SCIENTIFIC ABSTRACT NIEWODNICZANSKI, H. - NIFANTYEV, E.

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• Collection: Scientific Abstracts
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• Publication Date: December 31, 1967
• Content Type: SCIENTIFIC ABSTRACT

OMM
A
POIAn/Optics - Spectroscopy K-7
Abs Jour Ref Zhur - Fizika, No 3, 1958, No 7024
Author Les F.
.. NteVo4niczan ki, H.
In8t Jayellonian LIniversity, Cracow,, Poland
Title Hyperfine Structure of the Forbidden Une CdI 3141A (5s2 lSO--
5s5p3*.
Orig Pub Bull. Aced. polon. sci., 1957, Cl. 3, 5, No 3, 2,.Qg-303
Abstract An investigation was made of the hyperfine structure of the
forbidden 3141A line in the spectrum of CdI. The source of
light was a Schuler lamp with hollow cathose. The spectral
instrument was a Fabry-Perot interferomater, crossed with a
quartz spectrograph. The microphotogram shows that the Line
consists of a single component. This is in good agreement witb
the Bowen theory (Bowen J.S.j, Reviews of Modern Physics, 1936,
8, 58) according to which the transition with J 2 is due
to the interaction of the magnettic moments of the electron
shall &ad of the nucleus. Cadmium was used with a natiu-al
isotope content; 74.9% even. Since all the even isotopes have
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(F-j:- ln.3tylt,
L~J)-)rato,-'-)w B;id~:,,iczyc~ Frzerry-31-.1
Y-),ithly List of ~t n-,

PCLAVP/Optics - Spectroscopy. K
Abs Jo X Ref Z2i--,r Fizikm, No IC, lqc1q, 236,z4
A t" Liszka, L., Ili ewod.,ic za.,.oki, H.
1-st J--6ic',l 'J..ivergity, K,-ak,,w, Polai,d
Title Liteisity Ratir, in te "F~rlAdde. ' 11,oublet a i,-A
N2927 A. V - li-.- t1 c Spectri m of Atordc Ozyge-
Orig Flub Acta phys. pc~io.i., 1958, 17, No 5. 345-351,
Abstract A st day was .nde zjf tLe i-.te.-,sity ratio of t,-.e li-es :~f
the forbidde.i doolet 01, corvespoi.di;ig to tlie tra si-
tions --S 3P ( A,) and !So ---. 3P2
X3 --- i ,\ ~ 29'72,2
2958.1 . T:ie fonier li-e, previo~,.sly disccvered;
correspo:lds to ma,,, ctic dipoie radiatio:-., while t.ie se-
c,D,id li-e, first D"gerved i.i this i.,vestippti c-reS-
po-.dg to electric q adr pole -adiati.D:-,. A specia.
shaped V,,bc -was developed for t;ie o'b9orvatio.. of tLis
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POLM/Optics - Tnstr,_,aeiLt9 for Optical jUmlysis. K
Abe Jour Ref Zhur Fizika, No 10, 1959, 23686
Author Kisiel, A., Niewodme A-~~
List Jagiellonian University, Krakow, Poland
Title A High Limiin6sity Quartz Spectrograph for the Far Ultra-
violet Regior 2300 ft-- 1850 A.
Orig Pub Acta PhYs. Polon., 1958, 17, No 5, 361-364
Abstract The a thors describe a prism quartz spectrograph of high
luminosity (1:1.822) for the-'far ultraviolet region (2300
-- 1850 71). The optical systeim of the spectrograph con-
sists of two plane-convex short-focus lenses (collimator,
f = 65.2 mm aad camera f - 87.7 rm.) and a Corni: prism
(length of base 47 rLm). To eliminate absorption of light
by the atmspheric ox-jgen, C02 is blown throug~i the ins-
trument; in this case the absorption for t\1860
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- 121 -

POUM/Optics - Spectr-.3scopy. K
Abs Jour Ref Zhur Fizika, No 11, 1959, 26io6
Auth,)r Lee, Z&, Mrs, Niew)dAcza-.1ski, ff.
List Ja,;ieIl-)nian University, Krak,~w, Foland
Title Intensity Ratios of Spectral Lines in CdI Triplets at
Different Conditions of Excitation.
OriG Pub Acta phys. polm., 1958, 17, go 5, 365-368
Abstract In vari3us s3urces :)f lidit (electrDdeless discharL;e in
va-,)Dr :)f pure cadnium ,and i~ri vapors -3f cadLLiuu in an ar-
-In or xenon atmosphere, a h.)llow cathode in the atws-
phere of heliur. or arGm, a spark, are, jr hi&i-frequency
dischar'-e) the rati:)s )f the intensities -)f the lines -;f
the triplet of CdI (5o86; 48oo, and 4678 R) are different,
depe;id jn the excitati.)n cLndIti..)ns in the source, and
differ in all cases fr.)m the the-,retical relati)a.
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:'OI,PdTD,/Iluclcar Physics - Inst-illlitioi,.s atid Instrw.,ci,ts. MethodsC
of Mcasure-Iilui,t and Researc.11
Abs J-)ur Ref 71-.ur Fizikan, lf~ 11, 1959, 24245
Author Niewodiiecz.~~igqlU,-Iieiirylt, Zakrzewscki, Jerzy
Inst
Tit~e Tl.a First "Large" CyciAr.)ii in P-ia:id
Grig Pub Priblemy, 1959, 15, TI, 2, -146-14g
Abstract Brief descripti3.,. and tecli-ical data.
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8

