of the dipole-maent in the complexj
whereas the increase in the partial weight of the acid residue sharpo
1y reduces it. From this follows that the stability of the complex
of the type ZrC14 0 *RCOCKI in the solution is chiefly dependent on
the quantity of the acid realdtx.~ Accordln& to tLe measurements the
complex compounds of ZrClj, with two oster-mlccults porisess a cis.
structure,
There are 8 tableaj and 19 references, 12 of which are Slavic6
SUBM?M: November 291 1956.
t,VAIWL?;: Library of Contreves
Caplax compounds-Dipole metsents 2. Zirconium chlorLds-Dipole
moments 3* Orpnio compounds-Dipole moo=ts
Card 2/2

nwmxo Tu. B.
ifff0t of blTalant aLopmag on Uw electrodeposition of slap.
Zhur,,Priklakhts. 30 no.811250-1252 Ig 157. (MIRA 11s1)
1.10stovskly cosual"raltst Iment T.MO Molotov&*
(Mangamse) (Zino plating)
ntD

'i - 7 t" ` f ` --` I - I, I ;. ~'. ~ ~-, - : - - - ,
- . - I I I ['~- 1Z '.1 1 1

Im--.vn'Irt YUOB*f CA~zd Chem Soi - (dire) "rhysioo-cbmiml tindy
of oortivin molecular comp*undv of halides or zirooni= =d titaiium."
Novooherhaankl 1950. 18 pp (HovoohorMsak Ordor of L~,.bor Red Bnn-
nor Polytooh Inut in So Ordshonikod2o). 150 copios List ~.f
nuthorle worke at and of text (10 titles) 41,40-599 102)

67033
'k I F 0 %.f I
AMORS t Kletenik Yu. B SO'r/153-2-5-7/3i
O#IpoY# Ot At
TITLIs ?bqatoo-chasical Ixamination of Several ega-plex, cogoaM4 of
Zirconium Halides With Raters of the Monobasio.Carboxylic Acids
MIODICALt Isvestlys, vysshikh uohobvqkh sayodenLy. XhimLya I khinichook"a
tokhnalogiya, 19599 Vol 2, Ir 5, pp 679-6" (USSR)
ABSTRACTs The authors continue their previcue studies (Refs 5, 6) an the
subject mentioned in the title. In the present papero additional
laws governingthe change in polarityp stability and the formation
omperaturs of the airooniu's-ohloride-bromide-ioaido **riae are
tudiad.-Th6 methods are desa'ribod In references 5-8e Table I
!
shows the measurement results of the di*lootrio constant (9)
and of the density (d) of bensona solutions of the complex
ZrOl4 is (M300002H5and the calculated values of its polarisation
(P). The polarization of the complexes ZrM4 OCYOOC29 5 shows
that these complexes do not dissociate in benzene into their
components in a narkod amer, The complexon ZrRal 40 203M"28 5
dissociate acoording to the #chose ZrH&l #28stel ZrRal #Not +
4 4
Card 1/3 + Nat. The tendenay for disnocistion increases in the order

67033
PhYsIGO-chemi0al Usaination of Several Complex 3OV/ 15 3 - 2 - 5 -7/31
Compounds of Zirconium Halldom With Inters of the Mongbasic carbol7lio Acids
Card 2/3
chloride - bromide - Lodide6 Tables 2 and 3 list the
measurement results of the dielectric permeabiliI7 and the
density of ths beassne solution of several complexes of
zirconium - bromide and sirconium - iodide an won " the
polarisation values oomput*d for these complexes. A marked
change in the polar properties of the complexes investigated
cannot be determined in the tranaition from zirconiun-Aloriae
to -bromide and -ladide. The polarity of the i"ide cozplexes
Is lower than that of the chloride complexes of eirconlum.
In the tranaition from vixcouium-ohloride to zirconium-
bromide and x1roonium-lodidet the influence of the alcohol
radical of the *star rises which increases tho polarity
of the complexes. The complexes ZrH&l 4' 2CH3COOC2 H5have a
cis configuration, The addition temperature of the 2nd ethyl
acetate molecule to the zirconium halide is much lower than
the addition temperature of the lot molecul*# The transition
from siromium-ohloride to zirconium-bromido has little effect
on the reaction temperature with *thyl a4atats. There are
3 tables sad 0 references# T of which are Soviet*

67033
Physioo-ohesioal Ixamination of Several Complex SOV/153-2-5-7/31
Compounds of Ziroonius Halides With Seters of the Monobasic Carboj7lio A*IAs
ASSOCIATIONs Rostovskiy-na-Donu goeudarst-yonnyy univeraitst; Kafedra
fisiaheakoy i kolloidnoy khimli (Rosto-nkDorm State,
-University, Chair of Physical and ColloU&I Chemistry)
SOMMED JIq 299 1958
Card 3/3

