SCIENTIFIC ABSTRACT FR:MAMEDOV, S. TO:MAMEDOV, S.M.
Document Type:
Collection:
Document Number (FOIA) /ESDN (CREST):
CIA-RDP86-00513R001032000010-6
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RIP
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U
Document Page Count:
5
Document Creation Date:
November 2, 2016
Sequence Number:
10
Case Number:
Publication Date:
December 31, 1967
Content Type:
SCIENTIFIC ABSTR
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s/2o4/~~/oo~/ou5/uah/uo7
Synthesis of new plastici.zer~+ from ... CU75/E13b
distilled under l nun tlq. The fraction boiling l,etween 200 and
2,4Q �C (yield 7'G;'~a} con,~tituteci the new plasticizer named "F~NP~S "
{ANAZ}. The plasticizer has negligible volatility (U.U~~-U.q~o at
1,o0 �C}, good light re:~istance, low freezing temperature (=40 to
-~6~ �C} and gvod compatibility with plastics (does not sweat out
from plastic films } and their solvents. It is insoluble in water,
stable to heat and cold and non-poisonous . "ANAL" C 5-7`b }
successfully replaces dibutylphtha late in collodion cotton and J
butadiene-nitra~le rubber and castor oil in d+ermateen. It elso ~
replaces satisi'actorily tricresylphosphate in perchlorvinyl.
~, name is .
There are 3 tables.
~-S~aC1ATI0Ns Institut nefte~ktiimicheskikh protsessov AN A25S~R
{:institute of Petraer~emical Processes, AS Az.~SR}
~iUBMITTED : M~~rch 31, 1862
(;ard 2/2
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s/zoo/6z/oozla~o5/oo6lotr7
~a75/I";136
A-UTlIURS : Alemedoy, Shamkha 1 �
.._ _._ ~ltzayev, A,S, ~ and Nixker, 1. L.
7'1~TLL: Synttaesi,nl of new plasticizers from keno
rlal:~tithenic acids sane
~'~%RIUllICAL: Nef"tekhimiya, v. ~, no. 5, 1g62, 7ti~-792
TEXTt A search fo:r new methods of producing ~chea hi
quality plasticizers led to the utilization of� naplythsnic e~cide
as the raw -nateriai. Thp new plasticizers were ohl;ained ae
f~pllaws:
CH2C1 NaUOCR CH2O0CR
+ ~ + 2NaC;1
CH2C1 NaOUCR CH2000R
wherQ R - naPhfihenic radical
fractions of thE~ acids (keroseneonaphthQnic~~cXdeIndrviduaY
1]�0 to 14p �C _ acid value ~. r ~ 5~-60io fraction,
acid value ^~ ~7"0_2t30) were neutralisedOwithagolin~ 140 to 160 �C
SD'-100 �C. Dichloroethane was introduced at ,~ d ,NaOH at
reaction being continued for 6-~S hours. The 70-lgip �C, the
Card 1/2 products were
J
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` �.v ~ ~ 1 ~ 1,.... .. ..o e w a ow. 1
~{ ' a u.~. .t: 4'
~ f
~ ~
r~ter;ials of the Scientific Conference (Cont. ~ S
r aVj'bx95
Yos~~~ ~3ynthenia of Some Organic Com~;ourds of Sulitir
Wii;h Inseatiaidal and Aoarlridal Aotivity
' 344
ANALI"PICAI, CI~,idiS3"~ty
~gban~Y..~."~L., and T. R. l~itrzo eve.
met~rio a~iethod of De erm n n ym Volunetrio-Iodlato-
ploying Complex Compounds ofg' T~ j,entuChromiumina ~.
1 352
- ~ cx~rtzcAZ, ~rr~zrr~RIrra
Melik-.Akhnaz
`----~~~~+ ~s-~'� znveetigation of the Bleotrical t
`'molting of pleas
Name ~, 361
' l~ and Y. Nizke
o as loiter AHA3=yy""'-"~, and A. Rzayey. Syn~thesie
375
Card lE- f ~
~~ ~~ . .
