SCIENTIFIC ABSTRACT LYULICHEV, A.N. - LYULYAYEV, V.K.

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SCIENTIFIC ABSTRACT
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AUTHORS, 7 Lyuli@-hev A, N. L,-,, -. r @ o -EV. 1 3 TITLE: The DeterminaT. on - f the V -I um,@ of Ref ra.: , cr i -s According to the Abscrption of I@Iamma Rad1--ar,---:r, 'p:--de _qhchen"r, obflyemnogo vesa -,gneupcrzqkh iLde3iy p@, j)-,,7 .- gamma-izlucheniya) PERIODICAL: Ogneupory '958 Nr PP 3 9 Y'd @USSR) ABSTRACT: The 1111110 @IabGra--d thiB math,@d ai,,! te-s'k--i it witti rm@fra--t@ rie8 of various dimen@i-c-s as weii fis wil@! ranges Of the volume weights -f g, : m' , The - c,, amr- weight can be det--@rzrir,.Pm f,r produ-, hav@rg twe, para: e3 surfaces. 1) Appaxatus ard me+,hcd of detp-rminaticr.@ The determratir.n of the volume weigh- i@i ta.-ied -.r. @he h.,-ira,J@r -f he at sorption of gamma rad;ati,-n paiisir,g thrlugh a si@ostat--, Th,@ apparatus has a ga-mm Boarre a-@ we,-! a,:@ a cluan-,- and prior to its u;.e 1-. 1,3 al..,brated by (F samples known density. The ---heme rf such an appara,,Aq i3 sh@@vn if; Fig 1. A Geiger Md-ler co,nter ;.Ge@gEr- Yit-y-- -r -ountqr@ @f Card 1/4 the type AIM, 4 as we' t -as a c -.mp., ter he t YPe PS 64 ax@@ 30VP3- -588-7 ?/'4 The Determinatioa of the Volume Weight of Refra--tori@-:5 A-cording to th@- Absorption of Gamma Radiation used. 2) The deperden,,,e I-f the a----ura@y cf deteiminaTi-r- --n the energy of the gamma radiatl,;n source: In the @.ase ::f a con siderable thickness of the samp1ca tc b-a 1&vestigated the error of determination 16 dependznT on the ina,'*cura-y c,f ,h@ calculation ln 1 /T where I denotes thq -adiati,-ri inter sity. After this th6 -al@ulatlon is --a.Tr@ed out in d@--*a-11- 3) The inflaen -@ c@f oth-@r fa;-t(---t3 or., the a.@----a-y of det@-r mination: Table f givev the reisa.Ts of th-@ m-z-a6uiaments as dependent on the position of the @ampla and in Fig 2 Thc9e for refractori@q @f diff,@@rer(@ chem'.cal composit-,or are shown@ The experimentaL 7al,@P--3 cbtained prc-s the appli-@:at'-' lity of *,his meth,@4@, 4) The arrangement of the graphical oalibraticr. plar. as sh-*w-n in Fig 3. It was made or IV-he ba.ais of meaaurements of -resorb irgsamples of diffairent @hi.-kaess, 5) The checking c-f the matriod rith varicus obje-..ts and th': determInatior. @,f the a.--uracy (@f the rvFsilts, Card 2/4 Refractories of different dimension,E@ and thickness as w&'' 3uvl'31 58-7-7/'ll The Determination of the Volume Weight of Refractoziea A,@cording t- the Absorption of Gamma Radiati3n as in different positions were checked as to their volume weight. The results of these investif7r,,ions are given in Table 2 and they show that the deviations between the valu@s obtained according to the gamma radiation and those obtaired by the hydx,,statl@- method remain within the framework set up by GOST specifications. Conclusions: 1) The possibility of the determination of the volume weigh' by means cf the absorption of gamma radiation for refracto ries of a volume weight of from 0,75 to 3,35 9/om3 and of dimensions of from 65 - -18o mm was found. 2) The optimum geometric parameters of the apparatus were determined. 3) The method was checksd on products of different kinds and it was found that it corresponds to the GOST specifications. Thera are 3 figures, 2 tables., and 7 references, 6 of which are Soviet. Card 3/4 SOV/1 3 1-58-7-7/14 The Determination of the Volume Weight of Refractories According to the Absorption of Gamma Radiation ASSOCIATION: Vsesoy-uzriyy nauchri, issledovatellskiy institut ogneuporov (All-Union Scientifi,- Research Institute for Refra-stories) 1. Cerami Gamma i-adjat.