5(2) SOT/TO-4-7-6/44
AUTBORS: Osipovj 09 At# Iletoniko TUG Be
TITLIs The Dipole Moments of lalidos of Zirconiusp Titaniumt ?in# and
Aluminum in Moreno (Dipollay
mo
tnty galogenidoy teirkonlyat
:
go
titan&# olova I aly"InLys. v 4 ks no)
PnIODICALt Zhurnal. nearganichaskoy khImlit 195% Val 4, Nr 7t
pp 1494-1497 (USSR)
AB3TRACT% In an earlier paper (Ref 1) the authors proved that In the
elements of the fourth group a direct dependence oriot* on the
ratio of the oovalent radii of the oomplex-forming &ton and of
chlorine for the polarity of the t*tr"hlorides in dioxanee
With a $rowing value of this ratio polarity Increases, In the
present paper the dipole moments of AlBr AIJ Snel
30 39 V ft.j4#
zrj4 and TIN In dioxane are mossurods The values for the 41 -
electric permeability and for the density of the aforementioned
compounds (at 200) are given In tables i and 2* Table 3 con-
tolue the data oonceralng the d1pols'nosents In dioxano of the
halides of Rgj All Tip Zrp Sn and As an measured by the authors
Card 1/2 or avallible in publications* The following was found: for

BOT/78-4-7-6/44
The Dipole Moment* of Ralides-of Zirconiust Titanium# 11no and Aluminum In
Dioxans, 4
SUBMITUDs
AlDr 3o3ODt AIJ 3 - 4*96D# SnCl4 5910D# SnBr 4 - 4ei3D#
SnJ 1055DO ZrJ Tift 5#05Do The polarity of
4 4 5*36D#l 4
aluslaum halides Increases In dioxane in the series Cl - Sr J1
that of tin halides decreases In tht same dirootlon. The
dipole moment of ZrCl 4 Is higher.than that of bromide and
iodido# TiBr4 has a higher dipole moment than T'C'4* On the
basis of published data and own measurements the following rule
Is assumed: The polarity of the halides of elements of the 2o
and 39 group of the parlodlo system increases In the series
01 - Br - J,, that of the halides of the elements of the main
subgroups of the 4# and 5* group decreases* The titanium sub-
group occupies an Intermediate positiono There are 3 tables and
16 rofer*nossy 11 of which are Boyle to
April 260 1958
Card 2/2

AUTHORSt I POT 0. A SOV/79-29-1-4/74
Kravtsovt Yeo Ye.
TITLEt Coordination Compounds of Zirconium Tetrachloride With Rotor$
of Mondbasia Acids. XY (Koordinatsionnyyo soyedineniya
totrakhlorida tairkoniya so slozhnymi ofiromi odnooonovnykh
kislot. XV)
PERIODICALs Zhurnal obehohey khisli, 1959t Vol 29, Nr 1, pp 11-16 (USSR)
ABSTRAM
Card 1/3
In the previous paper (Rof 1) dealing with the complex com-
pounds of stroonium totraohlorido with *store of monobasid
aoids it was shown that the formation of the complexes of
the type ZrCl 4* 29COORI is accompanied by an Intensification
of the polar properties. In such complex compounds zirconium
has the coordination number 6 which I* characteristic of this
element. According to Sidgwick (Rof 2) it shows coordination
numbers of the order 5, 6* 7 and 8 in Its complex compounds.
It to the aim of the present payer to investigate the presence
of complexes where zirconium has the minimum coordination
number five. Therefore, compounds of the composition
ZrCl 4' RCOORIwere investigated in benzene solution as pr*para-

Coordination Compoundo of Zirconium Tetrachloride
With Eaters of Monobaste Acid#. XV
SOY/79-29-1-4/74
tive method# and with respect to the polar and cryoscopio
properties. The determination m9thod of the dipole momeats,
molocul.ar,79ights and the purification of the used products
had aliiidli been desoribed-in an earlier paper (Refs It 3, 4)-
The following complexes were separated and analyzeds
ZrOlC 3C0OC2HVZrC1 4* HCOOC3N,ZrC14 CH 3COOC2959
Zrcl C9 COOC H and ZrC1 C H COW H,.* their d4ole Moment#
4# 3 3 7 4# 3 7 2 j -~
were determined In benzene. It was found that with ;noro::iQl
partial weight of the acid radical In other the dipole no nt
of the complex decreases. The molecular weight* of the above-
mentioned complexes war* determined according to the cry*-
sooplo method. The cause for the tend nay of the complexes
towards xseoclation was explained. Th: trIple"bomplexos
Zr01 4# HCOOC 2H500686 and ZrCl 4# HCOOC2HVC6K 5CH3were also
separated and analyzed. There are 12 tables and 6 references,
4 of which are Soviet.
ASSOCIATION* Rostovskiy gosudarstvonnyy universit*t (Rostov State University)
Card 2/3

5 (4)
AUTHORS: Osipovt 0, Is# Klotonik# TU, ~3, soy/79-29-4-71/77
TITLE: Physico-chemical Investigation of the Reaction of Zirconium
Chloride With Raters of the Monobasio Acids, 111. (Fisiko-
-khtnichookoyo isoledoyaniye vzaimodoystriya khlorida tairkalus
so sloshupi ofirsmi odnooonovnykh kielot*III)
PERIODICAL: Zhurnal obahchey khimii, 1959t Vol 299 Ir 4, pp 1375 - 1382
(USSR)
ABSTRACT:
Card 1/2
Publications do not point out the existence of compounds which
contain more than two aster molecules for one molecule 96C1 4#
Go go MOM V 3 Z (ester molecules) (Refs 1-8). It was tho.
authors# task to investigate the reaction of the complexes of
the composition Wl V 2 2 with a third aster molecule in b*n-
sonso For this investigation more pr*olso data on the solar
state of the complexes ZrCl 4* E and ZrC14 - 2 2 in bonsone were
necessary* The complicated character of the dependence of the
polarization of the complexes ZrCl V 2 E an the concentration
which was detected (Hof 9) and interpreted earlier by the

