SCIENTIFIC ABSTRACT SEBIK, R. - SEBOR, J.
Document Type:
Collection:
Document Number (FOIA) /ESDN (CREST):
CIA-RDP86-00513R001447610014-3
Release Decision:
RIF
Original Classification:
S
Document Page Count:
100
Document Creation Date:
November 2, 2016
Document Release Date:
August 23, 2000
Sequence Number:
14
Case Number:
Publication Date:
December 31, 1967
Content Type:
SCIENTIFIC ABSTRACT
File:
Attachment | Size |
---|---|
CIA-RDP86-00513R001447610014-3.pdf | 5.41 MB |
Body:
'o Stanists%~-
Attio ~hfiln bird
liball T,Lmfr V2cek.
I Pelt. Univ.,
t -I I p CO. from Crigtilln'T
a 9"1' "N atte
1i: y T%drated.to ilk
nes
ri~ d rt
g a on
gave the correspon( ing paraffins oil hydro en ti
RMgBr in 744 parts Et4:) was added with in f,
Coll ill
equal &,mt. of EtzO. and the mixt. was boiled fil. 130-40', bi d. 0AIrt, OAP-52, 9 19.050, (1.900, C-Ain
cornpd. with 1130 and 2070
IJISO.; evalin of the et erjeft 14 Cwtv1docckindient, ITC1 ill CON b?
the cryst. glycols contaminated with tuircarteit 1. front iX.Aecompd- on diOn. tinder 01 (tin
Which they lvere freed by sapon. 'rhe fipnowing giyculs
C.0 ,40614 11 e: 1 -466117 - d 0 kZ2. Q.W-M, q
re pre I (yield. m-P., b.p.):
JA
WIC P' iii 8% bit 181-2*; - ,ion of the diolk.fin ,I tit
88a AcOll 6vir 101-yieldcd paruffin4 in 95-8470
b, 1611.51; diethy1decan'4 in. -.181, his 118-20" n I.-laTil,
4K 5-A. 90.8* (front NfeXo). -. (1,1141kily'r-6-11- -, 1.43M0, dx 0.7778. dAd 0-7575, i 2,466. IAM.
TAAJ heradetanediol (V), 43.4%, 79.4* (from N'CICC), -'1 0.910. 4.9-DipropyMederane, in. -3(;.4*, ti.~ 149j)-
9.,.t-dioctyl,9,1.1-doc6saneylini (VI), 277%, 53.2% - De 50-W, 6 165.0-S,5; n - 1.43979, 1.4,1735, 1.451M.
hydration of the glycols gave diolefiliq with tuicertai"
n 1.44191, d. 0.7913, 0.7723. n 5.494, 3.349, 2..M1. 1.224,
positions of the double. bouds (glycol, diolefin. reagent and - 10-Dibislyttr1raderane, m. -11.8% bm 150.5-61.3*,
conditions. b.p.. and, unless othenvai,c stated. ns' for a, $- -- " 8W
26&-6.5'. ., L4,5474, 1.4522.50, 1.4152M. 1.44689, d. 0.
and D; d. at -M* and W*; aud 11 in ecinistokes at 20 0.7S31; tj 13.17, 0.04R, 4.808, 9,11-DiFocly1doromme'
.37.8*. 50*, and 08.9*): 11. 3,q4ir1hyfdcraf'"'e, iodine in MS. mij 1.4521, nl,? 1.44M. d" O-M; 29 5M'
03 '
above. 140% bis 123.5'; it 1AN50% IAO,591, 1.47-14
1AM8-d. O.M.I. 0.7815; q 2.130, 1.553. 1.324. 0.746;~
III, 4.9-dipropyl(fodecadiene.,-, -, d. 0,M)S. 0.7."7:
4.607, 2.957, 21149, 1.144. IV, 5,10-dibulyttetradetadiene':
CuSO, above 200'. b, 102.&-3% 6 201-1.70. it 1.4600-40
1.47001i 1-47579.1-46W5, d. O.SWO, 0=79, q 9.M. SW lei
3.927, 1.674; V, 11,11-diamythesadecadieue (CO.-H). at
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ut at ef ti;E !*!Lt~4 were breug"l. U
l
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1 i -, sec