SCIENTIFIC ABSTRACT MASLENITSKIY, I.N. - MASLENKOV, S.B.

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SCIENTIFIC ABSTRACT
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lp 41~ v No No M. 0 4. 4 0 It a v I I I pw b --JL_t_j 00 A coo as -.-0o pwattill AND 011cocat'41t Cox 001, v ?-00 Ole - low roligpdo 0 bit" WASM4111. L N, 00 A widogood JAI,. S. ILM li(IMU); Khoms. Z*dlr. IM. No.3. M.-Tbc ProPowd I'led-1 for '00 0 wartiva.al bausitor nthwrah I- IN-11 - the -k-cotive Of tfw curagoomomis of trauxitors. I(Cl 01- L191- -V `049 &1L40 .4n. immi VM RAM - pftqmwd a. -IV%-llvc tol- wf vj i - vull vc-cass Itar tryolmoritilAte. Attlamutio thew ublvetst% art W&%-iitv in chok actium the warloms ord-scolte, fm 4b, alforing tke ctrompawatti of bausitors uutkv ck-falitt! tmuh- 00 ilk lkm prortnit thdr we. A fi4o1A am(. 44 Koff (A-4 1'(4) IN oltfo~j to ibv Imiushe "11114V I)a a 17 "SO 00 pared with A water trath. var ortat. oil dirmaAwd AIP& owir,immid, N, j:09 00 thoo. 1,4144to,"t 44 hirthooloiluiv, 'M inutf. le,tt.114t. 1* tivall-11 1;. oluki low Nauk- vtoudilkous Wilk 11 104 11w "441s,10 14 Istilaniie I. 4kid. In the logo. Kaolaolv, and 414's'I"tot Iv- too 00 Ill.A. frAdur at RoLl". cm. lbr Arkyolorated kwAnisor wit It 7.11% 11 gil-). mut 0 ve tict. A40, icurort4korwAlas to kwifinitc) In the An. The vfftwr~ der Urge it tbr curotorats 44 tbectoin us are "Mw. ha, -AUXitV1. T1w powitatiommal %tVa. usetbutt w&q at-um"il fog C14Y (Ialoofiw(v I to IM41. toy womosm"t with 0 Atochilm-or (most'l to's or NW11). The foemilAw tool" sw of 1:61114 14 ilorinl. =10 thtmak a I" lied mild. ftorstitat oully In bravy id, 1. cuncAl. In the IiFht fracioxi. t < 2.31. k. Ife"" ADIS 04 LOO too Ii~o .. I-n I I Plot a a 0 1 w of 2 too 4 ot +a o, - - - - 4170 4so 6 0 *oe e ' n ' 1 u 'l 4 l . A -P- .0 IND G. 161L Oes 010clsits "D ONCONIT'll -004% 94- C I N -dan W r M ! A :T I o. 10 10- It. 3- ir7--'Lvb vwptr.- Ind. i . dii I . Rj -00 j on it* uatwal proerm of ttumitim 0 anhydtite to pVmm h M f i i -00 s ow t m o on is chm- t 4be birimmoSmeows reW hydrat b y It* pailual wk. of anhydrite to fixtu a super. acteg*d utd C*90 sals and The ta of sum The of at .00 . . . , r e 4 pp ap hydration dtpmb chielly an the uturt and concu. of the c salt swp. und. - Weak labis. (0.01-0.02 mol./I.). an Col. - l 4 vArvd Mi t U.0 rttAfd the Poem of hydn" In the ly With The virkwity oil hydra- nl::T % 6= 0= t Wa ibm drogm. The moot 480 bysul- fates al alk.~Wwth mrtels and a" clibuMn. ChkwWn of allt. eartliffietals iubibited the hydratlem umkr all con- illOons stuilitil. The ~kin proemls mint rephily at 1 10 sad Ai6m. prwoomr. Nowly minsing wat". Ivy rrmov- Isla IM tmmm velive lavet of Min Cat the anhydrile, rx- suffsAv. wit the rMid"s 0mrkration Cf see Proem. During the extid. perkmi td 3 deew of byOratim was 30% and 2-mm. f ornmi gypsum. Cf. Ronjak, C. A. Si. 4 ' M7 C . ISU. HIM 1 . to 41 34 O 4 N 0109 CA-ASIOICATI OTALL~AL 4.811 seem 11"41419" Yl I 144440 isle Omw dad - NA&SAI 00 O-V 611 N , AW 16 Ul; a 9 1 w glom ; :iq ;Tzq F 0-019,00 0 00 s o 000 WO 0 0 0 00' * 0 0 1 71 0 10 ' ,** 0 0:0 00.0-0 000 0 0 ' 5 0 wtv - *a 0 0 0 -W-0 0- v 0 0 0 0 0 0 v a It Atulaml ISO 00441 ass 'A -L-1-- 1 11 ! !--ft JXAR- MiT --1, 1. Ad .09. Rsilmbg oWtw vmWmkg bitummats by wAlbed. 1. N. MavArtlitskilLd. Chain. loadi (U q. 2.) tP, No. the bitumm in i 00 c1 j 8,00=16 W, Im novid by trvatioNg the loolten earth. but so much of the latter Is nettled that the prootial 11 lumonumic. Better tMita Orr oblatlawl If file 8 Is firtt tM(ni With 114011414t 11tW)4 At 11111' 10 11*111`0`0 11111101 44 -00 I t 00 a, 00 COO coo if 6 Irmo, 6*0 'aft, CIO* 01~ ILLWK41. U 140M CLs StWK&I 44 too 1`1 4 1 . 'at W ft~ 111 to 0 ad a IN It cc it it #A 1 5 0 ow a a 3 0 9 0 0 es 00.0 10 00 0 04 0 0 0 0 ot 0 ~100 so 4748 & : o 0 0 o10 0 0 * 0 0 0 : 0.00 000 WO 0000 & 01 1 1 6 F I 1 0 if a fl.u 0 M n axn a6va" all an mis 06 U-m-or-4 a W m I m 11 a L.- ..A_ - i P kV #I -*f.S lip R, l Poeltilill A"C' PROORONS -Wfo Mask-nit4kil. brorlity Metal. 19W, l4e. 4, 42-4.~-M.'d~*MkrdW4(&hWquc of prefig. lx,l- isbcd n- om of tailinits (or trik-rivropic v%Amn. by tv- An txv %&triple comisting of pyrite. ChAtoot'v - Rite Outt l SILOS trilaters1% was exatud. and jWrccnt*jrN of t lie itilortalti *vto cakd, Thv- rtuirsin. ithowed that chatv,)py. rite io meturally as-tociated with himp, tif pytitv; mviv 24117, of file villilvolly'rite k in a fret -talt whet, gromild - t Th6i li PO 0f1 k h t. caft, t miri m is( mmir Of 1,-c4 kit- to in due tn thitt nwh. Calm (vildivillfrif if) pyrile Zee of see 4 r gee 00 i t 0 wee Usti mill 0 ...... ll~.. -7, - - - , I -_ -'. -- M' wee . sill.) QvL ~'W u 0 All rw 0 06 0 1 IN a 9 a a In 9 R9 IT ; !1~-- OR J . 3 , i, 0 PIP OF 9 9 0 0 0 0 6 0 0 Al 0 sto 0 0 0 0 411 0 ~ 000101110000000WOO 'a 'a a of 0 36 a a W a a a a ewe A-JL 1 -4 OLM W!, D"limmkolim d bwAssas Is lump ft*W. 1. 9, --.sea CW No. toodbodit of Ft"raims nod i:vk, am sted 401 It"IdA Fleck MW Ward for t..: oleto. 40 MNOWN.- M "ieft gwbwt W* for Wk, too aew~* WA dmk am -M, is onsclost for Pam. The sodlomd of Freontho-WA is irk"= Mo. TU devistions Mc 40-W%. Tbh Is esplefised 8 by the Swumbox of stable 5 comp&. whkb aiv not &s#4. of at 3W (eaft to the prolianged codiact of fivied S with Mqnid bittiltestso). Oplintouts r"alts am ob(ained from the soetbad d FWtk and Wad which gins reproducible o0 Z rmolss. I I NJ is blimstras In lump tuid revat S. Will - i see 0 b% NOW to wain 0 tin "An. of S. fly The MWilk4f 'k goo vtortbodthade imbeA,beirvorcontentoolbitumew o0 0 adly vverv 2-3 sh In dttqk Instonm they devistio"t am esplahwif goo SOV lot tilpol. tMon. The mtihm of Firch 4tut Ward Iq StAll - sell 11 k Almille mill all Itt-141tolf do 000 W.14,11. woe goo goo foe woo floe ,A a, I L a 1101444.9016KA& im#41"I C16AWK4100 woo goo Mvj 0 goo" 0 600 o 6 0 0 Tt.s*Y.W9-0AusS. md Au-bessing FeS mirt the solubility of An it and (U) at -=& lactude measur4ble quamtitus nely dispers" awt vwbwkru*o*c As whkti cannot tw dcleCIINI Maftilly eM at h4 ,h Ma4*111catlosw In some cases this "a ..V- to lptodect of decomp. of primary AuSs In F. Ylphirbes wid is doe to the conditions of formation and sub- sequent cooling of (1r) and 1131. The torm of the An separating (=In cnemponds with the forms of natural An found in M. C. R. if. 000 0 606610 04 0~ 0. fnpw W.14 fl, ff'' 410. .0 0 00 A'~- Md't'.. TtOO 041 A f '-00 11 00~ 06 1M1W WAIG d IMM*G *141 k b" ftudge. .1. N. h1=1", 4MW-WIfP44I-,tvwpf. *00 00 a lee H W" ficakmi. to Class. by of cywtmtwu *00 00 9 -'i : " it I (d. C.A. W 4737; J9. 37,W). In ardw to invegigate 'e* The Itinvation of oKb Ali bcwiitg minerals. Aig sad Fe man(Wodivi4beticessi.S. thi riattloic. modal the Am 800 4 voCudfilvatbapintba4i4w :300 11i"Myrr. 001dif Stals. 