Physko-chosical Iniostigation of the Reaction of BOT/79-29-4-71/77
Zirconium Chloride With Eaters of the Honobasic Acids. Ill.
authors was in the present paper based upon cryoscoplo Investi-
gations of some of those components* The tables 1-3 and figure
I give the cryoscopio data of the benzene solutions of the coa-
plexes ZrCl 4* 2RCO0C2",�ZrC1 40 2CH3COOC2"5 and ZrCl 4* 2C 7 COO0295
The comparison of the results confirm the aforesaid assumption
concerning the r6le of the concentration. It was found that the
complexes of this composition dissociate considerably Into the
components in benzene solution. The series forsiate-acstate-
-butyrato shows a clear tendency to dissociation* A scheme was
suggsated for this dissociation. By means of the aryoscopic
method and by the determination of the dielectric constant was
found that the zirconium chloride reacts in benzene with two
eater molecules only* The dielectric constants of the complex
computed . ~- froa I the dqta of polarization and to the aryo-
soopio method were equal, Thop are I figuret 7 tablool and 18
.-references# 10 of which are Soviet.
ASSOCIATION: Rostovskly-na-Donu gosudarstvonnyy universitet (Rostov-na-zonu-
State University)
SUBMITTED: January 23f 1950
Card 2/2
7..

50) 50) SOV179-29-5-4115
AUTHORS: Kleterilko YU& B*j Os1povq 0. As
TITL4 Physical-Chemical Investigation of the Interaction of Zirconium
Halides With Eaters of Monobasic Aoids (Fisiko-khImicheskoye
iselodovaniye vzaimodoystviya galogenidoy tairkonlya so sloth-
nymi. efirami odnoonnovMkh kielot); 4-COMPlexas of Zirconium
Bromido (4#Kompleksy bromida teirk n1ya)
PERIODICALs Zhurnal obahchey khimiij 1959, Vol 29# Nr 5,
PP 1423 - 1429 OUR)
AB3TRACTo In the prosont paper the complexes formed fro& zirconium t~roaide
and esters of monobasio acids wore investigated by means of the
method of the dielectric constant and oryoscopy in benzene as
well as by preparation In a pure condition, The inyestigation
methods and the purifioation of the reagents used were described
previously (Rafe 3 and 5)o In tables 1-3 the dielectric constants,.
densities and molecular polarisations of the complexes
ZrBr HCOOC 959 ZrS CH CGOC R and ZrBr C 00C
4* 2 rV , 2 5 1 ~ C 3R7C 2H5 In
Card 1/3 barman* are summarized. The dipole moment* of those complexas

Physical-Chemical Investigation of the Interaction of BOV/19-29-5-4/75
Zirconium Halides With Setors of Xonobasic Acids. 4*ComPlexes of Zirconium
Bromide
(p), the dipole moments of the esters contained In then
and the difference I) are giveh in table 4. The fi"
shows the aryosooplo data for the complexes
ZrDr 4# HCOOC2H,j Zr3r4.CH,COOC2S, as well as for ZrDr4&2HCOOC2H5
and ZrBr4* 2C93COOO 2S in benzenes The tables 5-9 contain data
on the dielootria polarization of complexes ZrBr V 2RCOOC2 B50
ZrBrV 20H 3~00021~t ZrBr4 2CH 3COOC R7. ZrBr4' 2CH 3COOC4990
ZrBrC 2031~0002S. Table 10 presents data on the molecular
polarization of the complex ZrBr4' 2CH3COOC 2S In benzene colu-
tions with different excess of ethyl acetate. The polarization
was found to decrease In complexes of a ZrBr4.2E-composition
(with the exception of ethyl formats) in the series zirconium
chloride-bromide and the dissociation of the linkage with the
second molecule of the ester was found to Increase, The tendency
of the ZrBr o-1-ocomploxes towards dimerization is less pro.
Card 2/3 nounoed thai Insimilar complexes of the zirconium chloride.
R P"

M
Physica.1-Chomical Investigation of the Interaction of SOT/79-29-5-4/75
Zirconium Halides With Voters of Monoba4io Acldn,- 440000200 of Urconlum
Bromide
On the strength of the date concerning polarization and cryo.
scopy of the ZrBr4 *2CH3COOC20 -complex its dissociation constant
in benzene was calculated# It provod to be about 2, IC2 . The
polarity was found to increase in ZrBr -complexes with ethyl
sootate# propyl acetate and isobutyl asetato if the alcohol
radical Increases# The complexes ZrB ONCOCC jZrB CH 00COHr
r4 2H5 rV , C 5,
ZrBrV 0 07C0002H5 were separated and thair malting points de-
termined (1080# 1640 and 1570)o Also the mixed complex
ZrPr 4# BCOO020560686 was prepared In pure condition, It was found
that the bonsons In It is bound to a considerably lower extent
than in the similar 2rC1V8C00C2H5*C6H6-00mP1*x (Hof 6). The"
are I figureg 10 tables# and 12 references, 9 of which a" Soviet.
ASSOCIATIONs Novoohorkasokly politekhniohaskiy inatitut (Novochorkaosk
Polykeohnio Institute)
SUBMITTEN March 109 1950
Card 3/3