*1or,--AbsorpL110T1 3 Geiger ccunters --Applicaz,ions Ceramlo matef@ial--MierovoLumetrlc Card 4/4 AUTHORS: Kraftmakher, Ya. A., Lyulichev, A. N., SOV/32-24-7-51/65 Shaktid n, D. M. TITLE: The Investigation of,the Operation of Laboratory Mixers by Means of Magnetic Indicators (Izucheniye raboty laboratornykh smesi- teley pri pomoshchi magnitnykh indikatorov) PERIODICAL: Zavodskaya Laboratoriya, 1958, Vol. 24, Nr 7, pp. 893 - 895 (USSR) ABSTRACT: The apparatus constructed is based On the measurement of the magnetic conductivity of the samples in the low-frequency magnetic field. The instrument measuring the ma,',-netic susceptibility was constructed by Ya.A.Kraftmakher. The measuring unit is an H-shaped armature on which three induction coils are arranged. The sample to be investigated is attached in such a way to the measuring unit that the magnetic flux passes through it; thus the inductive voltage in one of the coils is changed and the voltage of the measuring unit serves as a standard for the magnetic susceptibility of the sample. From the schematic re- presentation of the apparatus given may be seen that a low- frequency generator, the measuring unit, a low- frequency am- Card 1 /2 plifier, a detector, a lamp voltmeter as well as a visual in- The Investigation of the Operation of Laboratory SOV/32-24-7-5 1/65 Mixers by Means of Magnetic Indicators dicator and a supply pack are assembled. The instrument has six measuring ranges of from jo-4 to jo-1 units of magnetic susceptibility in the CGSM system: the degree of mixing is de- termined by the measuring of the concentration of the magnetic powder in the samples taken from different places. The con- centration of the magnetic powder is measured according to the magnetic susceptibility of the specimens pressed from the samples to be investigated. Granular sizes of quartzite of up to 0,5mm were used in the experiments; iron powder of 2,5% Ca(OH)21 0,5% sulfite alcohol vinasse, 8% water and 1,5% iron powder served as indicator. The results obtained were ob- tained from the mean value of the magnetic susceptibility and an equation; a diagram is given. There are 3 figures, ASSOCIATION: Vsesoyuznyy nauchno-issledovatellskiy institut ogneuporov (All-Union Scientific Research Institute For Refractories) Card 2/2 SOV/32-24 -1 C- 92,'-0 AUTHORS: Lyulichev, A. N. Ch,,zprinin, F. I., K--@-,ralenk:@, S. TITLE: An Apparatus for Determining the Thermal Expansion Coeff,.cie-.- of Refractor'es (Prilor d1ya opredeleniya koeffits.'yen-,a ter-.@- cheskogo rasshireniya ognpupo rriykh materialov) PERIODICAL: Zavodskaya Laboratoriya, 19".8 , Vol 24, Nr 10, pF 1282-'28@ OSTRACT: In a number of cases the 1r.,,,,& sti6ations of me-chfinical ,,I,! properties of refractories MU 3t be carried cut at temprr-i- tures (about 2000c). In vJt'-w of the fact that differential methods use the application o f standards for ieterm,,ning th ermal expansion coefficient a, and that on, th--s occasion ilq- an addit4onai pressure on the sample r-iy ocaur, t*-e @r@sent cons true. ti or. of t@e appar,-i@,.@s is based or ar'absol,,.@te method. From the dipgray. and thf@, J@-s2 ription given it ma,-- seen ,at th a horizon *tal microscope of e type MG -1 (prov4le] 'enqeS to 4norp dispersion I - qSp the focal distancc!) Is comparator.. The measurem@@ntq were carried out at a temperat,-1- of 85C-49000 within ranges of 10CO each. The maximum absolut,: error of the method iescri4bed is , 0,07@o. The values of the Card 112 thermal expans: .i:)n coeM -4 ent of MgO calculated acccrdine @2 ti-- 0 2 / '7 Q ,07 lz 2-24- Co,ffic -ent Of I'Pf ,an5 r,,g t,,.,, Thermal cr kn kpparatus f in,3d agree vith thos' er; mer.,ta,p- nts al data obt of the exp experiment 'Ons arp 2 f ig',Ires The deviat'@ 'ILef ',). 04b. There are no* More than Ors - c,, 4s Soviet the curve referp C;ard 2/2 !D-@ 6.20 29997 5/170/61/004,/012,, 007/0 11 B104/Bl 38 -H, R3. Vis',nevs;,J@ I. I. it y, LyulJchev, A. N., Sukharevs.-@Iy, B. Ya- L E Liber.'-lDn -)f i7qjes fr-j:n vacu,,Ln-heated refrac--@r@: cera@ics @i z @hesk 4 Vzh-,,irnal, v. 4, no. 12, --7 X, - -hp a-@*.h:)rs tes-.ed the @-oruridum and V 'Ki and K no,is 1. 