04 Ail *fie SAW faww 1110th so (114111 60 400 the swulfakc of I and as I IsiskiA Sued Not gfty Wissims may have 1wris Amp%. elp zoo (b). cro"tion %is OffmiVe in "OWV64 the Sallue it Am fibits but sot The wbwknw%Vk%My ditlwfwd All. Zee This struthc4o ad Ali raws. I indinstes that naturaily ewcuriing. Au-broing pyritsit, ant kxmd is a shilites ase vber. Coyist. U wn4 pirrid. by %WijLvtim# Wd. 11 its -00 heatind 1=00 goo J we* I coo WOO It tolam') -At Ott, .14f #$&Ail ass d., b a AV I Ow 0 -4 4 1 W of ij a 316 v . %L 0 n so IS 0, to a Sir 'a a it a of a 1% if at Wo 000 00 0 0000 00 so 00 0646 0 0: a Ole 66 0*0 0 0 0 0 0 0 0 e_:_ go, : -**u a -0.9-0 * 0- 0 00 so to 0 0 6107- 0 0~ IIHII 04,vi-wo-Ir oft-1vefy klarof trig'. It US he 'be light 'IMUMMI IIIIJW941; ft I$ UQA11Y A. mint. With StAu"OVAHM111010 WW OctvduuAY with tainaz6 fit ushmm" "I""' ()f tbc-- f"1101361i"M Is the hatd- " (4--4.5) am$ Momi c!!bk, and PlatlrfikC &MCVAtM ThOr M4WA(ifff "dwral is deaributilt! thriteig"t its itt"ecture it, is tweliw (giAllus awl IfIl affAlfsk il"fkafro Ow ..4KIIINS. P-Tisit. 4IRw l( She ulskiso"ll lisimorals A Iwoi* its Iw -4 1 "All (4 0. M. K~a.,Iq-d KAISLENITSKIY, I. N. "I'lew platinum minerals in su-Ifide ores", Zapiski Leningr. gornogo, in-ta, Vol. XXII Part 2, 151,", p. 190-2f;5- SO: U-4393, 19 August 53, (Letopis 'Zhumal Inykh Sluatey', No. 22, 1949). I I ~ I KASLINITSKIY, I.N., prof.; KRICHEVSKIY, L.A. -1 Separation of copper-nickel converter mattes by mechanical con- centration. TSvet.met. 28 n0-3:6-10 My-Je #55. (MIRA 10:11) (Flotation) (Copper--Metallurgy) (Nickel--Ketallurgy) W_ 137-58-6-11331 Translation from: Referativnyy zhurnal, Metallurgiya, 1958, Nr6, pll(USSR) AUTHOR: Maslenitskiy, I.N. TITLE: F~lotatl`onSeparati~on of Copper-nickel Mattes (Flotatsionnoye razdeleniye medno-nikelevykh faynshteynov) PERIODICAL: Materialy Soveshchaniya, po vopr. intensifik. i usoversh., dobychi i tekhnol. pererabotki medno-nikelevykh i nikele ' vykh rud. 1956 g. Moscow, Profizdat, 1957, pp 222-230,"i"ri. ABSTRACT: A study is made of the relationship between the results of the separation of mattes (M) by flotation and the Fe contents thereof and the rate of cooling of the material to be separated. It is shown that in order to derive high-quality results in the separation of M under ordinary factory conditions, the Fe con- tents should be < 176. When Fe contents are > 31o, the separa- tion criteria are markedly impaired. The question of spparat- ing ferrous M was successfully sol *ved by changing the ia'te '. at which it was cooled prior to pulverization. A slowing of the rate of cooling makes for satisfactory crystallization of the phase constituents and permits separation thereof in the sub- Card I/ Z sequent flotation. Thus, the rate of cooling should be 137-58-6-11331 Flotation Separation of Copper-nickel Mattes determined in accordance with the Fe. contents of the M. In order to produce an Ni concentrate with minimum Cu contents, there is no need that all the material b6~wund until 80% is -40 microns, inasmuch as the Cu content of the Ni con(~e*ntrate diminishes to a definite level when pulverized until 501o is -40 microns, but remains constant thereafter, regardless of the finer grinding. It is recommended that materials be cooled more slowly before concentration and multi-stage flotation. A.Sh. 1. Copper-nickel ores--Flotation nickel ores--Properties 2. Copper-nickel ores--Separation 3. Copper- Card 2/2 MASLENITSKIY, I. N. Maslenitskiy,, I. ff. and V. V. Dolivo-Dobrovol Iskiy (Mekhanobr) "The rendering harmless-of waste water from beneficiation plants" vneented at t40 hft 861MUfle MA TWJJU~ Se"Un of the Ofteacbr Uftlugmd, IS-IA JWj 1956 MASLENITSKIYI I. N. 'J~ By Yaslenitskiy,-I.N. and P.N. Perloy 'Vhe present state of the autoclave-soda process of treating tungsten-ore beneficiation, products in the USSR;" report pmoonud a the 4th scientific and Tacbnleal Basolon of tbia Fakbawbr Iwt.. Leningrad3, 15-18 JUlY 1958 PERIODICAL,- Ma8lenitsk-ly, I. N. SOV/',' 63-59-2-1. 614 6 The Method of the Autoo ave eatment of Platinum Containing Mud Form d in the Nickel-Blectrolysie etod av-4.oklaynoy pererabotki plati-aosoderzhashohikh shlanov elektroliza nikelya) Naaohnyyg doklady vysshey shkoly. Metallurgiya, 4,958, Nr 24 pp! 98-103 (USSR) The treatment of the anode mud formed In the niokel- electrolysis Withoui acid was carried out in autoola-res at h~,'g.,Ier -tempara.- tures. In this treatment the sulfides of copper and nickel a=e oxidized to the --orresponding sulfates at constan;,, rxygE,-- pre.3- sura.1 these-sulfates can be separated from the mud. The oxygen. pressure at a temperatur.e of 70-1450C is 15-20 atmosphe=es ex.cess'-pressure. From the results obtained may be seen that, the oxidation crate of the sulfides increases with the inoreaeg in temperature. After a two hours treatment, of the mud in auto- ,cla-7es-copper is:completely oxidized and nickel almost to 90%; either.of them,passes into solution. The rare metals of the anode mud are concentrated to a high degree by a combined autoolave and hydrometallurgical treatment of the anode mud employing also mechanical concentration. The content cf t1--il SOV/163-58-21-I6/46 -ment of PlatInum Containing Mud Formed in The Method of the Autoolave Treat the Nickel Electrolysis noble metals gold, silver and platinum in the concentrate amounts to 50%- Based on 'these inx-7estigations an effialeat scheme for the treatment of the anode mud was, suggested. All processes take.'plaae rapidly without theluse of sulfuric acid, and an efficient coneentration of the platinum metals Js ob- tained. There axe 5 figures, 1 table, and 3 references, 3 of which are Soviet. ASSOCIATION-: Leningradekli-y gornyy institut Leningrad Mining Inat._'tutf~) SUBMITTED: Ootober 19 1957 Card 2/2 AUTHOR: slenitskiv. 1.N SOV/149-58-4-14/26 TITLFA: Autoclave Oxidation of Auriferous Sulphide Concentrates Before the Cyaniding Treatment (Opyt avtoklavriogo okisleniya sullfidnykh kolotcCsoderzhashchikh kontsentratov pered tsianirovaaiyem) PERIPICAI.-Izvestiya VysahikbL Uchabnykh Zavedeniy, Tsvetnaya cm% Metallurgiya, 1958, Nr 49 PP 103-108 ( S j ABSTRACT: Recovery of gold from sulphide ores and concentrates presents in maixy cases considerable difficulties owing to the extremely small particle size of the metal which is present in the miaerals (mainly pyrite) in such a finely dispersed state that it remains unexposed (i.e. inaccessible to the. cyanide solution) in material ground to contain 90% of -325 mesh particles. Oxidizing roasting treatment is often used to overcome this difficulty but unavoidable losses of gold in dust formed during roasting and the fact that a thin layer of low meltingpoint i1xi&s formed sometimes by certain ore constituents and enveloping the gold Card 1/5 particles may defeat the purpose of the roasting process, SOV/149-58-4-14/26 Antoclave Oxidation of Auriferous Sulphide Concentrates Before the Cyaniding -Treatment detract from the value of this method. The hydrometallnrgical process of autoclave oxidation appears tq be a more promising solution and caustic soda or ammonia have been recommended. (Ref.1-2) as suitable leftching reagents, However, these solvents are of little practical value owing to their high cost. On the other hand, it has been shown that sulphides (particularly gyrites) can be completely oxidised in water at 120 C, and the subject of the present investigation was to examine the feasibility of utilising this fact for developing an efficient and economical method of pre-treating the sulphide concentrates containing finely dispersed gold. The gold content of the five different concentrates used in the experiments varied between 6 and 43 g/ton. (The complete chemical analysis is given in Table 1.) The results of determination of the gold content in. various fractions of the concentrates with the particle size Card 2/5 varying,from -5 to +7411 (Fig.1) showed that all samples -44L-OC24. ve c 22 Or AlIz, j2jd44 . ez 042c, m -r ~mq taz ze e.l~e vra~22-t 'T J~, CO.O.