82713
.2~ 0
P104 60/005/001-2/008/008
A222%026
AUTHORt Niewodniczafiski, Henryk; Zakrzewski, Jerzy
TITLE: The First "Big Cyclotron" in Poland
PERIODICAL: Nukleonika, 1960, No. 1-~7 Supplement Nr.
TEXT& The authors present a detailed description of a cyclic reso-
nance accelerator ('first built by E. 0. Lawrence in 1932) built at the
Krak6w center of the In5tytut Badah Jadrowych PAN (Nuclear Research Inati-
tute of the Polish Academy of Sciences). Basic parts of the "Y-120" cyclo-
tron were furnished by the USSR according to an agreement on international
cooperation in nuclear research. The installation has been officially put
into operation on November 22, 1958. Chief contractor of the building con-
struction project, which started in the second quarter of 1956, was Zarzad
Budowlano-Montatowy (Construction and Assembly Administration) of Zjedno~ze-
nie Przemyslowe Budowy Huty im. Lenina (Industrial Union for the Construc-
tion of the Metallurgical Plant "im. Lenina"), while general supervision
was executed by Zarzad Inwestycji Badah Jadrowych (Administration of te"
Nuclear Research Inve'stments). Basic technical data of the cyclotron aret
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82713
P/046/60/'005/001-2/008/008
The First "Big Cyclotron" in Poland A222/AO26
diameter of electromagnet pole pieces - 120 cm; ineight of the gap between
pole pieces - 34.5 cmi total weight of the electromagnet core - 120 tons;
capacity of electromagnet winding at a magnetic field intensity of
15 kOe - 100 kw; stabilization of the magnetic field 0.03~-'; capacity
of h.f. generator - 120 kw; freauency of the resonance circuit - 9-15 mc;
frequency stabilization - 0.01%; voltage amplitude between dees - 150 kv;
inside height of acceleration chamber - 17 cm; effective edge radius -
52.5 cm; deflector voltage - 60 kv; energy of deuterons - 13 mev; energy
of particles - 26 mev; ion stream on inside beryllium window - 1 ma.
Gabarite dimensions of the electromagnet are 4.35 x 2.86 x 1.5 m. The high
vacuum diffusion assemblies are aided by cryogenic nitrogen-cooled traps
and capable of producing a vacuum of 5.10-7 mm Hg. Under operational con-
ditions, the vacuum in the installation is of the ordar i0-5 mm Hg. The
cyclotron draws 500 kw of electric power. The outlined program foresees
work on proper shaping of the magnetic field to make possible acceleration
of protons to 30 mev and more. The research program is mainly concerned
with stripping, especially with polarization effects relevant to the
phenomenono At present, research is conducted on the polarization of
neutrons evolved in deuteron stripping on 12C nuclei. To that end use is
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82713
P/046/6o/or),,/00' - 210081,008
The First "Big Cyclotron" in Poland A222/AO26
made of special equipment built by Zaklad II IBJ (Department II of the
Nuclear Research Institute), which consists of a proportional helium
pressure counter (about 10 atm) and proper electronic apparatus with a ten-
channelamplitude analyzer operating in coincidence with scintillation
neutron counters (Hornyak type) to establish the asymmetry of dexter and
sinister dispersion, thus determining the degree of neutron polarization.
Preliminary results confirmed polarization of neutrons from the reaction
12C(d,n) '~N for a reaction angle of 150 in a laboratory set-up. With a
view to further research work on these problems, construction of a magnetic
energy analyzer of neutrons evolved in the stripping reaction, and evading
under angles different from the deuteron beam is being prepared at the
Department. A number of advanced scientists of the Department were dele-
gated for practice to foreign research centers, among them two, who have
been working for 1 1112 years on polarization effects in the stripping
phenomenon at the cyclotron of the Nuclear Research Laboratory of
Liverpool University. There are 3 figii-res and 16 photographs.
ASSOCIATION: Instytut Badan' J~drowych PAN, Ohrodek Fizyki J~drowej
(PAN Nuclear Research Institute, Nuclear Phvsics Center)
SUBMITTED: May 1959
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P/045/60/019/02/01/013
B018/3011
AUTHOR: NiewodniczaAski, Henryk,
TITLE: Andrzej Soltan (1897-1959)
PERIODICAL: Acts, Physics, Polonica, 1960, Vol. 19, No. 2, pp. 125-131
TEXT: This is a detailed biography of the Polish physicist Professor
Doctorl Andrzej _~o-ff_a_ who died on December 10, 1959. A. Soltan was born
in Warsaw on November 25, 1897, received his secondary education in
Petrograd (Russia) during the First World War, and subsequently studied
physics at Warsaw University. Even before being graduated he was appoint-
ed assistant at the Institute of Experimental Physics of Warsaw University
and worked together with Professor Stefan PieAkowski. He was chiefly con-
cerned with spectroscopic investigations.. In 1926, he received the title
of Doctor of Philosophical Sciences. He spent one year in Paris where he
conducted studies on X-ray spectroscopy. After his return, he became known
for his de-zelopment of a new mercury lamp model. In 1933, he went to the
USA for I year (California Institute of Technology, Pasadena). Back in
Warsaw he continued his research work begun there. He worked together with
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Andrzej Soltan (1897-1959) P/04 60/019/02/01/013
B018YB011
Professor Ludwik Wertenstein and Doctor Jan Cichooki. Before 1938, lie
was Chief Assistant at the Institute of Physics of Warsaw University and
subsequently held the post of a director of the physical research labora-
tory of the Philips Works in Warsaw, During the German occupation of Poland,
he taught at an underground university. In 1944 he was evacuated to Vienna
with the factory. After the end of the war he returned to Poland and took
over the post of a director of the physical laboratory at the L6di Institute
of Technology. In 1950, he was appointed Corresponding Member of the
Polska Akademia Umiejetnos'oi (Polish Academy of Science and Letters) in
Cracow. In 1952 he became a Member of the Academy of Sciences in Warsaw. In
the same year he was appointed Director of the Laboratory of Radioactive
Isotopes, which was incorporated in the newly established Institute of
Nuclear Research in 1955. He also was Director of the Center of Nuclear
Research at Swierk. Besides other honorific posts he also held that of
President of the Scientific Council of the Institute of Nuclear Research
and was a Member of the Scientific Council of the Joint Institute of Nuclear
Research at Dubna (USSR). He attended numerous international conferences.
A list of the publications of this outstanding scientist is given.
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NIWCD?nCZAISKI, Henryk
Research activities at the Institutd for Nuclear Physics in
Krakow. Nauka Fol 9 no.l+:123-138 0--D 161.
1. Czlonek rzeczywisty Polskiej Akademii Nauk, dyrektor
Instytutu Fizyki Jadrowej, Krakow, ul. Radzikowskiego.

