SCIENTIFIC ABSTRACT PODURAYEV, V. N. - PODUSOVSKIY, V. F.
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Collection:
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CIA-RDP86-00513R001341520001-4
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RIF
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S
Document Page Count:
100
Document Creation Date:
November 2, 2016
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Publication Date:
December 31, 1967
Content Type:
SCIENTIFIC ABSTRACT
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3/121/63/00()/OOI/OWO14
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the el"t'le, 8"t" swi by tiew spoaal to
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sswat - woe
tallod.'ds4artp~lan of bmft.*~, dmwribo a vlbg*" *&Mw ift"UpM at vo
ba"o. 9f lavest4ptlam eatfted. mt by Mw W" Ig. - ftWMA ea%Mmio op fp%on
det*r%drdvS Ow. ddp-%,N*ft mcamaw am PC"* a*. ftal; the tut f"Uts eb--
t"ned.pre". tftt tMe fi. vlbfttft $%*a* Guam" T&LIG%e *AVtoodm
6 tiewaft.
SATELI, B.A., zas1uzhe=yy.deyatel' mauki i takliniki, do.ktor
tekhn.nauk, proL-,_ FO~DLqiAYE~-Y-N-,-kand_.teklm.nauk.. dot3ent;
TUKTANOV, A.G., irizh.;.SUVOROV, A.A., inzh.
Vibratio'n drilling of holes in stainless and,heat-resistant
steels. Vest.mash. 42 no.l-.67-70 Ja 162. (MM 15:1)
(Drilling and boring)
1. PODURAZRM. P.K.; STIKHIN, A.F.
2 USSR (600)
4- Meadows
7. Experience of the Khrushchev Collective Fam in rapid development of meado"Is, P.K.
Podurazhnyi, A.F. Stikhin, Sots.zhiv. 15 no. 5, 1953.
9. Monthl List of Russian Accessions, Library of Congress, APRIL 1953, Uncl.
AFENDULOV, K.P., kand. sellskokhoz. nauk; BOYKO, Ye.I., kand. sellskokhoz.
nauk; PEREMERAY, Ye.A., kand. sellskokhoz. nauk; PODLWZHI;YY, P.K.
kand. sellskokhoz. nauk; POIMYLPMNKO, F.K. ---- -- 1---,-----,-...,
Practices in the intensive use of land. Zemledelie 27 no.6:15-
20 Je 165. (pfflu 18:9)
1. Chernigovskaya oblastnaya sel'skokhozyaystvennaya opytna-ya
stantsiya. 2. Glavnyy agronom opytnogo khozyaystva Chernigovskoy
oblastnoy seltskokhozyaystvennoy stantsii (for Ponorarenko).
ZELIDGVICH, Ya.B.; PODURETS. N.A.
Evolution of a aystem of gravitationally interacting po.2nt masses.
Astron.zhur. 42 no.5.*963-973 S-0 165.
(MIRA IS:10)
-_ Amu-
ACM=Cff NR: AP4030M Bloom/
~11111001"0710010
AVZHOR: Zelldovichp Y&O BO Poduretej, M. A.
TITIR: Noutrim emission of a star during gravitational 0021W0 In thw amoral
theory Of relativity
SOURCE: M SSSR* Doklmkdy*p ve 156# no* 1p 1964, 57-450
ral
Top3:c TAGS: neutrino emission,, gravitational collapse,, star self 1ockIngp gene
relativity tbeory,, superstar conapseg, superstar
AMTRACT: The theory of a gravitational collapse was giver. by T. Oppenheimr et al
(Phys. Rev. 56, 455 (1939))o and is now of interest becox.se of the discovery of
superstars. The tbeor7,, based on general theory of relativity, shows that the
-exission'of light by the,star Into outer -space approaches zero when the radius
of the collapsing star reaches a certain value (gravitational radius). The star.
MVjtat4--1
is gravitationally self -locked. The authors have Investigated the 9
self -locking with respect to neutrino emission. The origin of neutrinos Is
anvinedto be In the conter of the star so that Doppler-effect Is absent. Two
cases am consIdereM (1) colbq?ss of dust, (2) collapse of a star from & cold
ILE
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PODURSTS, M.A.
totIc behavior of the optloal brightness of a al; at
Asymp 4ar
-Ivity.
gravitatimal nollapse in the general theory of' relat.
AstrGm. zhur. 41 no.6a1090-1096 hI-IT) t64 (mm 18a)
POT'n Of "'he FlJn3toin eqljntlcn-~ fc. 3D~'erical SY-mmetrical motion re
a contirrioUS jr;edjr,,n., Astrcn.zhur, 41 ncA?28-3~ 7p 11
1 64
'~MIRA 17-4)
PODUROVAO K.N.
Characteristics of -the function of the reticuloendothelial system
during the development of transplanted cancer. Uch, zap. Pod.
inst, Gerts. 179:277-295 '58. (MIR& 16:5)
(CANCER) (RETICULCENDOTBELIAL SYSTEM)
PODUROVSK.,"tY."i il.A. , o:-d'-I.ra4.--
E, ffectivenens of
body. Sbor. r,&uch. tru.U.
163.
,-,n4 ya ~zav. cj*vk;!1;7,r,~:.,i~,%~
Tz ginekologichoskoi-o otde
Gorodskoy bollnitu3y 1:0.2 ILostovtz-nal-;
nauchnyy riii-ovoditell -pro-1.
FETRAKOVICH, V.Ye.; EqRP_20UXAr-49*U"-TURIYAN# YEL.I.
Comparison of platimm oxide and glass indicator alectrod-30
in aaid-base titration. Effect of nonaqueous solvents, the
nature of the titrant, and various additions. Zhur. anal.
khim. 20 no.8:785-789 165. (MIRA 18:10)
1, Nauchno-issledoratePokiy i proyektnyy institut azotnoy
promyahlennosti, Moskva, i Yaroslavskiy nauabno-isoledovatellskiy
institut monmerov.
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catalyst. lnmviceksabilitYtoc=vettElOHintt;AcligraduaUydiappears.tfujuglI
iucatalyticactivity remains unimpaired. Better results are obtained by beating CuO at -00
100-95W followed by reduction. The mfioAcH/H, in the reaction producut ism,% at
2W* and #111% at 321P while the percentage of EtOH dreompd. increases from 17A to
"; 600
df 4M.4%. The time factor has noappreciable effect on the AcHili, ratio but affects the =00
0
0 priorntapoldroinnisdI.11-NOIC htsenor of HO inctraws the yield 4 AcOli. Thruse
of mixed catalysts was investigated. KAIACIJUVAKV
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PODUROVSKAYA, O.M.; YEFIMOVA, N.I.