& a O"a So 84c, 'Ir 4.Z,2 84bJe C &a -94 co2zr-r -10 cooc,.t 9-5, 902(1 zWe -4 opt'. colit ecl t Is Zz,% &/to 27a t-ea -1-4/ l4uj~ e2j& 0 t we c1 4 220t, -zloa pl, t J1 e se-ro ~~ t eirce X* 'Y t, t- he at he t F~~ . 0,,, eat 34e2y cl 0 ec, ~, Z.4 e c 'R - -1cQ t-ec, a -Z,ec 8/t ta~.z - 0-6ft 04,1. ~Q& at a22 Cl 600gve2D, x-ea ivaa ZL Ch bot or cheye t4 the Clet. 4t 8 t '40. 8bl(joaa M04Z e Z., U Vb,'&ee ,a, 9 Cove, XT~ZZ4 afte elaPe a0llzet,5100 ecl -V . z ~~to 421t ez,), ~zt c . l4zea O_r Or W12 Z Ch 8 -N04 ed Icze a t4e 901cl -n vaj~ ~02jj~ ~ q'Z440cj Aa alp 42t V4 v@ I the icl (20&."e 'facto 2t 'OcutW - dat-4 Ze8zi a~t`&e Q22Y z4e Ast < Cl 44d~ -4710 a4d tha 2et 444 tu zqaz 315 pazt iZ4,6 a -roea,7- b tjo 1,0 jr th Ifte 4toci Z4 R! at zlwz~ Q's OAZQ a di~ or .20 .4 84-It's QI% 1804 903) atr4l, . J.Z 0e Pzesq, 4? &4e 22 t. Ca -~-r ok. Iciatio, 44d 1 ~~te pzea A4 tho 0( 02 ?YZ~~ t 2 40 0 tl,~Se olg6 11 is al2a 0t the 84.z~ J~- Out, 0022d arae4 C04, lZilde X*a 41 zTlcat p2e t r ct., o the e e OP. _Zj, , pa (P~e e ox,(l.a2 44c1 4280 -zarecl 01~22 SOV/149-58-4-14/26 Autoclave Oxidation. of-Auriferous Sulphide. Concentrates Before L the Cyaniding Treatment insigaificant-proportion of arsenic passes into 'the solution, since practically all As is absorbed by iron hydroxide for=d as the result of hydrolysis of iron sulphate. In the experiments carried out by the present Author, all iron, 95% arsenic and 50% sulphur were precipitated in the form of basic salts, in which a small amount of free sulphur liberated during the oxidation process was present. After removing the sulphuric acid solution, the precipitate-treated with a lime solution to remove the last traces of acid and to extract free sulphur in the form of soluble calcium sulphido - was subj*cted to the usual cyaniding treatment, the results of which are given in Table 3. side by side with those obtained in cyaniding the roasted concentrates of the same composition. In the latter case, the maximum recovery of gold was 8?.5% with the ma5dunim gold content in the tailings equal 10.g/ton. The corresponding figures for the concentrate Card 4/5 oxidised by the wet process were 96% and 3-5 g/ton. SOV/149-58-4-14/26 Autoclave oxidation of Auriferous Sulphide Concentrates Before the Cyaniding Treatment These results confirmed the view that in some cases the gold-bearing sulphide concentrates can be effectively and economically prepared for cyaniding by autoclave oxidation. There are 3 figures, 2 tables and 2 references of which 1 is English and 1 Soviet. ASSOCIATICU:Ieningradskiy.Gornyy Institut,,Kafedra Metallurgii Tsv*tnykh i Blagorodnykh Metallov (Leningrad Mining institute Chair for Metallurgy of Non-Ferrous and Noble Meta4s) SUBMITTED: ~6th February 1958. Card 5/5 NASLINITMIY I*No prof' PIWN-of autoolave hydrometallurgy lu the flowsheet of copper- n1cial ore converslov6 TOwete set,, 31 no'4tl-5 Ap 158,(MM. IV5) 1*' IrAnIsgradskly gorzq7 Institut, Muforrous metals) (Autoclaves) (Hydrowtallurgy) SOV/136-59-7~7/20 AUTHOR: MaslenitskiY-.-L.U. TITLE: Flotation-Autoclave Method for Treating Nickel- Electrolysis Anode Slimes PERIODICAL: Tsvetnyye metally, 1959, Nr 7, pp 36-40 (USSR) ABSTRACT: The author points out that Soviet and foreign practice for primary*treatment of nickel-electrolysis anode slimes are extravagant in,plant size and,reagents. Drawbacks re- mained in the gravitation-hydrometallurgical method developed in 1940 by the Leningradskiy gornyy institut (Leningrad Mining Institute).and applied at a Soviet works. After research on this a gravitation-autoclave method was r.ecommended by the author (Ref 1) (Figs 1 and 2 show sul-' phide oridation as a function of temperature and oxygen consumption as a function of time, respectively). It was later decided to use flotation instead of gravity concen- trationl work abroad (Ref 2) having proved promising. In contrast to this work (Ref 2) the author dealt with Card 1/3 materials containing considerable quantities of sulphides SOV/136-59-7-7/20 Flotation-Autoclave Method for Treating Nickel-Electrolysis Anode Slimes and some nickel ferrite. Preliminary experiments showed that in acid solution flotation of sulphides, selenides, tellurides and noble metals is very active; part of the copper and nickel went into solution while the nickel ferrite and nickelous oxide were mechanically entrained in the concentrate. Optimum H2SO4 concentration in the pulp was found to be 20%, though 3-5% and 250 g/ton of reagent gives satisfactory results. Alcoholic IM-66 was used as frothing agent. With re-purification of the flotation concentrate its recovery was about 60%. To improve its quality wet electromagnetic separation was used, the pro- duct (mainly sulphides of nickel and of copper) being subjected to autoclave treatment. A flowsheet (Fig 3), based on these results, used to treat several portions of slime; the combined products showed a high concentration (Pt * Pd;;p 56%) and recovery of platinoids in the final concentrate (Table), whose yield is about 3%. Further improvement is obtained by roasting at 800 - 9000C. The 'Card 2/3 magnetic product and flotation tailings can be smelted SOV/136-59-7-7/20 Flotatioa-Autoolave Method for Treating Nickel-BlectrolyBis Anode Slimes under sulphiding conditions to give a platinoid-enriched product for retreating with the feed slime: overall platinoid recovery can then rise to 99%. Losses of rare platinoids in autoclave solutions were small, but the author mentions the possibility of precipitation from sulphate solution. The flowsheet provides for recovery of selenium and, in some cases, tellurium, a separate method for their recovery, developed at the Leningrad Mining Institute by T.N. Greyver (Ref 3), is also available. The author recommends the large-scale testing of this flowsheet. There are 3 figures, 1 table and 3 references, 2 of which are Soviet and I English ASSOCIATION: Leningradskiy gornyy institut (Leningrad Mining Institute) Card 3/3 MASLENITSKIY, I.N. ."Development of the Autoclave-soda Process for the Treatment of Tungsten Concentrates.. if report to bd presented at the Intl,. Mineral Processing Congress, London, England, 6-9 Apr 60. All:-Union Scientific.Reasearch Institute for Mechanical Processing of Minerals, Leningrad. MASLENITSKIY,, I.N.; POLMVSKU, L.K. Assaying materials containing a large amount of Izon or cbromi= o4 des. Izv.