P/045/61/020/003/004/004
B133/B228
AUTHORS: Boiek, E., Niemodniczafi-ski, H., Ogaza, S., Szymczyk, S.,
and Norseyev, Yu. V.
TITLEi Energy levels in the 166 Er nucleus
PERIODICALs Acts. Physics, Polonica, v. 20, no- 3, 1961, 257-266
TEXT: In the present paper, some gutm&-gamma coincidence experiments in
the decay of 166 Yb are described, and a level scheme of 166 Er is proposed,
which is more complete than that given by Gromov et al. [Ref. 7:
Gromov, K. I., Dzhelepov, B. S., Pokrovskiy, V. N., Izv. Akad. Nauk SSSR,
23, 821 (1959) The isotopes of Yb were obtained by irradiation of Ta
targets with 610--Nev protons from the synchrocyclotron of the Dubna Joint
Institute of Nuclear Research (USSR). The measurements in Cracow were
began 1.5 to 3 days after the irradiations, which were performed in inter-
vals of about two months. In the first two runs, the measurements of
gamma radiation were made at different times for the decay analysis of the
entire spectrum of the isotope mixture of ytterbium. From this analysis
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Energy levels... P/045/61/020/003/004/004
B153/B226
it was established that the coincidence measurements for 166 Yb may be
carried out in the first week of measurements. In the next two runs,
gamma-gam-A coincidence measurements were performed. The single-count
gamma spectrum was recorded by a scintillation spectrometer using a
1 11211 X I" Sal (Tl) crystal, an FJU 6097 F photomultiplier and a
100-channel pulse-height analyzer. The resolution of this spectrometer
for the 661-kev 137C9 line was B.2%. The gamma-gamma coincidence spectra
were recorded on the multichannel pulse-height analyzer, gating the
spectrum from one counter with coincidence pulses from a fast-slow coin-
cidence circuit (Fig. 1). NaI (T1) crystals 1 3/4" X 211 and 2" X 2" and
EMI 6097 F photomultipliers were used. Resolution was 9% for the 137cs
line. The resolution time of the coincidence circuit was 2,r-5.5x1O_ 8sec.
The existence of an 880-kev transition reported up to now only by Brabec
et al. [Ref. 4: Brabec, W., Gromov, K.,Dzhalepow, B. S., Dmitriev, A. G.,
Morozov, W. A., Izv. Akad. Nauk SSSR, 25, 812 (1959)] is confirmed by the
coincid.ence measurements of the authors, but they could not find the 155-
and 522-kev lines measured by Baranovskif and, Pokrovskir fRef. 5:
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Energy levels ... P/045/61/020/003/004/004
B133/B228
Barau.ovskif, W. I., Pokrovskir, W. N., Izv, Akad. Nauk SSSR, 23, 819
(1959)). Besides a confirmation of the results of [61 (see list of
English references), the authors obtained the following coincidences:
between the 710-key line and the 460-, 710-1 790-kev peaks; between the
790-kev line and the 185-, 460-, 710-kev peaks; between the 1180-kev line
and the 680-kev peak; between the 1270-kev line and the 185- and 600-kev
peaks, and between the 2070-kev line and the 80- and 185-kev photopeaks. On
the basis of these experiments and the energy values of transit ons given
by Gromov et al., the authors suggest a new level scheme for 104r from the
decay of 166 Tm (Fig. 6). The branching ratios of transitions between the
levels with K-2 and K-0 are calculated on the strength of klaga's theory.
For the level scheme proposed by the authors, they are in etter agreement
with the experimental values than for the scheme given in M. Thq present
proposal of the level scheme for 166 Er needs some more confirmation. To
get this, the authors are starting now gamma-gamma directional correlation
experiments in order to obtain definite values of spins for the 788-,
662-, 957-, and 2140-kev levels. The authors thank S. Chojnacki and
I. A. Yutlandov for the preparation of sources, and K. Malinowski and
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Energy levels ... P/045/61/020/003/004/004
B133/B228
T. Walczak for assistance in measurements. There are 6 figures, 3 tables,
and 7 references: 4 Soviet-bloc. The 3 references to English-language
publications read as follows: Ref. 1: Mihelich, J. W., Harmatz, B.,
Handley, T. H., Phys. Rev., 108 989 (1957); Ref. 2: Jacob, K. B.,
Mihelich, J. W., Harmatz, B., Handley, T. H., Bull. Am. Phys. Soc.,
3, 358 (1958). Ref. 6, Boskma, P. De Waard, H., Nuclear Phys., 12,
533 (1959).
ASSOCIATION: Institute of Nuclear Physics, Cracow; Joint Institute for
Nuclear Research, Dubna (Yu. V. Nerseyev)
SUBMITTED: October 7, 1960
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Energy leveIG...
P/045/61/020/003/004/004
B133/B228
AbJMJ
Fig. 1. Block disgrant. of electronics. j
Fig. 1: Block diagram of the electronic apparatus
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Energy levoln ...

14
P/045/61/020/003/004/004
B1331B228
Fig. 6: Level scheme of 166 Er
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KISIEL, A.;
Intensity ratings in doublets of the fine structure in the Al III
spectrm. leta physica Pol 20 no.8:633-645 161.
1. Inatitute of Physics# Jagellonian University, Krakow.

IES # Z.;. NMOMICZANSKI. H..
7160aft ratios of spectral lines in the sharp series triplets of
atoms of'the second oolumn of tho periodic table. Acts. physics.
Pol 20 no,S*.701-714 161.
1. Institute of Physical Jagellonian Universityl Krakow.

NIEWODNICZANSKI, Henryk, professor
The Institute of Muclear Physics in Krakow. Review Pol Acadeav
7 no.2:53-W AP/Jl 162.
1. Mamber of the Polish Aeadeay of Sciences and Director of the
Institute of Nuclear Physics, Krakow.

GRAECTAK Jerzy; NIEWODHICZANSKI. Jerzy
Natural radioactivit7 of wpper ores from derosits in the lower Silesian
region. MAIeonika 7 no.2.-115-122 162.
1. Katedra Fizyki 11, Akademia Gorniezo-Rutniesa, Krakow.

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KOIDNKO., N.; LE-WANDOWSKI, Z.; MAKOWSKA-RZESZUTKO, M.
WIKTOR, S.; WROBEL, Z.
Energy an 12 angulabdistributions of the neutrons from the stripping
reaction C(d,n) N. Inst fiz jadr report no.200:1-15 Jl 162.
1. Instytut Fizyki Jadrowej, Krakow (for all except Wrobel).
2. Instytut Fizykis Unimersytet Jagiellonski, Krakow (for Wrobel).

MINDL, L.; NIEW'"DVIC,'ANSKI H.; Nt"IYNSFI, J.; SIAPA, 1.'.; STR7,AIYOWSKI, A.
....... I J
Elastic scattering of 1;~.P MeV de:,,teron-- rr, so:~e n~.clei.
Inst fiz jadr report no.203:1-19 16~'.
1. Institut Fizyki Jadrowej, Krakow.

NIEWODNICZANSKI, H.; tA7 !,7y1
%/ ;')K I, ! . ; W I 1,Ci'YN')K1 , '.
Elastic and inelastic sca,-'.er!nF of "e-V le --r. -.,c.-e-.
Inst fiz jadr report no.204:1-6 '62.
1. 1notytut Fizyki Judr-owej, Krakow, I Imit-yttit )-'j7yki, ' Ww-r-Ily!.ot
Jagiallonski, Krakow.

OA&,A* LUbCW3Xj Woo. -AS JoZa;
13=t:Ltu" of Phy Lao of t1w univarsity of crtuow
k,3
x
Z" 2SQUWARA algAuu Tt*o 30 6~9
51 *
3-40tral laoto-~Io fira'46yals or rri= i7catab jr~rjf;n
&AJ J. _ cc

Polarization of neutr~-.,.~: 'i- re--ction
for deuteron energies betwe-n !n-., :1.3 :'eld. Inst
fiz jadr report no.
1. Instytut -'i~yrkl

GABLA, Lubra." r; I
Isotopi- L-J- *
deposits. A --I
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I I. 1 T : . 3 ~ l-'?-I r 1';~ -).-
1. hst-,I-l 41 ~ - .) .. I ~' 1..... .', Kra~ow.