Reastion of cyclohexanone oxime with potassium bromate. Zar.lab.
29 no.4s420 163. (KIRA 16:5)
1. GosudarstvenrWy institut azotnoy promyshlennosti.
(Cyalphexanone) (Potassium bromate)
PA
USSR/Chemistry BUtadiene Feb 190
Chemistry Ethyl alcohol
"On the Machanism of the Catalytic Synthesis of Butadiene from Ethyl Alcohol, It
M. Ya. Kagan, G. D. Lyubarsl-y-, 0. M. Podurovskaya, 8 pp
"Izv Ak Naulk Khim" No 2
Preparation of butadiene from ctotonaldehyde in the presence of the catalysts which
make possible the hydrogenation of the latterthrough conjugate dehydrogenation of
Alcohol'.
8T5
PODUROVSKAYA, 0. M.
Tj,,SIR/:hysies Adsorption
Aug 48
wAdsorption of Vapor Mixtures on Porous Adsorbents," G. F. Lesokhina, 0. M.
rodurovskayaj, K. A. Gollbert, Physicochem Inst imeni L. Ya. Karpov., Moscow,
6j pp
"Zhur Fis Xhim" Vol XXII, No 8
Deduces that there is a very close relationship between adsorption from solutions
and adsorption from vapor mixtures of the same balance as these solutions.
Approximate predictions can be made for adsorption of vapor mixtures on carbon,
given adsorption from solutions and relatively high pressure. Submitted 8 Dee 47.
PA 55/49T80
PROTABHIIVLIsi,iy,,-Anufriyevich; ZOZULYA, Nikolay Vasil'yevich, inzh.;
YNV. Yu*riv Borisovich; UDALITSOV, A.H., glavny7 red.; KONARBY,
M.L. k:and.kbimonsuki red.; PODUROVKAYA, O.M., kand.khtm.neuk,
red.; TOLCHIlIbIlY, Ye.M., inz
[Jiquipment for gauging the surface of hard objects by adsorption of
radioactive carbonic acid. Device for measurin& the thickness of
liquid films in a vpcuum. A receiver-condenBerj Ustanovka dlia
izmereniia poverkhnosti tvardykh veshchestv po adsorbtsii redioaktiv-
noi uglekisloty. Pribor dlia izmareniia tolshchiny zbidkikh plenok
v usloviiakh vskuuma. ?riemnik-kondenBator. Moskva, 1956. 12 p.
(Pribory i stendy. Tome 8. no. P-56-439) (MIRA 11:3)
1. Moscow. Institut tekhniko-okonomicheakoy informataii.
(Radioactive Bub6tancaa--Industrial applications)
(Surfaces (Technolot,7)) (Thickness measurement)
FODUROVSKAYAv Q;M.; PETRAKOVICH, V. Ye
Titration of acids*and bases by meial oxide electrodep. Zav.
lab.27 no.2:157-150- 16.1.- (MIRA U:3)
i.,GosudarstvennyZr~.naiiehnc~-isoledovatellskiy i proyektnyy.
institut asolroy ptomyshlennosti i produktov m~ganicheskogo
sintezj6. '- 7 .. - - .
(Acida), (Bases (chemistry))(Blectrodest Oxide)
PODUROVSKAYA, O.M, KIJTILINA, R.A.j rEFIMOVA, N.I.
Bromatometric determination of cyclohexanone oxime. Zav. lab. 27
no- 4:403-405 161. (MIU 14310
1* Gosudarstvennyy nauchno-ii3eledovatellskiy i proyektnyy institut
azotnoy promyshlennoote i produktov organiAeskogo sinteza.
(Cyclohexanone) (Potassium bromate)
W_DUROVSKIY, I.M., inzh.
Now methods used in concreting the Krasnoyarsk Hydroelectric
Power Station. Mekh. strri. 17 no.3-1:28 1 160, (MM 13:3-1)
(Krasnoyarsk Ilydroelectric Power V-,ation)
(Concrete-Transporation)
P--:k~27A-
PODUROVSKIY, I.M.; TOROPOV, L.N., red.; LARIONOV, G.Ye.p tekhn. red.
(Overhead cable conveyirg at hydroelectric construction
projects] Kanatnyi podvesnoi transport na gidroenergetiche-
akom stroitellstva. Moskva, Goa. energ. izd-vo 1961. 93 p.
tMIU 15:3)
(Cableways)
MIRONOV, S.A., doktor tekhn. nauk, prof.; MALININA, L.A., kand. tekhn.
nauk; FEDORDV, V.A.,, inzh.; KAYSER, L.A., inzh.; KRONGAUZ, S.D.,
kand. tekhn. nauk; PANFILOVA, L.I., kand. tekhn. nauk; SEMENOV,
L.A., doktor tekhn. nauk, prof.; PQQUROM1Y,__N_I., kand. tekhn.
nauk; VINNITSKIY, A.M., kand. tekhn. mauk; KLIMOVA, G.D., red.
izd-va; SHEVGHENKO, T.N., tekhn. red.
[Instructions on curing concrete and reinforced concrete products
at plants and building sites]Instruktsiia po, proparivaniiu beton-
nykh i zhelezobetonnykh izdelli na zavodakh i poligona-kh. Mo-
skva, Gosetroiizdat, 1962. 33 P. (MIRA 15:12)
1. Akademiya stroitel'stya i arkhitektury SSSR. Institut betona
i zhelezobeto4a,Perovo. 2. Chlen-korrespondent Akademii stroitell-
stva i arkhitektury SSSR (for Mironov).
(Precast concrete--Curing) (Autoclaves)
I I -~ i , .-1 -r
V "! ~ -I r, f~ i~IIIII
i SEMOV.I IT.A../, ~oktor tekhn. nauk, prof.; PODUROVSKIY, N.I., inzh.
Heat-mwing of concrete using clean saturated S' sam. Bet. i shel.-
bet. no.12:480-486 D 157. (MIRA U.-I)
(Concrete) (Autoclaves)
KONOPLEND. A.I., kand.takhn.nauk; PODUROVSKIY, II.I.. inzh.; ROMODANOV, A.N.,
inzh.
Determining the relation between small and large agrxegate particles
in aelecting concrete mixes. Bet. i zhel.-bet. no.6-2o6-2o8 je 158.