2 @ 21 Rf" @ind 19A (7G :ind VL) , and aluminosilicate refractDres AA and A 1 2 (AL1 and AL 2). The amount -3C gas liberated was estimated from press--ire ,iariations in the experimental apparatus, which was evacuated pri@jr tz) the exder 'the pressure variations were measured with AM -2 "Li@-2,' and )IT-2 (LT-2) pressure gauges and with a 90T -1 (VIT-1) vacuum gau6e, 21-P Test chamber was a steel tube 50 mm in diameter and 1@00 mm lGng (capacity @ibout 3 liters). Eight cylindrical specimens -56 am iri iiameter and 3@- mm 3 were placed in ter of the heating zone. To eliminate impuri- !on, the cen ties, the specimens were previously annealed in air at 10000C f,,r )ne ha, i r Before starting the tests the chamber w 4 th specimens in it. was @Vac,,I-Itej to ab'Jut 5.10-5 mm Hg. The speciziens were heated a 29997. S/170/61 _2 1, 22 L,-berati-m of gases from vacuumi-heated B104/B148 rate or 0/min. As can be seen from Fig. 1, gas liberat!-Dn peaks a,@--,ear @Ot.'--OOC -and 700-80()()C. a I It is shjwn that the first maximur... is re- iate@ t,-) ies,)rption of -asi@!g, and thesecand to reduction ol- oxides. Finally, th- quality of the varit)us refract)rips is estiimated fr,-)r-. @.he The @,-ec mers u n t -,t s -_@s lj,@@ ru were supplied b-, A. 1. R3yzen. There are 2 fL@7ares, 2 tables, an@ references: 2 Soviet and ' n,,n- scvlet- A .33",, 1'@ T.-@@j:Institut jg@neuporov, Kharlkov (Institute of Refractory 07aterials . Khar'kov@ 3 BM - ITTED: February 10, 1961 Te::i,,eralure 3r time' de-)endence of inf'ltrat4on @A o. I Im in (2) K (3')Br(VG); (4)13)1 (VL); (,)A-@, 'AL.'.. t.,.) la: 2 AJ1_ (AL ); (7) ilie run sys@em (w;tbjut s:@ecimens). 2 1b: @1 ') first test; @tfter 2-hours in air; ift,@r Fi, --'.'ter 2@lj hr in al, 1 roasting at 1000OC; (@7) Ldle r_@n a r d 2/0 ACC NRI AP6007917 UR/0125/66/000/002/0010/0014 AUTHOR: Verkin, B. I.; Kravchenko, Ye. L.; Lyulichev, A. ff. ORG: Physicotechnical Institute of Low Temperatures, AN.UkrSSR (FizLko-tekhnicheskiy instLtut nizkikh temp;ratur AN 1IS-SSR) TITLE: Interlocking of alumintum YLth copper in high vacuum Y. SOURCE: kvtcmatichaskaya avarka, no. 2, 1966, 10-14 TOPIC TAGS: metal bonding, cold welding, gas adsorption, compressive stress hi h vacuum ), tt" -T M - I.L Y-ej@A-4@ ABSTRACT: This investigation was intended to determine the effect of the purit) of surface an adhesion Ibetween metals (Al ani Cu in high vacuum -- 10-9-10-5mm Hg), with the required compressive stress used as the criterion of adhesion. A specially developed experimental setup was used for this purpose (Fig. 1). Mounted within the chamber are: working assembly 1-5, device for cleaning'the surface of specimens 6-12, and manometric j1pamps TZ-2 A IH-12 .@Pe working assembly is designed to compress the specimens togither. it is-4,611 pri-s-entJ by two identical inserts, each consisting of punch 1, rod 2, guide bush 3 and sylphon 4. Specimen 5 is attached directly to the punch. The load is applied via rods 2 by means of a 'Brinell press. To remove oxide films from the surface directly within the chamber, use Is made of a cleaning aseembl: 1--card- 1/3 UDC: 621.792.8 c i L 2 27-66 ACC p., Ip@6007917 -Toward N 5 PUMP f setup: uuci;palct 0the hydr,096U PUMP caudettstug 1. Diagram o ,,trogen-trapsi 11 wgter trap; 9 213 card ACC NR'AP6007917 consisting of scraper 6, sylphon 7, rod 9, pivot 10 and washer 11. Peepholes 8, 12 make it possible to observe cleaning. The setup is evacuated by means of a N-5 dif- fusion pump. Traps I-III are designed to assure reliable freeze-out of the pump's oil vapors as well as of the decomposition products. Findings: even insignificant contamination 0f @fl Cnd Cu surfaces increases the required.com ressive stress by one order of magnitud Ieaned surface of Al in a vacuum of 1 17 MM Hg is contaminated by adsorbed Sasesk he degree of contamination is proportional to the product of pres sure and exposure time, i.e. to the amount of gas adsorbed at the surface from the chamber's interior; mechanical cleaning of the surface is naturally ineffective in such cases. Thus more effective methods of surface treatment of specimens are needed before the aspects of adhesion between metals in high vacuum can be properly investi- gated. It can be established, however, that the compressive stress is not a physical characteristic of thqkadhesive properties of pure surfaces, since it is a function of surface roughnessV'rhus it is theoretically possible that atomically smooth and pure surfaces can mutually interlock without requiring mechanical compression: Orig. art. has: 6 figures. SUB CODE: @ 11, 13, 20/ SM DATE: 09Sep65/ ORIG REF: 006/ OT11 REF: 005 vappum diffusion bondin ig b2jnding of dissimilar metals LYULIGHEVA, N. N. "Application of the Methods of Sratial Metallography in Exposing the Influence of Phase Separation on the Mechanical Properties of Carbon Steel." Cand Tech Sci, Khartkov Polytechnic Inst imeni V. I. Lenin, Min Higher Education USSR, Kharlkov, 1954. (KL, No 1, Jan 55) Survey of Scientific and Technical Dissertations Defended at USSR Higher Educational Institutions (12) SO: Sm. No. 556, 24 Jun 55 AUTHOR. Lr,.;-! 