SCIENTIFIC ABSTRACT SDOBNOV, L.P. - SEBEK, V.

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CIA-RDP86-00513R001447610010-7
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December 31, 1967
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SCIENTIFIC ABSTRACT
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At qom JIV isms.;,asphaltenes formed-'during,the -'Aotption-process..have~. Idwer aromatic -factor.-and cfttaitv'd-. mgher:--cono art-- has:- ble' q 4 figures-and-3-ta ASSOCIATION: Institut,khimiche kh nauk"i-aradei ski Of -,he'mical Sci'ences':.Academ-3r,::'of.,Sciences-ok'th SO: Referativnyy Zhiirnal-Mel-ilaniia No I Jan 54; 28 July 19-54) 3t--engt.a Under Prolonged Loading of AlloY EI-43?B Under Complex Both tubular and~solid specimens were employed with..a working length of 100 mm. and t =ies-to-fracture were measured :for, 1!arious,values c+' normal (d) and tangentiai.( r) stress,''the '7alue of 'A-~or a :being zero in the case cf pure tension 0 r pure torsion., re ec-tively. The investigations were-za,ried out 4 at the.Strength,laboTatory, Institut mekhaniki, kN SSSR (Mechani(,s Inst.itute, of -the Ads Sc *USSR) on a test , rig IMF.Kh 2a designed'and built.in~]'6949,, 4hich is capable, of exert'ing:a maximumaxial-tensile load of-I 0001kg and a maximum tcrque of 20 kgm. -The machine was provided.with.~an electric-furnace in three.sect.ions, -each with: a rheostat,. Axial~ load was applied through a.,le-trer.arrangement and~torque through a pulley, arrangement. Three:lwhermocouPles were',fitted to each spec~lmian'. for measuring its tempe-rature._Strict precautions were.obse_-V'ad to ensure comparability,of results: the specimens were accu~z-. tel. machin heat-.~Ireated and ]Loaded- as a check on soundness ed., I of-sampl material the Rockwell hardness of~each specimen w s e a determined and the spe-imens with an.-abuormal value of hardr-es-s. were rejected; Ithe:temperature fluctuations during,:a test periodweremaintained within + 1 5 .C and the maximum temperaS ture variation over the:specimen Card2/3 iength-did not exceed *2.5-1 C-~ Photog-raphs -shcw that spe-aimens tested,in pure t ension ana Strength Under,Prolongel Lcadin'g: of Alloy BI-43?B Under Complex Stress Conditions combined- t6ns:Lon/torsicn fractured aiong_planes at right angles the axis- -those in pure torsion.- along p lar--, s*. at an: angle of 45t,. to the axis. The ~test -Aesults are gi-,,ren 4n the form of tables and graphs of a, VS. 1 g-100T. In~ cantrast to Jdnson *s and:FroGtIs:r;_-sUlt$, ajlart~froz a certain scatter they form a diB-1-4ne"- tZ, igh line for each type,cf~loading, s a the line for pure torsion 11yi be" ag Low the~.other two. Furthermore, the values ef ~7,. obtainad for the solid specimens we-re nearl,7 4- as hi h ag those f r -he,tubula Uwice 9 0 r ones.. Jo,hns,cnls~and Frost I s, empiri-sa.'~':- f ormulae, expressirg. Ig ~ T as ~ a I unction- of and -.0i, or Of a ahd~'L we-re 'tried, with the prezent'~resultz.but were ound unsat afastory in that the,7.gave no e b~u+. two cr,~, t on three straight. lines.. Subseq lentl,7 some further fc~rmu.'.Lae were examined and it was 111,owad that one of them, A. -(Ig 100T) 1. 66 (2.2) satisfactorily described the ::-eaults of a*11 the thrree, types of loading.- There are 8 -f.iguzes,, 2 tables and 5 referenc_s.~2.of which are Soviet -and A Eng7 Lsh~ SUBMITTED: Julv 5,~ 195"T. Card-3/3 'n *6,~, U, ta n K Fa t- o lad t on OieskEd, t eldinli Y ~4 a.! a ~raa.,~ -o m Z) I r, S, C. p ro t, c t i o, 0, oad to 0. ;,i i:t d ,~l tic, Z! 11-4-:7KI fa f, ax L L th 3, t d E tr, c 6 -~~2 c, rA wa s. mea ur A s t A A-07- c r c.) r. ar with a:.ri- M. t! Y! 