(MIRA 11:6)
(Goncrete)
PODUROVSKIY, N.I., assistent; SAVIN, Ye.S., assiatent
Evaluating the quallty of steam curing of concrete. Trud7 RISI
no.15:63-72 158. (MIRA 1-3:6)
(Concrete-Curing)
PODUROVSK I Y, N. I., CAN D TECH SCJ V "STEAM IN O~=RE~t 114
A MEDIUM OF PURE SATURATED STEAM." MOSCOW, 1961. (MIN OF
HIOMER AND SEc SPEC ED RSFSR. tvlOSCOW ORDER OF LABOR RED
BANNER ENoINEERINQ 40& CONSTRUCTION INST JUENI V, V. Kuy-
BYSHE~V). (KL-DVI 11-61, 222).
-175-
SEMOVI L.A., doktor tekhn. nauk., prof.; PODUROVSKI7, R.I., inzh.;
CiMRKOSKAYA, L.R., red. iiA-va-'14MZWA-,-A-.A-.j-tekhn. red.
[Presm=eless autoclavel Beznapornaia proparocbnaia, kamera. Mo-
skva, Gose- ie-vo lit-ry po stroit., arkhit. i stroit. materialan,
1961. 105 pe WU 14 -. 10)
(Autoclaves) (Precast concrete)
LAYROVA, I.
assistent; PODURTSEVA. Ye., khirurg
Away,with accidents in everyday life. Okhr.truda i sots. strakh. 4
no.5:39-40 My 161. (MMA 14:5)
1. Kafedra organizateii zdravookhraneniya 1-go Moskovskogo medi-
tainskogo instituta (for Lavrova). 2. Mediko-sanitarnaya chast'
zavoda, *Kauchukw (for Podurtseva).
(Moscow-Safety eduqation)
I- -- ... -%-- ~-Vr,
f
A.
26171P Iz ap ta rukovoclstva kyllturno-massnvoy ra-,otoy (TSK PROF. so,-uxa ralochildi
Y .3
eleirtrostantsiv) Prof. sovriizy, 1~41Q, F~, s. 16,20
SO: DITOPIS' 110- 35, 1949
POMMIN, A. , zave&Wushchiy.
Augment the role of trade-unions in the development of Soviet trade.
Sov.proftoiusy 1 no.3:55-60 N 153. (MEBA 6:12)
1. 2hIlIo.hcbno--b7tovyy otdol Vessoyasnogo teentrallnogo soveta profes-
mlonalln~-kh voyasov.
(Trade-iiions) (Retail trade)
7
PJWT.vHIN, M,G.; LOGINOV, FG.; ZHIMWIN~ D,G,,; PAVIMMO. A.S.;
KUIW# I.Ae.; PPICHRM# V.I.; BWTSJOV, A.I.; IlKITRIUVt Ll,;
TXMMTO VvSo; SOSXII, Lake; PODU ' I-SUIRNOT. Mesa;
TARABOV, N.Ta.; YIEDLISKIY,, Go 0; KRYLOT, 1,A,; KO~W# G.I.;
AMMSOFq Me; TAM=. N.D,; CHIZHOT, D*Go; UGCMS, I.I.;
NInFOW# Y.N,; PWONOV. N.A.
Vladltdr Nikolaevich Sergeev; dbituar7. Xek. eta. 27 =03:63 Mr
,56. 9:8)
(Sergeov, Vladimir NUmlaevich, 1903-1956)
L 38910-66 EWT(m)/EWP(t)/ET1
ACC NRI AP6019563
c. jj)pjB
SOURCE CODE1 UR/0080/6611039/006/1249/1256
AUTHOR: Goplyonko, V. G. Goplyenko, G. N.; Timofeyevi V. V.; Podushkin, D. I.
ORG: none
TITLE:
SOURCE: Zhurnal prikladnoy khimli, v. 39, no. 6, 1966, 1249-1256
TOPIC TAGS: titanium, chloride manganese, chromium, vanadium, molybdentzm, nickel,
corrosion, steel / steel-3. lKhl8N9T steel, 2Khl3 steel
ABSM CT: (The article reports on a study of the behavior of certain steels (steel-31
l1,hi5N9T,12Khl3) and metals (Mn, Cr, V, Mo, NI) in melts containing TiC12, TIC13,
-and TIC 4 in various proportions, carried out mainly for the purpose of obtaining
melts with lower titanium chloridgs, and also to determine the conditions of qjQctro
winning and refining of titaniuml:~n melts. In melts containing metallic Ti and TiC12
virtually no corrosi of steel-3 is observed; on the contrary, the formation of
titanium coatings on the steel takes place. Alloy steels (11(hISINT and 2Khl3) dis-
play a greater corrosion than does steel-3, owing to a selectIve dissolution of
chromium out of the steel. In melts containing TiC13, all the steels corrode and
contaminate the melt with iron chlorides; a lesser corrosion is exhibited by steel-3
in this case as well. The most pronounced corrosion occurs on all the steels under
Behavior of steels In malts containing titanium 911LmIdea-11
I
11,41-
PODUSHKO,.~.,_)E..,-.inzhoner-podpolkovnik; ROYRNKO, P.V., inzhener-podpolkovnik
Improve the system for keeping track of failures and defecLs-in
equipment, Vest.protivamd.obor. no.3:39-40 Hr 161. (141RA 14;7)
(Airplanes--14aintenance and repair)
PODUSHKO, T.A.; ODINOKOVA, V.A.
Unusual course of acute leukemia. Probl. gemat. i perel. 1=ovi
no.10:56-58 162. (1 17:1z-
,=--A ,
1. Iz 1-y terapevticheskoy kliniki (zav. - doktor med. nauk
M.G. Malkina) i patomorfologicheskogo otdela (zav. A.A. Naurp--v)
1.1,oskovskogo oblastnogo nauchno-issledovatellskogo klinichesPogo
instituta imeni M.P. Vladimirskogo.
PODUS,110, T. A.
"Fever Reactions in Cases of Acute Atrophy of the Liver., " Klin. Med.. 27,
No.6, 1949
lst Therapeutic Clinic, Moscow Oblast' Sci.Res. Clinical Inst.
1W.6c v0smaxt on Ora 4 as I ti
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ACCESSION NR.- AT4019293
8/0000/63/003/001/0690/0099
AUT14OR: ~ Florinskaya,' V. A. PodusWco, Yo. V'. ; Gonek, T. N. ; Cherncva, F.