KOLONKO, N. Mrs.; LEVANDOWSKI, Z.; MAKOWSKA-Rzeszutko, M. Mrs.;
NIEWODNICZANSKI, H.; WIKTOR, S.; WROBEL, Z. Mrs.
Energy and angular distributions of the neutrons from the stripping
reaction 12)C(d,n)13N. Acta physics. Pol 23 no.2s225-234 F 163.
1. Institute of Nuclear Physics, Krakow, and Institute of Physics,
Jagellonian University, Krakow.

FREINDL, L.; -NIEWODNICZANSKI, H.; NURZYNSKI, J.; SLAPA, M.; STRZALKOWSKI, A.
Elastic scattering of 12.8 MeV deuterons on some light nuclei.
Acts. physica Pol 23 no.5:619-628 My 163.
1. Inatitute of Nuclear Physics, Krakow.

BOMOE.; LEMMW,N.A.; N1EWO1fJ1C=1S1U,H.; OGAZA,S.; RYDICKAJI.; STYCZE21,vl,
Gamma-gammm directional correlations in 14~k. fLnta physioa
Fol. 24 no.1t131-133 J1163.
1. Institute of Nuclear Physics, Krakow. 2. Joint Institute frr-
Nuclear Rasearch, Dtibna, USSR (for Lebeday).

KOTMALEWSKI, T.; NMOMIICZAIISKI, H.
Intensity ratios of spectral lines In the visible trip-
let of XnI in the temperature of liquid nitrogen. Acts,
physics, Pbl 24 no.5:601-609 N'63.
1. Institute of Physics, Jagiellonian University, Krakov.

F,V,~

BVDZANOWSK39 A.; GROTOWSKI, K.) MIGEK, S.; Nl~;WODNIGZUNSKI, 11.j SLIZ, J.3
STRULKOWSKI, A.; WOJCIEGHOWSKI, H.
Elastic scatterJng of 24.7 MeV a.!Fra paxtic-Ies. Iaz*, flz Jadr
report no.347.1-46 My 164.
1. Institute of wtmcl~~ax Fhysiss, Krakow and lnstiL~lLe of Paysiess
Jagiellonian University, Krakow.

v
KOPTA, S I N ~AUK. I , H, : B.
:',oulomo e/citatL,~n of rhoollum nlicleus. Acta physi-ca Pol 26 no.6:
1133-1141 164.
1. 'Lnstltuta of Nuclel3r Physics, l(rakow. Submitted May 8, 1964.

HRYUKIT-',WICZ, A.Z.; N1FWO!)N16-'AN3K1, It.; PUK ~i-,;Y,1, ',
Rapid identification if isobar.3 tj ~ne 1qr agi e r--;ng o.-'
low energy alpha pqrticl-s fr~)m ri. Ir3t *'~ z .~f,-4r
report no.402: 1-10 1, - -c,.
1. Institute of Ibiclear Phys:~s, Krak )w.

BUNANOVISKI, A_ OWSK: , K A:!(
N1WWOPN1--lAN,9K:, H- S"qZALKOWSKI A,; W"Lf"".
Energy de.pp-nA-r-:e
I,U,
n r Ir. 3 ad - r#~ p,--),
, a n Li - 'f, - up
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'ns- -
ute of Nu-lofi.- K r- ay.
of t ne ag i r-, 1 -in 1: r~ K I a~

NIEWODNIM11*3KI, Jarzy
Congress of Nuclear ;'nysiccis! -s , KTR KOW , "e ~ r Z. - I . "!- .
Nukleonika 'i no.10:bbl-662 I .

CZARNECKI, Jozef; NIEZABITOWSKT, Aleksander
Leukemic infiltration of the central nervous system during
the course of acute myelocy-tic leukemia. Pol. tyg.lek. 18
no.50:1892-1894 9 D163
1. Z III Kliniki Chorob Vewnetrznych AM w Kra-kowie (kie-
rownik: prof.dr.med. J. A-ieksandrowicz) i z Zakladu Anatomii
Patologiczne4 AM w Krakowie (kierownik: prof.dr.med. J.
Kowalczykowa).
4-

CZAMEEK1, Jozef; NIZUBITOWSKI, Aleksander
1,eukemic infiltrations in the central nervo-uq system. A,~ta
med. P01. 5 no.4s453-1+62 %64
1. Hlid Clinic of Internal MedActno, Rodical Academyf
Cracow (Di- -tor! prof. dr. J. Aleksandrow-ica); Depar"Lment
of Pathologic Ahatomy, Medical Academy, Craoov (DireCtG7~
Prof. dr. J. Kowalczykowa).

Z-Hil( ) Taiei.sz ,f F, I zbie La ; KI, TadeusZ;
Alekj3and~,-
Studies on chemical protection from ionizing radia*.!~,L. Pt, 4.
Acta med. '-o'. 6 no.2:1'11-177 165.
). bepartment. uf Pathologichi Anatcmy, Mecioa'. Acn-.em'v,
Wirector: Frof. Dr. .1. Kc,walczykowa); DeparUment -!' J,~y,-,-.-,-
gical Chemistry, Medical Academy, (,ra-;ow (Rirector; At;~v-(,. f.
Dr. W. Ost,-c.wvki,,, arid ",Te Radiclogical CA"inic-, Medl,:Ij;
D I r E. c r :Frc fT r-. -,L. 'anuszkiewir: z

KOWA LIC2YKOWA ranina; N!F7AHITCIvISKI#
F Alekontiderj 37CZUDIUWA, Jerzy;
T -L:~ '- *
,OIAjtS.LK, Bronl~
Morphological and clinical picture of tumorn of paragang:ionIc
bodios or the parasympathetic npitem, Nowotwory 15 no.2t]15-122
Ap-Je 165,
1, Z Zakladu Anatomil Patologicznej AM w Frakowie (Kierowniki
prof. dr, mad. J. Kowalazykown) I z Pracowni Anatomopatolo-
gicznej NiaJokisgo SzpItala Socjallqtycznego Im. dr. Anki w
Krakowle Werowniki dr. B. Tomasil).

NOWAK, Jan; LLZhB!TGWS.'I,-', Aiekjardpr; M'FR-VA., Kazimier-,:
ST
Value of radar,,rg-fe f
blastoma. Po-'. przegi.
1. Z Zakladi_ Anatom-i -4 Kra~owlt:
prof. dr. , Kowalczykowi. 1 7 Li,~ ist.. 3zp ta'.6
dr~ A. Pl~zk-_c
Dzieciecego a Kielcach (I. - -v,,cz

FAFROWICZ, Biruta; NIEZABITOWSKI, Kazimierz
Bronchial cancer co-existing with pulmonary tuberculosis. Roczn. pam.
akad. med. Swierezewski. 9:351-361 162.
1. Z Kliniki Ptyzjatrycznej Pomorskiej kkademii Madycznej Kierownik:
prof. dr med. Zbigniew Garnuszewski i Zakladu Radiologii Pomorskiej
Akademii Medycznej Kierownik: prof. dr n. med. Czeslaw Murezynski.
(TUBERCULOSIS PULMIONARY) (BRONCHIn NEOPLASMS)

NIEZABITONSKI, Kazimierz
Retrospective analysis of the fate of patients before establishing
the diagnosis of bronchial cancer. Fol. tyg. lek. 17 no.1;13-17 1
Ja 162.
1. Z Zakladu Radiologii P94 w Szczecinie; kierownik: prof. dr.
a. mod. Czeslaw Kirdzynski.
(BRONCHI neopl)

NIF.7RORAI,A
fhe use of reinforced concrete -n the construcUon of flour ralls. p. 69
FRZFGLAD ZROZOW04EYNARSKI (Polskie 'vvydawnictwo ',)spodarcze) Warszawa, roland
Vol. 3, no. 3, Mar 1959
F.onthly List of East European Accessions (LIAI) LC, Vol. L, no. ~,, 6epterher JV59.
Uncl.

