SCIENTIFIC ABSTRACT SHAFIR, G. S. - SHAFIYEV, A. I.

• Document Type: CREST
• Collection: Scientific Abstracts
• Document Number (FOIA) /ESDN (CREST): CIA-RDP86-00513R001548520004-2
• Release Decision: RIF
• Original Classification: S
• Document Page Count: 100
• Document Creation Date: November 2, 2016
• Document Release Date: August 9, 2001
• Sequence Number: 4
• Publication Date: December 31, 1967
• Content Type: SCIENTIFIC ABSTRACT

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15 03)
AUTHOR. Shafir, K. F., Engineer SOV/119-59-8-9/15
TITLE: On the Problem of the Additional Treatment of Polyamide
Parts of the Nylon Type
PERIODICAL: Priborostroyeniye, 1959, Nr 8; pp 25-26 (USSR)'
ABSTRACT: In the introduction the use of polyarddes as parts of instruments
is explained on account of their good physico"mechanical
propert4es, and it is said the'
. they belong to the class of
amorphous crystalline polymers. The latter fact shows that they
have a number of properties which are found also in crystals.,
Figure 1 shows as an example a schematical picture of the
division of a micromolecule into crystalline End amorphous
domains. In the present paper the microsiructuxe of gears,was
investigated by means of the microscope MBI-1 at 400-fold
enlargement. The aftertreatment was carried out .after thousual
production of the gears in castor oil at.temperatures-of 140 to
2400C. The aftertreatment lasted from several minutes to 8 hours,:
after which cooling down to -400C followed. Sj--C:Micropictures
(Figs 2-7) are given of the experimental result .s,:which demonstrato
the effect of the aftertreatment. It was found~that in the case
Card 1/2 of an aftertreatment at temperatures slightly below melting point

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r
S/653/61/000/000/008/051-c
P42/I242
AUTHOR: Shafir, K.F.
TITLE: The application of cast polyamide com
.ponents. in the
construction of electrical equipment
SOURCE: Plastmassy v mashinostroyenii i.priborostroyenii.
Pervaya resp.. nauch.-tekh. konfer. po *opr. prim.
plastmass.v
-aashinostr.-i priborostr.,:Kiev, 1959.
Kiev, Gootekhizdat, 1961, 74-84
TEXT: Among new plastics with outstanding wear resistance are
.the Soviet polyamide resins ITA-68 (PA-68), AK-7- VA-6, (PA-6),-
no-54, no-548, etc. These resins have a low coefheieht of friction'P
good adhesion to metal surfaces, resistance to mechanical shock,
mold, and bacteria The Vsesoyaznyy nauchno-issledovatelskiy insti-
:tut elektroizmerit;lnykh priborov-(All-Union Sc*ientific Research
:'Card 1/2

3/653/61/0W/000/008/051
1042/1242
The application of cast plyamide...
Institute for Electrical 1'~eters) is working on the replacemont of
metal componento by plastics * The manufacture of plastic compo nents
by pressure-molding is discussed in detail. Some.of the factors
considered are the air and moisture content, heat distribution,:and
~coarse temperature.control. Polyamide parts, subjected to wear for
2000 hrs at different tl~mperatures and relative humidities, showed.no
damage, whereas their metal counterparts lost up~to 0.2 mm of surface
layer. Among other advantages of polyamide components are shorter,
production time, lower cost, and better quality* The'.manufacture of
,polyamide gears for electrical equipment ia discussed in detail The
VNIIEF is studying the replacement of metal and textolite gears~by
~thcir plastic counte,rparts. Polyamide bearings uri.der smalLloads re-.
..quire no lubrication-. The replacement of steel roller-bearings by
self-lubric ating polyamide bearings is under study. There are
figures and 2 tables.
i-Card 212