~ vys. ucheb. %&v.; tsvet. met. 4 no.5* 139-144 l6r. (MIRA 14:10) 1. Leningradskiy gorayy institut,, ~afedra metallurgii tyashelykh tevetnykh i blagorodnykh metallov, (Tailings (Metallurgy)) -AimaypJA) (Slag-Analysis) (Metallic oxides-Analisis) -.91 C6 ACCESSIO N NR: AT4043065 5/2834/63/042/003/0025/0034 AUTHOR: Maslenitskiy, 1'. N., Zverevich, N. V. J~V i~. TITLE: Amalgamation of Fe-N1 alloys f SOURCE: Leningrad. Gorny*y Institut. Zapiski, v. 42, no. 3, 1963. Khtmiya, Ary, metallurgy, ore concentration), 25-34 metallurgiya, obogashcheniye (Chemir TOPIC TAGS: nickel Iron alloy, permall' kovar, alloy E1996, platinum, Armco Iron. OY nickel iron alloy amalgamation. zinc amalgam, alloy surface wettability, oxide film effect, amalgamation ABSTRACT: Amalgamation of Permalloy, Kovar (18% Co, 29% M, 53% Fe), alloy E1996: (2% Be, 93% Ni), platinum and "Armco" iron was studied by measuring wettability by mercury under various conditions calculated to prevont formation of oxide films. These included hydrogen reduction of the test plates and wetting under an acid layer following -electrolytic reduction of oxide films. Surface preparation and experimental techniques are described. Other experiments involved effects of temperature, environment, hydrogen pressure and the Hg-Pd contact period on solubility of Pd coatings in mercury, as Well as the wetting of these metal and alloy surfaces by zinc, ammonium and sodium am The results Indicate that amalgamation of Iron-nidwl alloys cannot be effected _1/2 KASLENITSKIY, I.K.j ZVERMCH, N.Y. . Hydrometallurgical separation of metal2lzed copp"r-itickel matte. TSvet. met. 38 no.ld,,6-47 Ja #65 (MIM 18 o.2) to o o mo Wir t 0, I l v to n a a t. A. v it 11111pultillau isso* 41 va moi~i A toll "Ll 4 t- fl.vt.t wattir from flaud" can- -00 two. (1]. S. $- R.) 17. i;;~i cf. CAA. 20, ~.-Fcw -s- till", "rs h; thi, wt llf r11031161" IV" IttAn -.'317, to matelial Oftn t -00 e e the cowealf,t ' r l i * ~ Redl A of Itmirt Oliver than 14if it wth apAl 9 t3 / C- u# ; &;4c insit. go day in tht The A 70 X =00 . alk P matralle reducts The *W of 3 c"a wfwn rittire than A is pggqt C. ntmate of - tillurnill(ms materiail ;;(" tjwSyW. cky 2-2 5% belawne alld XAA% A044 Ifudd'd, 4():,. too t should be liciall"W. %lica mo" than . ` I of the reWnts should tx- 4047, day is Pleme t. 2- B% Jl 0 i it addtd. and the k"Ovitne sbmtd be k-A tha 4 9 H. M. Leimttr_ -:Zoo see wee i I CL 1 Aftell c Z_ - _ - ----- - solcal Ott Ckv (301 __ Ito* 12 is u it AV 0TjTi zw t__~ - I An & A - I s it ad a -i 1 10 a 5 a ; ; I c 9.0 , _ 0 3 f I I a -1 " A I've 0-0 0 Wo o 69000 0 09 o 0 * 0 0 0 fe 0 0 0 0 e o oo 0 4 * i * 0 o 04 0 o o 0 00 0 0 0 *0 6,96060 go o & offo o :I SOV/ 137-58-9-18748 Translation from: Referativnyy zhurnal, Metallurgiya, 1958, Nr 9, p 85 (USSR) AUTHOR: Maslenitskiy, N.N. TITLE: Major Trends in the Investigation of the Soda Process of Treat- ment of Scheelite -molybdenum Concentrates (Oanovnyyo nap- ravleniya. issledovaniya sodovogo protsessa pererabotki she- yelito-molibdenovykh kontsentratov) PERIODICAL: Obogashcheniye rud, 19 5 7, Nr 4, pp 3 - 10 ABSTRACT: A discussion is presented of the two fundamental operations in a flowsheet developed by the Mekhanobr Institute for a soda autoclave process of treating VI-ore concentrates: Autoclave leaching (AL) and separation of the W and Mo. The conditions for maximum extraction of the metal in solution and the methods used to reduce Na?C03 consumption in AL and of reacting Na2C03 with CaW04 are examined, as is the efficiency of the introduction of balls into the pulp in AL and examples of AL of products' high in W and Mo. The Mekhanobr investigations have established, and industrial practice has confirmed, the possibil- Card 1/2 ity of high recovery of W and oxidized Mo in solution when the SOV/ 137-58-9-18748 Major Trends in the Investigation of the Soda Process (cont.) temperature of the soda solution is ZOO-ZZ5'C. The highest level of W and Mo separation is attained when Mo is precipitated by NaZS. Pilot-plant tests of a flowsheet for. the treatment of crude scheelite concentrates with delivery of W03 and MOS3 yielded-an average monthly extraction rate of 90,416 of the W (94% technical recovery), The properties of the W03 derived satisfy cur- rent technical specifications. ., The treatment of rich s che elite - molybdenit e concentrates by AL yielded an I-Mo product containing 30-4076 Mo. The MO/WO3 the".. ~% oduct was quite well suited to the needs of the ratio came to >10, i.e. pr 0 ferroalloys industry. The artificial scheelite obtained contained 69-7216 W03, 0.1-0.2% Mo, 0.008-0.018%R, and 0.5-0.876 SiOZ. The soda autoclave process has been adopted foruse In hydrometallurgical plants under construction and the hydrometallurgical shops of dressing plants treating W and W-Mo con- centrates. N. P. 1. Ores--Processing 2. Molybdenum--Separation 3. Sterilizers--Performance Card 2/2 T!5 0 ols, Is J3 -4.z Hh. . 9-.- al Pai- 4 V ~11 Op. all J414 ON.4 i m 2 v "a I'a it 3.0 AS. 'a R.- a 1:31--, 5. 01 .4.r *op, 0!1-4 d!Z '21 a a !!:a So. JIM Efl 73. 0 v3qj , . '.~p a I i OP ON a V Vol lip 0 0 43 A_, 0 am . .1. z "a UO a UP d ;.?JO 4A lot 1 ov a - u , C. 01 As a. ].3 i. go fit 1119 J '.4 SO a' "a J~v d-d-4 [~. .0 -0. "-a "n 00 a '~R '2 9 S MM3 j'63 /000 iOl 2 /04 38/04 38 12L90 Abs N. N.; Perlov, P. M. ;i!roclav-soda pro(-css For ~he- treatment of the enrichment products '.) r ~! s SOIL-4CF: Tr. 4 Nauchno-takhn. sessii in-ta Mekhanobr., 1958. L., 1961, 342- i-s. 4(A)--'0-19 ~U~~tefy refi-ninr,', tungsten motybdenum separation, turigsttn ore, h k.; ebnerite, scheelite. ferberite, soda entraction ___!aF'O'rW -Stu t e- ata-g-ev--d TIRANSTATTON: Th6~ bjj~_ 4~ F-.orm the W-containing minerals echeelite, ferberite, huebnerite and -F tn'e "i-I-tion tf the amount of of the 8t,)IchIomc-tl-'Ic. e-xcept that rhAre was poor _XL14LLIQu Wi Lnt:-, ,I- j) 4 4,_:~ W was also achipved of ~-nl, rij cf- ''.'ie amoun,'. Addition tilt, c'? )Sllmip! i in , Alc;ng the treatment ')f W_.'MO )1%. ~Zw: AR3010292 c es , Mo was removed from the solutions by the sulfide method; the pH of and to a lesser extent the Mo concentration and the MO:W ratio, :j 'nave a decisive efZect on the separation of W and Mo. An industrial worked out for the att-1clav-soda treatment of tungsten pro- -ttveyav SUB CODE: :12iti- MSLENITSEY, N.N.; LEONCHMOVA, Ye.T. Interrelation of nickel and pyrrhotits in sulf*A coppu-nickel. ores. Obog. rud 7 no,2:21-23 162 (MIRA 16-;4) (Pyrrhotite-Amlysis3 (Nickel-Ana*sis) FILIPFOVAp Nina Aleksandrovna; I=IXOJLAI., kand. tekhn. nauk, retsensent; AFMLOCELISKAYA, M.S., red. izd-,wa; DOBUZHINSKATA, L.V., tekhn. red- (Phase analyste.of nonferrous metal ores and the products of their procossing] Fazovyi analis rud +.4vetnykh metalloy I produktov ikh pererabotid. Noskva,, Metaillurgisdat, 1963. 211 P. IMIRA 16:8) (Ore dressing) PLOTNIKOVAI. Yo. N., assistant; MASIMMA, A. M., vmch P~mctional characteristics or anom-Hes or the maxillodental system according to data from physiologic masticatory tests and mastication graphs. Trudy KCHI n-o.2:215-220 160. (KIRA 15:7) 1. is kafedry ortopedicheakay siomatologii sav. kafedroy dotsent, M. A. Solomon(m. (MASTICATION) il-A 0, HIP alp, I im 9 10 :3 1 Hill 6 0 R - r, Be 0 V%P i I Ski 10 F- h a ti C.. 0 ig SIR --a na-must 'nu-M, mr.r MIZ 0% ACC. NRs AR64D2652.3 SOURCE CODE; UR/0372/661000/004,/GG08/9008 AUTHOR: Pqchenen V. L; Maslenko. Ye. A. TITLE:' A method of engineering c~lculatJod of nonlineai a$omatic systems SOURCE. Refe zh. Kibernetika, Abs. 4G63 ti M zh ed -IREF SOURCE: jkvtomatiz. proiiMO'protsessov v mashinostr.' i priboros a v resp.