SCIENTIFIC ABSTRACT FR:MAJER, V. TO:MAJER, J.

• Document Type: CREST
• Collection: Scientific Abstracts
• Document Number (FOIA) /ESDN (CREST): CIA-RDP86-00513R001031400027-6
• Release Decision: RIF
• Original Classification: U
• Document Page Count: 99
• Document Creation Date: November 2, 2016
• Sequence Number: 27
• Publication Date: December 31, 1967
• Content Type: SCIENTIFIC ABSTR

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~~roceedi~ngs (Cont. ) C;l1CII/`~~+33
Tockstein, A. Derivation of the Extended Equation of
the Polarographic Curve 721
[Russian Translation] 725
[German Tranela.tion] --'''~'`'
~~~
Vogel, J. A New Apparatus for Oseillographic Polarography 731
[Russian Translation] 736
[German Translation] 739
~/ /
Riha, J. Polarographic Derivative Curves 743
[Russian Translation] 746
[aermat~ Translation] 748
Nesvadba, 0. Artificial Regulation of the Drop Time 751 ,
Russian Translation ] 757
English 2'ranslatior~ ] 758
E2r, K. Vacuum-tube Polarograph 760
[Russian Translation] 763
[German Translation] 767
Card 13/14
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Proceedings (Cont. } CZE.CHf~~33
i
Svatek, E. Study of Catalytic: Reactions at a Dropping
Mercury Electrode 667
Koryta, J. Decomposition E~atc; of the Complex of
Nitrilatriacetic Aeid W~.t'.h Caclr~ium 6"(~
Smutek, M. Slow Electrode Rec~etions 683
[Rus,sian Translation )
[En~;11ah Translation) 687
Hams, tip. Polarographic Study of the Recombination of
PhPnylgl,yoxylic Avid 691
r
Koutecky, J. Linear Systems of Electrode Reactions in
Which a Chemical Reaction in Solution Takes Place 699
Fliva, J. Contribution to thE~ Theory of Diffusion Curve ' ~�
rents 708
[Russian Translation] 712
[English Translation) 717
Card 12/ 1~
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Proceec~i~ngs (Cont.
Santauy, F. Polarography of
of Same Morphine Derivatives
[Russian Translation]
[Gerr~an Translation ]
C~~CH~~~33
the Oxidation Products
635
637
638
'~ ~ en iM Blood 6~+0
Simane, J. Polarographic pet~.rmination of Oxyg
,r
Daskocil, J. Polaragraphic St;udy of Some Biological Redox 6~5
Indicators 643
[Russian Translation] 649
[Er~~;lish Translation
Daskocil, J.
Ox~.datic-ns
[Ru~taian Translation ]
[Eta~,lish Translation ?
?~omolka,, J. and V. Krupicka,
Reaction in Serum;;.
[Rubasian Translation ]
[Gea~xian Translation ]
Gard 11,~1~+
Polarographic S1~udy of Some Perio~.datic
651
65~r
659
Study of Brdicka's Filtrate 6
62
66~+
66.
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Proceedings (Cont.)
[Russian Translation)
[Eng:li~h Translation )
Knoba,och,, E. Hydrolytic Decom,posit.~on of the Oxidation
Fraduct of 2--methyl-1..4_anl~.nonaphthol ('Vitamin K5)
Bitter, I3. Polarography of Ascaridole
C Z:~J Fi/Lj ~ J J
Kleinzell.er, A, , and Z. Fencl, Muconic Acid in Bacteria
[Russian Translation ]
[English TranslatioM)
N~aeh, J.J., 0. Krestynova, and R, Padivinsky, Polaro-
g p y of Steroids
[Russian Transl~.tion )
[English Translation]
5antavy, F. Polarography of Ca:rdiac Poisons With F1ve-or
Six-member Lactone Rings
Card 10/1,~+
60l
60~
607
61.E
61.9
620
622
62~
628
630
632
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Proceedings (Cont.)
czECx/233
Kalvoda, R., and J. Zyka. Po~~arometric Determination
of Derivatives of Barbituric Acid With the Aid of
Mercuric Salts
J
Blazek, A. Polarometric Determination of Some Unsaturated
organic Compounds
[Russian Translation]
[Eng;lish Translation ]
Pleticha., R. Determination of Diacetyl
[Russian Translations
[German translation]
Buchnicek, J. Content of Colc:hicine in the Development of
the Meadow Saffron
Sandhol.ec, B. ~ Uae of Pola.rographs 3.n the Paper and
Cellulose Industries
Zuman, P. Polarographic Determination of Sulfhydryl
Substances in Fruit
Card 9~1~
550
555
561
563
566
56g
57~
576
579
582
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Proceedings (Cont.)
Trnka, J. Polarographic Study of the Degradation of
Glucose by Alkalies
[Russian Translation]
[German Translation]
CZECH/2~~33
Zuman, P. Reactions of Carbonyl Compounds With Primary
Amines
Suchy, K. Polarographic Determination of Cyanuric Acid,
Cyamelide, and Rubeanhydride
Pleticha, R. Some Comple~:es of Amino Acids With Metals
[Russian Translation]
[ Ger7man Transatidn ]
Roubal, .J., and J. Zdrazil. Polarographic Determination
of pheno;L in Water and Urine
Dornansky, R. Upe of Polarogra.phy for the Determination of
Fentasans in Cellulo$e
Card 8/14
512
516
518
520
530
53'+
536
539
5~-~
546
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Proceed~,nga (Cont. )
Prchlik, J. Polarographic Dei~ermination of Oxygen in
Illuminating Gas
r
Jelinek, T. Uae of Polarographic Methods in Control
Analysis of the Treatment of 1~ietal Surfaces
Zabransky, Z. Determination of Thallium in Biological
Materia~~
[Ru~3sian Translation
[Gey~man Translation ~
t+f) Nn~ ' '~~ .!'r
/l1i.:v ~ L~'TJJ
Doskoci:l, ~'. Polarographic R~aduetion of Hydrogen
Perox~.de in the Presence of C~~talysts, That is, Complexes
of T.ron With Catechol, Pyroga,llol and Ascorbic Acid
/ +~
Na,~er,_._]~., B. G. Simek, and G. Sebor. Polarographic
r~i~~i,a of Benzoic Acid and :Phthalic Anhydride
Capka, O. Pola.rography of Co~a.marin
Card 714
478
485
4~0
493
~~q5
498
504
5~~9
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Proceedings (Cont.)