5 (2)
AUTHORS: Ostpovi 0. A,$ jC1 atoulk, ju,.B&~ BOT/79-29-7-3/03
TITM Physivoohealoal Investigation of the Reaction of Zirconiumi
Halides With FAt*rs of Nooobasio Acids (Fisiko-khiaichookoye
issledovaniya vsaimodeystvi7a Calogemidov tsirkoniya so sloth-
nymi efiraml odnoosnoynykh kislot) * V;)Conpl*x*o of Zirconium
Iodide (V. Nomplakay yoalda tairkonly
PERIODICAL: Zhurnal obahchey khiniiq 1959# Vol 29# Mr 7, pp 2119 - 2124
(USSR)
ABSTRICTs In the present paper the results of the Investigation of the
polar properties of zirconium iodide complexes with esters of
monobasio oarboxylio acids in benzene are mentioned* The Lai-
tial. benzene solutions of the complexes were produced by dim-
solving sirconium Iodide in tens*ne which contained an equiva-
lent amount of motor, The dipole moments of the complexes-
ZrJ OR 0000,9,t Sri -, 2H0000 2CH COOO
'4 3 2S' Sr'44
4 3 4 2B,9 Sri
2CH3COOO3Rv ZrJ4 # 2 'so-CR3COOC489 and ZrJ 4 0 203 H7C000215
In benzene were determined. It was found that the Increase of
the aoid radical of the esters reduce* and the Increase of the
Card 1h alcohol radical increases the polarity of the complexes investi-I
4

Physiooohomical Investigation of the Reaction of BOT/79-29-7-3/83
Zirconium Halidoo With later* of XonobasiO AOids.
V. Complexes of Zirconium Iodldo
gated, The dissociation constant of the complex ZrJ 4 9 2CH 3-
0000 295 was approximately determined by means of the diol**-
trio constant# In the complexes of zirconium totrahalides with
the asters of sonobasic &aide in the series of alroonlua chlor-
Ida# bromideg and iodido an Increasing tendency of the com-
plexes ZrHA2 4 a 2B (&-ostor) towards dissociation (separation
of the second *star molocule)p on the other handt howovorl a
decreasing tendency of the complexes Zrftl 4 # 2 towards asso-
elation and an increasing Influence of the alcohol radical were
observed. The tendency of the completes Mal 4 , 2E towards
dissociation increases with the Increasing *old radical, A coa-
parison of the polarity data of the complexes ZrUal 4 e 9 and
Mal 4 * 2S Q tables) loads to the conclusion that all Mal 4
2S completes investigated have *is-struoturo. Thor* are I fig-
Card 2/3 uret 7 tablong and 8 Soviet references.

sicoohosical Investigation of the Awtion of BOT/79-29-7-3/03
Ziroomium Halides With Setere of 1(onobasio kolds.
To Complex$$ of Ziroonium Iodide,
ASBOCUTION.. lavodherksmskiy polit*kbulcheekly institut (Norocherkaesk
Polytechnic Institute)
OVEXITTED: June 100 1958
CArd 3/3

8/07qj6o/oo5/oiO/023/030/XU
B017/SO67
AUTHORSt
TITLEs
PnIODICALs
Osippvt Oo A6 and 119teniks Yu. be
The Beat of the Reaction of Zirconium Balides With Rotoro,
Zhurnal noorganicheakoy khimlit 1960p Vol# 51 No, 10t
ppo 2220-2222
TEXTs The heat which Is generated in the reaction of zirconium bromide
and zirconium chloride with ethyl formiate# ethyl acetate, and ethyl
butyratoo as well an the heat of solution of zirconium Iodide In ethyl
acetate were determined* The ratio of zirconium bromide and zirconium
chloride to the eaters was I i 1t and I i 2v roopootlv*ly.4 The heats of
solution of zirconium halides and their complex compoundifin these
eaters which were also determined are gly-9575 Table 1. Table 2 shows the
heat of formation of the complexes, The complexes could be obtained only
as solutions, not in the solid form* The heat of formation of complexes
with the composition I t I was, In all oases Investigated# higher than
that of complexes with the composition I 1 2. This result confirm# the
Card 1/2

The Beat of the Reaction of Zirconium S/078/60/005/010/023/030/11
Halides With Esters 3017/2067
dissociation scheme suggested earlier by the authors (Refs. 45)* In con-
trast to molecular compounds of tetrahalides of tin in the order
chloride - bromide - iodide with these est*rst no continuous decrease in
the hosts of formation in the above order was observed in the complexes
of zirconium halidose The beat of formation of complexes of stroonlum
bromide with these asters is somewhat higher than that of complexes of
zirconium chloridoo The heat of solution of zirconium iodide In ethyl
acetate is 4% lower than the heat of solution of sirconium chloride in
the same enter. There are 2tables and 9 references, 7 Soviet and 2 US.
SUBMITTEDs July 3v 1959
Card 2/2