- iiauchno-tekhm ob., vyp. 2, 1965, 12-18 TOPIC TAGS: nonlinear automatic control system, harmonic oscillation, servomotor, friction ABSTRACT: An approximate graph-analytic frequency method of determining the parame ra -of jhe natural oscillations of nonlinear systems is proposed. The method is based on the harmonic balance method. The stability of the derived periodic solutions is investigated. Further, the article presents an example of the determination of natural oscillations in a sy4tem mith three nonlineariUas which are determined by backlash in the transmission from the servomotor to the control unit and by dry friction in the servomotor and mcasurlng-ampU- fying element. 4 illustrations. Bibliography.of 4 titles..V. S. [Translation of abstract2 SUB CODM. 09 UDC:.A,-601.3. Card K&Muroil W__ - kandidat takhnichsoklkh n&uk; BURKOV. V.L. redaktor; I.MOVA,,A.P., tekhaicheekly red&ktor. [Production of crate boards. staves. and lathes In lumber camps] Prolsvidstmoternol doshchachki, kclepki I drant v losproukhosakh. Mosicia, "elesbunisdat, 1953. .74 p. WU 7:12) (lumber-) (Lathing)(Staves and stave trade) 2UULM, 149, redaktor; MILWKO# LoAe, radaktor; ..UV71. mero. toldmichesidy r9daktor, [Bingle-chaln wood-splitting machines and their operationj Odno- teepzWe drovokollmye staidd I mbota ne. nikh, Moskva, Ooslesbum- iz"tt 1=615 P. (KM 8:3) ring-mackonery) A-PAVASIYU, F.S., kandidat takhnicheakikh nauk; KASLENIOT. P.N. Trandidat, takhnichaskikh nauk. retsensent; KAKOVSKIT, N. chankikh nauk, redaktor; TINHONOV, A.Ta., teirchnicheekly redaktor (Designs of woodworking tools] Ironstruktoif derevoobrabatymin- shch1kh stankov. Nookwa, Gas* nauchno-takhn, izd-vo mashlnostrolt. I sudostrolt.-Itt-ry. Vol. 2. (Spectalized tools] Stanki qmtslalt- sirovanWe. 190,443 P. (mm ?.-10) (Woodworking nachinary) AFANASIYL7. Pavel Some novich. jAnd. tekhn. nauk.; MUZHOS. P.M., prof..doktor takhn.nauk, retsenzent.; NASLIUM -F.U..insh., retsonsent,; TSHILVSKIY. A.r.. insh...-r~:- T AN adT. ~-FR~" TtWA. L.G.. idd. Idd-va. TIKHMOV. A.Ts. takhn.red. [woodworking machinery] toustruIctaii derevoobrabatyvaiushchik,h Eitankovo Moskva, Goo. nsuchno-'tekhn. Isd-vo mashinostrolt. lit-ry. vol. 30 (Installation,.repair,,and operation] Nontash, remout i ekspluatateiia. l958. 566 p. (KM 11:12) (Woodworking machinery) SIHOTOV, 1.1.9 dote.; SIROTOV, V.I., inzh.i. MTY.NXOV, F-U.-t dots'.; STUPMV.. G.K.9 afitsialfrgy reteenzent; SULMOV, A.N.9 red.; PIESKOv U.P.0 red.-izd-va; SHIMOVA, R.Ye., tekhn. red.; 'MMEISHCHICVA 'V.I.# tekbn. redo (Forest ex~16it&Uon]l.~soakopluatataiia. Moskva.-Gosleabum- izdat, 1962. 359 pe (KIRA 15:3-1) 1. Direktor Krestatskogo. lesoprob7shlewwgo khozvaystva TSentrallno nauc isaledovatellskogo instituta mekhani- zataii L eharget leanoy proc7oblennosti (for Stupriev). (la=boring) STOGDV., Boris Nikolaevichs dots.; SIROTOV# Ivan Ivanovich#,dots.; dote.; SHALAM, S*Aop Its- Font ;;PITERMAN,, Te.L.9 red.izd- va; SHIBKOVA, R.Ye., tekbno redo, [T9cbno3zgy*:*echanization,, and planning of the landings of lumbering enterpriseelTekbaologliap mekbanizataiiq i proekti- rovanle nishnikh sklimby lososagotovitellrqkh, iwodprliatii. Moskvas, Goolesbumiulat, 1962. 44 PO (KIRA 15 s 11) 1, Direktor Oleninskogo lesopivagablennogo VW3Wsystira TSento- rallnogo nauchno-iooledovatellskogo instituta mekhan12ateii i. energetiki lesnoy proaWshlemosti(for Shalayev). (IA=berIj3g) "New mechanization and organization of the gallery entrance in drilling tunnels in solid and very-:solid-ground.!! p. 29. MApparatus for luminescent analysis of fruits and potatoes." P. 34. "Innovation in the work of construction long-distance electric lines with high and low ti 35. Vol. 5, no. 3/4, Mar./Apr. 1954, Elektroenergiia, Sofiya SO:. Eastern European Accessions List, Vol 3, No. 11, Nov. 1954, L.C. ,"Methods and conditions for faster drilling of tunnels for water-power plants." Vol. 5, no. 5/6, Yhy/June .1954 p. 7 92ektroenerglia,, Sofiya. Eastern European Accessions List, Vol 3, No. 1-1, Nov. 1954, L. C. MASLEENKOV, I. I "Overexcavation of muck in construction of hydraulic tunnels." p. ? (Elektroenergila) Vol. 8, no. 7, July 1957 SO: Monthly Index of East European Accessions (EEAI) IL. Vol. 7, no. 4, April 1958 AUTHOR : Maslenkov M Yu (Engineer). TITLE : go-creirnis-atio-n- of (diesel) engine 8A,P30/50- (Modgnizatsiya dvigatelya 8 A? 30/50) - 114-wT-22 14 FERIODICAL: "SnergomashinostrozeniYe" (Power Machinery Construction) 1957 No-7, V01031- pp,33-36, (U.S.S.R.) ABSrRACT Since i948 the ".Russkiy dizell" works has been making en- -gines of the families A and AP 30/50-with outputs of 400, 600 and 800 h.p.'at 300 r.p.a. which hava been widely used. The most extensively used are models 6 AF 30150 and 8 A?30/50 which are used as the main engines in ships vith direct drive-of the screw. Engine AP-30/50 is two-stroke, trunk type, compressorless reversing engine,working on solar oil or diesel fuel. The prin- cipal data of engines-A and AP 30/50 are given in Table 1. Engines A and"Af 30/50 are simpler and convenient in operation and repair and cheap to.produce. They are very reliable but they have a number of defects suc4 as the appearance of cracks in the pistons of engines made befote 1951, contamination of the lubricat- ing oil system by fuel and high wear of the universal joints of the lubricator drive and various other defects. Therefore, the Russkiy dizell works, in 1955, worked out a project of modern- .1 isation of engine 8 AVL30/50-2, a general view of which is given 1/3 in. Fig.l. A most important item in the modernisation is the introduction-of oil cooling for the main pistons. This makes the Modernisation of (diesel) engine 8 Ai~ 30150. (Cont.) 3a4/7/3.e/i4 engine more reliable and^affords the posiibility of'increasing the output of the engine by increasing the speed and using super- charging. The construction of pistons with supply of cooling oil through the. crankshaft And- connecting rod is illustrated in Fig. 2. The use of oil cooling made it possible to reduce the temperature of the piston head from 600 - 635 C to 400 C. The piston rings and particularly the oil control rings were altered and are now of longer life. With the introduction of piston cooling a greater quantity of oil is required and the output of the oil pump, filter and cooler have been increased. The design of the super-charger pump, illustrated in Fig.3,'has been considerably altered. The driving mechanism of this pump has also been simplified and im- proved. The compressor cylinder, which is little used, has been removed from the engine, which simplifies servicing and improves reliability. The governor has been improved. A new main starting valve has been.designed and is illustrated in Fig.4. It is more reliable than the previous design. in order to cut down the time required to approve the modernised engine as a whole, most of the parts were tried out for considerable periods in standard engines. 