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EVIT (d )/EVIT (m)ZEEC (k) -2/T/FSS-2 DJ/WR
L-44600-66
xc--c Nal AP6005365 SOURCE CODE: UR/0413/66/000/001/01-1-1/0111
AUTHORSt Krichever, S. S,; Novikov, N, M.- Shafir, S. He
OW: none
TITL'Et Hydraulic tracking device Class 42 No. 177695
SOURCE: Izobrateniya, promyshlennyye obrazt5y, tovarrWye znaki, no. 1. 19660 Ill
TOPIC TAGS: tracking equipment, hydraulic equipment
ABSTRACT: This Author Certificate presents a hydraulic tracking device made in the;
form of a casing with openings for allowing the working- liqui \~to.pass in and out.
The casing contains an internal plunger with ports for passing the working liquid.
To regulate the sensitivity and stability of the hydraulic tracking system by changing
the amplification factor,, the working head of the plunger is made in the form of two
rectangular symetrical ducts interacting with the corres ponding rectangular ducts
in the sleeve (see Fig. 1). The perimeter of the working aperture is adjusted by
turning the plunger in respect to the sleeve.
Card 1/2

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8 (6) SOV/91-59-11-5/27-
AUTHOR-. Shafir, Ya.K., Deputy Boiler House Chief
TITLE: Adjusting the Load of Gas-Fired Boilers
PERIODICAL~ Energetlik, 1959, Nr 11, p 13 (USSR)
ABSTRACT: The author reports an error found, on page 17 of a pub.
lication of the "Kiyevgaz" trust,:, titled "The Opera-,
tion of Heating Boilers". This passage deals with the.
air control of gas-fired boilers.,'."For increasing the
load, the gas supply must be increased first and then
the air supply. When reducing the load, the air, supp-
ly must be decreased first and then the gas supply."
The author says that explosions are po .ssible, if the
load adjustments are performed in~the:indicate.d: se~
quence. For increasing the load, t.he air supply,must
be increased first and then the gas supply. For.redu-
-cing the load, the gas supply mu *st beJowered first
and then the air supply. The "Kiyevgaz" trust should
correct this error immediately.
,Card 1/1

SHAFIRA, L.E.,, dotsent
Rupture of the tubercle of the tibia and rapture of the ligamentum
MMSCle
patella due-to contraction of the quadriceps 0 the hip.
Xhirurgila no.4:82 Ap 154. (W-RA 7:6)
1. 1z kliniki obahchey khirurgii LeningradAkogo~pediatrichipokogo
instituta.
(TIBIA, wounds and injuries,
*rupt. of tubercle & rup. of ligamentum patella caused
by contraction of quadriceps femoris so.)
(KM, wounds and injuries,
*rupt. of ligamentum patella caused by contraction of
quadriceps famoris musc.)
THIGH" ixuacleso
*qaadriceps femoris, contraction causing rapt. of
tubercle of tibia and ligaawntum patella)

L 46045-66
ACC NR' AT6034089 SOURCE CODE: HIU/2502765/0"/003/0293/029
AUTHOR: Botarp Laszlo; Safarik, Imre--Shafarik,,I.
ORG: Central Research Institute of Chemistr (Magyar Tudomanyos Akademiaj,
Budapest
KozponEl mi
TITLE; Some thermodynamic considerations of the hydrated electron and other
intermediates in the radiolysis of aqueous solutions
SOURCE: Acta chimica, academiae s ient..-rum. Hungaricae, V. .44, no- 3, 1965, 293-299
TOPIC TAGS: radiolysis, dissociation ccnstant, redox reaction
ABSTRACT: Acid-base dissociation constants for H, H2, OH, and H02 were calculated
on the basis of the appropriate oxidation-reduction half reactions using standard
thermodynamic methods. The formal half reaction: e- aq + e- was introduced-for
the calculation of KH. The importance cf these equMbrium processes in the radiolyai3
of aqueous solutions is discussed. Orig. art. has: 1 figure, 8.formulas and
1 table. [Orig. art. in Eng.] [JPRS: 33,540]
SUB CODE: 07 SUB14 DATE: 160ct64 OTH REF: 021
Card