TITLE': Infrared spectra of glassy and cryZailized silicates of the system lithium oxide-
aluminum oxide-silicon dioxide + TiO? and their relationship to the structure
S.0,URCE: Simpozium po stekloobraznomu sostoyanlyu. Leningrad, 1962. Stekloobr.~znoye
soqtoyaaiye, vy*p. 1: Katalizirovannaya. kristallizatsiya stekla (Vitreous state, no. 1:
CaWyzing crystallization of glass). Trudy* simpoziuma, v. 3, no. 1. Moscow, Izd-vo,
AN SSSR, 1963, 90-99, Insert between p. 90 and 91.
TOPIC TAGS: glass, silicate, crystallization, glass structure, infrared spectrum,
infrared spectroscopy, lithium oxide, aluminum oxide, titanium dioxide, spodumene
ABSTRACT: Infrared spectra of glass 13 with TiO? were determined over a range of
7-14 microns, along with the spectra of several natural minerals. The effects of
variations in thermal treatment on the spectral properties and structure were Investigated.
The"results show that transparent crystalline glass containing titanium with a composition
close to spodumene has essentially the same crystal structure as found in pure crystallized
spodumene glass. These crystals are formed below-800C. Inss of transparency in
crystalline glass of the same or very similar composition is caused by the different
Ca,d 1/2
ACCESSION NR: AT4019293
appearance of crystalline phases and by the larger dimensions of the crystals which are
formed. The temperaturc conditions during, the crystallization of glass and the addition
of oxides can affect the composition of the crystalline phases. Glass crystallization Is
preceded by a period of latent otructurization. Orig. art, hag: 8 fipres.
ASSOCIATION: None
SUBMITTED: 17May63 DATE ACQ: 21Nov63 ENCL: 00
SUB CODE: MT OP NO REF BOV: 000 OTHER: 000
2/2
Card
nr
ACCESfZON NR: AT4019295 5/0000/63/003/001/0101/0104
AUTHOR:' Kondratlyev, Yu. N.; Podushko.-Ye.-Y..
TITIJ~x A study of catalyzed a-r- y-a-tallization by cb&nges
SOURCE: Simpogium PO stOkloobrannomu sootoyaniyu. lAnir&girna2pbal9n2tionitakloobras- Y,
noys, oftoyaniye, vy*p. Ii Katalisirovennaya crys tall iz&ts iya stakla (Vitreous
state, no.l.- Catalyzing crystallization of glass. ) Trudy* simposium, V.3, no.l.
Hoscow', Ind-vo AN SSSR, 1963. 101-104.
TOPIC TAGS: catalyzed crystallization, silicate glass, glass, absorption spectrum,
opticalldensity, glass crystallization
:ABSTRACT: Glass of the system Li2O-Al7O3-S'02 with TiOZ admixtures, with varying
unto-of-L12O but in the region close to spodumens, was used as test samples.
Two temperature ranges were investigated, one in which no glass crystallization
occurs and the other in which crystallization and a further rearrangement of the
structure take place. The change in optical density with time and temperature was
plotted, and a general equation was given for these curves:
.. !,Do
-101
Card 1/3
ACCESSION MR: AT4019295
in which KI is the constant rate of change in optical density at a given tempera-
ture. The activation energy for the U14~ displacement, calculated by electrocon-
ductivity data, is 16-19 kcal/mol., but the observed activation energy war. 2.5 times
as large. The main stages of the conversion to crystallized glass during heating
are indicated, and the changes in optical density of glass due to heating are ex-
plained. The crystallization process is said to consist of two stages: the diffu-
sion of light ions and the diffusion of elements of the lattice, terminating in the
formation of more or less ordered regions; the precrystallization period is the
period of covalent diffusion. The wthod proposed for the study of the processes
of precrystallization and crystallization is convenient because absorption of light
by glass is a property which in sensitive to structural changes. The materials for
the synthesis of glass contain colored indicators (in our case iron). This makes
it possible to investigate these processes and connect them to the formation of
centers of crystallization and a substance intermediate -between glass and the final
crystalline structure.' Orig. art, has: 5 figures and 4 formulas.
ACCESSION NR: AT4019293
SUMMED: 17fty63 DM ACQ: 2lNcFv63 MM: 00
SUB CODE: INT NR REY SOV: 006 '003
Card 3/3
ACCESSION NR: AT4019288 S/0000/63/003/001/0074/0081
AUTHOR: Podusbkop Ye. V-1, Kozlova, A. B.
TITLE: Mechanism of the catalyzed crystallization of glass of the lithium oxide-aluminum
0~ide-sllicon dioxide system with titanium dioxide
S~Ul CE: Simpozium po stekloobraznomu sost6yanlyu. Leningrad, 1962. Stekloobraznoye
s6stoyantye, vy*p. 1: Katalizirovannaya kristallizatsiya stekla (Vitreous state, no. 1:
Catalyzing crystallization of glass). Trudy* simpoziuma, v. 3, no. 1. Moscow, Izd-vo AN
SSSR, 1963, 74-81
TOPIC TAGS: glass, glass crystallization, catalyzed crystallization, titanium dioxide,
lithium glass
ABSTRACT: Glass of the system Li2O-AI203-SIO2 containing titanium dioxide as a catalyst
(2. 0-11. 0% by weight) and with a composition close to that of apodumene was investigated,
and"the two main stages in catalyzed crystallization were studied. In the first stage, the
action of the catalyst appears and the conditions for the subsequent nucleation are croated,
while the second stage, nucleation and crystal growth proceed. Defects due to the catalyst
-are described. The effect of the amount of catalyst at different quenching temperatures
Card 1/2
ACCESSION NR: AT4019311
S/0000/63/003/001/0164-fo r66
AUTHOR: Kalinin, M. 1.
TITLE-. Crystallized glasses based on cordlerite
SOURCE: Simpozium po stekloobraznomu sostoyanlyu. Leningrad, 1962. Stekloobraz-
noye sostoyanlye, vy*p. 1: Katalizirovannoya kristallizatslya stekla (Vitreous
state, no. 1: Catalyzing crystallization of glass). Trudy* simpoziuma, v. 3,
no. 1, Moscow. lzd-vo AN SSSR, 1963, 164-166
TOPIC TAGS: glass, glass crystallization, cordierite, titanium dioxide
ABSTRACT: The catalyzed crystallization of glasses of the systcm '1(j{)-A1Z03-S;0Z,
ei ther having the coinposi tion of cordierite or containing at least ~f llz~ of this
compound, investigated using 8-Z0-,'Ti0Z as the cautlyst. The efiect of cata-
lyst contant and of prr.11minary heat tr*eaftn'lent on the subsequent :o,i-1-se of cry-
stailization was determined, crystal] ization being carried out b-, !`;.e polythermal
method at 700-1200C for 24 hours. Studies of the thermal effect and of !-he co-
efficient of linear expansion in relation to the temperature of cry-stallization
showed that preliminary heat treatment had no effect in the presence of large
amounts of catalyst, but that such treatment was required with small arrounL5 of
Cord J/q
ACCESSION NR: AT40)9311
catalysts to provide the optimal number of centers of crystallization. Thus, the'
curves were quite sirollar for samples with large amounts of cataly5t and pre-
heated samples with small nmounts of catalyst (e.g. the presence of three- exo-
therinal maxima), while samples containing small alwouas of caLalyst and not pre-
heaLed showed a strikingly different curve (one endotherni"I and two eyothermal
effects). orig. art. has; 2 figures.