Spalenka, M. Some Examples of" Uning Polarography in
Industrial Laboratories
i
Novak, J.V.A. Determination of Phosphates
[Russian Translation]
[German Translation]
J /../.V ILL/G ~ .J .J
Komarek, K. Polarographic Determination of Small Amounts
of Thorium
Komarek, K. Polarographic Determination of Bases
Korecky, J., F. Nademle~nsky, and B. Neliba. Experience
~.n the tJae of the Polarographic Method in Steelmaking
y /
Mo,~zis, J. Polarographic Dete~r~nination of Manganese i
a Triethanolamine Medium
Linhart, F. Polarographic Determination of Gold
Card 6/ 14
433
433
439
442
444
455
461
464
470
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Proceedj.ngs (Cont. )
Arend, H.T. Polarograph~.c Shady of Basic Trivalent
Chromium -Sa].t Systems
Krivanek, M. Complexes of Iron wifih San~harnaa
CZE~~H~243;;
3~.~~
j~~
Dratavak:y, M., and M. Ebert. Effect of Gelatin and Thymol
un Cathodic Deposition of Cat~.ons at a Dropp.i~ig Mercury
Electrode 404
[Russian Translation] 407
[German Translation] 41.0
Kuta, J. Study of Hydrogen Overvoltage With a Mercury
Electrode With Controlled Drox-ping Time 413
~~
Dvorak, J. Efi'ect of Capillary Constants on the Maximum
of Oxygen 418
[Russian Translation] 421
[German Translation ] x+23
Vavruch, I. Attempt to Classify Refined Sugars by the
Polar�gr.aphic Method 4~7
Card 5/ ;~~}
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Proceedings (Cont.)
[Russian Translation]
[German Translation]
ORIGINAZ PAPERS READ AT THE CONGR~:SS

Kalousek, M., and A. Tockstein. Va:li.dity of fihe Nernst
Equation in the Deductive of tl'~f~ Folarogr~.phic Wave Equa--
V1cek, A.A. Polarography ~.n Concentrated Sulfuric Acid
[Rus~gian Translation ]
[Eng;l.ish Translation ]
Valenta, P. Study of CurrentDiscontinuity Appearing on
a Calome:L Beam Electrode
Masek, J� Discontinuity on Po:larographic Curves Observed
in the R~:duction of Some Inorg:~nic Oxygen-containing
Anions
[Rus~~ian Translation ]
[English Translation]
Card ~F/ l~4
286
33~
J J J
366
370
373
377
382
386
390
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Proceedings (Cont. )
[Rus-aian Translation )
[EnE;lish Translation
Zuman, P. Organic Analysis
[Rua~sian Translation
[Ger~at~ Translatian ]
antavy,, F. Polarography in }3iochemistry and Medicine
[Ru~asian Translation )
[ Gez~an Trat~elation )
Fore,jt, J. Apparatus for Osc:illographic Polarography
[Rusasian Translation
[German Translation]
~L?~ CN/2. ~; 33
Heyrovalsy, J. Oscillographic Polarography
[Ru~aaian Translation
[EnE~liah Translation
Brdicka,, R. Kinetics of Electrode Processes in Polaro-
graphy
Card 3/1.4
1..1.8
1.32
~ ~~ `~
.i6U
17'r
194
21U
226
2 ~+1
25U
259
268
273
279
286
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Proceedings (Cont.)
cz~cx/233
have not been published in Volume I are presented. ThE
fo7.lowing scientists participated in the opening of the
Congress: Professor Wiltor Kemula, Dean of the Faculty
of Sciences, Warsaw; Doctor Jaromir Dolansky, Minister
of Planning; Professor Jaroslav Herovaky, Chairmen of
thE; Congress; and Professor Jaroslav Fukatko, Chairman
of the Center for Scientific Research and Technical
Development. References follow each paper.
TABLE OF CONTENTS:
REVT.EWS READ AT THE CONGRESS
Heyrovsky, J. Fundamentals of Polargraphy 13
(Russian Translation 22
[English Translation]
Maier, V1. Polarography in Inorganic Analysis 32
4 ~~ass~.an Translation ~ 80
[German Translation]
Hanus, V1. Polarographic Behavior of Organic Compounds 103
Card 211~F
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~~.~ ~~ ~E~ ~ PHASE I ~300K EX.pLpITATION CZE~'H/2~+3:~
InterY~ational Polarographic Congress. 1st, Prague, 1951
Sborn'~k I. Mezinarodniho polarografickPho a~ezdu. Dil 3: Hlavni
referaty prednesene na s,~ezdu. YP~ocee~ings...Vol 3: Reviews
Read at the Congress. Praha, Prirodov decke v;,~d-vi~[1952~
~,~.~._~
774 p� 2,000 copies printed.