ACC NR: A-16036600 SOURCE CODE: UR/0000/66/000/000/0236/0237
AUTEOR: I:uzin, R, A,; Nevskaya, G. F.; Popov, V. I.; Sych1cov, Lirkin, A.V.-
Yurgav, V. V.; Abramova, G. M.; Ginzburp,, Ye. V.; I(alandaroval i. il.
none
ntal investigation of the effectiveness oil local ra dioproZective
sh i C Iin,-,TLari)ie`r0 Presented at the Conference' on Problems of - Sp~ace Madicine held In
~bscow from 24-27 May 1966/
SMWZ: 1,onferentsiya po problemam kosmichaskoy meditsiny, 1966. 2roblemy
kosmicheskoy meditsiny. (Problems of space medicine); materialy konf 0 rents i I
rbscow, 1966, 236-237
IOPIC TAGS: radiation shielding, solar flare, cosmic radiation biologic effect,
radiation protection, radiation dosimetry
ABST11M
IVIany '"'E'cult'106 are oncounte-L'ed in selection of a radiation method
suitable foi- study o-f the effect of local shieldinrr. The radiation field with-
-III Lle linnits ol' the irradiated object.must not vary more than. 4.1001a*. , The
dose differential amonre absorbed doses must. not.exceed 10% Local
A. the dose. Further~-
shieldi;n- rnusz pzoduce at least a tenfold weakening o'
=.ore, do-e -ower must be suffliciently high to model solar flares con-
L~;ard l/ 3

ACC NR: AT6036600
siderinig, t1ne limited stay of 'the irradiated animal in a fixed position. Ex-
-~erinaental calculations of the passage of protons through tissue have shown
at 'd h 'he average
-energ-y protons sca"er very little. For example, 6
ano e of' mu'lt-.ple scatterina for 660-Mev 'protons passing through a lead
2 is
-&Ulter with, a thiclaiess of 1010 g,/cm approximat tely 2%
Selection of poroton energies was made u'sing data on the distribution
of absorbed doses created by monoenergetic. pto~ons with energies.from
103-600 Mev in a water phantom. Since these distributions 'liave a dose
2
L.L 0 cn-,
czi::aren"al greater than 1076 with shielding thicknesses up t 3 20 g
it -%%,as dec-.ded to irradiate the animals from two sides.. Maximum equaliza-
Llor, of distribution with this method was obtained with 250-M.ev protons.'
lia local s"eld used was made of paraffin. A radiation field,was.produced,
a'. z'.,-.e irraciated objectwith a difference of =20%. To obtain more'uniform
radiation, an~nals were placed asymmetrically to the axis of, the proton
bea,-n and each side received half of the dose.
This me~,.od was Perfected with a he' terocteneous bone -paraf ffin plhantom.
Yeasurements made with this phantom showed a radiation field varying,
only 11% on the animals I surface. Furthermore, the differeh-Lial of absorbed
doses did nz,' . exceed 50/6. When individual body part's were shielded. the

A C C N R - AT - ---------
dose decreased 10-15 times behind the shield. Thus tha described satisfies
all the requir ements listed above, and can be
OAC-)-l
used in radiobiol study of the
effectiveness of local shielding. ZU. A. 'No. 22; AM ReporT, 66-i16
SUB CODE: .06, 18 SUM DATE: 0014ay66-