2/3 The complete modernised engine 8 AP-30/50-2 has been tested for 3000 hours including an 800 hour acceptance test and this Modernisation of (diesel) engine 8AP30/50--(Cont-) confirmed the reliable oberation of 'the irarious mo&riised parts. The main parameters of the engine, which are tabulated in Table 2, were of satisfactory stability. The operating economy of the engine has been improved. The fuel consumption has been reduced by 4 grams per horse-power hour and is on an average 178 grams per horse power hour, the oil consumption has also beEnreduced. The works has now turned over to regular production of the modern- ised engine. By increasing the speed of the modernised engine to 375 r. in. it can develop 1000 h.p. With the use of super- char using the energy of the exhaust gases and relatively ,Silt pressures of blowing air, the engine power can be in- creased to 12~O - 1300 h.p. The factory is carrying out work on the application of a closed cooling system for the engine using fresh water. The closed cooling system is particularly effective on the modernised engine which is capable of using cooling water with an outlet temperature of 70 - 80 C. The fuel consumption is 3/3 then reduced bY 3 - 4 grams per horse power hour. 114-7-29/3-4 There are 4 figures, 2 tables, no literature references. AVAIIABLE: BOV/126-7-1-20/28 AUTHORS: Maslenkov, S.B., Skako~ir, Yu.A. and Ya-S. Umanskiy TITLE: ~Structural Chang in Aluminium Bronze Under the Action of Cold Plastic Deformation and Annealing (Strukturn-y-ye izmeneniya V alyuminiyevoy bronze pod deystviyem kholodnoy plasticheskoy deformatsii I otzhiga) PERIODICAL: Fizika Metallov I Metallovedeniye, 1959, Vol 7, Nr 1, pp 137-141 (USSR) ABSTRACT:.The structural changes after deformation and annealing of monophase aluminium bronze containing 6.02 wt % (17.1 at %) Al (alloy 1) have been investigated electron-optically and byX-rays. In order to solve auxiliary problems of the investigation an alloy known to be two-phased, containing 12~wt % (25.0 at A) Al (alloy 2), was cast. The ingots were hot forged and were given a homogenizing anneal 1 at R)CP (9009C, 10 hrs). After annealing alloy 1tnB*q,rd that a = 3#6451,m kX; this.result, as well as that for the lattice parameter of the cK-phase In alloy 2 (a = 3.652) agrees well with data on the relationship a w f (at % Al) Card 1/4 (Ref.6). Thus alloy I is in the monophase cK-region of SOV/126-7-1-20/28 Structural Changes in Aluminium Bronze Under the Action of Gold Plastic Deformation and Annealing the:existing constitutional diagram. According to eleatronographia data (Pig.!& and Table on p 140) the lattice parameter of the face-centred cubic solid solution of a specimen of alloy 1, annealed at. 60000, is 3.75 kX. Anelea.tron mi,ciosoope analysis has shown that in this spqoimenothere are,, In the vicinity of the grain boundaries, micro-sootior,, having regionsrising above the surface cf the a width of 0.3 to 0.4 micron4 which are difficult to etch.(Fig,2_a). These regions represent a solid solution (cc')` with an Increased concentration of aluminium and Possible other impurities. Comparing this result with the known,x*elationship a = f (at'% Al), it-ean be assumed that the doncentration of aluminium in the grain boundary regions of the solid solution is close to the composition of the I Y-phase. Deformed specimens give different i diffraction pictures, according to the etchant used. After! etching4n aqua regla, a system of lines of the ot solid solution can be seen in the X-ray pleture,-having a sharply Cal~d 2/4 defined texture. (Fig.lb). Etching in a mixture of alkalis SOV/126-7-1-20/28 Structural Ghangesin Aluminium, Bronze Under the Action of Cold Plastic Deformation and Annealing leads to the appearance of a system of diffuse lines, ~instead of textured ones, in the X-ray photograph (Fig.19). The interplanar disit-oances are close to those given for the Y.-phase ('see Table). The eleetronographio data on the appearance,of the y-phase as aresult of cold deformation are in agreement with the photomicrograph shown in Fig.2b. On the basis.of microhardness tests after 30 minute. annealing at various temperatures (Fig.3a), the authors have chosen.for their further investigations a temperature ~range-of. 275-3000C for annealing. Annealing at these temperatures leads,to a pronounced ordering effect. Micro- hardness measurements after various annealing times at 27500.~(Fig.3b) have shown that the hardness of the alloy is not fu117 removed after very lengthy soaking (up to 100 hro). Structural changes on annealing consist, firstly, in'.anincreased struotural.non-uniformity, and in an increase n e i"s ofthe -~ -phase. This is evident from the micro- t, i strueturea'.-In Fig.2( new slip lines are visible. These are regions in which the. y -phase, or the-solid solution of Card 3/4 increased aluminium concentration, has separated out. SOV/126-7-1-20/28 Structural-Ghanges'in Aluminium Bronze Under the Action of Cold Plastic Deformation and Annealing Secondly,.a basic change in the fine crystalline structure ..of the solid solution occurs. The lattice parameters of the at-soiution in specimens which have been aged for up to 106hours at 2750G, as well as for 5 hours at 32-5- 35000, differ negligibly from the lattice parameter of an undeformed specimen. There are 3 figures, 1 table and 6 references, of which,5 are Soviet and 1 English. ASSOCIATION: Moskovskiy institut stali (Moscow Steel Institute) SUBMITTED: April 1., 1957 Gard 4/4 28 (09 18 (7) AUTHORSs Netuling G. V.,,!aslenkpTj_S. B,_ SOT/32-25-9-22/53 TITLEs An Investigation of the Structure of Fractures Under the slociron. Nicroscop* PERIODICALs Zarodskaya laboratoriya, 19599 Vol 259 Nr 99 Pp IOBT-1089 (USSR) ABSTRACTs In the case under review impressions out of carbon (4 fs 3t 4) were used for examining the structure of fracturle (F In alloys@ ; The carbon was applied in vactium of at least 10 -It mm Hge The carbon film w4m removed by electrolysis with &'current density of 0-5-1 a/cla'. For steel an sloatro4te (75 9 of potassium chloride, and 5 9 of citri o acid I in I Ii *or of water) md for the nickel alloy an electrolyte (3-5 e NaCl, 3 g FoSO 4 ~ 10 ml R so in 100 ml. solution) were used. The (F) of 20KhG2 steel 2 4 and of nickel alloy were examined. Comparison of the micro- hotographs obtained (Figs 1-3) ahowe'that the structure of the . of the nickel-base. casting alloy Is Ina ft details different M from-that of the steel fractures. Thin in attributed to the fact that the alloy is cast and the main component of the alloy has a kind of or3(stal latticedifforent from that of steel. Card 1/2 There are 3 fiaures and 4 references, 1 of which is Soviet. An Investigation of the Structure of Fractures Under SOV/32-25-9-22/53 the Electron Microscope ASSOCIATION. Tsentrallnyy nauchno-issledovatellskiy instit74* chernoy metallurall, (Central Scientific Research Institute for Ferrous Metallurgy) Card 2/2 BSTULIII. G.V..;~K&SLA=. S.P. Studying.the fine structure of fractures in heat-resistant alloy*. Issl. po sharopr. oplay.6:314-317 160. 