Jiri Koryta, Doctor; Chief Ed of Publishing Howe:
Resp. Ed.:
Milan Skaln~k, Doctor; Tech. Ed.: 01d'~ich Dunks.
PURPOSE: The book is intended for chemists, chemical engineers,
and physicists.
COVERAGE: The book is a colleco~iaoo ra hiciCongressohegldnin Prague
read at the Internatl,onal P g p
in 1951. Uaea of polarographndustrialnchemistryoarendiscussed~s,
biochemistry, medicine, and i
In tYiyi~ section, Reviews Reapaiationscofgeach~reviewaarend
either German or English tra
presented. In the section,R~aalanalGermana anddEngllsh whicheas~
only those translations in ,
Card l~l~
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In n crs,nilar}� .rf tbesr tittucnc,t)ns the lt,tl vapJr+ r

� � ti
barn.�t a cohnten I �'l :nttn I+,ug and st'n�cd a5 a tttuplxt .� �

� ~ W lxGJrr thr Ilg dwtlilatrrntrrrd thccttpiilary t ndrr Ihc~� :��
'
crmdrur,m thr flg rr+alcrx`rri iatu v slugtc drop, Aud ,Ilt~r
*a ~ w�a.lnng xtth t�,tUli tm ttt u glass �htk�, ttrc diam NA`i t��

!'~ >f u,ra;utl(1 unary a n)u�rtrsLtilpr ut 11iU .it',l) magn:tl..llt.m .��
li n.unv drugs funnrd, thry Nrn tt)alr9rct7 by h+�atut>t the
rAp7IlrlrY q'1 J trtlfh)t1N1Ut' of rraahc�+l >v11h laU}{ Inr(1 1 ~� �
i~ : f Jt.rgrrrr.n t�uununY. chalnl,er The dn,ps rnt(�rrtl tlt`� ��
~ .� nlukur;;s uttd wcrr� raspy mcacurcd undrr Utr mfr n,rr.+tla: _.
~~ ~ As tltatJtr ay till tSr/)q)�, x'rrr -ut-Axurrt! wlttr a 6nutlkr :v :~��
rrr+,r than d thr f(x h.w! iron rt t!~r t~~tts (:d � u~r;E- +lr,.p

~~ ~ . ~ S r S - ~ r :
rFrAI LLRWC-l UfrOAiU r�.��rG ~.(arrsh -ti �
ri / ~ -
t J , r i -._g i ~ + , t j.i.~_ 7 '+ ' 7t at t t ,r r). ~ `. . a r w ~ � ^, o :~* �
i : - u 'r ~. w; {t a H n ,7 ~r u K t. ti tt K n tt 11 `?t;xta n 1 rr t+r;
APPROVED FOR RELEASE. 06/23/11 CIA-RDP86-005138001031400027-6

APPROVED FOR RELEASE= 06/23/11 = CIA-RfflP86-005138001031400027-6
^^Iw ..a.�a--
~��� ���t � ��� �������� �1~�
1 7 ! 1 1 i t 1 - >y1 it ft IJ N IS it N U if ~ ~ 11 IJ
'#: ~rl. ` -tl..i..1 .L...s
Therma]. properties of paiy-~ ;, . ~ E112/E435
but also change 'the structure of the basic crystalline lattice
thus af'fec~ting thermal cohesion, There are 9 figures and
24 referenceso 2 Soviet-bloc and 22 non�~Sovietmbia~,~ The four
most recent references to English language publications read as
follows,< Ref,.9; Willbour�n A~H~ J~Polymer 5cio 34s 569 (1959),
Ref~13o Goppel JoMo flrit~ Plastics 32, 207 (1959)9
Ref,15s Na~tta Go J~ Polymer Sci~ 34; S31 (1959)
Refo19~ Hai^ban A.~AU et al, J, Polymer Sci� 41d i5~ ~1959)~,
ASSOCIp-TIOt+1 � Vy�zltumny tistav makromolektxlarnx~. chemie , ~3rno
~Resear�ch Institute of Macr-omolecular Chemistrys Brno)
SU'HAiIT7`ED
Card 5/'S
July 24 1960
I/
__--
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z/oo9/bl/ooo/009,/002/003
Thea-tna:l pr~~perties of paly�� ~ , E. ]. :L2/F;435
accord:rtr,* to Vi~:~~t :> t,e~~i Gc~l.irr~r-':i.sorr~, with t'~isylr-p:rr,,:3~,t.trc
polyethyle:tie brave s~rarvrr that the correspandirlg copalyurex�s ..llou~.d
have the following compositiono 9 to 1296 by weight of propylene
and t)l ~�~ ~(iio ethylene y this being a~.so in agreement with the
preuiousl}r established -~techanica1 properties
g) `t'emperature of softening vso densityu Correlations are
similar to Yicat ternperatureo A similar relationship to the
graphs for Vicat temperatures i:~ also shown when temperatures of
soften:i.ng are plotted against inverse functions of logs of
viscos:i.ty or propylene content af.' eth}T.leile�-�propylene copolymers,
(Vicat's test and softening temperature test d~.1'fer only as to
a~~plied load.,) General conclusions from the different tests are
that tine graphs correlating density and thermal properties show a
great sr.atter of points which cannot be accounted for by
variations in methods of preparation cif the samples or by
experimental errorso According to the author; it is doubtful
whe+.he:r the relationship between density and melt characteristics
can be expressed. by a common function f.or the different types of
polyethylene s].nce these differ as regards the number and
~.har~a~.ter of short cross~~hains, which not only lower crystallinity
Card 4,/ 5
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z/ao9/61/000/009/002/003
Thermal. properties of poly ~ o ~ E 7-.12~t~~~35
It seems that the negative gradient of this linear function is
the greate~^ the higher the degree of cross-linking
c) I`ielt;ing point vs , propylene content in ethylene-prapylene
copolynaer~ The melting points show first a decrease with
incxea~red ~propartions of propyleney until a minimum i:~ reached at