Card 3/3

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BNN3SzfXVlCH, I.I., kandidat tekhnicheskikh nauk; BOGIN, N.M., kandidat
tekhniche8kikh nauk; BYKOV, Ye.l., inzhoner; RASOV, I.I.. kandidat
tekhnicheskikh nauk; GRITSEVSKIT, M.Ye., inzhener; GRUBRR, L.O..
lnzhener - GURVICH, Y.G., inzhener; DAVYDOV, 7.N.. inzhener; TRR-
SHOV, I.M., kandidat tekhnicheskikh nauk; ZASORIN, S.N.i kandidat
tekhaicheskikh nauk; IYANOV, I.I., kandidat tekhniclieskikh aauk;
KRAUKLIS. A.A., inzhener; KROTOV. L.B., inzhener; LAPIN$ V.B..
inzhoner; LASTOVSKIT, V.P., dotsent; LATUNIN, N.I.. inzhener-,
MARKYARDT, K.G., professor, doktor tekhnicheskikh nauk; HAKHAYLOV,
M.I.. professor. doktor takhnicheakikh nauk; NIXANOROV, V.A., inzhe-
ner; OSKOLKOV, K.U.. inzhener; OKHOSHIN.L.I., inzhener; PARYINOV,
K.A., dotsent, kandidat tekhnicheakikh nauk; PMSOVSKIT,,L.M.,:
Inzhener; POPOV, I.P., Inzhener; PaRSHNNY, B.G., inshener; RATIMR,
M.P., inzhener; ROSSIYAVSKIY, G.I.. doteent, kandidat.tekhnicheakikh
nauk: RYKOV, I.E. kandAdat tokhnicheakikh nauk; RYSHKOVSKIY. I.Ya.,
dotsent, kandidat tekhnicheskikh nauk; RYABKOV, A.Ta., professor
[deceased); TAM, S.A., kandidat takhnicheakikh nauk; KHAZEN, M.M.,
professor, doktor tekhnichaskikh nauk; CHKRNYSHRY, N.A., doktor
taidinicheakikh nauk; WIN, L.Ye,, professor-, doktor.tekhnicheekikh
nauk; YURNNIV, B.H., doteent; AXSENOV. I.Ya.-, dotsent, kandidat*
tekhnicheskikh nauk; ARKHANGBLISKIY, A.S.. Inzhener; BARTBNW, P.V.'
professor. doktor tekhnicheakikh nauk.- BURNGARD, K.A.,-kandidat
tekhnicheskikh nauk; BOROVOT. N.Ye.. dotsent, kandidat tekhnicheakikh
nauk; BOGDANOV, I.A.. in7htner; BOGDA30V, N.K.~ kandidat takhniclhs-
skikh nauk; VINNICERNKO. N.G., dotsent, kandidat ekonomicheskikh nauk;
(Continued on next card)
11 11, HII d: 111,1111: 11111 P I ii;' i I iiT~~.

ERNNSHVICH, I.I.--(continued) Ca rd 2.
VASILOYEV, V.F.i GONCHAROV, N.G., inzhener; DARIBIS, A.T.. inzhener;
DOBROSELISKIY, K.X., dotsent, kandidat tekhnicherkikh nauk; DLUGACH.
B.A., kandidat tekhnicheakikh aank; YIFIXOV. G.F.. kandidat takhni-
cheskikh neuk; ZIMBLINOV, S.V., professor, doktor tekhnicheskikh
nauk,- ZABILLO. M.L., kandidat takhnicheakikh nauk: WIN. K.P.,
kandidat takhnicheskikh nauk: KARNTNIKOV, A.D., kandidat tekhnich(q-
skikh nauk; KAPLUN, F.Sh., inzhener; XANSHIN.X.D.. KOCHHEV. F.P..
profeasor. doktor tekhnicheskikh nauk; KOGAN, L.A.. kandidat tekhni-
chesklkh nauk; XUCHURIN. S.F., inzhener; LIVASHOY, A.D., inzhener;
KMINOVIGH9 B.M., dotsent, kandidat tekhnicheskikh nauk; MARTYNOV.
H.S., inzhener; MIDILI. O.M.. inzhener; NIKITIN. V.D., professor,
kandidat tekhnicheskikh nauk; PADNYA, V.A., inzhener; PANTILBYRY, P.I.,
kandidat tekhnicheakikh nauk~ PRTROV, A.P., professor. doktor tekhni-
9
cheskikh nauk; POVOROZHRNKO, V.V., professor. dcktor tekhnicheskikh
nauk; PISKAREV, I.L. dotsent. kandidat tekhnicheskikh nauk; UWIYIV.
Ye.S., kandidat tekhaicheskikh usuk; SIMONOV, K.S., kandidat tekhni~
chekikh nauk; SIMANOVSKIY, M.A.. inzhener; SUYA20V,.I.G.. inzhenerl
TALDAYEV, F.Ya., inzhener; TIKHONOV, K.K., kandidat tekhnichaskikh
nauk; USHAKOV, N.Ya., inzhenr; USPINSKIY, V.K.', inzhener; FELIMUN,
N.D., kandidat tekhnicheskikh nauk; FAWORrOT ~ G.T.. inzhener;
KHOKHIA)V, L.P., inzhenr; CHIRNOKORDIK, G.I. pr
9ofaaaor, doktor
takhnichaskikh nauk; SHAKAY.MV, M.F., inzhener;
inzhener; YAKUSHIN, S.I., inzhanor; GRANOVSKIY; P.G.~', redaktor;
TISHCBXNKO, A.I., redaktor; ISAYIV, I.P., dotsent, kandidat takhni-
cheskikh nauk, redaktor; KLIHOV, V.F., dotsent:kandL.da,t takhnicheakikh
(Continued on next card)