131-9) (Heat-resistant alloys-Metallography) S/032/60/026/009/004/018 BO15/BO56 AUTHORS: Maslenkov, S. B.9 Dqmkin, Yu. I. TITLE: Methods of the Metallographic Investigation of molybdenum PERIODICAL: Zavodskays. laboratoriyal 1960, Vol. 269,No. 9. p. 1093 TEXT:, Anew.nothod. of visibilizing the.molybdenum structure is describ- ed, After haying,~besn.xeohanically polished, the metal surface is elea- ~trolytically,polishsd.in an electrolyte41th 95 ml 9 SO + 5 ml methanol 2 4 at 144. The'sample-is then rinsed in water and etched in.a solution of the following cbmpbsition;-,10 g'KOHY 10 g K p9 3- (CN)61 100 ml H20. For cast sampl*st-the etching takes 40-50 seo,, and 90 seo for sintered ones. The method produced-~good results for cast.and forged,molybdenum samples (Fig. miqrostructure)#' an well as for samples produced by powder metal- lurgy. The'tiz*-riiquirsd for visibilizing the structure could be re- duced to'15-10 min. There are 1 figure and 2references: I Soviet and I us Card-1/2 3/032J60/026/009/004/018 of Molybdenum B0151BO58 ASSOCIATION: Teentralinyy nauchno-ifisledovatel Iskiy institut chernoy motallu"rgii, im. It P. -Bardina (Central Scientific Research fnatitute of Ferrous Metallurgy imeni.I. P. Bardin) methoIdo of,the,Mot.allographio Investigation Card 2, 34552 ,/61/007/000/041/044 S/659 1114 D205/11303 AUTHORS: --a1PpkQ&m.AeA4p.and Estulinq G-V. TITLE: Investigating mosaic structure changes on the ageing of nickel alloys SOURCE: Akademiya nauk SSSR. Institut metallurgii. Issledova- niya po zharoprochnym splavamg V. 7, 1961t 342 - 348 TEXT: The changes of the physical and mechanical properties accom- panying the decomposition of a supersaturated solid solution were investi atedo Alloys on a Ni base alloyed with Al (I)y Ti (II)p Cr Al MI), Or and Ti (IV) were investigated. These alloys also contained minute amounts of Fe and So The alloys were smelted from pure naterials in an induction furnace of 30 kg capacity. 4 ingots of each composition were prepared and forged at 120000 into 20-mm diameter cylinders. Rings of v7 mm thickness were cut and used as test specimens. The specimens were hardened by heating at 11500 - 120000 for 5-8 hoursp etched with 1 : 1 HC1 : H2 029 electropolished on one side and annealed in the presence of titanium hydride at Card 1/3 S/659/61/007/000/041/044 Investigating mosaic structure D2o5/D3O3 10-2 mm Hg total: pressure. X-ray diffraction patterns were taken at not more than 600 imp/min while the specimens revolved at 60 rpm. The reflection intensity from the (111) planes was measured. The ageing was performed at 6000Y 7000 and 8000C for periods of 0.25 to 50 hours. Along with the intensity changes, changes in the hardness were also measured. The ageing of all 4 alloys resulted in strength increase. The changes of both the intensity and hardness depend upon the ageing temperaturet but are not parallel. Thus, the intensity of reflection does not always increase in the initial stages of ageing as..does the hardnesso At relatively low ageing temperatures the strengthening is not accompanied by appreciable changes in t* mosaic structure which contradicts the data of Pivo- varov et al (Ref. 7: Nauchn. dokl. ryssh. shkoly, no. 49 1959). Ti hinders the change in the mosaic structure and gives finer grain before,and after ageing treatment as compared with Al. Introduction of Cr levels off this difference in the influence of Al and Ti~ Strength of the samples, corresponding to the same development of mosaic structure attained at high- and low-temperature ageingg dif- fers since the strengthening is related to the amount of the second Card 2/3 J( 8/659/61/007/000/041/044 Investigating mosaic structure D205/D303 phase and the degree of dispersion, The ageing of the Ni-Cr-Al al- loy was similar to that of the Ni-Al alloyp but the change in the substructure was less pronounced. The Ni-Cr-Ti alloy showed similar ageing, to that of Ni-Ti, the process being slower. It is concluded that the strengthening during ageing cannot be ascribed to the chan- ges in the mosaic structure alone. The contribution of Ya.S. Umans- kiy to the field is stressed. There are 4 figures, 1 table and 17 references: 13 Soviet-bloc and 4 non-Soviet-bloc. Card 3/3 S/032J61/027/001/013/037 B017/BO54 AUTHORS: Maslonkovq S.. B. and Deakin# Yu. I. TITLE. In=est1gaMnof Molybdenum Fractures by Parallel Electron- microscopic and Microscopic rixaminations of Film Replica of the Destroyed Surface PERIODICAL: Zavodskays. laboratoriyat 1961o Vol. 27, No. it p. 62 .-TEXT: Film replica were separated from the fracture by a solution of 25 ml of H so in 175 ml of methyl alcohol. A chrome nickelilamina was 2 4 ,Used as- 'Cathode. Samples were etched for 20-35 sea, and films wore. separated:by inaressing the voltage from 2 to 14 volts- Molybdenum fractures showed atranscrystallins 'character under the light microscope. ASSOCIATION: Tsentrallayy nauchno-isoledovatelinkiy institut chernoy metallurgii (Central Scientific Research Institute of Ferrous Metallurgy) Card 1/1 40988 S/659/62P9/=/023/030 I003/IM3 AUTHORS: Krylova, A. P., Madenkov, S. B., Fa4 Zharkova, D. N. TIT LE: The kinetics of oxidation and the structwe of oxkta of some industrial heat-resisting alloys SOURCE- Akademiya nauk SSSR. Institut metalturgii. Issledovaniya po zharoprochnym splavam. v. 9. 1%2. Materialy Nauchnoy sessii po, zbaroprochnym sptavam (1%1 g.), 162-164 TEXT. The purpose of this work is to investigated the kinetics of oxidation and the phase composition of the oxide layers formed on the surfaces of 3K-813, and 311-835 stools and of 3K-559A and 3K-652 alloys when they are heated in the air from I to 100 hours at 900*, 1000*, 1100* and 1200*C. The high corrosion resis- tance of these alloys is due to the formation of oxide layers of the spinel type on their surface. The EI-813 and EI-835 steels have a high heat-resistance up to 1000-1050*C due to their high chromium content. The authors refrain from explaining all the experimental data obtained as they consider their investigation to be unfinished. In the discussion, Prokoshkin D. A. pointed out the inconsistency of the data on the position of the Cr,203 layer, There is I figure. Card 1/1 39762. S/126/62/ols/oWoo6A18. 9193/9383 AUTHORS: Maslenk Y. S-13- and Estulin, G.V. 'Le TITLE: The effect of heat-treatment on the properties and variation in the fine structure of a nichrome-base heat-resistant alloy PERIODICAL: Fizika metallov 1 metallovedeniye, ve L3,, no. 61 1962, 869 ., 874 TEXT: Lack of direct experimental data on the relationship betwden the strength of metals and alloys and the m saic structure 0 as well as anomalous dependence of the creep strength of the alloy X20"80T (Kh2oN80T) ("Nimonic 80") on the.solution-treatment tempekature prompted the authors to undertake the present investigation, in the course of which the effect of heat-treatment (quenching followed by ageing) on the fine structure and mechanical properties of alloys of this type was studied. The code marks and chemical.analysis of the exporimont,al:alloys are given in Tible 1. The experimental specim*nss- cut from hot-forged rod, were held for ~8 houis at 1 030, 1 080 or 1 130 QC,_water- orair-quenched and* then' aged at ~'700.or.750 OC for..,various perl6do. One face of Card 1/# The effect of heat-treatment..