approximately 120�C~ Tl~le curve then rises with increasing
propylene content until a maximum is reached at 160 to 165�C
(melting point of pure po~lypropylene~o
d) Yicat temperature vs, densitya This function showed
cc>nsidi;rable scatter of points , The values found by the author
were a few degrees highez~ than literature datao
e) Vicat temperature vs~ inverse function of logs of viscosity,
The thermal stability increases as the molecular weighty and
consequently the viscasii;y of the amorphous phase; increases,
f) Vic;zt temperature vs, propylene content in ethylene-propylene
copolymers u The introclttctian of polypropylene into the poly-
ethylene chain causes noi~ only a reduction of crystallinity but
also a decrease of molecular weight, Even small additions of
propylene will cause a distinct reduction of thermal stability
Card 3/5
"'
---~.-
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z/oo9/61/000/0o9/ooa/oo3
Thermal pro7~er�ties of poly E1_l.n/F.h `,>
tertiperal;urG is increasing 0 II3'C/min
3 : Te>up~=.rature of softening :, determined on a Noeppler
oonsistomet~erS under a load of 2 kg/cm2, while temperature
is incrE:asad at a rate of 0,6�C/min,
Results are presented in the form of graphs;
a) Melting points vs � density This function i~c char+~c terized by a
considerable scatter of points The graph indicates, neverthelessY
that thn melting point of low-prossure polyethylene decreases with
der:reas:ing dF:nsity, A similar functionality is shown by
~.~thylen~e-propylene capo~.ymers with low propylene content ,
Ina,rezsed propylene proportions give rise to anorncila.os � The h~.gher
thermal stability of the propylene chain will be apparent in
copolymors where the propylene concentration exceeds equimolar�
ratiosp The melting point rises and approaches the values
of pure polypropylene
b) Melting points vs. invf;rse function of the logarithm of
~riscosity (r~) ~ The author has established that this function can
be defined by the expression,
melting point ~ ~7/~r~f + 13b (+h)
Card 2/5

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~~ ~ ,~
z/oo9/61/000/0o9/ooz/oo3
E112/E435
AUT`HOR; Majer9 3osef
TITLEr Thermal properties of polyethylene and ethylene-
propylene copolymers
PERIODICALS Chemi~clc~ prumyslg Noo9g 19619 ppa48q-493
TE~To Tn a previous paper (Ref~21o Chemicky prumyslg Vol,llg 196 1
pp9?-lol) tlae author has cc-rrelated mechanical properties and
structur^e (chain-'branching) of polyethylenes and ethylene- ~""'
propylene copolymers, The presE~nt study correlates structure and
melt characteristics of the foliowing~
l J Commc,rci,al t high pressure polyethylene
2, Expe~~~ime;ntal samples of ?ieglers' polyethylene,
3, Ethylene-propylene copolymer
The products are defined by the logarithms of viscosity (r~) ;
density h25 and ash content anc~ the following melt chharacteristics
weY�e es~tab~ished�
to Optical melting points lye, temperature at which crystallinity
di;>iappeared between crossed Nicoll on a hot stage microscope,
2, Vicat te;mperatureg i,.e~ temperature required to give 1 mm
perxetra�tion with a 1 mm2 needle under a l kg loads while
card 1/5
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t3gi~a.~
I~I(~clart t r. n 1 1�'rt)ne1' f ~ (~ ~ r)!

~'
chtnvri I hrt t rt r r~rlu l ytliei~ w i t: h 1(l t. r) l r~l+ F1 nrl ~~(-~'+, i)r+~~.IV I c~rtc� z un ! t~tt t.
1`E',~i~l(~~;'t~LV(?.].y (;C)t'1`(~!3llUrl(.~$ 111 I('S ~;'( 1(~t~11f,`,~ t lliiri)f�tC1'I~il t:ti 'Q llliT,t1
~)r~trti� lti�r� nc)1 yel hyl(~11t'~ lnli I;lr� i v r c; ,~t r t'f ttr.- ~ I ,,,
:�y~tal:linity aTlci ~til'{rrc,.~~~ rac~rr ~ll~monstl~rtr{i Sur ht>^11
1� :. �,�Iare SpolyetiTylettc~ try St~r'rn 1 i crr~~i I Itc~ ,cc-t hns� It~~-, rr~,r, I - ~�i1 - , Irl
ri-: -,r~e~eirit. paper a15c, CuT� aura--l~T�t~~~rlrc E,c>fyc'.th~~lc~n~~ ,tll~i ;1,~.
t~ t i~v.Lc~ne~'r,roFiy) ene ec~l,c- l yuler s , T I i ,� cie~ulcnl ~~ l:.l�,/{; ~t , `,
fr- .-t~f~rtieri . '1'lrr F~reKeni: ir;-aF~c~r sc~l.s c~c~t 1 i~ prav.~.dc~ ;,clii+ t ~.r~n;a 1.
inf'c~rniatican :rn that f'ielci, ;1 study of cif~resit.+es, rigidity.
st.rc'ss~-str~~arn per�openi.es in te~~;:~ic~n, i.rpprr yi.elci str�c,~~ tc~n~l lc.
trc~n~th aria ult. _i mate c~longaCic~n cat' ;.+ wi.cic' r~~t>;u;E� cat ~~t.t>ivlrol~oseci tc~ j~r~7d~rc~e the
same -~ranchins~ effect by r.ol~nl~rmeri~r~tic~ri cif' ethylene and
Pr'oPYl,Fne, Two copalymerisation methods ~rre 5ug~e~;tc~d
~.~ : f~rnatirlg and random polymerxsati.on: Itif'ficral ties w.i t.li ranc.i~m
?fit) ~ 'y;(`r19,at ion clrE'. d15(:USSf'd ~ Ttlf? 1.1sE' ()~'7,'reS~a (?T'~ Ca tit ~ Vii t.