1- -he -,-a, N, N, 126-2-119/30 TITLE. Volume --Laiv3-s 5-- 11 1' -1 e T La s e d:.-, 1 4 11 -L eMpp J. E _ring of St,@!. (Ob"yemiye izmenerLya kapbidnoy fazy rri ctpuske a! e MiIODI@@-, "Fizl@a Metall@v i Metallovedeui.@e'l (Physi--s of Metals and 1957, P-1,-'319-330, (USSR), @A.BSTRILCT: In investigatirg the st-racture of temj' ,ered steel b7 means of an elect-n3n mic-zos-:cPe it was found that the quantity of the detected carbide phase is considerably larger tLan it should be on the basis of' the :.ontents of' carbon in accord- ance with. the formula Fe C (1-3),The respective alltilCT-5 repan,@-4 9 t@@ tLe screening of tLe ferrite attribute this disc, by tile protruding -:arbide particles and other inadequa@-ies of the method of pL6tcgraph-ing, by means of a-r, electroni,:, microscope; however, their assumptions Lave not been con,- firmed by experiment or by calo-ulation. On the otLer Land a number of experiments are described in literature, on tLe basis of which th-e respective authors c.-onclude that low temperature carbide contain-5 more iron than 4-.t should on Card 1/5 the basis of tLe stechiometric ratio in accordance with the formula Fe3C . The author of tLis paper investigated by methods of 3z-dimensional metallograpLy, using am opticad Volume Changes Of the carbide p@iase during tempering of steel. (Cont. ) 1?-6-2-19/ 30 microscope and an electron microscope, the changes in the volume of the carbide pLase and steels with a heterogeneous structure. The investigations were effected on carbon, silicon and manganese steels in the tempering range 450 to 700 C and relations were establislaed which govern tLe change in the volume of the carbide p@iase as a function of the temperature and the duration of tiae tempering. An assumption was expressed on the structure of the carbide phase during low temperature tempering. T@ie specimens were of the steels 25, Y7, Y10, containingg respectively 0.31, 0.68 land 1.06% C and also silicon steel containing 1.65% Si Of and 0.6p C and a manganese steel containing 1.7% Mn and 0.41% C. For obtaining structures with various degrees of dispersion, the sppoimens were hardened and then tempered at temperatures between 450 and 700 C, with holding times of between 2 and 50 Lou-rs at. the given temperatures. The cuts were produced from heat treated specimens, photographed with a magnification of 1200 in an optical microscope and Card 2/ 5 with a magnification of 4500 in an electron Microscope (using the method of lacquer imprints in the latter case). The technique and the results are described in some detail. Volume chaiv:,es of tLe --arbide P@iase durii t em @6 periz@g of steel. (Cont.) 126-2-19/30 .L Graph FiF-.3 S@aows the influence of the tempering temperature on the volume --hazges of the carbide phase in the case 3f 10 twur holding time; in Fig.4 the influence of the carbon content on the volume of the carbide phase is plotted Mailst in Fig@5 tLe volume changes in the carbide phase ir, the case of tempering witt various holding durations are plotted. Graph Fig.7 shows the influence of the silicoLL and manganese on the volume of the carbide phase in the case of 25 hour tempering for several steels and graph Fig.8 shows the inf-',uence of the tempering temperature on the dimens- ions of the carbide particles in carbcn steels. it is shown that the observed volume of the carbide phase at low tempering temperatures is considerably in excess of the theoretical value and that the observed phenomenon cannot be explained by inadequacies of the experimental method. It was established that on increasing the temperature and the duration of tempering the volume of the carbide phase decreases re8-ularly, remaining all the time larger ttLan the Card 3/ 5 calculated values. Only at temperatures above '050 C and durations of 25 to 50 hours will the volume of the carbide phase correspond approximately to the theoretical value (in Volume changes of the carbide phase during tempering of steel. (Cont'.) 