,~
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,.
i .. ..~
{~ r' i
I
Materials of th� Scientific Conference (Cont.) sov/61g5
i
Vartanyan. s A., S. K, Pirenyan, and a~ g~khanyt-n.
~_,....--'' ~ Polymerization'ahd Reaction Mechanism of Acetylene in Vinyl
Acetylene i 192
i
Mamedov hamkhal. and A. Rza~ev. Investigation of Simple
,..,-,.,~,...,,. _.., ,-..._._w_
~
""~iTyaoT"E~at~xs and Their D�rlvativee: Synthesis of Simple
' "~
~~~~ Ester Derivatives of Methylene Glycol 223
~~ ~
I ~~, " Azatyat~~ V. D, Synthesis and Conversion of Cyclooato~tetraene 241
Lagidz~~~i.. Investigation of the Condensation Rea~at~ion of
""Ace'tie Esters of 1,3- and 1,4-Butanediola and Y-Aa~etylenia
Glycols With Aromatic Hydrocarbons in the Presence oP O
Anhydrous Aluminum Chloride 252
Sadykh�Zade. S. I. Direst and Organometallic Synthesis of
~ rganoailiaon Compounds With Functional Qroupa. (Inatitut
~--- khi~uii, Akademiya nauk Azerbaydzhanakoy SSR) 279
An industrial method oP synthesizing organoailiaon aompounda
CPrd--~,,~1,~ ~n
.~~Sg ..,
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. .~~
PHASE X BOOK L~aCPLOITATION SGV~61g5
Nauchnaya konferentaiya inatitutov khimii Akademiy nauk. Azerbayd-
shanakoy, Armyanakoy i Qruzinskoy SSR. Yerevan, lg5r.
Materia~.'~ nauchnoy konferentaii inatitutov khimli Akademiy nauk
,Azerbaydzhanakoy, Armyanakoy 1 Qzv ~inskoy SSR (Matar~lals of the
Scientific Confarenee of the Chemical Institutes of the Acadeiniea
of Soiences of the Azerbaydzhan, Armenian, and (3eorgi,an SSR) Yerevan,
~ Txd-vo AN Armyanskoy SSR, 1962. 3g6 p. 1100 copies printed.
Sponsoring Agency: Akademiya nauk Armyanakoy SSR. Inatitut organ:L-
cheskoy khimii.
i
I Reap. Ed.: L. Ye. Ter-Minaayan; Ed. of Publishing Hauae: A. t}.
Slkuni; Tech. Ed.: (}. S. Sarkisyan.
,/.
PURPOSE: This book is intended for chemists and chemical engineeres,
. and may be useful to graduate students engaged in ch.emical.re-
search.
COYEAA4E: The book contains the results of reaearoh in~~hysio+sl,
inorganic, organic, and analytical chemistry, and in ohemioal
engineering, presented at the Scientific Cont'erenae lheld in
~, Yerevan, 20 through 23 November 1957. Three reports of parti-
~ aular interest are reviewed below. No personullties are mentioned.