~~t�u~lrr, 1g58, No 1051r
Author I~~.'cr ~..
Inst Hither Institute for itacromoJ,ecular Chemistry, Brno, Czecl?o-
slovakia
Title ; Viscoelastic Properties of Polybenzylmetacrylate and Po1;;t-
metY~vneto,caylate in the Transition 13ci,ion
Orig Pub :Chem. prumysl., 1957, 7, No B, ~33-~37
Abstract Tine author ha,s investigated the viscaelastic prokaertic;s o~
po?~rbeazylmeta.crylrxte and polyr~nethylrnetacrylate, cont~cinin~;
5-~ dibut;y].phthalate, in the tra.nsitian ref,ion (using c?~ee~
curves measured by mean.; of a co;,istornetex�. Tho lirni.l;i n
moduli were calculated zr~ith the aid of the principlo o:E' ta;a-
pera.turc-time superposition of ~.t'bbol'ckiy. The charar:te7~i.,tac
clel,rzy tir.nes and tha clI.fferentia.tion tenrp~-~x~ature.~, ;ahir:i~i axe{.;
iii ~,ood rr~rcement with the vit~�ii'icn,tion �l;empc;ruturer~, tlr, ~~
calculr~.ted far both polyr:~er,:;. `frze liven equation of ~:trto
is fulfi:Lled in the region I~.�5 o � 95
Card 1/l
APPROVED FOR RELEASE. 06/23/11 CIA-RDP86-005138001031400027-6

APPROVED FOR RELEASE. 06/23/11 CIA-RDP86-005138001031400027-6

NR:
~~~$
GODD:
QQ4
~~
1~U"~~OR; l~~a~ ar Jaros;~av~13a3~er, 'ta. (Dacant; Pharmacies; C~rx~.ida~~ of Sc~3n~9B;
Brai~a.5lav~x ~ ~o~ica,_ks..~~i1~-,n~Ko~tauchok, ~~~. ~Gradua~ pharmacist; ~~ratislava~ i
Dvoa:�akova, Fdi~~a-~vo;cz a ova, E. ~Graduato pharmac~,st; Bra'~i.slava) ~~
OP,G:: Dep~~rtmont of l~nalytical Chemistry, Pharn~ac�utical.,Faculty, C,Qr~nius_Ux~,~er~
rati l~v?~ tKatodra an~~,y~.ak+~;j cher~.e I{'armaceut~.clas~ faku].ty Univ~elrx~.ty Komonsloaha
~lfi'C~: Ptl~t~ co~splexans (V}. C9mRlaxes~ of vthylowod3.ampno�N,NtMdiprc-pionic-alpha,
alpha' acid, and of arlenedia~ci.na-~t3,N ~-dipropionic~.pha, alpha ~..p~,N ~ -diacata,a ac~,d
t-3.t1:~ tha ~cat~.ons of a7.kald. �arths, and. ti~ith soma other diva~.ent cations
~OTJ~CU: Chonsi.cke zvesti, rw. ~, 1~6, 242-2;Si.
`iOP~C ~~`~GSr cation, alkali earth mi.ner~d., amine said, acetic acid, dissociata.on
consiaa~t, 5'i,a~7.17.'~31'' C,On3tarit, fntern~alec:ular complex
,~~`~Cr.~: Scl~rarzenY~ach's method was used for paterr~iamatric anirestigation of the
da.ssociat3on cox:stant of the two ac~.ds ~x~ntioned abo'+~re, and of the complexes of these
acids ;~rith divaYent cations of T~, Ca, ~~r, Da, Cu, Cd, fin, 1?b, Mn, and Fe. the dis-
sociation arx~ stabil3.ty constants found era aampax~d to those of ett~yleneMd3.amdna-
is,i~ t-ds.acetia said, ~~nd of etl~glene~clial~~ano~t,N,N~,Nf ~-tetra.~aoeti.a ao3d. Orig. art.