ASSOCIATilON: none
SUBMITTED: 17MaY63 DATE ACQ: 21Nov63 ENCL: 00
SUB CODE: lrs~i NO REF SOV: 000 OTHER; 001
Cord 2/2
CHERNEVA, E.F.; FLORINSKAYAp V.A.; PODUSHKO, Ye.V.
Infrared reflection spectra of the crystallization product's of
glasses of the U20- SiO system in the 7,7 - 14/,j-region.
Zhur. fiz. khim. 37 no.lf:2556-2560 11163. (MIRA 17:2)
ALEKSEYEV, A.G.; VERTSNER, V.N.; KONDRATIYEV, Yu.N.; PODUSHKO, Ye.V.;
TIKHOMIROV, G.P*
Catalyzed crystallization of glass. Dokl. AN SSSR 154 no.l:
178-180 Ja'64. (MIRA 17:2)
1. Predstavleno akademikom A.A. Lebedevym.
W
ACCESSION' VR: AP4010759 S/0020/64/154/001/0178/oi8o
AUT POR.S: Alekaayev, A., G.; Veetaner,-1. X.; Kondrattyev, Yu. N.;
Podushko, Ye. V.; TikhomiroV, G. P.
TITLE; Investigation of catalyzed-cry~dtalljz_ation of glass
SOURCE: AN S8S.R..Doklady*, v. 154, no. 1, 1964, 17"8-180
TOPIC TAGS: glass crystallization, catalyzed crystallization,
0
,glass opacity, spodumene, glass thermal treatment, Li O-Al 0
sio2 Gla3s, Ti02 catalyst 2 .2 3-
ABSTRACT: Glasses of the systems O-Al O,-SiO2 (similar in
composition to that of spodumen6 'i ?.
) . th 5 addition of TiO as a
catalyst were studied. Structural aAalysis was perfoxhied 9y
electron- and X-ray diffracti6n. Inladdition, chans esiin light
absorption were measured. Spdcimens were heat treated in air for
25 hrs in the temperature range between 600 and 10000. There was
no noticeable structural change in glass up to 6250. In the range
from 625 to '7000, small crystals in some parts of the specimens
appear. Above 7000, small-crystalline phase in the whole volume
Card '1/2
ACCESSION NR: AP4010759
is formed. The crystals remain small up to 8300. Above this
temperature large size crystals are formed, and the glass becomes
.opaque. Orig. art. has: 3 Figures.
ASSOCIATION: None
SUBMITTED: 06jun63 DATE ACQ: 1OFeb64 ENCL: 00
SUB CODE: CH NR REF SOV: 001 OTHER: 002
Card 2/2
. ~__ W,
ALEKBEYEV, A. G.; VERTSNER,, V. N.; ZHUKOVSKAYA, 0. V.: PODUSHKO, Ye. V.; TIKHOKMOV, G.P.
C./
"The structure of some glasses of LiO -Al _S102-TiO2 system and its
variation in thermal treatment over t9e fcd7i4 teiq~eratxire range. "
report submitted for 4th -All-Union Conf on Structure of Glass., Leningrad,
16-21 mar 64.
AUTHORS: Vargin, V.V.~ Parlijahka, XC.V. 72- 58- 6-6/ 19
TITLE: The Melting of Glass in a High-Frequency Elcctric Field
(Varka stekla v elektricheskom pole vysokoy ohastoty)
PLIMODIOAL: Stelclo i Karaillika, 195B, !. , - Ar 6, pp. 16-i9 (vsmi)
ABSTRACT: The melting of glass by means of a high-frequency electric current
can be carried out in crucibles of any shape; the glass mass does
not come into .contact Yrith the electrodes, %Yhioh improves the qual-
ity of production and simplifies the construction of furnaces.
There are two methods of using high frequenoies for the purpose of
melting glass: the method of the electric field and that of the
magnetic field. For the method of the electric field a frequency
of 20-25 ko will be sufficient, and melting can be carried out at
room tesn-erature vrithout any preheating. For the method of the
magnetic field arlaitional furnaces with an additional equipment
for preheating the layer is necessary, which renders this method
less valuable. The idea of melting glass by the method of the elec-
tric field was first developed in the USSR by A.V.Makarvv, who, in
1941, succeeded in obtaining glass by means of a high-frequency
system of 10 Y61 and 75 kc frequency in a crucible having a cubic
Card 1/2 capacity of 100 cm3. Two apparatus of this type, UVCh-80 and
The Melting of Glass in a High-Fraq7aency Electric Field 72-58-6-6/ig
UVCh-2DO, are at present in operation in the USSR; their power
p7ara us
output is 80 ard 200 1W respectively. Fig. I shows the a-
UVCh-80, which is also described. A double quartz crucible with
interspace, filled up with crushed fire clay was found to be the
most stated. Fig. 2 shovra the cooling of the plates by means of a
spiral t~he which is soldered on. Control of the sirelting process
can be carried out according to efficiency and temperature. In
the high-frequency systems a number of multicolored as well. as of
optical types of glass, and of such as are particularly difficult
to smelt vras smelted, the temperature attained amounting to up to
18000. By the smelting method of the electric field it is possible
to obtain glass rrith a very low degree of light absorption. In the
case of smelting carried out in an electric field the crucible is
less liable to become corroded than in a reverbatory furnace. The
entire process of glass smelting takes place in an atmosphera of
oxidation, which fact exercises a favorable effect upon light, ab-
sorption. The degree of efficiency of these plants is considerably
higher than that of reverbatory furnaces, and the quality of glass
is partly better. These systems can be used with good success both
in production and in experiments. There are 2 figures, and 1 ref-
erence, 0 of Aich is Soviet.