UZTENIX YU,B.j OSM1,9 0.10
Reaction of titwd= totrahalidoo with eaters of acetic aelde
Zhur. 6b. We. 3120.3171"16 W 161- (KUL Us3)
1. KhImiko-mata2lurgicheskLy institut. Sibirskogo otdoleuiya AN $=e
(Titanium compounds)

OSIPGV 9 O.AiL-==--I-XL Audi
Reaction of virooidum chloride with organic additives having
various funatioma Omps, Zhur.ob,khlx. 31 no.8tUS1-U56 Ag
.161, (HM Uts)
tiromi= chloride)
inanita organic mopounds)
R

KLCMIXO lu.B,
Rdraotlon of trlydant iron b7 isowql phosphoric Odd solutical*
Isy. Sib. otd. AN WR noo6t99-67 t62 (KIRA 1717)
11 Khimiko-catallurglabaskily inatitut Siblrakogo otdalenlys AN
MR# Novosibirsk#

OWerenco on Utraction in An&Wcal Chemistry. Zav,lab,
no.4151&517 f62. NVA 1515)
(Utraction (Mmistry)-Conposses)
(Chemistry, Atalytical)

ZUTENIZ. YU.B.-
Separatlou of Uou for Its mant1tative detendow
tion. Zhur. !M!! -
0 4i. (NIPA 1$ jU)
L MWO140-MOtAUlujiftl Instituteg AaadmW of solmoes of the
U-S-SeRaq Siberlm D"rtment, Novagibig%k;
(Iron-U&Ws) (Extraction (Chadetry))

YIATSNlxt luad~
Jbv extractloo-pbotometric method for the determination of
titanium. Report lools Peroxide caVlex of titanium in an
isCapylphosphorio extra.6t. Zhur,anal.khin. 17 no,9:1063-lW
D 162a (MMA 16t2)
1, Chamico-Metallurgical Institutsp Academy of Solencemp
V,S,S 6H, j Siberian Departmento Novosibirsk.
(Pbotamtrr)

'ih

B/ID75/63/018/001/007/010
Z07i^452

AUTHORS
Kl*fonik

TITLZI A now extraction-photbootric method of determining
.titanium. Communic tion tz' Stobilination,of
diisoamylpyrophomphoric acid. Determination of
iti
tit
i
ti
t
i
i
l
on*
an
um.
n so
u
ons a
var
ous compos
PERIODICALt Zhurnal analiticheskay khimii# v*'l4j no.10 1963t 66-70
d
ith 19 benseno
TEXTs Tetravalent titanium can be extracte
i
,io and dilsoo."Im
ho
solution or a mixture of dlisoamylarthopho
pyrophosphoric acids with awide-rango onceptrations of
g
!
On Imhaking the extract
sulphurio, hydrochloric and nitric acid:
with hydrogen peroxide a coloured.titanium complex Is formed which
can be extracted with benzene andlean be used 6r the photometrio
determination of titanium directly in tho.extraits Thq results
-6e
,of application of this'nethod forAhe determination of titanium
.
solutions of-variouslompositiou'are given,, The efficieney 6r-, i
the extraction of titanium depends on the content of ditscamylpyro-
phosphoric acid. It'was,found that the reagent# which hydrollson
on storing, can be stabilised by an addition of pyridino or
aniline, the former being used in all experiments as more suitable. ,.
Card 2/2

8/073/63/018/001/007/010
A now extraction-Photometric:-,
Z071/E432
The method devisloped for the determination of titanium consists.
in its extraction.from~stronSly scid.obluti6no with a benzene
solution or &-mixture of Isoomylphosphoric acids. formation of
peroxide complex or titanium dilsoamylpyrophosphate, separatio.0 of
the organic and aqueous,phoses, dilution of the organic phase' to
a known volume with ethyl alcohol and determination of its optleal,
don.00y. The maximum relative error for solutions contAln$ng
20 ms/t of T102 amounted to + 6% and for solutions contalni"j~
500 NVI +3%, Ths~ presonco~of Large quantities of coloare'd
ciLtiono Mo, 141, Vul CO+). does not Interfere In the determinaUvis
however, trivalent iron should not exceed 2 S/1 and aluminluw
10 I&A. 'Thor* are 2 tables.
As5OCTATIONt 1(himiko-imotallurSiohoskly Inatitut Sibirskogo
Otdolonlya AN SSSR, Novosibirsk (Chemical Mst&1lurgjftL-
Institute, Siberian Branch AS,USSR,,Nnvos1b1rsk).,
SUWITUD s may 9j 1962
CaLra 2/2.
~A
HIM

XLEMIX. YU.B. (gavosibirsk)
Design of -a mixer for studying the kinetics of rapid reactions
in solutions by -the flow method. Zhure fis. khIa. 37 no*5:
1193-1195 W 163. (MIRA 17s1)
Ig

KIETINIX, Yu.8.; BYMMSUYA, I.A.
Determination of Iron by extraction with 2~-sthylhsxylphosphorio aoids,
Zay.lab. .29 so.ns1306-1307 163* (KIRA l6sl2)
1. Xhimiko-wtallurglcheskiy imatitut Sibirskogo oAelsniya AN SSM.,

