SCIENTIFIC ABSTRACT SEBIK, R. - SEBOR, J.

Document Type: 
Document Number (FOIA) /ESDN (CREST): 
CIA-RDP86-00513R001447610014-3
Release Decision: 
RIF
Original Classification: 
S
Document Page Count: 
100
Document Creation Date: 
November 2, 2016
Document Release Date: 
August 23, 2000
Sequence Number: 
14
Case Number: 
Publication Date: 
December 31, 1967
Content Type: 
SCIENTIFIC ABSTRACT
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PDF icon CIA-RDP86-00513R001447610014-3.pdf5.41 MB
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'o Stanists%~- Attio ~hfiln bird liball T,Lmfr V2cek. I Pelt. Univ., t -I I p CO. from Crigtilln'T a 9"1' "N atte 1i: y T%drated.to ilk nes ri~ d rt g a on gave the correspon( ing paraffins oil hydro en ti RMgBr in 744 parts Et4:) was added with in f, Coll ill equal &,mt. of EtzO. and the mixt. was boiled fil. 130-40', bi d. 0AIrt, OAP-52, 9 19.050, (1.900, C-Ain cornpd. with 1130 and 2070 IJISO.; evalin of the et erjeft 14 Cwtv1docckindient, ITC1 ill CON b? the cryst. glycols contaminated with tuircarteit 1. front iX.Aecompd- on diOn. tinder 01 (tin Which they lvere freed by sapon. 'rhe fipnowing giyculs C.0 ,40614 11 e: 1 -466117 - d 0 kZ2. Q.W-M, q re pre I (yield. m-P., b.p.): JA WIC P' iii 8% bit 181-2*; - ,ion of the diolk.fin ,I tit 88a AcOll 6vir 101-yieldcd paruffin4 in 95-8470 b, 1611.51; diethy1decan'4 in. -.181, his 118-20" n I.-laTil, 4K 5-A. 90.8* (front NfeXo). -. (1,1141kily'r-6-11- -, 1.43M0, dx 0.7778. dAd 0-7575, i 2,466. IAM. TAAJ heradetanediol (V), 43.4%, 79.4* (from N'CICC), -'1 0.910. 4.9-DipropyMederane, in. -3(;.4*, ti.~ 149j)- 9.,.t-dioctyl,9,1.1-doc6saneylini (VI), 277%, 53.2% - De 50-W, 6 165.0-S,5; n - 1.43979, 1.4,1735, 1.451M. hydration of the glycols gave diolefiliq with tuicertai" n 1.44191, d. 0.7913, 0.7723. n 5.494, 3.349, 2..M1. 1.224, positions of the double. bouds (glycol, diolefin. reagent and - 10-Dibislyttr1raderane, m. -11.8% bm 150.5-61.3*, conditions. b.p.. and, unless othenvai,c stated. ns' for a, $- -- " 8W 26&-6.5'. ., L4,5474, 1.4522.50, 1.4152M. 1.44689, d. 0. and D; d. at -M* and W*; aud 11 in ecinistokes at 20 0.7S31; tj 13.17, 0.04R, 4.808, 9,11-DiFocly1doromme' .37.8*. 50*, and 08.9*): 11. 3,q4ir1hyfdcraf'"'e, iodine in MS. mij 1.4521, nl,? 1.44M. d" O-M; 29 5M' 03 ' above. 140% bis 123.5'; it 1AN50% IAO,591, 1.47-14 1AM8-d. O.M.I. 0.7815; q 2.130, 1.553. 1.324. 0.746;~ III, 4.9-dipropyl(fodecadiene.,-, -, d. 0,M)S. 0.7."7: 4.607, 2.957, 21149, 1.144. IV, 5,10-dibulyttetradetadiene': CuSO, above 200'. b, 102.&-3% 6 201-1.70. it 1.4600-40 1.47001i 1-47579.1-46W5, d. O.SWO, 0=79, q 9.M. SW lei 3.927, 1.674; V, 11,11-diamythesadecadieue (CO.-H). at LZ: i", C and it. 743Lt t t x-, r 'b f t ~c S t I* c U4 r - ~ C n c 74, L t IT. - io 1 e XPe I C) D, k- 1 e! - y t ne va r 4 . 'Ua S lj t-, b e t' o f , . IT. ) I i0o 1 ~ sesen ~4e j in a 2 C~ 0 m- e X~ r, I c- d wrr- (~I- s a and ti'e e-S ut at ef ti;E !*!Lt~4 were breug"l. U l --k as rude C'f 't he. and dEtErmin~6ti,)n 'w of t l"' 6 e xt: co=.Arlu~ed c r -:- ed se~ c t C- VLlr and en c' S. of . werE a al , It writs found ~lhat o"t, u hE~ ac-~eous extra;ct ed S or'. e n a . ~le intensi+y Of Sh-L-L.Lr,) 1 i -, sec