' Referl:naes accompany individual articles. v
..T~~..~.....~_.~.__._,_... _ _.. ~ , ~.. .___..,.__~........,... ~a~.,.,,~ ,
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The New Plasticizer ANAZ
~'s%~~4 5~/44c/~7/Cr~7~'4, ~,
B005~123
rvriilQ the glycol esters at' the naphthen~.c acids are distilled
cuff at 184-210�, w:~ich are alr. lady the xeady product o The f:! rs't
runnings are once mare ester1fied. The yield of the plastic:ize:r
amounts to 74m80',~, compared to the used naphthenie acid mix~p
lure. Prod.uctian costs of ANAZ are comparatively low. Tree n~>w
Lalaatic:ize~r was tested in the dsrmatina~k].eyenorhnaya fabrilsa
:Lm. No~;ina. ~Dsrmatin 4i1 Cloth ~Va, rks imeni No, ,~r~) in Kuntss~ra
for thE3 production of dermatin and nitrolinoleum. Results s~~tis-
:fy technical demands. &ioreover>' ANAZ ryas successfully used :in~
c~tead of tricrasylphos~phate as a plastiel.zer for enamr3ls of tha
type P1~V, and instead of ricinus oil. far the production of
nitro dyeel in aIPIa4 ~~tats D,.~s{~,,,�~n�d,~,'.,nni c, n ,;~,~�_~~____
i~earo_h_ 1ne~t~.tutuo~`.~~~rz,~,~.f~,~._....~.~,..~T.s~~X ~ It ws.s fo4uad
�~~~~M'that coatings contain~.ng ANAZ can be coo~.ed aPP to ~>~G� without
,any loss cif stability. In NII rez~.novc~y promy~ahlennasti ~Sc;G~r :.._....,
tifia ~~ss~~arch Institute of Rubbax Industry} good reeultc wire
r~chievr~d with thee ngw plasticizer. T ere are 1 figures 1 table,
c~nd b a~eferences, ~ of which are Soviet.
Card 3~3
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~ry7~~
The New ~'lasti,>~.z+~r ANA?.
~/Obi 5~/a~~~/~i7 j~~7/�~,
J~ooS ~T ~~
'100o fox ~ hours} era Compared to quali~.ieS of other popular
;~plaaticizelra. ANAZ is a ps,le yallr~wg nearly odorless oily l~.quid.
;E'or the production of 1 mol of this plasticizer one needs
'1.1 mol off' the napYrthenic said mixtures 0.15 mal of aodi~rm
l~ydroxide and Oat mal of dichlurnethanee For the esterifical:ion
of the acid mixture distilled in vacuum9 it is neutralized at
'120~160o with solid sodium hydroxide. The water produced is
distilled off. The teuiparatuxe is thWri increas9d to 130�. Ait
this temperature dichl.oz�aethane vapc?ra axQ led thxaugh the raix~-
ture while mixing it tharougllly, The melted sodium salts of the
rlaphthenic acids react witl~ the dichloroethane aceordir,~ to the ~
:following Schema: RCOONa C1CH2 RCOOCH2
~ ~ -~--�~ 2 NaCl ~ ~ a
RCOOPra C1C~i2 RCOOCH2
After csoolirr~� off the ~�aac~l.an mixtu.ze tc~ 50-40" wo~te;~ is r~dd~ad.
~~Che addition of water cs,ur3aa the pracipitatiora of sodium chJ.or;Lde
~.n crystalline faun which deposits readily. The eater is de��
czanted and distilled in a vacuum. With a pressure of 2 torr up
Card 2/3 to 1704180�y the excess naphthenic acids are distilled off9
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~� "'~"`{~ _ _. C r n ~ ~~? 7th 7
ART$ORS : s/v64 ~~/OG1/07/G~7/C3~
,w~Q~~ov . Slz . A,. r Rza~~ P ~ B005 B4 23
Riz cer �
TITLE: The New Plastic AN',QZ I,'
PERI~~DICAL; K:himicheski~ya promyek2lr'nnosto p ~ )59p N.r 7p PIS 580 �� 582 (USSR)
AB$T].~ACT: I;n the pre,~ent paper the manufacture and. qualities of tl~ie nevi
plasticizer ANAZ (abbrEa~riation far ~1,2d ,~zerbaydzhanslcoy SSR
(
AS of th
.
e A~erba.ydzhanekaya SSR}}~ ~.re discusasd. Th~.c~ pla~ti~-
c;f,zer whicY- ~7as for tliE9 first time produced ir. 19491950, con-
s;iste of glycol sster~ of naphthanic acids and ie �apec~ally
,~
suitable for plasticizxn~ colloxylin. In the beginning the
strong odor of thi9 planticizer ~ caused by the content of c:r�ude
n~iphthez~ic acids -, pre;-ented its being used to a lamer exte�t.