POIAND / Farm Animals. Poultry. Q-6
Abs Jour Ref Zhur - Bi 1., No 14, 1958, No 64555
Author :Gorski, L.; Niewiarowicz, A.; Hnjan, U.;_ Niezgoda, A.-
Inst :Not given
Iltle :Experimontn in the Utilization of Vitamin Bl,) (APP) and Peni-
cillin for the Industrial Fattening of' Chickens.
Orig Pub :Przegl. jajcz.-drob., 1957, 51 No. 3, 17-18; No. 1, 20-21.
Abstract :Chicks receiving vitamin B12 in their rations, when aged 1
to 2 months, showed a higher increase of live weight than the
control ones, but at the age of 3-4 months, yielded to the
latter as regards weight gain. The combination of B12 with
penicillin increased the gains of chicks even at the age of
5-6 months. A higher food conversion was obeerved both when
B12 was fed alone cr in combination with penicillin) espe-
cially when the rations were lacking in animal protein.
Card 1/1

,,P)~F,ZGODA , Jerzy
Experlmntal testing of the Gaussian distribution of certain basic
parameters of receiving tubes. Frzogl elekt-,Oniki 3 no.8:476-.4,80
Ag 162.
1. Przemyslowy Instytut Elektroniki, Warszawa.

FIRKOWICZ, S.~_Al~~ODA, J.
Dist-ribution of basic parameters in rece.1-r-ing, -~uk-es. Ar c r. -' -.;
elektrotech 11 no.2:285-297 162.
1. Przemyslowy Inetytut Elektroniki, Warszawa.

KOSMOWSKA , Alina; NIE7GObA , 'erzy
Practical utilization of the equivalent failure rhte
method. Przegl elektroniki 4 no. 10/11:639-641 O-N 163.
1. Przemyslowy Instytut Flektronikf, WarBzawa.

KMGZKOWSKA, Irena; NIEZGODA, Tadeusz
Investigations on carbohydrate metabolism in liquid culture of the
tetanus bacillus. I. Ann. Univ., Lublin sect.D 16-323-339 161.
1. Z Katedry i Zakladu Chemii Ogolnej Wydzialu Lekarskiego AkELdemii
Medycznej w Lublinie Kierownik: doc. dr Irens, Krzeczkowska.
(CARBOHYDRATES) (CLOSTFIDIUM TETANI)

ANDaWEVSKI, J.; DOt4ZAL,T.; FUCHS, 1j.; LAGINSKI, 3-; NIEZGODA. T-; SWIZ"TLIK, M.;
SILKA, S.; STRAMKI, A.; ZFLUDZIhWICZ, j.; TEHAJhV1CZ, A.
Amputations in hospitals of the Olszytn Region during the decade af
1950-1059. Chir. narz. ruchu ortop. polska 26 no.6:797-799 161.
1. Z Oddzialow Chirurgicznych Szpitali w Olsztynie oraz Szpitali
Powiatowych w Gizycku, Ketrzynie No Miescie, Ostrodzie, Szczy-tnie.
(AMPUTATION statistr

ND,Z(',O!)Z,T_[ -,YI, Y.
:`Akinj7 use of so7,e by-products of 3laut!'!~terinf-, 'or "he -~roducti--~-, of enzymes.
p. 12.
Vol 7, no. l-, Dec.1955. YA -171-7,i'It. ',Iarnaw, Poland.
So: ---Astern European Accession. Vol ~, no. 4, ApriI 1-,56

PHASE I BOOK EXPWITMON POL/3626
Kurovski, R., and M. E. Niezgodzifiski
Wytrzyma):o& material& (Resistance of Miateria.1s) 4th ed.,, rev. and eal.
Warszawa, Pafistwove wyd-wo naukove, 1959. 503 P. 5v200 copies printed.
Ed.: Zbigniev Brzoska.
PURPOSE: This textbook Is intended for students at polytechnic institutes.
COVERAM. This Is the fourth edition of a textbook on the strength of
materials used in polytechnic institutes. The text covers simple came
of stresses in bare, composite stresses, the study of the def2ection Mae,
staticali.y Indeterminate systems, and the dynamics of elastic systems.
The author thanks Professor Z. Brzczka. There are 8 referenoess 2 Soviet,
2 Germn, ~ Fcli.;'J., and 2 English.

MZGODZINSKIO Hichal Edward
Influence of the dimensions of the specimen upon the tensile strength
of low carbon steel. Archiw hutn 7 no.2t197-22,4 t62.

NIEZGCDZINSKI, Michal-Edward
-",-
Micromechanical tensile strength testing of plastic aluminum
alloys. Archiw hutn 8 no. 2: 141-153 163.

NIEZ;Oij~'INSKI, Micha-I Edward, dr Inz., adiunkt
Quasi-nondestroying metal Strength tests. '~rzegi mecr 23 n,-,.
12035-338 25 Je 164.
1. Department of Materdal S)trength, Technical UniversIty, Lodz.

V,:~ Y Po 19 nd P
GENNERAL&SPEC.ZOOLorY. i 6,,SECs
t
~3S. JOUR.; Ref Zhur -Biologiya, 4, 1959, No.
Author zr - -17,
1 N -, T
A.
OIRIG, PUB.1 P') 15 ki 1.13 m r) tvoi -i r-, 195', B, NO-59 13 2 2
ABSTE~ACT r n T,
r v
c, rs s e!. Y, e, ril q.j S! e c
1 V-t I -
e1
r r.v -L.3 o-J Jr K-~- I
ve." Arrlf-,tl-~ 1- 7 --1
z) u co (I
CAI-%D 2
6o

MANIKOWSKI, Witold., dr; NIEZGODZKI, Lech
Helpful pneumatic micropipette for quantitative meazuriyl,7 of golutionB
in Chromatography. Farmacja Pol 19 no.7-.126 10 Ap 160. .
1. Zaklad Chemij TokBykologicznej i Sadowej, Akademia Medyczna,
Poznan. Kierownik Zakladd: dr Witold Manikowski.