JU ' K
_7WO. Yu.;J.p kud. khlv,. nauk, otv, rod,,- TIVAINA,
red.
(Cheadcal analysis of nonferrous and ritre zotala) Xhl-
micheakii analls -Lovetrqkh I rodkikh matallov. NovosibIrA,
fted.-Izd,, otdol SlbirAogo otd-niia AV 33M, 19(4. 1,58
14, kkader.lys neuk SMR, Sibirtkaye oldqIenlye. KfAmIko-
LAtal-lurgichoakly institute

4CCMION NRi AAW223 s/oW5/64/019/0002
AUTHOM laolmnik, We Be
5.7
rain
TITLE: A now extraction photometric method kor dot* Ing tit"lum 'I
3o The use of an ethanol solution of hyYdrogen roddee
1u
Deterzining titanium in solutions containing f orine long'
tichaskoy khImils ve no* 2. 1.964, 208-411
SOURCE: Zhurnal anali
Il9
,TOPIC TAOSt titanium) titanium determinationp extraction photometric
.analysis, fluoride maskingo titanium peroicide oomplox,, benzwo Iso-
~amylphosphorlO acid extraction
ABSTRACT: The possibility'of using an ethanol solution of bydrogen
peroxide to form a peroxide titanium caiplex In a benzene-isoww?L-
~phosphorlc extract has been studied. By using this solution the doa
-pendence of the color intensity of the extract upon %
ic aster oontent is greatly dear"sed, thus Inor"GIZ 4,00urao
-of the titanium dotermInatlon and making the extraotlon *on tFA
e&.1. 3/2.
-4

4camaK us APWA223
Of sms" amoun possib
ts or ti lei A mthod was dova"
.'.the extraction determinalit"IM; of titanim in solutions contaln"Ant
fluorine ions. which normal2l su"ress the extraotdon
IscwqlphosphorIG acid, Is od Ma iking of the fluoride Ions W1
UZZY
aluminum Is most effective 111um and boric acid.wero also tried)
-containing solu-
Almost complete extraction 'of t~twdun from fluoride
!',tions in possible if sufficient aluminm (PtAl ratio must not exo
!:2:1) is added said the extraction Is conducted In 1-5M H2304--~w HMO
art. has: 2 tables and 4 figurea.
ASSOCIATIONS MWdk ats,11132-giohaskiy Institut, Sibirskop otdol"Iri
"AN SSSR,, NOW 01mloo-Metallurgioal Institutep Ubw1m,
~sibi=
Didsimq AN 09)
"4'SUMMj%T=: We,tZ3 00
12K"454
DAn ACQ.
OEM 000.;
-SUB CODES CH WO MW $Ws 003
,Cwd

IiP r, X 1 /0110 /0 113
e t e r. IY U
jlphorphr) ~-i a C v
kadiokhImlya, v. 7. no. 1, 1965. 111-113
170PIC TAGS i reactim
ethylboxylphosphwic saids tribt4tylphosphate, octane. heat of
ABqTXAC'T: The purposo )f this article was to study the isomolair serleo of, mono-?-
acid N2tWl and tribu-VrlphDsr~,ate (TPP) in water-saturated
q"I'jti'mq- measurewnt of the heats of mixing was ;Izr-,e in un adiabatic
I I .~ -cannot be used
-:-1-r witli vn inothermal 4acket. The !ieats f t 3'ne
Ao-erminat of the heaT o" !--F i j- I M-.LF.7 in(-' TBF because
t Im
hp,it of mact ion therv an hea f ~e-. 'f, 'Le I L ! h C. dl lul i,-;n of
~n %Adltim to this, a mignifi~_ait !,.e cater phase !a liberct~
~-r tlehvdriftion of the -otm:cnen-~-
Cmd 1/2

L 442S4-65
ACCESSION IM Apsoopool
ftvtnt in which tbo ratios of M213e to TEP am 1:1 and 2:1. Orig. arot.
=P 02J=64 ENCLt CO SUB CODE: Gc. OC
ix- Yt t v to() 7 OTHERi 024
Card 2/2

I.g017-63 VsM(x)/L1WP(t)/WP(b) XJP(c) JD
ACCESSION HR: AP5013499 M/0075/65/020/005/067/01b
S%3.70 5"'1
AUTHOR: Kleteftlk Yu. 0.1 Bykhowskays. t. A.
TITLE: Extraction of titanium uAing 2-othylboxylphosphoric acids
')~'Ihlodl, V. 20, no. 5, 1965, 567-573
$SOURCE: Zhurial analiticheakoy
~TOFIC TAGS: titanium, extracting agent, chemical analysis
APSTP,ArT- The purp"ce of this work was to develop a wre sensitiv,~ method for the
defer"ination of titanium, based an Its tbxtractLon using bcanzene solu'llonn of di-2-'
-ofhylhe, ".Ipho!3phoric acids. Titanium was reextracted in!o tho aquerxus Phase un-
jnF hydrogen peroxide and tributylphosphate 21multaneously. The mi)cttjT- of mono-
inl ii- -PthylheKylorthopho3phoric acids was produced by rracling 2-ethyLhexyl al-
: w i th phosphorus pentoxide follotmd by hydro Iva i -, of t h-~ ~ yr-iph,.%Pha~ 0 ,It
w -is 0) -wn thit mjno-2-ethylhexylphosphoric acid extr"'acts t ilanium ra;,idly 4nd with
n iz~, iint ribition coefficient froo sulfuric, hVdm-chloric suid nitric acid salu-
tions in a br"d range of concentrations of these acids. extr-act ing u-s ing dt
-2-ethyihexylphosphoric acid to less favorable. In the case of wmo-2-ethylhexyl-
Card 1/2