126-2-19/30 accordance with the formula Fe C) It is shown that thee carbide particles observed in @he'microscope contain less carbon than cementite; low temperature carbide consists either of individual submicroscopic blocks of cementite or of a solid e-solution and appears to be a solid solution of cementite and of the a-phase. On increasin6 the temperature and duration of tempering the carbon content in the carbide increases. The generally accepted conception that with in- creasing tempering temperature the size of the carbide par- ticles increases continuously has not been confiremd. It was established that with increasing tempering temperature, between 200 and 500 C., the size of the observed carbide par- ticles decreases whilst on increasing the tempering tempera- ture between 500 and 700 C the size of the carbide particles increases. It was establisbLed that,compared with carbon steel, the carbide-forming element (manganese) increases Card 4/ 5 and the non-carbide forming element (Silicon) reduces the observed volume of the carbide phase. There are 8 figures, 1 table and 14 referencest of w1aich. 11 are Slavic. Volume changes of the carbide phase during tempering of steel, (Cont.) 126-2-19/30 SUBMITTED: December 13, 1955 and after revision July 6, 1956. &LSSOCIATION:Khaxkov Aviation Institute (Khar1kovskiy Aviatsionnyy Institut). AVAILABLE: card 5/ 5 18(2) AUTHORS: Lyulic,,.eva N. N. , 1"isar eva, '1. 7. TITLE: The Mecnanical, 11ronerties of Cold Hardened C",romium-nickel- austenite 3teel of the T@,, j,,.e 18-0 at Low Tem-,,eratures (Mekhanicheskiye svoystva nagarto vannykh khro::.Gn'.--.e!evYkh austenitnykh staley ti-Ia 18-8 ,;ri nizkir:!@ te--@,erat@zrakh) PERIODICAL: Nauchnyye doklady vyss@iey al.koly. Mletallur@iiya, I.P; I Nr 2, pp 217-220 TISSR) ABSTRACT: The mechanical --onertie3 -f 3tainless austenite steels of &'Li LR:z23`TT_ -,.re investi@,,ated at te,.-,-,era- the type 11,1 7 e tures of +20 ano -lq5' @ifter rollin,, at rooz: te%,' r-,,@rature (Fig 1). The dependence of' the relative extens-on of the austenite steel of the type 18--8 on differe.,it temperatures is given in fi,-@ure 2. -he hi,,her pla3ticity of' the austenite .,3teels determined at 183 0after rollin,, at +20 0 @s caused by the occiirrence of cubic face-.centered lattice3. The mechanical properties of the metals and alloys after the treatment under pressure at room te.liperature are summarized in the table. '"he tranoformation of rnnrtens@te into au.9tenite steel iuring the deformation proceno at 1@;w te::;ioerature increa!)- Card 1/2 es the stren,;th of the alloyo. A ;reviOL]d The Mechanical Proz)ert es of -'oil I -e Steel of the Type 1@;-8 at Low T6..iperat@irea is expedient fur tho uu(@ of auste:,ite striel f-,r te!:1;-,era- turea since the flow li::iit Is thue inc,veas,@l rolu- tion of the plasticity. -'here are 2 1 3 reference - 4 of Soviet ASSOCTATION: Khar'kovskiy aviitsionnyy in-:tit,,;'4 (V-li;,r'kov Inutitute of Aviation) SUBMITTED: May 28, 1,J59 Card 212 -1 .2 J- -T @J_ "Y p I q.L 11/01 P..:) Aq 'T_H Ir.42 :41 MI J. P-7 s r I H Aq Z.'j..j '4' @'.u VTP ... . Ip Aq -0. Aq p.. TV, P-3 WI-T-A 0- V;p Aq 71 V Aq OTTV p!, Jigg T.. .v 4q T '.;'3;2.; 1422TV 'IT 1*11"3 '*Plo P- q% .0. ...,d:g Aq v .7--W I.. 'TV ... j -3 A q 1,1,,K J* -1111111114 I'll J* T*P@. .3 J. wa -14 j-n ,jqt qMq-.2 P- '4191 '44 '6C61 A-H .1 I.LIVUI,gv jo7-zql 44 1, N -6 61 umAq.q,. 