'U V. 7" 6. '! y p I e r a- tu re,.c. up tc OC 41~1:~ j rp-,n- ~15 5 Efim Qoan diameter -111 7, (1 cured r tion was: trim U-41 f.,:r I ca s s wa niske 0 5 - 0 95~% Al Tli,~ allo7 n a r e r, al 01C f ror, 10 0 . Otl afte-, b ci:l di ag foA"~ S -50 OC liours, followedi by air t _'cVo6/ol3/029. A Criterion,of Endurance. Strength~.for Cert* I -ilea t Re ~;Is ting Alloys in a Coripb nd U Utros3 Oondltiwi cooling..:'Other tests were carriod:out with a ferrous. alloy EI-405with 0 1 2,'~'C 0 6414 Mai, a 591j; Si, ~ 15. or.' Cr, 13 Ni, ~2.301; 1-16 11 b 0 05,! ~ Ti I and, ,,pociftcd mrities. I . /'i . V ~). I P ~ i Aurtenitic treatment vias.giv~rjn at 1100 Q~' GO fol 10 116ul's. folLanted.by cooling in air I ageing 'At in, the evaluationof "the tests)~a criterion of endurance streng. was used which Is the bLr:LthLqetic mean of tile 41-to ~h Is principal stresses and whir, ed against the plott logari thin of - -the endurance peribd.:,In all cases, the pres ent t6 s ts . corif irm the linear rela tion be WOO 11 tile p1. .Iotted.quantities (a*s noted by, A.S. Johnson a i N.B. Cross of them British.National Phys c La bo r 6 ry i al a in 195.4-1 -and by Zverilcovi B V Teploenerge tilk, ! 19.58, ~Nr 3). ':_ The "empirical. relationship previou51 od Y, pr opo I s- r dobyrev, V.T Izv. fi-M 33SR, OTN, 1958, jNr )f) o t bu6h confirmed: '~, The proposed criterion, OF, On ..Card obtained in numerous tests for Ondurance period.,. u p to 2/3 a400 hours and ml",e 'of evalu- Lion of ther t; t, is thrught to bo Significant. The -I'valation be,!, Line temperature and the- lo-arithm of the endurance p - I erini i LP /3 i7 ---------- .MTV Ic-f 1 J4 r al, --,e, cla Tktic tiv-'tio t in Vv_cl~:'~' T"Ic lc.".t -)I: End L T ta tl Or i i'lfth iv. A llva~~-, 1~ 5 5, 1 1,~1 53o-67 Ge"~ -i-=- , A,I t ro. c t` "Al-C117:1- canUti6m of '-'.c IVIc cl-U-1 znalti%rantio n is ills C, Y-, c a; 7riculturc; only in of~ Tul ir. L~;tr"z n;u! Ae, c n'~_"bbw-ias -soil 0 L lz-~- c ~ arQ Pc'r -the ct.+fruit -trees. -u-i r u n ~Y'J 17 all .roes nn-t routs; the _10. anx:. tLcir~ yicL' 115~T Z I i I I:K. v IS 7-- 11 y; a a 7 - RE~ 1 ag t% g - -of tho t Im -------------- Z 38/62/000/001/001/003 /0 -D291/0304 AUT11ORS,. Zitflanakf, Bobumil,. and gabastifin, Imrich TITLE: The use of.a single-channel scintillation spectrometer for radioactivity measurements PERIODICAL: Jadernfi energie, not 1 19621,9-14 TEXT: Thepaper-points,o'ut several possible applications of.scintilla-, tion gamma spectrometry especially~for studying multicomponent radio- isotope systems.obtained by activation in a nuclear reactor. It des-.: cribes-in particular.the use of the Belgian.SGXA-3 single-channel.scHtil- 9 lation gamma spectrometer for quantitative analysis of the system Fe Mn54 CR51WI810 Scintillation gamma spectrometry can be.usedtD.great ad- vantage forstudying the various physical,and,chemical processes and be- havior of alloy steels, their thermodynamic constants, such as the eva- poration rates of the.individual components, determination.of their partial pressures and of the components thermodynamia activ,ity, partial, enthalpies and entropies, determination of the formation and/or decompo- sition of intermetallic phases, and study of diffusion coefficients of Card 1/ 2 D The use,of a 291/D304 the components in a.multicomponent: system., ThisImethod permits analyses of such systems withouCIpreviousseparation of the individual components:_~_~_~ which are frequently,present in such extremely minute quantities that they cannot be determined by any of,the,conventional methods* ~The dis- advantage of the.,gamma spectrometer is that it also.records the back- ground, the scattered gamma radiation, and the