*. S/126/62/013/0o6/oo6/oA 9193/Z383 each specimen after quenching was descaled and electrolytically polished and since the dimensions of the block of the mosaic structure of quenched material were large, their variation during subsequent ageing in vacuum could be studied by deter mining the intensity of low-angle scattering of X-rays. The ratio where I is the~intensity of scattering from specimens.studied, and IM03 is the intensity oficattering from a specimen deformed plastically by polish1mg and chatacterized by the smallest block dimensions, Was-taken as the relative measure of the block dimensions. In addition, the microstructure of 'alloy A was examined.wLtht`hs aid of an-electron microscope, .,creep tests -were carried out at 700 '~C under a stream of 30 k rdness miasurements were taken and the 0.2% proof S/GVj2, ha -treatments Web ddt*rMLfi~dG stress of alloys after Various heat The results for ailoY aLA43?A (91437A). are reproduced in Fig. 1, where 1/1 hardness (HS)'and 0.2% proof stream Card 2/# 5/126/62/013/oo6/oo6/018 The effect-of heat-treatment.**. W3 Z193/ 2 0., kg/mm are plotted against time (hours) of ageing at 0.2 750 OC (circles) and 700 OC (triangles), graphs a, 'G and B ..relating, respectively ., to material quenched from 1 030, 1 080 and-1 130.0C. The results 9f creep tests for the same alloy are 8xven In Table 3.' Several conclusions were rea6hed. 1) Theroom-temperature strength of alloys of type Kh20NBOT .in the age-hardened condition depends mainly on the quantity and e of dispersion of the second phase 9i (Al, TI). egre A 2) The resistance of the alloy to plastic aeformation and fracture at elevatqd temperatures depends not only on the degree of homogeneity of the solid solution and on the quantity and degree* of disprsion-of the second phase but ' alio on the mosaic structure of the ma*rix;- the lower the block dimensions the r ter sh6uld b the high-temporatuke strength of the alloy. 9,ea e n in the mosaic stru -hardening 3) The variatIo' ature during age depends both on the initial state of the matrixand on the composition of.the alloy@ The results of age-h.ardening can be esence of small quantities of considerably affected by the-pr Card 3/0 5/126/62/013/006/006/018 The effect of heat-treatment,*... 9193/9383 elements such as B, Ce or Nd. There are 2 figureis and 3 tables. ASSOCIATION:- Itiatitut kachdstvennyk4,sta1ey TzNIIChM (InAtitut6 of High-grade-Steels of TzNIIChM) SUBMITTED: July,.21, 1961 Table 1 (pac-1-i nomin 1 17' ------ B. Nd Allay Cmian C S1 Mn Cr 8 P Al T1 Fe 3H437A (A).-, 0,03 0,13 0 28 20 0 005 0 001 1,1 2.68 0.46- 3H4375 k8) 0,06 0,3 0:126 20,2 0:005 0:005 0,86 2,55 0,63 0,01 30437+Nd (C~ 6,08 0.05 6 OW .20.8 0.,006 0,001 1,,2-' 2.,63 0,21 .0'1 (ONC4) Card MASLENKOV,, S. B.; MOLOTILOV,, B. V. Microwave T~ray spectroscopy of Fe-AI-C anoys. Piz. mt. i metaUoved, 14mo.4:03-635 0 162. (MIRA, 15:10) 1. Institut kachestveWkh staley i Institut pretsizionnykh splavov Inntituta noroy metallurgicheakay tekhnologii imerii I. P. Bardina. (Iron-alimimm alloys-Notallography) (X-ray spectroscopy) I- -- ~ .-- - - - ir- ---. - - - - - S/032/62/02e/012/003/023 B124/BIOI AUTHORSi Maslenkov, S. B., and Yegorshina, T.' V. TITLEt Application of microspectroscopic )I-ray analysis in metallo- graphic studies PERIODICAL: Z.avodskaya laboratoriya, v. 28,.no. 12, 1962, 1443'- 1446 TEM A device developed by R. Castaign (Rech. A6ronaut. 23, 41 (1951); ONERA, 55, 10952)) was used for the microspectroscopic analysis. Castaign's microprobe was used to study the dendritic liquation of sili- con in 55C2 (5532) spring iron (3-5 tons) containing 1.66~~ silicon. The liquation degree is very high in the axial- part where the dendrites are especially large; the ratio between maximum concentration in the inter- axial region and minimum content in the axes is 2.0. Vihen the steel is rolled, regions of low and high silicon concentrations appear in the form of thin bande which# after homogenized annealing for 12 hrs at 1200 0 C, at some places leave a broadq blurred band. Data obtained by X-ray spectrum analysis on the distribution of nickel in the digfusion layer resulting after.5-hr boration of metals and alloys at 900 C, were in good Card 1/3 S/032/62/028/012/003/023 Application of microspectroscopic B120101 agreement with 0the data calculated. Examination of 30811 (EI811) steel heated to 1100 C showed redistribution to occur between the cz-phase and T--phase of 24.4 and 20.7%, Cr and 4.47 and 6.85% Ni, respectively. The change in composition of the solid solution and phases separating on the ageing of alloys were investigated. -:)A 726 (E1726) alloys were studied in the initial state and after 20.000-hr ageing at 7000C. In the initial state, only an excess phase (phase I) can be seen on the screen, whereas after ag-eing small and large bMsh segregations (phaso II) appear. In- solid solutions, age-ing causes a cLecrease in tungsten and niabium contents owing to the precipitation of an intermetallic phase with a high content of these elements (phase II) An W-type lattice was determined by A-rqy Fe2 analysis. Phase I containing 71~u Nb appears to be a niobium nitride or niobium carbonitride. Carbide contains no tungsten and does not change its composition even after long-time ageing; other carbide-forming elements are probably not contained in niobium carbide. In the Fe-Cr-Ni alloy type :)M 767 (141707), primary carbides form a solid solution of titanium mono- carbide and tungsten monocarbide (551/; Ti and 201/k W). The X-ray spectrum analysis showed that the cubic Ni 3(Mo, Cr, W) 3G is deposited alon g the Card 2/3 S/0 3 2/62/0 28/012/00 3/023 Application of microspectroscopic ... B120101 grain boundary on ageing of complex alloys. There are 3 figures and 2 tables. ASSOCIATIONt Tsentrallnyy nauchno-isoledovatellskiy institut chernoy metallurgii im. 1. P. Bardina (Central Scientific Research Institute of Ferrotis Metallurgy imeni I. P. Bardin) Card 3/3 (Caot iron-Astallography) MALINOCHKA, YA.M.; MASIENKOV, S.B.; YEGORSHIMA, T.V. Investigating the dendriticliquation of silicon.in spring steel with the htlp of an electronic probe. Stall 23 no.lOt937- 939 0 163. (MIRA 16sn) 1. Institutchernoy metallurgii v g. Dnepropetrovske i TSentrallnyy nauchno-insledoiratellskiy institut dhernoy metallurgii. MASLENKOV. S.B.; YEGORSHINA, T.V. Using the X-ray'spectroscopy for the study of metals in micro- volummis. Sbor. trud TSNIICHK no.35tl54-163 163. (KMA 17:2) 1(.il(,rlLg after ,;~-.!.ur:jtp-m bv chroqi!um fiu ring rapid hf-al im, Z , Ch-c-nn-va meLallurg-,v:i !w. 6 -or-itin) diffusi(~i S chi u steel ufi!isson of chn"Ilp;f1i 1-1 10.2 C) urldl.1- varying con(-n! tm~, lw:i~; . . - ~ 4*. I,.: ., NTj: AP4049073 n . - :.. ~w.;.Lion with the chro-nium wis in-poniouS to iliLr,.c - cid. -',! *!o dO ~ :'.,! - I - 2 -_ - - Cord 2/2 BUROVA, N.N.; MASLENKOV, S.B.; ESTULIN,, G.V. [deceased) Studying the nature of niobium and niobium allay layers underlying scale. Piz. met. i metalloved. 17 no.6098-902 je t64. (MIRA 17:8) 1. Institut kachestvennykh staley TSentrallnogo nauchno- issledovatellskogo instituta chernoy metallurgii imeni I.P. Bardina.