41,14.!AA . ...... J..3 rill I A IVoj"v DeO/otQ/w/oo0/66/z*'(/v SOV/129-5"--4-4/17 AUTHORS: h (Candidate of Technical Sciences) and 4'iLs-'alr@ea W(Engineer) v 'V. TITLE: Influence of Rolling at Low Temperatures on the Mechanical Properties of Austenitic Steels (Vliyaniye prokatki pri nizkikhtemperaturakh na mekhanicheskiye svoystva austenitnykh staley) PERIODICAL: Metallovedeniye i Termiclaeskaya Obrabo.ka Metalloi, 1959, Nr 4, pp 19 - 22 + 1 plate (USSR) ABSTRACT: Stainless austenitic 18-8 steels are being used at room temperature and at elevated temperatures, as well as temperatures down to -1960C, for instance in cooling equipment for manufacturing liquid gases. The purpose of the work described in this paper was to investigate the influence of the redu--tion on the mechanical properties of austenitic steels. The deformation as well as the testing of the mechanical properties was effected at temperatures +1000, +200 and -1830C. The s onsisted of 1.2 mm thick sheetsof the steels lp@clmens c 18N9T and lKhl8N9. The blanks were first quenched from 10500C in water and following that they were rolled at -1830, +200 and +1000C with reductions of 15 - 60%. Card 1/3 The results of tensile tests at +200 and -1830C are SOV/129-59-)+-4/17 Influence of Rolling at Low Temperatures -,n the Mechanical Properties of Austenitic Steels graphed in Fig 1 for the steel lEnl6NqT, and in Fig 2 the influence is graphed of the reduction at 20CCon the ductility for specimens tested at -1830 and +1000C respectively. The authors ar-rive at- the following conclusions: 1) Rolling in the cold state of au3tenitic Steels for the purpose of improving the strength is more effective if it is carried out at sub-zero temperatures; in that case the strength characteristics will be 20 - 3)0% higher and the ductility will be the same, as in the case of ordinary rolling. 2) At low temperat-res, austenitic steel3 have good plasti:@ pr,_@pertl_es (@, ana 4; p irrespective of the degree cf prela,minary wl-.rk har--aning, at above freezing-point temperatures,, 3) For work hardening of austenitic steel c.-,,mpone.,ts oi)e-ating -at below freezing-point temperatures it, 1'3 ad-.--'sable to cold-work them at above freeZ.J__-1---1,i1-_Jnt t,@-mperat,.@res-, such I P4 t cold-working will bring abou' an reduction in the plastJc prcper ias -f n@ateriai at Card 2/3 low temperatures. 4) The effe_-,'Lveness @Df shaping by pressure of austenitic Steels at low ter,-.@orat,.@res is the SOV1129- 59-@@-'-t-/17 Influence of Rolling at Low Temperatures on the Mec:iA_n_-'3al Properties of Austenitic Steels same irrespective of whet@,er t@ie material has or has not been cold-worked before. 5) Plastic de."orriation a", IOW temperatures is accompanied by formation of iparten-;ite along three planes of an octalaodron. Formation of martensite at room tempera'@ure during the prrcess @f plastic deformation is observed predominantly in a S_Jn'-'le crystallographic direction. There are 3 figures and 3 references, of whi,@n 2 are Soviet and 1 English. @l`ard 3/3 18(3) 18(7) 24(6) AU`i;HO@: Lyulicheva, 11'. TITLE; Determination of Mechanical Properties of Steel by Quantitative Metallographic Methods (OT)redeleniye mekhanicheskikh svoystv suali metodami kolichest-e=oy metalloi-rrafii) PERIODICAL: Fizika Metaliov i Metallovedeniye, 195c,', Vol 7, i'r pp 265-273 (USSR) A-BSTRACT: The aim of the investi.ation was @o find -,,he relation-ship between the mechanical properties of steel in tension and the quantitative an' dimensional caaracteri3tics of their grain structures, as ,,iell as uo collecc experi- mental data as uo quantitative metallo_r@aphy. The carbon steels 25, 35, U79 U8 and U10 carIroon contents of 0.31, 0.38, 0.68, 0.78 and 1.06%, resrec-cively, were, investi ated. In order @o su-udy the influence o carbide formiii'o'- and non-carbide formii;@ ele,-ents o-- the quan@iUative and diLiensional structure characLericu.-LcEl uhe steels 45G2 (0.41% C and 1.Wo Mn) and 60S2 (O.@ and 1.65% Si) were used. Granular structures of v,arious Card 1/6 dispersions were obtained by chan;in:' the te:,iperin@: ,'OV/126-7-2-1E/z,@ Determination of Mechanical Properties of Steel by @uantitative Metallographic Methods temperature from 450 to 700 0C and soaking from 2 - 50 hou-rs The study of microstructure was carried out from photo6raphs taken through optical ( X1200) and electron ( X4500) m croscopes. The number of carbide particles n per 1 mm@ of microsection was determined by direct count of t@ie photomicrograph. The volume of ferrite Vf can be calculated accondinF- to Moroz's formula (Ref 1): 1 - c Vf 6.68 (1) 3/2 n where c jc@ ihe carbor. content of steel. The specific surface of separ--itior, of _7@3 and the specific spread of brain bouc.