has: 2 fgaras, 10 #'ormulas, and 6 tab7.e~. ,rJPRSt 36,~G4,4J
SUE. COD; : O~ / ~?3M Di11T~ s
2O2tiay~~5 ~~ OR~G RLFs 003 / D~ R1~Ft 044
APPROVED FOR RELEASE. 06/23/11 CIA-RDP86-005138001031400027-6

L 360406 ~~~~~ (~) ~r~
~cc~ rv~Goz737o _~..__..._..-._.---_~.__ . _.___.__ _ . soU:~cL~cov~a: cz/oo~~3/G~/ooo/~a~~/a~~z/o,~60

~ ~-TU_`:i0 ~: iiovalcL V].ad.mir {Ln~.neer ; ~rai;isl.a~~) ; Svz_cekoTra, I~;ar~.a--;~,, ~.c c:~o�:�~ , :. ___
(Gr~.duate pharmacist; Dratislava}; 1T~, Jaroslav---Mayor, '~a. {~}rcont; ~~h~~.c~,:~.c:i.;;;,;
j Candidate of scionc�cc; Bratislava)
ORG: Departmont of Analytical Chom~.stxy, ~'har~-1aceutical Faculty, ~omonius Ut~i.wr~i~y~_
~~~ (Katedra ~-nalyticloe j ch�ma.o l~armacouticlce j fakulty Univerzity ~iomensko;io}
TTTT~~: idow comploxazis (VT). Stability constants of rs:comi.c-~,3-cliamino-~butano-
N,2~,N~,N~-tetraacotic: acid with lan�than~ldos dotormi.n�d by the polarographic mothod ,
of oxchamge Qquilibrj~um aystams
SOIP'~G~C: Chomicl~ zvosti, no. ~, 1966, 252.�260
TOPIC LAGS: stabiliiy constant, acetic acid, lanthanum, polarographic analysis,
cherrri.cal equilibrium i
i
ABSTRI~CT: Th� po7.aro~raphic invnsti~ation of tho axchan~e equilibrium syster~~ S~ras
usod for the deterrrri.nation of tho values of the logarithms of the stability constants
of normal. co lexes of the racema.c-~2,3-cia.amdnobutane-N,iJ,N~,N'-tetraac�tic acid with ____
La. Tho~stability onstants are axpressnd as a discontinuous function of the atomic
number of La forming the central ion of tha complex. Orig. art. has: 5 figures and
3 tables. [JPRS: 3Ei,~+�r '-
SUB CODES 07 / 3US~~ DA`.~s l0Apr65 / ORTG REFS 006 / OTH REFS 401
Card 1 /1 /ih ~' _
APPROVED FOR RELEASE. 06/23/11 CIA-RDP86-005138001031400027-6

3u03~-b~ ~~l~P
ACC N~~U:' 02027
f~~~
---~ - _ ~r; - ._~;, : cz o0~3 jb6 000 oot~� a433; ~. ~ ~.
._~.~ . ' r. ~ N- t r ~-4 ~: r ~j , /` . 'rl c~'.~~LZ iS lr~i J.:4s~ �+t.: ~i ~.'.~ +.. ~ .~~ a:~v.:..r ~ ~P,.~i ;,: ~ , ~....._..
Au;, i:at, l~y_o~:ova . ~.c.ita ~"~ ax Lc.~ , ~ ~. t ~.� _
I~o~~, Jaroslav-~I;ayclr, Ya. (l~ocont; ~Iu~�,:u~ca.::; Cand:i.da'~E) o.~ ,,cioncc~;.; J:~~;;:i.;s"~.,:s-,ra~
~V.~t p
Ci~.C1.: )department of 1!nu1;~:i.ca1 Cherxi.u ,~.~,,~, I'ha;-,r,.aco~ati cal t~ acuity, Co~.o~rius li;:i v_'r
r~ratislava Kauadra tulaly'~xcke j choJni.o I~'a'rr~.cou'L-a.cl;o j fa?salty linivorza.~y ::or';=;,:;i, y o) ..[ ..--
_~
T?'I'LK: Irai~r com+a?oxari3. (N). Poton~;iariotric investi~,ation of corro~ , or of. mryMo- ~~~.~~
racarri.c acids: 2,3-d~.aminobutano-iI,I1,i~1' hI;'-to'L'raacet,c acid tirith uor~~ ~3:~valont c~.,;~.on:a
SO'S'~C~: Chcmi.cl:.o avejsti, no. ~, 1966, 233..241
TG sC TRIGS: cation, acotic acid, cherriaal stabilit;r, cholat6 corrpowld, arzino, ion
ncutralisration, ion c;oncontration, pala~~a~ap:~~ic un1J.;rsis
i1~~S'i'~tf!CT; Potontiometric determination of pH was used i;o find the ,
stability constants of chelates of stereoisomeric complexans of
meso- and racemic: 2,3-diarninobutane-I~,ht,Vp,N~-tetraacei;ic acids ,
with cations Cu+~-, Cd++, Zn++, Mn-~-+, and Fe++. Schwar :enbach~ s
method of oxchan~;e equi~.ibria With 2, 2 ~ , 2"-trisaminot7~iethylamina
wr~s usedo The stability constants of cornplc~xes with Fc3++ and I-L~++
ions wore determined from the pH values of thn neutralization curve --
of the acid with the equimolecular concentration of the metal ion,
The values of th~r constants ware compared to those obtained ~olaro-
graphically: orig. art. has: 2 ii0uros, 11 formil.as, Fund tr "i,.ablcs. L~i~.~.5: 3C~,4~~~ __
StT~i CO~~ : 07 / SU13ri ~~
Card l/1 /1/i ;iJ
20~;ay65 / OitIG ter: 00~ / Oli ~ '~ : ; 006
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J~C~Ri`~~G2 5~TRGL GUll~;: u~/wr43/p~I~/mow/.,~.v~.~.,~.vv
� Pharmacist �
~ll3THORl~ Jekl~ Maur---Yok1, Y. {Doctor, Doctor of natural sclertces, ,
tand3.dE-te a~f seier:Ices ; Maier Jarosl~v--~a~erj Ya. ~Dac~or; ~didate of sciences;
t . ~n .~
~UftG: l~epartme~t o.f Analytical Chem~.s try, Pl:axmaCeutical . Facult~r, Comeniu~ Univer$it~r,
~3rat~,s:lava ~Katedr+a analytcke~ chemie Farmaueut~.cke~ fakulty Univerzity Komenskeha
' ~'� 7~Si~s Study of ocmplex compounds in ~lut3an by means of paper electrophoresis ,
~, IV. ~. 4~omplaxes cif stereaiaca~er~.a 2,3wd~,amit~obutape-N~N~N+,N~-tetraaaetio ao~,ds
E~' ~ ~>OjJRGE; Ghemicke zvesti,~~o. ~+, 1965, 281-266
~~
`: 'cO~IC TAGS: a,nter~olecular complex,. electrophoresis, paper chromatography, organic
~~3.tragen coanpound, butane, acetic acid, stereachemistry
~~ i~BSTRA+GT: The evaluation of elsc~bro~Ihoretic mobility of complexes of meso- and
;roc, acids with same di- and tr~.valent central sans a1loWed to determine the
~~ 'format:an and suat~i7-ity of the$~ com~-lexes. The complexem are aimi.lar to those
`~ of ethylenediamincltetraacetic acid; the m- farms have the same stability, the r-
~.:
have every high e~tabili.ty similar tc; that of the aompleates of 1,2--di.aminacyc o-
�' heacanetetraacetic ac3.d. The difference in stability ie due to the effect of the
~' steric arrangent~nt. Tlie authors thar-k Vies Oregorova for part of the work
k` (x-~DBT.A~ whioh wa,e done w3.thiti the framework of work toward a ~~egree. 4r~.g,. art.