RIEZIMINSEU I lIftma."OA Iku 0 p '~= 0
&VefGpwnf can&tjous fo-r tale awmill t%~%mtmjant of foUlage timber.
Przem dnew 12 no.12:4-9 161.
1. Redaktor dzfalu mlesieemiks OPrswqal Drzevny' (for RzadkowBki)
(Poland-Savmills)

BORMENKOY V.G.; NIFAGINA, A.A.
physical and mechanical properties of limestones of the V78okopollye
and Belokrinitskoye bauxite deposits. Sbor. nauch. trud. NIGH
no.7:77-79 160. (14IRA 14:12)
1. Nauchno-issledovatellskiy gornorudnyy institut (for Bcxisenko).
2. Mekhanobrchermst (for Nifagina).
(Dnepropetrovsk Province-Limestone)

BUSHUYEV, V.P.; GUBIR, G.V.; GONCHARENKO, Yu.I.; KARMAZIN, V.I.;
HARGULIS, V.S.; MITROV, V.A.; NIKOLAIENKO, H.O.; BOBHUSHKI'17, L.G.;
BUROV, A.I.; RYBAKOV, V.N.; SOSHIN, A.F.; TATSIYENKO, P.A.;
TOVSTANOVSKIY, O.D.; YUROV, P.P.; Prinimali uchastiye:
NIFAGIXA, A.A.; CHFRNYY, I.I.; GERSHOYG, Yu.G.; KOSTIKOV, A.G.;
-DOLGM, M.A.; MOVSKOVICH, S.A.; STUPIN, D.D.; TIEVOTSA, G.G.
Hagnetization roasting of Kerch ores in the experimental
factory of Kamysh-Burun Combine. Gor. zhur. no.12:30-37
D 162. (MIRA 15:11)
1. Institut Mekhanobrehermat, Krivoy Rog (for Busbuyev,
Gubin, Goncharenko, Karmazin, Margulis, Hitrov, Vikolayenko,
Nifagina, Chernyy, Gershoyg, Kostikov). 2. Kamyghburunskiy
zhelezorudnyy kombinat, Kercbl (for Bobrushkin, Burov,
Rybakov, Soshin, Tatsiyenko, Tovstanovskiy, Yurov, Dolgikh,
M.A.; Movska7ich, S.A.; Stupin, D.D.; Nevoyea).
(Kerch Peninsula-Ore dressing)
(Iron ores)

NIFANTOV, A. P.
Pycnometric Method of Analysis of the Mechanical Composition of Clayey
Suspensions
VaRr, gidrosol. L jgzh. geologlip 1953, pp 127-129
The author discusses the deficiencies of the existing pipette method of
Robinson. He indicates the expediency of taking samples of the suspension
in a picnometer with capillary stopper, since this permits one to deter-
mine the uantity of solid substances without regard to evaporation and
drying. rRZhGeol,, No 3, 1955)
SO: Sum. No. 639, 2 Sep 55

NIFANTOV, A.?.
Rspid methods for granalometric analysis of fday F;oils. Yop.
gidrogeol. i inzh. geol. no.17:130-137 159. (MIRA 14:1)
(Soils--Anal7ais)

NIFANTOV, A.P. --
Preparation of clay soils for granul tric analysis. Vop. gidrogeol.
i inzh. geol. no. 18;93-105 '59. (MIRA 14:5)
(Soils-Analysis)

MFANTOV Aj,
~Z~-
Grari-lometric azalyata of clay soils by means of a separatory fu=el.
Vop. gidrogeol. i inzh. geol. no. 18:106-109 159. (MIRA 14:5)
(Soils-Analysia)

NIFANTOV, F.P.
Determingin the sagging of constructions built on loess loams in
the Kuznetsk Basin. Izv. TPI 90:165-173 158. (MrRA 12:2)
1. Predstavleno nauchnoy konforentsiyey geologorazvedochnogo fakul'-
teta.
(Kuznetsk Basin--Soil physics) (Foundations)

NIFANTOT HIT OZOT, T.m.
- - -.-- 9,24MUO KOR
Grader attachements for the D-179A heavy trailer. Stroi. I dor.
mashinostr. 2 no.6:18 Je '57. (KLRA 10:6)
(Road machinery)

NIFANTIYEV, A.
Authoritative agency. NTO 3 no.e:34-35 Ag 161. (141RA 14:9)
1. Zamestitell predsedatelya soveta Nauchno-tekhnicheskogo obsbehostva
shakhty No.47 "Kopeyskugoll".
(Kopeysk--Goal mines and mining)

icient metu-ol ul in t.- I
workings. Aj
1. i:orkinskoia I w-P---.ontazhncyF- u; r~c; I nl-ye
SPt!t.smontazh (for P no-%,'). 2. ':c.47 trt
flifanttyev, Viret,

PAR FrlNCV, A P., "'I V,
'Js-' T-,07 rA -e.- ng mf r - r;
;-:k' n ~y e 5
Soy., Z.9l.akh' -ci 1:-~r 10
tregr.,-.

KOCHITIOV, S.K.; VIFANTITBV, I.Ts.; USKETABOT, A.B., akadealk.
Now synthesis of substituted aaphth&1enes. Dokl. AN SSSR 104 a9.3:
422-426 S 155. WAA 9:2)
I.Mookovskly gesudarstysmayy universitat Imeal. H.VAssomeseva.
(Naphtalene)

ACC NR. AP601~-98'9 SOURCE CODEs UR/0079/66/036/00;;1244/-ii-~~-
AUTHOR: DivLoskaya, Le Pol LLuanovv V. To.; Skvortsovev Ye. K.;
Pu tyatins, Go M. I Starkov, A. V. I GrLashtoys, ff. 1. 1Y.0.4r, F.Y&.
ORG: Central Scientific Research Disinfectant Institute (Teentrallayy
nauchno-isoledowatel'skiy dazintaktsionnyy institut)
TITLE& Search for bactericidal preparations among organophosphorso
compounds
SOURCEs Zhurnal obohchey khLmLL, v. 36, no. 70 L966, L244-L246
0 &Cp-
TOPIC TAGSs bactericide, as6unwphosphorua compound, organophosphoness
chloride, alkylauLnophosphonate chloride
ABSTRAM
In a search for new bactericides, e*v: am o Fj -1 sphorus cospounda were
synthesized and their bactericidal properties studied. The'reaction.of.-

ACC MRs AF60Z5939
-diethyl chloramethylphosphonate vith tertiary mines. at 120-LSOO yielded
diethyl dimthylaninowthylphosphmate ethochlorLde (1), mp 179% and
diethyl dLmethylamInomethylphosphonate ethechloride (11), up 178'C:
0 0 +
C1_1
(Rh"'+ CICH)(OCA)s 14RhN?-C11e)PjCxffgh1
'At 130'. decyl chloride reacts with phosphorous hexaethyltrimide to form
..Wounds IV and V were
phosphonium sALt 111, up 217% (mee,table).. ~o
-0-1
tained under similar conditions. it 160" In nitrogen atmosphere, tri-
,(hydroxymethyl)phosphine reacts with cetylphosphanium bromide or octadecyl
phosphonium bromide to form the corresponding bromides (VI). The reactIou
of tri(hydrozymethyl)phosphlas with decyl chloride at 1800C gave VII and
-with octedecyl chloride under similar conditions yielded VIII. Compoel-
.tion and bactericidal activity of the now compounds are shown.in the
table.