-Jaries ZP were calculated accordint@ to Salt,-,,,kc@r's formula (Ref 4): S 2m MM- 1 (2) I.ard 2/6 P (3) 'DuV/126-7-2-16/39 Determination of Mechanical Properties of Steel by @uanti-uative Metallographic blethods 2 where m is the avera6e number of intersections/mm Gf random secants. The mean, path throu:.-h ferrite waS calculated by Lyulicheva's equation (Ref 9): % V @ k L = @ 1 @ 00) (4) m ( where 2/m is the distance between the centres of carbide particles, and Vk is the volume of the carbide phase, as determined by A. A. Gla6olev's ac@@ura@-,e ruethod (Ref 4). The yield point was chosen as the fundamental mecLanical property associated with the structure, as it has the greatest practical si,@nificance. In Table 1 the tempering condition, a few limit-inj@ values of mechanical properties and fundamental results of calculations of structural dimenosions,are shown. In order to verify the limits of applicabilit,@ of conditions expressed by several authors (Refs 1-4, 7), graphs for the dependence of yield points on the corresponding characteristics of Card 3/6 structure (Figs 1-3) viere plotted. In order to derive @-@V/i 26-7-2- 16/ 79 Determination of Mechanical --Properties of Steel by -ua-n-titative Metallographic .'Aethods an equation for a straight line having the greatest correlation with the experimental results, mathematical statistics methods were used. The straight lines -plotted in the diagrams corresT@ond with the correlation equations (5) to (10) in Table 2. Fro @,@ 4Uhe graphs of Figs 1 to 3 and from Table it follows that no -ene-ral relationship between yield point and any 0 structural property, Vf, Es or L exllsts for all carbon steels. In FiC 1 the @p,,ndence of t'ne logarithir, of yield point on the logarith--r. of the free quanti-ly of ferrite, is shown: a - optical photomicrograpl@s, Eq (5); ZD b - electron photomicrographs, Eq (6); B - i-.!G-oz's correlation equation (1). la Fi@@,@' denendence of yield point on trie specific surface of T)@ias@2 separation is shown: a - optical photomicro@_-rraphs, Eq (7); b - electron Dhotomicro-raDhs, E-i (8). I-n F the dependence of yield points on tht@ ]-@@-'-arithm of zhe free path through ferrite shown: a - o;1-tizal p1--otumicrograpl',s, Eq (9); 6 - electron photomicro-rapns, Ea (1u). In Card 4/6 Fib- 4 the influence of temperin-, te,@rpera,,ure on the 7 -` /126 Determination of ilechanic@l Propert-les of Steel bY L - I 16uar-titative Metallographic Nlethods thickness of the delayed reaction layer is shown: 1 - 6OS2, 2 - 45G2, @ - carbon steels. IL Fij @, the dependence of the yield point @jnd of tlr@e true ultimate tensile stress on the reciprocal of ,-'te area of tl-e soft r)hase , is shown. From the above ex-Derij:ients, ,he uathor has arrived at the follo,;,@in- conclusions: 1. In the tempering temperature ran,.--.-e of 450-'/60 there exists a correlai.ion reiacionship betwc@,,n the quantitative structure charact-eristic !,.,ic! characteristic of steel. 2. An experimental foriiuia for z-,he de1.eY.:,inaLio-,-- of che yield point in -ianular structures is su %,hich @Jves a ._,ood correlation in a wide te",2perinE, ran@;-e, and applies to carbon steels con-, uainint@ from ancl to 1.06% C, as .-jell as -,@o u-@Iie allo.@ stet-1::- 6OS2. 3. A linear relationshiD exisus between tne true and overall ultimate tensile stress, on the one *iand, an"' the reciDro-cal of the specific area of t-e soft pha-le u-,n. ard 5/6 the other. @,G-V/126-7-2-16/39 Determination of Mechanical Properties of Steel by @ua_ntitatlve Metallographic Methods 4. The influence of silicon and manganese on the improvement of the mechanical properties of steels is asLociated with a chan-e in quantitative and dimensional characteristics of the structural-components, of the properties of the soft phase and of the nature of the phase boundary surface under the influence of hese elements. There are 6 fiLures, 2 tables