Card ?/2 1.'Gla,ss--Mel~ing 2. High frequency currents--Thermal effects
15(2)
AVTKORI low ai,en SCY/72-59-5-1/23
TITIJ11 Class Set@=* at the THY Vendoloyev Com4gress
(Sauk& o stekl- Me 111t Nend.loy.,skcm a-y*sdo)
ISSIODICALs Itoklo-1 k.ramika, 1959. Ir 5. pp 1-4 (U-)
ABSMC?g Is the beginning a proolses.tion or the Tax Krss to the
personnel of the building Material Industries for aqualitative
and, q"ntlt&tLvt increase of production is mentioned. The
Congress took ploco in Mosco. in the second kalf or Ka-sh of
ths current year and was devoted to the 125th anniversary of
Use great schol"Is birthday. Outstanding obsolete of the
Soviet Union &M the People's Democracies attended th.COng"ss.
The principal problems of the development of chemistry we"
discussed at the plenary meetings and the matinee or the
19 Congress sections. 11rofassor 1. 1. nissycorodskly opened
Use meetings of the ~%ib-eection for glass &ad gave a survey or
the stage. of development of Soviet class Production as wall as
of a number of promising tasks in the field of glass toohnology.
11orveTer. the following Ilocturso were holds Doctor %or&"
(Peoplo*o Republic of Hungary) investigated the structure of
ONES 1/4 the top-lay..& of 61.041
A
0; 1. Avruotiwdk (LTI imenj JAnnowet) discussed the formis on
a finely dl.prae crystalline ph&.* from the gl-s-lik.
phasel V. V. Vargin Rod O,2A_1SrA%tj o1) reported an
(r
absorption spectra, ~Botochesic&L proportis.
of **rium-gleas typal A,.j6_Y"Lpv (001) "POrt'!d On the
q~01tativ* rooip"cl relations between ordered "d die.
ordered class ph ... , Y..J~~_Ko ~., X"Altut khl.li
allikatov AN SSSR (Institute of Silicate Chemistry of the
LS USSR) d1scums*d the reasons for the disagreement
problem of the structure of glass-like substamossi Poonfahs:or
0 S. 1. Anaftich, and X. L. AkMapv., Inatit.1
Insatitute-T-reported on the -Investleation of the
Close Structure by the Method of Thorms.2 Analysis "d Optical
larI:atI:nj to, T. Podushko (COX) diocamood the me: metb:d
ol. Sri the molting of silicate To)' "a
of hiSts-froquency currents To. 0. Shtsynborg reported on
glazes Itj`oZM_.ad "A boran for f.lossoo
&a4 mosJolloa. which have been developed in the Coaudarstroac"
k.romichookly Inatitut (state
3alentific Research institute of Corssics)o L. S. Tmatrobova,
~Cwd 2/4 !~k_!,%_NUUhwT!.SGOI) discussed the =18 VIsJ`9W_FY_th_4
gosrface protection film in the destruction of silicate slawasal
pre (001) discussed the coloring cha-:terlatice
0. ii,!orbb
a so O._Y'_X&2
a" a e.hwlogy of phosphate Classes$ __~Lrift (m)
reported an the mobility of odIum loco in 92:-s type- of the
sy:t.. Na2 O_RO.9iO21 Z. A. Nos*,. (X11 St"Yk "Mik-i
Al. cus"d the Proia'soof subduing the glasom by load
azIds a" olivonluml L._2.J,[0jL1skqhen~o, rha"kavokiy
pelt tolth-1 chookly Inatitut (Khar-kOv ~clrtechlsic Institute)
reported an silicate formation and siat.ring processes AM %be
briquattod else. layvrl K.. . qymtrgp-y I I= ... tIc-to4 -^ri.um
"a of cl.ess W_ ov also@ Institute) reported on the
7 open I Iyel.1
determination of Impurities In allies b troc
t :T a MR
.d Ye. V. Orlova (Class IRA Itt To P.,t.d
a
atroda gl"s-411ch has been devised by the*.
Tu._!,_XA&oshin (Glass Institute) discussed the kinetics Ot
the formation of crystallization atntero In photo-sonsittwo
a :' I . ayrit.kay. (Cie.. Institute) dl.ou.*.d
ft". uit!':; L!*ANTrmr~~Mn of the tendency Of PhOmPhAtic
systems t-do 91-4- formatioull I A Qrochazsik,
Kr ~ lj~' 7!,~~L
1--ratroryk1s, Rod V o1j. I-Ahl-
type&* or svalcon4ucting oZ14w glass OR %%A
basis of 1,05 1 S. L. A. Cr.cb--Ik. I-
and Is. A. Y"pb.rg (SIXES) discussed the production Of
anductiv.-files on type. of class which a--t&i- cc-PQ-ut#
:
.wily to be "generated.
-_L 11869-66 EWT(m)/rVIP(e) /EVIP (b) GS/WH
ACC NRs AT6000503 SOURCE CODE: UR/0000/65/000/000/0351/0356
AUTHOR: Alekseyevs A. G.; Vertsher,,V. N.; Zhukovskaya, 0. V.; Podushko Ye. V.;
Tikhomirov, Go F 1W
ORG: None
TITLE-. The changes in the properties and structure of L12O-Al2O3-SiO2-TiO2 glasses
during heat treatment in.a ivide range of temperatures
SOURCE: Vseso uznoye soveshchaniye po stekloobraznomu sostoyaniyu. 4thl'~Leningrad,
1964. Stekloobraznoye sostoyaniy! (VI-treous state); trudy soveshchaniya, Leningrad,
Izd-vo Nauka, 1965, 351-356
TOPIC TAGS: lithium glass, silicate glass, aluminum silicate, solid solution,
catalized crystallization ICIA-fA
ABSTRACT: The properties and structure of lithia-aluminosilica glasses catalyzed by
T102 and treated.within a wide range of temperatures have been investigated.
Special attention was paid to glasses the composition of which was close to spodumene
(S102 -60.5, A1203 - 28.0; Li20 - 6.5; T102 - 5.0 weight %). The results cover the
dependence of the index of refraction and glass density on the duration of treatment,
the comparative-x-ray and infrared reflection spectra for glasses treated at dif-
ferent temperatures, and the dependence of the index of refraction and glass density
on treatment temperature. Curves of the differential,thermal analysis are also
given. The results show that at temperatures of 700 to 800C the resulting crystals
-1-Card IZ2
ACC NR- AP6018727 SOURCE CODE: UR/0057/66/036/006/1027/1033
AUMOR: Golant, V. Ye.; D'yachenko, V.Y.; Novik, N.M.; Podushnikova K.