1 ACC Mlit AP6025989
Table 1. Antibacterial metivittes of tertiary
Noe* Coutpouad Tovard e. coli
C. I N Cif 11090211101 2o tnfu:
all j n
or 1) v4
I not acti
.111" not "etime
t1i flf-
JAOC1112.11 Ijur am not &give
Vil j(HOC111031,414611UP t a i've
0 ILP
Vill MOC11141'ap 30 ~ an..
I Ix 1(iloputArjul
I
'it is adftCb= 1868i Citil".
Otis* act, bass ~ 1. table#,-
SUB COD8s -O7,X#93K1DAT6' 29K&*651
LCcwd 3/3
9311:9
is mLn.
0.2 1
Pflin.
actLv4i
-OC400,
IV
active
17)
r'satt".,
1% not ai~pve.
(W.A- 50;,CBE'No. 101.
OR IG EFt 005/ OTH REFt 001

-.0 -g,
their dft
It-
V Lam =_RF,-_.5mm-
S-S.R., Oad-
"Lh and as It,
A 44- T
107. 09
I~o
'5'% hra
added with 140,0-kc Ln 1
(cm0al- CjjCj. 3o W. 1-40 ~ddtd Rud dic Inix
114r]md " days at -1.1 LEMP. ylodl" 5117"
ttl'8-&oxofdnS (1). N 82-3', rs*,? 1.4400. d. 1 IOR4.
66%" LIT i.4427, .&140,
dicl..'Jaw ,I ,, b- Q'2"' 1 4429. 1-0181; 242-OXOhe-
JI) CW7
l,"iaWpo $M), 65%, b, 117~- 15', i.447,
J.
o*,,y;rmd,hyV.,-3-di4vxdw;c (V). 80, 5"~. Km
I ovitalght 100Z FICI give IriaraAmum" M. 162~
-H,CjijoMe), Mth (Cfl~'Q' wilh , little
:UtuAln PTCOC
KDH &114) ga 14 2 b" 860M U TO Ph HIMIC, from
iol V._PbCIMa~ pAp ~" A&~ 13.2 g. t. yieldiag rifter
mu=t tbA irWe tertlarY ajc~ lihieb wa3 dismwedi
iw r4usla0wolf isnd UeateA -4ith 110 m'_ 42%_
44~
Mae viddinvaterbM reOldlo fleHtnd!latlUnj'4U4
m. 344% p~aate.'ta.
-C
28% 2
ib,r,% Mso~DuVjl b
7'. 61009TIY, JU g3ve
6732,-0.qV6; 45%
O.qM4-(WnlW)jww-=I.. Complex, rA! 7
1101-1.6*;
~Iel

KOOH12KOV, N,K,: NIFANTIYMV, II.Ya,; SHIRAYN, T.N.
Syntheeis of acetyl-2-chloro-cyclealkenoo. Dokl. AN SSSR 117 no.2:
241-244 9 '57. NIRA 11:3)
1. Moskovskly gosudaretvennvv univeraltat im. H.V. Lomonosova.
Predstavleno aknAemikom A.R. Reameyanov".
(Cycloalkenes)

16
50)
AUTHORSs Kochetkov, N.K.,and Nifantlyev, E-Ye. SOV/55-58-5-18/34
TITLEt On 5-Haloidpyromucic~__Aoid (_0_5_-W,_Md_P1roslizevykh kislotakh)
PERIODICALs Vestnik Moskovskogo universiteta,Seriya matAnatiki, mekhaniki,
astronomii, fi7dki, khlydi j, 1958tNr 5,PP 119 - 122 (USSR)
ABSTRAM In the synthesis of a natural combination with furancycle it be-
came necessary to produce 5-halogenpyromucic acid and to investi-
gate the possibility of replacing the halogen atom in these acids.
The following results connected with these questions were ob-
tained j By oxidation of 5-halogen-furfurol by sodium hypobromide
the authors obtained an easy method for the synthesis of 5-bro-
mine- and 5 iodine-pyromucic acids (outlet more than 50 %). it
wL-s stated that under influence of sodium methylate on the ether
of 5-bromine-pyromucic acid there results the ether of 5-methozy-
pyromucie acid. Results of Z.F. Hazarova were used. - There are 12
references, 3 of which are Soviet,4 German,3 American,and 2 English.
ASSOCIATIONsKafedra organicheskoy khimii (Chair of Organic Chemistry)
SUBMITTEDs September 5, 1957
Card 1/1

E-
i e n e ", r ou r, o ~c
,-I c wle 07, :1~ 1-1 1~ v !~I enov( -.7. v
:i.RTU-~-- L jo'K la I y A i:njerp, in;,u K SSSR : I ~~B . Vo 1 2 1 pp , 4;~~
usqR
,~?"~TRIXT 'In rt ~7,,n t t i ~ n 9 k.~ I o,,~ ce L ti ', v h,,! ve v- en mcire an I
pp n r;~un ic !ijn thes 12 ~ T t -J , triie t ~in t t a ve t.- a
acz,ess.blp --:hers Cyciic 12-'--etoacetals recent', p:-od-,cod
in the 1, boratory of the authors turned OUt to bO VDrtJLCiJILr-
ly ~cl,vantageo~io hecwiee of their higin stability ( :;I e f 4 ) ,
Vi thertc 0111 thi- con-lensations -witli c t to tl~e k,~Lc,
~,rom- ot' hwre beer, tised for purpoaps of .9 yn t h v
Re f:j 2 or the r t ranoformi, t. i oivi accord in - tne
t -t iP oi rci,c t ow~ Of d ,,;arbony I Th i e (1~,n~-
mainly fc-r pui-popps of synthesis of het.-rr~,cyc'ic (: om I l.) 1-1 nJ a
( e T. Refs 1 , ( ')~ Tne reacti-on of rephcement of rl-ketoacet, is
in thp methylene group is oi' particular intet-est since it
Card 1/3 will render -ic,~3nible t!:e-,r ap lic~!tion in -: C(jMrjt-tej-/ I~pv:

u b f- t 2 li i n R.
~v: r s e ri(: e ha r --,~m i~ v -,n t.
I, %w~- ver C(-,M", lcate:ll b", T :I-,- C ~ilv
-n u L. ~3 ob t r, i
1
L or. i 1" p
ace t a! gr u huw~-vo.- m6 in t a i n e d k9 f)u t a 1 n
ac~-,., 1,3 c r. ne , ~~ r t ',iv r i is e I f or d ', f f rent yu rpose,~~-
r. Q zi t. r,,-, p 7, t3 s ilb 1 1t i e ~cwever
C i-~ Ll 0
a f ii r e c,- - f
'K Tr, 1 n
o h 'if further t b ii,,4 fc~ rma t i o n of' .-a
4 t! Q -i c he r c t I n it, ri A, I n i p, L
h e on b y me a n a o f I cc d I. --- t r aacp t t, t f
eto acealdehyde liziethyl
-,f~ r~,a~ t,:. i ~,l z-, ne - or ~! cc- t Ous 0 1 r, a
lard 2 10 tz
:.,3 wroup., 1 n