This odor can' ha~~vever9 be removed by a vacuum distillation I~f
the naphthenic acid mixture used for synthesis, or of the rei~dy
p~�oduct (Ref 3}
In
t
bl
,
a
a
e thc~ mast important p~rysicochemica~l
qualities of ANAZ (r~ialecular tiveight9 boiling point
freezing
,
pointy ignit3.ori pointy d~09 refraction index at 200, sa~,vnifi ca�~ ,
Card 1/3 t3.on numberp content oY' volatile in~;xedienta when }ies,teci t'v
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Inv~esti~tz.tion in the Field of rl~lcol Et::crs end `~ticir SCy~~-2~-f-~3%~r;
Derivatives. 7i:XXIV. The Che;.lical Conversions of the y-Eth;;leie Chloride
corresponding y-h~.lo~tTer~ ethers ~ p~eared as reaction productu;
accord~.n~ to the I~~ar}:ovrii~~ov rule. ~.~}1c xe~,~;tiora z~~a.t}i t}it;: c~~,t:t
TI'PLE: Tnvesti~ation in the Field of Gl;~col Et~~ers a,nd T~eir Deri~~;,tines
(Issl~~dovaniye v obl~~ati prast~';h efirov Ulikolfi~~ i il.h ~r.~i~~-
vodn,r~h} XXXIV. The Gher~ic~a.l Conversions of t~~e ^r-L~'th�'l~uU
Chlori~'f:~�(XXXIV. 1~hit~ics~eslciLre prnvrwshciieniy, prosty?:la r~_~~.';Ic~r
firov}
~'~):tIt~DICAL: Zhurril~,l obshchEy l;hir:~ii, 1~J- Fj`tl, Val 2f3, Pt:r ~,
pp 1113 - 1C3f3 (USSF't}
ADSTF~ACT; It tival~ p~' interest to tYte at~thars 'to investi,;~~~te the propea�ties
of th~~ ei;her harnolo~,r~ of t~la e~11~ 1 alcohol (For;;lt~l~~ I1:) is~
dett~,i;l, ti~~hicYt lzc:a,s re-~Fl,inc.~d litt:la itive:.7ti;;.t;~tcad as i'ar rj.~: c~~z~
be ~~,u3~ecl fr~rn publ.a.c~>,tio:~.,. Orl thc~ ~,c~ti~a~~ of ri;~riz�a,.~;ori h}:t;l.i.rl+~~
on al:lyl ~31h~r(II)t~ Bauble ether corepound rerno.ir~e: pre �;rve~Y {~r,~.~
only the oxygen bride is dcstxoyed under t?'ie for~nxtion of un~-
saturl~,ted (I1I} ~~,nd :~s.turatec~ (IV) hala;en deriv.:,tives of i,he
hydrocarbons. The experiments: :showed, ho1~ever, ths.t over; in the
cold (0~) HC1 and IInx can combine in the presence of ~~, c~~t
Derivatives. XXXIIT. On Somme Cl.e~~l.c,:~l Convers7.ar.s of the p-Et~,;3. Br;~.^.~~c:~� of
the Fatty Series .
yield orb;�inamaE;nesiuln compolxr~cls (IIZ}, e~riich fora 1:4-~;lyco:l-
ether (TVA tivith a~chlaric ether. This reaction process (see
reaction i~che~ie~ points uo t~zc passibility of s, nee; s;;-ntuesis
of glycol ether r~ith various allioxy ~roul~s in the positions
1,q.(IV). '1,3-dihalo~eri deriveti'~ives (V~ for,~~ on t};e actio:~ o:~'
HBr or HJ on the yMet;;rl broridea This, e~ay six ~neti~ 1 ~ j-dih~.:to~en
darivativE3s of fatty l~ydrocc.rbon;; t,~are sfnthetizerl (T rile:)-, I~11.
above ~~eni;ioned ticonve,^siana make possibly the production of
furthex cornpaunds on the ssrle basis., There s.re 1 t~~G,le snd 'j
refere~lceF;, 4 of cihich are Soviet.