ORG: Physicotechnical Institute im. A.F.Ioffe. AN SSSR.-I&ALngx"L(U:;iko-tekhnich-
eskiy institut AN -5zia K )
TITLE: Investigation of electron cyclotron heating of plasma
SOURCE: Zhurnal tekhnicheakoy fiziki, v. 36, no. 6, 1966, 1027-1033
TOPIC TAGS: plasma heating, cyclotron resonance, hydrogen plasma, magnetic mirror,
plasma electron temperature
ABSTRACT: The authors' experiments on.heating plasmas in a magnetic mirror system by
supplying energy at the electron cyclotron resonance differed from other such experi-
ments in that separate oscillators were employed to produce the plasmas and to heat
them. The plasmas were produced in 9 cm diameter 18.5 or 30 cm long copper reson-
ators containing hydrogen at from 5 x 10-6 to 10-1 mm Hg. The shorter resonat6r
communicated via a 3.5 cm diameter hole in an end wall with a glass tube. The reson-V.
ator in use was mounted between magnetic mirrors (mirror ratio, 1.8) 30 cm apart.
When the shorter resonator was employed, the glass tube was in the region of one of
the magnetic mirrors; in all cases the copper resonator was between the mirrors. Ap-
proximately 100 W of rf power at 9.3-9.5 kMHz was continuously supplied to the
1/3 UDC: 533.9
L 41208-66
.~CC NR, AP6018727
resonator to ionize the gas and 4.12 to 30 microsec: pulses of rf power at the same
frequency with pulse powers up to 100 kW were employed to beat the plasma. The
visible radiation from the plasma was recorded with a photomultiplier, the x kadiation't
from the plasma was recorded with a 0.1 x 3 or a 3 x 3 ca Nal scintillator shielded~
with 1 cm of lead, and the plasma was probed with 10, 3.3-4, and 0.8 cm wavelength
microwave beams. The continuous 100 W excitation at 9.3-9.5 kMHz produced plasmas
with electron densities of the order of 1012 cm-3 when both magnetic mirrors were
operating, and part of the plasma produced in the shorter copper resonator appeared
in the portion of the glass side tube that was between the magnetic mirrors. The Uhf
pulses were strongly absorbed by the plasma; under favorable conditions 30% of the
pulse power was absorbed. The maximum energy thus injected into the plasma was 0.2 J.~
X radiation was observed when the plasma was excited by the powerful uhf pulses. From
the absorption curve of the x radiation it was concluded that electrons with energies
up to 100 keV were present with a concentration (estimated from the total absorbed
energy and the volume of the plasma) of the order of 1010 cm-3. The x-ray pulse was
delayed by some 4-5 microsec with respect to the exciting uhf pulse, and when the uhf
pulse duration was less than 5 microsec the x rays did not appear. In view of the
fact that plasmas produced during the experiments within the shorter metallic reson-
ator appeared outside the resonator in the glass tube, it is suggested that it may be
possible simultaneously to heat both the ions and the electrons of the same plasma
2/3
L, 26!?71_65
ACCESSION NR: AP5003260'
energy'. These::result6 are-similar-to,.those obtained by A.Gibson and D.W.
Mason (Proc.Phys.Soc~79,326,1962). for the "zeta" Installation. The interpretation
~o the re ults- is, discussed. very briefly, and it is suggested that refloction from
fields fluctuatibim.:Prevents any considerable number of electrons from being con-
tinuawly I accelerated s 6 that the -effect of the.longitudinal electric field is
to render'the electron velocity distribution alightiy anisotropic. Ne are
;grateful to B.P.Konstantinov, V.Ye.Golant and D.G.Bulyginskiv for the interest
they have shown in the work and f or much valuable advi ca. Orig. art. has: 2 f igures.
SUB CCDE-. ME
l,iiAVD/,9 Z.;
Amino acA-ds and pep ~-hem `9 no.!
2626-2632" N Y64.
I.. insititute of Orgamc Ch,-UL~.3try and Biochemistry of thr.
Czachoslcvnk AcaderW ot' Sciences, I -ria gue
~y end Mlcrob-'Ogy,
2. Pre3eri~, address- 7nstit-ute of
pragul~ r F v d a. J~ *
L
XV1. Peptides of lm-a~s-
VA'aslao,azids and peptides
* (from
dicarbokit;yloxy-bL-a,ft-di~rmittopropi&ytak, in. 801-01
_
1lMTM1Vpr4=~C -acid. Ar.1 '(Wit!i1a. jo~.vef l1rdlogrr,
and FrantRA �Ory (*' , Prastue). Chem.
VW Ac-(.'Ft-P(:tr. ethcr); asnide, by treatment witb McOllsad
8IC70 yield, m. 172-3* (from :'0% AcOll)..
`
371
1111
i
h
0
t
j
oustnuns.
731-44; Colleclon Uwhorlav. Chou. (
LiSW49 u
.
t
t
1
m
- Hydrolysis of the ainide 1(0.73 g.) w
o
,
*
*
3
,
,
20 1174-82(195fiXin English); cf. C.A. 50, 159je.-
i
i ) and dilu. Nvith
and W min. a! 40
AcOll (20 win, at 20
Ft.0 gave after,l hr. at 0* U.51 g. di-IlBr sail of 1. decollipg.
tto.
ans
llr6ns. of (1), iiia,fl-d
4
t&iOjg1yCisJ9 (11), I)L-4,13-diansitioptopionylgi)-rintj)iiiik
0
2.13'.- The El ever (M) of di(carboben.-)-loty~DL-o,R~i"-
'
in2%yays: Reflu%u-L
i;sc(X)%-asprel)d
i
n
l
t
"-z1.YcY1-DL-*,"iaMi"ppr ionic acid (IV), NA-
i~ (V)
j3-
t's t
biT-g1YCy1-DL~
d .
anit
o
noprop
w
y
g
1.97 g. V11 in 10 mt. Phitle 2 lirs, with 0.72 g. OCNC113-
,
,
and of :be derivs. are described.
diamissu
ropsmic acid (VI) CO~Rt. distg, off the solvent in vacuo, triturating the residue
,
p
Ifeating 40 S. BrCl1-CIIBrCO_-I1 with 400 nil. aq. NILOH
' 'with sad. soln. of NaHCOf. and washing the crystals- with
0 gave 2.2 g. ][Ka, in. 141-1.5' (train
N HC1 and H-
11-0
in an atitoclave, distg. offthe Nii,
said. atOl 3-4 his. at 100
-ir wxupunder Ndissolving the residue in a min. amt,of lit% .
.