E - 7/ 2 2 1 51 4 T
',.iethylene Grouu of ','e t,)L,,: ea I a
o t h o I I, n Y r c P! b t I
e f! c n g" c, r.
i e , mo re z, -:7, c- o c I i c
-a a s
iyd e ac a t I ;,, 1 t h be n I d e !~ _f,,i e in ves
'u ci (I ,here fre 12 references, 4 Of which are Soviet.
ASSOCIATIONS -oz~kc-i:oiy Posudbrstvennyy univers~tet im. T', V, Lomonos-.)-~P'
,.,ersit
y imen V L(rm-jnc s ov
PRESENTED: llar-h 10 by A, 11. Jesmeyan)v, ';Iember, ~.cademy of
USSR
arc-,.
SUBMITTED,
Card 3/1

JqjFAjjTIyKVP E. Ye*, Candidate Chem 9oi (diss) -- "The syntbests and chemical
propexties of beta-ketoacetals". Moscow, 1959. 9 pp (Moscow order of Lenin
and order of IAbor Red Banner State U im M. V. Lamonosov, Chem Faculty), 100
copies (EL, No 24, 1959, 128)

5-3400
v,/ 6 6 -
AUTHORS: Kochetkov, N. K.,
TITLE: Brief Communications. New SynthejLs if Phenanthrene
PERIODICAL: Khimicheskaya nauka i promyshlennost', 1959, Vol 4,
Nr 6, p 8o8 (USSR)
ABSTRAM A new method of synthesis of the phenanthrene ring
system was developed. The above method allows ob-
taining 10-alkyl-1,2,3,4-tetrahydrophenanthrene, arid
9-alkylDhenanthrenes (new Droducts) according to:
.~o 110cl
AIC~~ K(A I
oil
COR
0-0 11
0
Card -1/4

Brief Communicationa. New Synthesis 77 ~?97
of Phenanthrene 1jOV/63-4-()-31//i'i'
Cyclohexanone was condenspd vilth )cl.d chlorides -'n
the prejence of' AICI j I*c)ryjjlr)g acy) -,',-(-h1orocYc1oj-,,,x-
-2-enes (II), R = CH 3, b[, ioB-1oqO,/i5 mm
n20 1.4985, d4 20 1. 12'4 11 ~,' 1v y I id; C, H~
D
bp 102-103 0/9 nn. nD 1.4~12q, d, 1-0903, In 1~9-~
20
yield. R = iso-ClIff9j, bp'~0-'(-'L/0.1, nD 1. L1859,
d420 1.01120, in 11~% y1eld. The above compGunds II
were converted with fAhylene glycol and with alkall,
into monoethyleniketaL.-; r,,f' I-acylcyclohexanones (III).
Card 2/4

Srief Communications. Ne'd
of Phenanthrene
R
CH*~
C H
2 5
iso-C H
4
CH
3
CH
C H
2 5
i5o-C H
4
C a r d 3"
Lp C

e,
,,"ydr 3 xj a c el a6
6-7
Aromatic CYclodenydra~i:~n -a
tetrahydrop'-enan-:7renes

Brief Communicat.iDns. New Syn-,~es's
of P.'-,enan~'-ene
De-yal-a-
threnes 1,~ F, a
picra-e, 7,p
ASSO'CIA-1011: L,)rn-!~ M
F,o s -adar, sv et
3UBMITTED: June 4-1, i
Card 4/4

5 (3)
AUTHORS: Kochetkov, Y. K., NffantVev,_Z_. Ye.., SOV/79-20-7-48/83
Shibayev, V. N.
TITLE: Synthesis of the i-Acyl-2-chlorocyclopentene-1 and Ethylene
Ketals of 2-Acylcycl'opentar-ones (Sintez 1-ateil-2-khlortsiklo-
pentenov-1 i etilenketalay 2-atsiltaiklopentanotiov)
PERIODICAL: Zhurnal obahchey khimii, 1959, Vol 29, Nr 7, pp 2324 - 2329
(USSR)
ABSTRACT: Up to the present date only open chain derivatives of the im-
portant P-chlorovinylketones have been investigated in detail
(Refs 1,2,3,4,5). Alicyclic representatives of this class have
practically been unknown up to the present. Two contradictory
reports have been given concerning the synthe3is of I-acyl-2-
chlorocyclohexenes by the condensation of cyclohexanone with
acetyl chloride in the presence of AlCl 5 (Refs 6,1,). In exten-
sion of a previous thorough investigation (Ref 8) of this re-
action, which up to date presents the only possible way of syn-
thesizing the hitherto unknown compounds of the afore-mentioned
type, the authors carried out further extensive studies. The
reaction of cyclopentanone with acid halides in the presence of
Card 1/3

Synthesis of the 1-Acyl-2-chlorocyclopentene-1 and SOV/79-29-7-48/63
Ethylene Ketals of 2-Acylcyclopentanones
AM 3 was of a general nature and yielded the hitherto unknown
1-acyl-2-chlorocyclopente,ies--i.-
COR
AM,
+ RCOC1 [Cl where R-CH V C2H50
C3HV iso-C4 H9'
The reaction proceeded most favorably when cyclopentanone was
added to a previously prepared mixture of the acid chloride and
AM 3 in dichloro ethane. The reaction mechanism is given in
scheme 2. The 1-acyl-2-chlorocyclopentenes obtained were rather
instable oily liquids. Besides spectroscopic data the ozoniza-
tion of 1-acetyl-2-chlorocyclopentene-1 was decisive for the
verification of the structure (Scheme 3). Thus, the experiment-
al results showed that in the cyclopentanone series the above
reaction yields a,p-un8aturated ketones, cyclic analogs of
Card 2/3 P-ohlorovinylketone, whereas in the cyclohexanone series the

Synthesis of the I-Acyl-2-chlorocyclopentene-1 and SCV/79-29-7-48/63
Ethylene Ketals of 2-Acylcyclopentanones
same reaction gives p,r-unsaturated ketones as main products.
It was shown that the halogen in 1-acyl-2-chlorocyclopenteneo-1
is less mobila than in P-chlorovinyl ketones. By the reaction
of the above pentenes-1 with ethylene glycol in the presence of
KOH the hitherto unknown ethylene keta,18 of 2-acylcyclopenta-
nones were prepared. There are 19 references, 16 7,f which are
Soviet.
ASSOCIATION: Moskovskiy gosudarstvennyy universitet (Moscow State University)
SUBMITTED: June 5, 1958
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