bremsstrahlung caused by beta particles. The selectivity of asingle~-channel scintillation gamma spectrometer can be considerably raised using large-area scintilla-. tions or large-volume well-type scintillators.,,A still greater selecti- I vity can be obtained by,,using multicrystal gamma spectrometer.sl in which Ithe parts of the single-channel spectrometer are duplicated. In-Czecho- such spectrometers are being developed by the n.p. Tesla Pardu-I bice (TeslIa Pardubice, National Enterprise) in Premyslent near Prague* There are l0,figureB'and,4 references 3 Soviet-bloc and.1 non-Soviet- 6loc..:(Technical.editor: J. gilar)o ASSOCIATION:~ Vyzkumn~ fistav zvfirar~kf Dratislava (Welding'Research'_ Institute R tislava) ra Card.2/2 84125 7,/017/60/C49fOll/OO8/013 ~1300 (/0 //.? . .1 ~ - ~ I . . . . I .. 1 -1 E073/E535 AUTHORS: Pf" Engineer, sa, duitav, ~Engineer,~ Spiess,:_Petr, Engineer Sebek, Svatopluk Engineer.- Vendlerova., Vera 'W~~ - ~tor nopa ~,Jaroffilr, Engineer Doc. TITLE: New Knowledge Gained in the Development-of t hjg, Technology!:of Germanium and Silicon Rectirier93mements PERIODICALzElektrotechnicky obzor,,1960,': V01.49,No.119PP-579-583 TEXT. In,addition to reviewing world trends in semiconductor development, theauthors deal briefly with.,results of development work in the Semiconductor Laboratories of CKD. Prague. The problem of dislocations in germanium has been dealt with extensive- ,ly in Czechas well as in foreign literature,(Refs 3,4,5)- Therefore,-the authors deal only brIefly with the results of Iextensive experiments.' the aim-of which was to determine,the influence of theabso.lute number of dislocations on the quality, of the P-N junctions and the.influence.oflaccumulation of dislocations And of microscopically vtsible disturbances caused -by accumulation of dislocations within a smallvolume. A more, B'0 1. -detailed treatment!-of, theseis -given -in a paper by urger and Card 1/6* 84115 :Z/017/6o/c 49/oll /008/013 E073/E535, New-Knowledge Gained Development.of the'Te.chnology of, Germanium and Silicon Rectifier Elements~ from three germanium crystals'.,,Thel.characteristics of the.three types,of.discs .are reproduced in Fi .1 and it can be seen that- the- diode :of the group (c) reaches only about 40%.of 'the voltage of the diodes of group (a).~::All the results obtained for the three groups of diodes were.used for plotting average value curves. These.are simi lar to the curves in Fig.2. The characteristics*of diodes from group.(b) w ere below those,of::. -group (a).and on the.average were nearer to those of group.(c). shown the quality of.the P-N transitions The.experiments have l is.decisively_influenced by the poorest transitionspot, i.e. by .the spot thatcontains a high accumulation of dislocations and it is this spot.which determines the properties of the P-N. junction. In studying the inverse voltages of diodes, investigations were made an materials.with,,various average. numbers of dislocations between zero and several tens of 2 thousands.per cm As a result, the dependence was determined of.the.inverse voltage of.junction rectifier's on the number of Card 3/6 p. 64115 Z/017/6o/c 49/011/008/013 E073/E5.35 New-Knowledge Gained in the Development'of.1t.he Technology o f~: Germanium and :Silicon:Rectifier Elements varnishesand silicon vaselinewere-used but ~these:did not prove, satisfactory. Subsequently,~polymer type synthetic materials were used for this purpose.-and the.characteristics~of a diode 'after... etching With hydrafluoric:acidi the above.mentioned etching mixture and protection by embedding in a synthetic niaterial,,,are plotted in-Fig.,3.