Wolf). atlug 3 g. V11 in 20 mt. ClIC13 at 5' vrith
SO% Trel
1
,
and trmting the solo. with activated C, mid filtering gave
* , adding a cout
0.03 g. I-EtCslliPN and 1.12 sez-BuOsCC1
of 0.87 g. 11,NCIJ,CO~Et in 10 wt. CIICI,,
(-5') Wis
.
r)L-HsJVC1]sC11(JV14)CO.H, dwompg. 230 -2
g.
"iamixopropio?jic acid, decutup
9-
NA-carbobcnxylax~DL-a .
letting the mixt. stand 2 hrs, at -5' and 12 hrs. at room
,
234-5*, yield 15%.' Vl-bmZOYI-IVA4atbOben*VXY-L)L-,i3-
-
' ternp., evapg. the solvesit, and treating the residue with
NaHCOz gave 84% M. M (3.33 g.), 8 ml. N NaCil 1, 6
, Treating 5.4. g. dicur-
acid in. IWA
diatminopropfoxic
6-diaminopropionic acid (M) in 60 mt. dry
nzoxy-DL-a
bobe -
mt. MeOH. and 10 mt. dioxdne shaken 1.5 tirs., acidifi,:1 to
1
-
.
CHO, at 0' with 3.8 g. POs until the 110. dissdved, evalig.
' .11 g.)
Congo red with dil. RCI, and the cryst. residue (2.
rcpptd. train NaHCOj gave 1.6 g. X, m. 170-l'. X wits
, and extg. the ressidue with petr.
the mixt. in racuo at 40
aher gave 3.54 9. DL-44rarbobenz3,loxyaminof)ielkyl)oxazoli.
* treated with HB-. in AcOll, the buse liberated J~y ineaus, of
and treatt-d with picric arid to give
an ion exchanger
(frain AcOEt-
dino-2.5-dimu (MI), decompg. 139-40 .
9
,f the Et
01
Sat
U5
210' (from 11
f H
Pets. ether). Shaking 1.61 g. VL11 at 2D' with 30 jul. bs. .
g.
g.
, m.
,
pkrale o
MeOH with Nils at 0', keeping the
ester of X in 30 nil
MeOH contg. 10 millimoles IlCl, letting stand 12 lirs., .
e MeOH, and cryst idue from MeOH-
distg~ off th g. the ressi
EisO mist. ve 1.60 g. of the 110-salt 61 me Nxi~arbobemyl_
'
r
137-8*
In the same
k
n
Wi
.
.
Wona
, t
l
wpi 0
was.prepd..85% HO sail of FJ NP-carbabenSY1OXy-DL-
.',Wway
:a, "satntnoplopimate (M); in. 143-4.5*. Treating 1.12 g.
~_TU with 20~ N HC1 in EtOll overmight gave 1.1 g. Et
mixt., avernigh --tEe-
I&distg. Offwme n ri:PaiRTS
procedure with residue give 1.18 g. of the amide of X, ~
in. 17".5" (from aq. EtOH). Treatment of 0.8 g. of this
conipd. with HBr in AcOH, with Amberlite, arid with Picric:
" gave 0.75 g. of the dipiaole of IU, m. IDO-I * (from aq.
Eto
H). IX (from ~ 2.12 g. 1X.HCI and NIIj In CHCI;)
treated with 1.64 g. PhCHi0ICNHCHsCONs gave EJ-
ester. of ~VA-rarbobensyloxy-N*-mrbDbMZYIVXYIIYCYI-DL-*,#-
dia
d Prol fc 'he Me ester was prepd.
'io* uaci4 (X" 'terof)(1bykeepitig
_t
F
P.
t~,
.6 ith IV .1. free XI. ni. 120-2".
L of 11 ~i'h H gave 1. g-
Br I. AFOHi fitteringthe sain.
through Amberlite, evalig. the soln. to 10 ini., and adding
to 4 mi. OM g. picric acid in 3 jal. V
- tOH pptd. 0.3 g. of thc~
picrateofIV.decumpg.-'08*(fron4,1110). Dissolving2-lg.
of the HBr sAt
.11 in 1.30 rul. 2N
NuOH, cooling thc.~:4a- toO'. aild trtaiing during 35 inin..
with 35 g. ti.-.vISlycine Oiloride'ln EtIO and with SIX) ml.
N NaOll. stirting tht: mixt. 35 inin. at W. sepg. the aq.
layg, extg. it ttsice witit
4.0, acidifying with IlCi to Congo
red, reppig. thexpil.~wAlos 3. thues. and crystg. the prod-
uct from da. AjcOH gave 7-Vt's.'di1Ydrq!ir
(1j7ry1j1ycy1)-Di_a.84ja ' ' * cid (XII), In. 80-2%
MS"PPr*On1C a
-mother lh~uora to 7 and letting the
Adjusting the pH of the
soln. stand several hrs..at 0" gave 10.57 g., and by eviipg' tin
addrd. 1.94 g. N~LIOSylglyCyl-DL~,ft-dianjinopropiotjic arid.
(XUI), decompg, 2D2*. . Heating 2.77 S. XIH, 2.0 g. PhOH,
and 44 mi. 37% HBr In AcOH 2 brs. at 70* in a pressure
bottle, cooling the inixt., potuingit into 150 ini. EttO, allow-
ing to stand 2 hrs. in the icebox, washing the aystuts 5,-vrral
times with JUA dissolving them in HjO, removing the Br'
ions with Amberlite in un acitate cycle, evalig. the filtrate
in vacuo, and treating the restoilf-Arith 30 mi. Moll colag.
15 ruillimolesHO pptd. an oil which cr std: an tritura6onat
.3
5U*.
the On. with 20 mi. Etx)li contg. p
~1 ljj"~ L, V. J e
addingEtzO pj)td. 1,44 9. of the 11 pg.
210'. The 5~ame prt)dtxct was obtained froin !K1II in 48%_
Heating 0.53 g. XII
yirld 1by feductiun with Na in NFli-
((ljed in ~vcpo over P:O,), 0.6 g. PhOll, and 10 in]. 3G%-
IlDr in AcOll 4 lirs, at (15" and worLing up tht: inixt. fix
dewTibed above 5ielded 871:~V of the ainino ncidand, after
761' (if t lie Picrole of VI, In. 2,104-5, (de-
adding nc aci
I .~Iie
coinp I (fruju H,O)' Additigat 0' 1 g. tos)'Igb-cille 011wide
in Et-O Eoln. to 0.91 g. IlCl of the sah of ES A'#-cvrbobertzy!-
ox);diaininopropionale iii6int. N NaOlL, shalking-the mixt.
1.5 his. at 0*, 5