ASS~~CIA'Z'TO2t: ~Azerbaydzhanskiy ~osuda~.~stvennyy pedf~~o itlesl;iy in titn.t
(Azerb+~ydzhan Si; ate I'E~da,~;of~ic Tnstit~.ite7~
S17B1k~T`.~"!:'ED : t~pxil 1 ~ '~ X57
C~art~ 2~3
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i
AUTHORS: ~lamedov Sharnkhal, Zeynalov ~ a, K, SC~,'`7 __2,:~_ _1L~`~;,;
.r t,
f:=h
TITLE: Inveati.,~s.�~ian in th4 ;~'1.~1t~ of Glycol Ft~~ers rind T:k~Esar Ac;r.~.v,;~t~.~ve
(Iosladov,~niya v oblaati proat~kh afirc~v ~lilcaJ:o;~ i 1.i.k~ ~,r~;~;i:;�-
vadnvkh} XXXIIIo On Some Cher~ical Conversions of t~.e y I~tl`-y:l
Bromides of the Fc.tty 8eri~o (XXXITI~ 0 riekatoryl;.h ~ti.m~.+~k~esk~.kh
prevrashcheniyakh prostykh y-brornefirov zhirnol,o rJ ~,.da)
PERIODICAL: Zhurnal o'bshchey khimii, 1856, Vol 28, ter 7y
pp 1831 ~- 1834 (USSR}
ABSTRACT: Continuing an earlier peper (Ref 1} the authors crLrried out some
little-known conversions of ~-ethyl bromide� The hydroiy_sis ex-
periments of these ethers carried out in the presence of ti'a2C03
and CaG03(10-12 hours shovred that on this occe.sian HBr is split
off under the formation of ethers of the homolo~;5 of ~~.llyl
alcohol (II}a In a.ll these cases none of the incornp:~ete y�~,:~, ~~_
ethers to be expected, but only unsattxri~ted ethers r.;ef,ulted,.
In the crlse of hery.tin~, tho y~~-r~tl~yl bran~a.der~ (x} :~ra.th r~lcr>holz.~t~Ea
the HBr cleave,~;e to,kec~ only ?-~ houx�r~ �~r-d rzo etkierif'ict~,tion b~~t
a forrnatian of allyl etY~era (IT) to,i~es place vrhic~~ corre,,pon~ls
Card 1~3 to the ~Z~.:rkovnikov rule (Ref 1 } � The y�~ ethyl bromides easily
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U93R~Organie Chem~stry� $yn,~hetic Organic Chernietry.
labs Job t ReP ?~hur-Khi~a~ya~, Ito ~, ].957, 19051.
Author M+~nadov Rhatc~shal, I~bdullayev A �
~na~t �~E.
Title : 5yathe~ia of si~tpl� ~I~ycol Rthere . ,
o~ Dil~rc,o~q�'c~erivatives o;e Diwethyl Ethers of Tetraalkyl
gubstitu~t~d EtY~ylene O~.ycoZe �
Orig Pub: Azerb ~~tR e;lmler Altad- kheberleri, Txv. ~IJ ~1x8SR,
~,g56, I~Gr 5, 49-56.
Abstract; T'he authors synthes1~substituted ilycolesPai'i behtype
ethers c~P tetraa].ky a
R2C(O(:~20R',~ (I) according to a previously described
method (Tr. In�~akhimiyi AId Ax3gR, 196, 6) by the
e,ct3on of C1CH OR' (II) on ~R~C (OMaX,~]~ (TTT} a product
of the :Lnterac~tan aP R1~X with ethyl, ether aP
~luccinic acid (ether sa~ution, +~.me oP reaction ~+-~
Card : ].~2
E-2
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:~;~ ,~ ~ .....~,.......,....,M.,,..,.~,..~.,,,....~.
-~-- ~ =~
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APPROVED FOR RELEASE. 06/23/11 CIA-RDP86-005138001032000010-6
APPROVED FOR RELEASE: 06/23/91: CIA-R~P86-005'13800'10320000'10-6
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