~ Tor..the manufacture of,silico,n P-N junctions'.,, with inver-sevoltages exceeding 1000 Vitl,is advisable,to,use silicon With a specific resistance of 100 t0,300 Ohm cm and.a minimum lifetime of..the,minority carriers of 200Ao 300 lisec w:Lth a.~homogeneous crystal lattice'and without, in'ternal.stresses'.an*d -undesirable disturbances. of.:etching,of silicon plates in etching,agents:of-various compositions were tested. !The speed And the depth of etchingincreases with'the concentra-, the;etching agent and,with temperature. The decrease in the thickness as.a function ofthe etching timein various etching .agents is plotted in Fig.4'.- For 150 A rectifiers, a junction area 2 of 200 mm was chosen.in order-to obtain longer service life5 better heat removal and to-avoid excessive over-loading when the Card 5/6 84115 ,Z/017/6o/o49/011/008/013 _~EWVE535 New Knowledge Gained. in the Development. of the Technology of Germanium-and Silicon. Rectifier.. Elements Junctions are fully loaded. CKD manufactures re6tifier ~system3. 'with N-~type .silicon,with Junctions:produce.d.by:rthe fusion method in vacuum, Type N silicon is the most easily available in Czecho-~ slovakia~and so far.has proved.satisfactory. Manufacture of.P-N junctions,by the diffusion method Is'also being studied.,,~ sx n c eit 1s..*considered to be more.suitable for P-N-P-N.junctions. Thebest, method of protecting P N silicon junctions from the.effects of .the:atmosphere is to encapsule..them.in.vacuum-tight containers.*--' in.tests~so far good results have.been obtained by protecting -the, ''junctions with a.silicon,vaseli.ne prepared.in,.the.Research -Institute for Organic Synthesis.without any addition; thevaseline, must.be absolutely,,pure without moisture and degassed in vacuum. silicon.vaseline with additions of.halogenized alkylsilanes has not ~Proved satisfactory.' The ~encapsuling of, the rectifier systems is also,briefly described. There are, 5 figures,, I table and 3 Czech, l_Soviet, 2 German and 9 English. ASSOCIATION: CKD Prafial,:.n.p.- zavod Stalingrad: (eKD Prague, Stalingrad Plant)., SUBMITTED-. July 20, 19bO Card 6/6 -AP6631483 SO(JRCE CODE: CZ/0008/66/000/004/0433/()450- ACC NRt ovaropluk AU7HOR: Sebek, Svat ---Flant Frague (CKD, Zavod Polovodice) ORG: GO ~~ condua& 0 i i Ei TU-m 1f; In dsilicon surfaces TITLE: Chemical refining f e SOLECE: Chemicke Usty, no 433-450 TOPIC TAGS: . silicon single crystal, germanium singlecrystal) grinding, grain refinement, metal etching) hemical,engineering 0 j /-a .- . ABSTRACT: Surfaces, Aigermanium or silicon prepared by a section f ram 6L single crystall%ay be cleaned by mechanical grinding using silicon carbide or aluminum oxide. 11oating in very.high vacuums -or bombarding the surface by positively charged ions or electrons can~also ield a very 6lean surface.-Chemical methods maybe based. on.etching in gas phase,, :spraying in an:electric.discharge under vacuum, etching molten metals, heat etching, and electrolytic etch-i" ing, Chemical etching.is made by subjectingthe surface of the material to the action of a solution of~molten salt...~In chemical,~~', etching the oxidation component oxidizes the materialt'and the,sdl-r vent component romoveD the oxidized component from the surfaces Nitric acidj hydrogen peroxides and alkali nitratea are usually used for chemical etching. Detailed instructionsfor etching procedit.- es...pimilar for both Ge and Si are given. Removal of byproducts of etc om the surface is descrl~b~d. Orfj; has'. 15, figurei -2 'formulas hi~g fr and 2 tables. EMS: 36,4643 SUO CODE: lip 20# 07 SUBM, DATE: nonelj~l OTH REF: L-CcHid 1, A Z. SEBEEK, V.; HXIoCL, J. ,-,:r I-Ir it I I sl miwerejoulid ie- d 6tur. W;:~ Ot bi~ Otovr~[ .It