L 5W'--65
ACCESSION NP! APS013499
ph-nri,,? 7 ac I I a &.ngle reextractlon with hydrog"n ponox" dti In S F 4-2SOu Mec"".
A. tha aluskolts phaso. It wa5 found thAt mexlr4rtir~n fmm maflo-2-
acid Is also better than frc= acid.
--p ;.riposed extraction mo?hc-i f,~~r -vnrl ;,e-paratinr of
-r,,t :AT,; r -v ti-
hAr. 7 tableS.
T
Firtiko-khImichaskikh ostiov pk-"r4l~~Tki vinernl'nogo syr-ya
ria t Ut ar~ f "--~ 1: -h,-i -so
ing
4.1 p r Ia I aAN 3Z-~k
gm
7'-
Card

OSIFOVt O.A.1 VINKINp V,I.j KLETENIKO Tu.V,
(Vanual on d1pols moments] Spravochnik po dipolln7m zo-
mentam, Rostov-va-Donu# lzd-vo Rostovsko unly.,v 1961.
248 Pe rvIRA 17s10)

HAVEL* HOLICKTs J.
Contribution to the Als aim of liver abscess, Ceske gastroento
vP# 21 n0,0273-271 h 161. 1
I., Vnitrd oddeloni OMM Berotmo prime dro Vladislav Havel
Chirurgicke oddeleni OUIM Beroun. prim. dr. Jaroslay Holicky.
(LIVER AJOMS diag)

YUHLAKOVA, I,X.9 imabol insh.
Experlme with polyethylene pipe for carrying highly xineralized
water,, Vod, t san4 takh. no.5t26-28 W 163. NM 16W
(Pipe, Plastic) ()dneral watem-Transportation)

NUTFmff I Josef 0 ins.
Technical standardization in cattle breading. Norm&Uzace 11
no.9t275477 8 163.
1, Hinisterstyo sewdelstyip loonibo a yodniho hospodars.tvil
odbor tachnicksho rosvoje.

mndsbv *mstr-few bw oWt MIA Wgados In
BorAts 8"1n ulwas Aotes tnd 7 nool2sllO-U3 a 162, (KIRA 26s2)
1. Dov*Ukiy oo"tl*"dwgo khoqWtva,
(Dowto hwi&--Coal sines and
Malls

XLMIIIj A.G.; 141MIALISKITO S.Z.; WISEW),, A.M.
Effloient means for determirdng the potentials of improvement
in mine operations* Ugoll Mcro noo6slO-22 Je 161,
(KIRA Ut7)
L, Donstskiy naucbno-Inplodovatol'skiy ugollmyy institut.
.(Coal mines and mining-labor productivity)

KIATKINt A.G.
Make anUable to &U Masine miners the vork upmyio=w
of the lagawk simors, Ugolt Mw, 6 no.6:25-26 jo 162 '
(;;;A 15t7)
1* Zamostitelf nachal fnika -a+AoIA tru& L sarabotnoy platy
Donotakogo saymrkhou.
(cma aims MA alang)

DUBOMWVp V*Ae, germyy lnsh* I XLZTXIN, A.0.9 Cormy insh,
Rapid mining of divelopment vorkings In the nbes of Doustak
leonudo Realone 'Utoll Mm. 6 no.W4.6 9 162. (MIRA 15s12)
1. Donetakiy sovet narodnogo khosyuyitva,
(Donets Basin-4041 mines and Xining)

That In how v* work with children. Zhil.-too. khos. 8 no.Utl4-16
(NZU nt22)
198ok"tarl torgaMsatell domupravlonlys No,053 C. Xiy*T&.

Operational safety mA durability appraisal of agricultural
machiness Amaele &Via sootsh 17 zoW52-160 I-D'63,

'-KL9VJA*-UJ6
Chmoteristico of veptation on the rigbt shore of TsImilyawk
Resemir as Interpreted from aerial photogmphso Trudy Lab
4417 t, 10119%4m 160, (MIRA 2,01i
(Tsimlyawk loservoir region-PbAMography)
(rhatographic Interpretation)

orc%~.Sjh YEFIMOV,, prnf.t rcd.; !k0l:~.COVA,
David Vlkt__
ren*
(Problems In analytic pometry) SWmIk zadech po analiti-
chaskoi geomtril. 14ovkvs* led-vo "Vauka," 1964. 254 p.
180)

ANNEKWVA, V.Z.I_,IJCMS A E.
Using Iran ore as a kind of leaning addition in the caking of
coal. Trudy V1 no.20:237-143 '163.
(HIPA is: 2)