has s ~~ 2' figure s and 1 table ~ , C~'RS,~''
StIH G4DE: 07 f SUBM DATE: 16Ju1G~4 / ORIG FiE~' : 009 / 07~H REF : 006
~� ~
..~a~d1, ' ~~ - -- -- --
~.~ _
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__ _. _
=' MCC ~R~~ - O ~43~- _ SOURCE Gt~DL: CZ 0~3/&5 OOO Q04 X49 O25
.~ A~UTf~C~i~ Jokl V3:~, ;-.Yak1, v. ~Daatar; Doctor of natural sciences; Pharmacist; ~~
.,~m:..ac.~..,..
Cand3,c~tite of".'~dci"e~~ der, Jaroslav: Layer, va. Doctor; Phar~aacist; Candidat~e~
~~ c-f sc3.~inces~ ~
._
~ ` CiRGs I?epa~tment oiP Analytical Chem3.s�Gr ,Pharmaceutical Faculty, Comeniu$ University,
~m Itratie?`arts ~Katedra analyticke3 chemi~e ~armaceuticke~ faku3tY University Komenskeho)
~~~; - 'T`ITLE ~ .Study of c~>mple~c compounds iri .solution by means of paper electrophoresis.
I;V. Conaplexe~ if 1~~-diaan~.nopropanal (2 j,N,I~,N~,Nf tetraacetic acid
~~:
~~ SOURCE; Chemicke s~vesti,~ ho. 1~, 1.965, 249 25g
~'OPIC 7?AGS inte~aalecular complex coordination cheml,stry, orSara.c nitrogen
. _ c;ompound~ acet~,c. acid, hydroxyl group,. electrophoree~.s, paper cr~ra~atagraphy . , ._
`"~~~TRAtT:. ~~1, ~-D~ami~aopropauvl ~2~j -te~ra~a~t~ii._aaid (PTA j is fou�8 ~
~ener:~l,Iy as a. ;fix-donor exielate�fox~ming agent, and l,ts Qomplexee
~~~ro firmed s-~m3�~.~r1y tp thoo of et~:yle~ed~.a~inetatraaootio said
~~~~~nTA j by first .forming mononuclear ahelates having a 1:1 metal ~
~Eo ag+~n~ ratio ; ~ ~b~. alcohol .grain of ~PT~ dose not t$a~e part i~t .
~b~e cl~alats forcnato~. ~ The ~'b_ chalets- Pb~~." ie stable at pH ~- #;
'~urin~ its form~~tion a proton. of the hydroiyl group ins relea$ed ;
..nd D~'TA ~be~iaves as a 7-donor agent.. Fel ' al$o probably releases
~L hy~dro~yl g~ou'p above pI~ ~a Clhelates of DPTA are-,~.ss~e stable ~'
~h8~t....'tb~os~~:~of B:q~b:..I~B ahe~.ato is. `per t~7tstabl8. The ~-ut,~ora~thank Prof.-
a o Stank va;t~s~Y' .::for tb;e dndou~a _..~acus ana oncerning tn3.s work. Orig.
..~-r~ k~~e: ~-f~ .ss ~ formulas find ~ ~ablee
-~su~ ca ! ~ su~t~ nAmE: zy~~ / o~x~ : / cncH s O~.l
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~6~~ ~(3)
ACC RIR: AP6o21;201t SOUR `~ COI)Es Cz o443 5 000 011~81.7Joi3z5~?
11UTxi0R s lJovalc Vladimir (Fn~.noer; Bratislava) ; ISa~er ~ Jaxro 1'la,~ox - Ya � (Doc$nt;
Phan.�mac ~; Cnn~didate o~ saioncar~; LarAtiaZ.ava); ' %~'.4'^~aholtova, },. l
~~
(Graduate pharmaoist; Brat~.slava) /3
I
ORG: DoP}artment of llnalytical Chom3.stry, Pharmaceutical Faculty, Comenius Univorsit ;
a an icke chend.e Farsnaiaeuticke~ fakulty Univrjrsity KomonsTcoTzo
Bratislava (Katedr alyt ~
TxTI; ,d complexanrs (III) Polarof~raphdc detoxml.nation of $tabil:lty oonstants of th ~
con lexe ~~f ~!4.~4~.3~~'3~~.butane",1~N N ~~ .!-tetraacetia a~ tJ1 lanthanum com- , ~
poukxls. This papar was presented at tha Symposium on the Structure and Quality of 1
Coo;rd3.nat:ion Compowxl.s, haLd in Bratislava from 2 to 4 September 1'~b4,.,~
SOtTtCL : Chomi.cke ~vaati ~ no . ll ~ 1~5 ~ $17�825
TOPiC TUGS: stability constant, po~roi~aphy, complex compound, exchaniro reaction,
larrtllanum compaund
AI3S".~1t11C`Pt The stability con3tants wore determined by polarographio moa3uremants at
20�C in a medium of ~sattiasium n3.trato. The La was trivalent and the cationo used for ! __._
exchanCe �quilibrium dotorminationa~ were Cd, Pb~ Gu and E'u+ La ~raa ~.n th� foss of
O.OIM solution of I.a(P103)3. Impurities contained usually in La strongly the r�tsults.