and 18 references, 17 of which are Soviet, 1 ---'nglish. ASSOC IATIUT-@: IC@,ar'kov@:,iy aviai;sJLorL__y-r insti-.U@' (Khar"ov Insti-,,;ute of Avia,,ion) SURIIITTED: April 15, 1957 C ard 6/6 /JP S/148/60/000/002/004/oo8 AUTHORS,, N.V. TTTLE@ Corrosion Resistance of Austenite Steels After Pressure Work:Lng at Low Temperatures PERIODICAL, Izvestiya vysshikh uchebnykh zavedenly, Chernaya met&llurglya, 1@60, Nr 2, PP 78 - 8o In chrome-nIckel austenite Steels low-temperature deformation entails Intensified increase in strength due to marlensite transformation, It must be expected that the second phase, namely martensite, developing during low temperature deformation, will change corrosion properties of steel. This assumption was qhecked by speeded-up corrosion tesLs of lKh18Nq steel by a method recommended by [Ref 31, Loss in, weight of electropolished specimens was determined after 100-hour holding 'kn 3,6% HC1 dissolved in technical water, As a result the curve of N@-Ight. loss versus degree of compression at - 1830C" showed a maximum correspondIng to the loss in weight increased by a factor of 2 (Figure 2), After rolling at room temperature and high degree of compression, corrosion resls-'@an3e of 7ard 1/3 S/148/60/000/002/004/008 Corrosion Resistance of Austenite Steels After Pressure Working at Low Temperatures the steel was leas impaired and a ma@cimum on the curve ("weight loss versus degree of compression") was not observed, After rolling at low temperature X-ray examinations of the phase compositlon in austenite steels were carried out to deter-mine, to which amount of martensite corresponded tne maximum decrease of corrosion resistance. COMPar'-son of curves (Figures 2, 3) show a maximum weight loss in LKhl8N9 steel after oompriE@sslon by 15 -- 20%, which corresponded to about 50% martensite. If compression was increased u '1) to 40%, corrosion resistance improved and then became &1most equal to that of steel rolled at room temperature. Thus after rolling at. -1830C and 40% compression, the night loss was !4 9/m@ and after rolling at room tempera- ture it was 11 9/m . improved corrosion resistance in the presense of a martensite content of over 50% in steel rolled at low @temperaturss, proved that high-alloy martensite ens-ared sufficiently high corrosion resistance, The conclusion la drawn that in austenite steels with non-stable aaztenlte, Card 2/3 S/148/60/000/002/004/008 17orrosion Resistance of Auqt,:@nl@,e atel@ls After Pr@5su-.'@ Wcriking @ - To@-mperatures ' the pre-izure working at low temp9raturea, carried out to rais- .he- s@r-!rlgth, dit not considerably reduce their corrosion resistance, There are: 3 graphs and 4 references, 3 of which a-re Soviet and I English, ASSOCIATION4 Kharlkovskly avlatsion-ny-y InstItut (Khar'kov Aviat'lor inStItute SUBMITTED, November 21, 1958 e Card 3/3 S/185/60/005/004/020/021 D274/D306 Bubley. and Lyul. @ cheva, N. IN 'ITLE A simple cryostat for mctalLographic invcsLig;itiois i'Ll< iuD IGd, Ukr;iyiiis'kyy fizycllj-@iyy zhurnal, v. 5, no@ 4, 19bO, 570-577 very simple cryostat ,,,as desJLg,.ic6 and teste6 for tlie pur- V/ pose of stuc@ying and photographing :,.ietallographic ;)oLisn at Low t empe r at u re s 'Zile cryostat is a 11rind of D@war cyL'i-ndrical flask ,,,,ith -11-it transoarent botto-, t`trough which tnie o-)servations were car-i-o , __ , ,) u t 10 Gimensloas of LiLe cryostat were as folLows: 'ReLght 100 rxa, outer (.liarneter 60 ram, in;.er diameter 40 mnii, thickness of doul-Ae-walled bottom 7 ;,-in, The more even in t[iick-tess the bottom, t;ie I'otter the picture obtainedl. @y using a Lozins'kyy microscope times, twhereas ,i *L @r-focusing objective, the -,,,agnification is 400 @@n ord-inary objective mae-J-dfies 20(7) Limos. But in the latter case tiie thick-ness of tiie cryostat bottom has to be limited to maximum S1185 /'bO/005/004/020/021 s@ D274/D306 @nmLc crvostat 7 r@n ior studying str(lxtures at low tempera-lIxes, the polLshed inv,-Itigati-on, was put- ut the oottom of tke rryostat, ii-te cryostat itsuLlf pl,!(:c_l u-ider a -.(,taUfLcr()scODc, LiqLlid eL:c,) was Poured inLo Lite cryostat. :v - '1'@c n t o'