Materials for the study of hematostoo parasites In rodents In
Sastern Siberia, Report N*92* Isve 1rk egoeprot ivochum. toot* 9s
91-95 151 (MIJU 10:22)
(BLOW-4PARAMM)
(SIMUo XA&MV-DISRAUS AND FW3)

Materials for the stWy of bowtosoto parasites In rodents in
Xestarn Siberia. Report Noo3o Isw, 1rkgos*protivocbumAnst. 91
96-99 1514 (MIRA IWO
(BUXRU,, 2A KWLII--ROMYT IA--D IMAM AND PISTS)

EMS. V.I.j. IMMUMS11Y. T.?.,. VDISSAIK. H.bo: lUDMTA. L.Ss;
'-~~IXOTA. N.V.; SNVJOTA. 141.
Susooptibility of tarbscons srA beressan susliks to e2porimentol
plaps. Tossl dokl.kanf.Irk.goo.asuah.-tool.protivochux.inst. no.
1Z15-17 6510 (MMA 11:3)
(ROMTU--DISZASZS AID PUTS) (PIAM)
NCR
ON
~
9

7 F
XWS. 2.1.1 ]COMMIX, R.S.; MOROV, G.P.
Jkporisental date on the use of compound vaccine to control bmaellosts.
Test I doklo konf* Irk* gos#rAuch#-1ssl.protivoohum,, insto ooo2t
19-20 '57, 1113)
(BRUCRUDOIS)

X. 1. KOIAVIX, R.S.: IWAMA, Ye.Ps; YTBOkOfo O.P.: SHTWSs gel,
Axperimental 4sts on corpound imunization with living maine$.
Ton, i doklakonf, Irkgoo.asuch.-to olprot ivoc hum olus t. noo2t2l-22
157. (UCOIM I (MIRA 1113)

I.I. XOIMNU* 2-8-.1 EWHIBSIAYSIff. V.Po; SMIRNOTA, L.A,; XWIMWAI
OLIZOVA, N.Y.
Uporiments2 plague laterbagons and Oversoonn suslikso To2oi dok2*
konfe Irksgooovmwbo-lssltprotirooh=o last. no.2%23-24 157o
(PUGUS) (91U 12:3)
(W U--DISXASXS A9D PMS)

I.P.1 KWMZ, 1*3*1 KOINOTA, Z#S,j
CLIVYA# V~T#j MWWA# L~A,
Basseptibillty of Ilborlas varmets aind Ing-talled mwUkn
to ozWrianially tufted pUgm, hmsIrkagovessimbs-4sel,
Prot IT00bun. last. Ih3-48 157.t~l (WA 23M
-DI Bugs)

ye
'131-jahnnn nrv-1 Aninal S
P'.'ripheral NorvMS System
580 8m9
bbe Jourl tht Zhur Didloo so Igo 19
Lu%orr I Klebdo 1, To$ x0lowaiks Ale
Inat s Irkutsk Scientific Hosomch Anti-.3arw Institute of
Sil%rla awl tho J"Pr East
Title s On the PmUsA of 'Investlestion of tho Vopstativo
Oar4ia in Oulwo Pies Infected with tbo ilarm
Oric, rubt W, Irkutakoe In-to Siburi t
Dolln Vosts.� i957ja4s 82-mW
;,t-3tracts Move puinon pies wor* infected with P virdent,
strtiin of tho pathomm of plagw (Nos 92) 1 cno
part of tho -atitswas abdtanoously rocoivod unti-
plarjo serums or luminrl ims given prior to the
in1botion, Tho superior corViCO19 the nottoso mylp
Card 1/2
USSR / Hiorobi0logy. Human and Animal Pathogons,
Pastourollao.
Abs Zour: Rof Zhur-Biole, NO 20 19590 5598.
Author i
.41. Kolesnik, R. S.
Vott LS
Inst I rKutslc Sol.Ros. Antiplague Instituto of
31boris and Tho Far East.
Titlo Exporimontal and Horphological Data on tho
IffaOts of Divalant, Living Plaguo.Vaccino Upon
tho Organism.
Orig Pub: Izv. Irkutskovo n.-i. protovoohuan. in-ta
Sibiri i Delln. Vogt., 1957, 14, 188-206.
Abstract: No abstract.
Card 1/1
49

OWE .4~
1"Irlmostal and merphologloal data on the effect on US 'boo
of Uvaled live plaae vualso, hv.I*.CoI.uaVOb.-lIIl.pr*tl-
Test=, last * 251137-142 157, (KM 1397)
(TA001138) (FXAGUN)

EM3 A. 1. XMISM, I.$.
1kralessuess of UvalerA llv* placum nocluo from strains 17 and
iff lo gulma pies, hm, last,
l5tl43-148 157. (KIRA 1317)
(TAOCIRATION) (PIAOUN)

ILI"# met*
oustrook of Inureds, In Ilsbamdla* metriat, ltv,l*,gos,
1511854 057* oalA 13 t?)
(11 1 m SIMICT-4MAMU")

IrL
Mam# Role
- - - - - - - - - - - - - - - - -
fterivedal pusumocoopal I&fUmm&timk of the Ings in vMte
Sias. 25421-W
(NDA 13:7)