Orig. art. hays 5 fjlgures and 3 tables. C~~
SUB CODL: _ 07 ~ SU13Fi DATI~s OlMar65 ~~ ORIG R1;Fs 007 ~ 0TH AJFs 401
APPROVED FOR RELEASE. 06/23/11 CIA-RDP86-005138001031400027-6

APPROVED FOR RELEASE. 06/23/11 CIA-RDP86-005138001031400027-6

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~~
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j ~tCCES3~~ON NRt A24272
~uT~o~: ~ok1 v
czI�~~/1000/0o8/o5e4/o5gb
f . QYokl, V, ~(Doptor o;~ natural, aciencesr pbarmacistr Candidate at
eaienceia~ (B~tiel~ira) Ma (i~$ } Docent, Dootor of rzatara~, a~�ienaee
~~~~~ r Ya. r
Candide~te a~ aGien~~ee~~DxatisLawe); Mit$acova~ Me ~Kasachava M.
(Bra~i~~lavs) s- } ~az~aduate pharmaoiat~ j
~'1TI~t Stas~r of cc~mp~x compounds in solutions by means of eZec~trophcresia on
pater (III, ahexa~tion bar alcoho~,ic hydroxyl
8C(IRC$s Ghemiclse $~v�sti, no� 81 196~t, 58tt�596
~.1PIC TAGSs chelat~onr ~;Iycine, chelate co
mpoundr elsctrophoresi:r, solution property
Al35TRAC'ri The cnr~es of the electrapbaret~.c mabil3, of ~
dt3tarm3ar~d ~' gene complexes trere j
by meagu.remet~t~; NrN-bi~rhydro~y ett~rl-glyciner imit~~cli-acetio acid, and
N~~'dro:~�ethyl i~l:no di-acetic a~idr ~N'i.th a number of dim std t~ri� ~ralent central !
icsns xeue +~tndied, Oa this babia t~ ,pa~obahls strutcture aAd appa~oxisaate oan8tante
oi" tis� istabiZ~.~jr ic;~ tie complexes ~rere d�termi~nsd. ~ubat~.tn~ion by h~O~-e~Yl
~'~p iii diacusaod~ and toe aharaoter jai the cbelatea prepared, in this manner ie
deaoriberd. Orig. Wit, h~aat ~ tornuirt~Mr 6 g~'ephaq 2 tables. - ,'-
Card l/2 ~ .
APPROVED FOR RELEASE. 06/23/11 CIA-RDP86-005138001031400027-6

APPROVED FOR RELEASE. 06/23/11 CIA-RDP86-005138001031400027-6

APPROVED FOR RELEASE. 06/23/11 CIA-RDP86-005138001031400027-6

APPROVED FOR RELEASE. 06/23/11 CIA-RDP86-005138001031400027-6

~� �# ~Fa
y 160'-6b EPF(e)/EWPt~l/T/EWA~c) ~
sxcm t~s Z�~~7 ~ cz/cx~3/64/oo%~.z/o8t.3/o8~2 ~~.{ .
5Ai1THORs S rin ex 'V~Shpringer,Y.)~Graduats pharmaci$t)(Bratielava~, Ma er, J.
riaicant, Pharma~i~~, Candidate of gci.ences)~Bxatielara) -'" ~ :~;"'~.~y~~: ~
(Slayer, Ya
T:CT~E. ~pectrophat~ametric i,nvestig~t#.on o f the farmatian of ahelates `af the meeo-
a~xd rac+~roia fornns of ~, ~~diaminobutan wit capper ions ~
{ - ~ i~~~
{ ~~~tlRCE: Chemiotte zvesti., nv. ~.1., ~.~~aG, $13~-$22
~'~OPIC TA,a~s spgCtxop~to#,omexric nxtal,y~~a.s, ~.~oi~F~3', bt~tann~, fvn3,ne, aheZate Gompauna,
cl~emicgl ebeorptian;, abe~orp~#,+an spectrum, ca}?p~~�, f.vn
A~STFtAC'T. Uesaripti:c~n oi' experimtsra#:s.1 re~u~.1:~ of a spectraphatam~tric inrrest~.gat~.on
`of the fgz~s~tit?r~ a~' the space 3.sran~ers vt r ,;~~dinminabutane is presented. The campa~
s~.~ian of the ~heleGtes~ their forr~ca.t~.~Fn ~s a ~unctian of the ptt, anal the ab~orp#;i.an
~. epe~tra in the rrie3;ble rind ultrav:~c,.lc#; r~*gi.an are d3.scussed. The cheiates of th@
Cu++ ion e~r~ vi~ale#~ in color; the, lratre sxm#.lar a~sorptien spectra, absorpl::ton.
�axicaa, ~.nd abaorp#;ion roeYficinnt~s. Orig. art.hes: ~ forrr+uias, $ graphs, vablesa

APPROVED FOR RELEASE. 06/23/11 CIA-RDP86-005138001031400027-6

APPROVED FOR RELEASE. 06/23/11 CIA-RDP86-005138001031400027-6

APPROVED FOR RELEASE. 06/23/11 CIA-RDP86-005138001031400027-6