BMSHEVICH. I.1.- (continued) Ca ri 3 -
nauk, redaktor; MARKOV, M.V., inzhener, redaktor; KALININ, Y.K.,
inzhener. redaktor; STEPANOV, V.H., professor, redaktor; SIDOROV. H.I..
inzhener, redaktor; GXRONIKUS, B.Ye., kandidat tekhnicheakikh nauk,
rednktor; ROBICLI, R.I., otvatstvannyy redaktor
LTechnical reference manual for railroad engineers] Takhnicheakii
spravochnik zheleznodorozhnika. Moskva, Gos. tranapzhel-dor. izd-v'o.
Vol-10. Dilectric power supply forrailroadel linergoonabzhenie sh-eles-
nykh dorog. Otv.red. toma K.G.Markvardt. 1956.- 1080 p. Vol.13.
[Operation of railroads) Ekspluatataiia zhelez~nykh dor-og. Otv. red.
stoma R.I.Robell. 1956. 71-9 p. (MIRA 10:2)
1. Chlen-korrespondent Akademii nauk SSSR (for Petrov)
- (Zlectric railroads), (Railroads--Management)
I 211-L, iil!'M lf~ El A15! I I I E: LP 1;1-f A :1 11 :1 1 ~A I'VE:

MARKOV, Aleksandr Vladimirovich: SHAFIRKIN, B.I., redaktor: BOBROVA, Ye.K.,
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_58-1
Shafiro, 'Ya., 1Sh.

TT T LE' -a Yergeni (Novyye dan-
'ez, Data on the Tectonics of Severny~
ryye po tek+on.-Lke Severnykh.Yer.-eney)
PERIODICItL: izve3tiya Akademii nauk SSSHL, Seriya geologicheskaya,
19551 Nr,10~ pp 46- 55 (USSR)
ABSTIMPICT. The study of the complicated structure'of the "Severnyye
Yergani"~ showed bliat this region has been subjected to many
Apetonic "ransfcrmat4ons since the Paleozoic Era,~when the
formation of the folded structure of 'he scutin-western part
of tihe region and the sagging of its larger~part occurred.-
T'he sagging became more intensive in-the Permian-Trias.sic
period and the depression was filled in the.Lower Triassic
+
period, - ii thick layers of multi -col'6red rodks. Sirce, the
end of period the whole region has been subjected, to
alternate sagging and elevating processes. -In the Oligo-,
ce-an epoch, the wqole region was covered with a sea, which
--all-reated in the Miocene epoch when the region finally.be-
came dry lani. Its eastern Dart sagged again in the. Sar-.
Doch.
matian *tage, but emerged at the end afthe 111.1iccene a

Card 1112 -
-.a authoz deecr4bes the various strud-tural changes and

-he ~ec+on,,-s o~ 'evcrnyye Yergeni I n-4 1
Data on
di_"Ierent eedimensary formaticn3 resuIt-ing from these tec-
tonic transformat--ons. He ment-Iona the following geolo-
gista whose work he has summarized.in 'chislarticler A.P.
Karpinskiy, A.D. Arkhangei~skiy, 11.5:, Shatskiy, 71'e. V.
?.'iIano,73k_iY and A,G, Brazhnikov, Therc are maps.
diagram and 8 references,,
SUB1,11WED: June 10, 195T
ASSoCIATION: Tsentralt'naya nauchno-issledovateltskaya laboratoriya
tresta Stallngradnefte-razvedka, g. Stalingrad.(The:Sta-
lingrad Central Ssientift"co-Research Laboratory of the
Stalingradnefterazvedks. Trust)
l._Geology-USSR 2. Geophysics--USSR. 3. Geological-time
Determination
Card 2/2

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SKIMIOT9 Aloksey Tsevolodovich; SKIRUOTA, Kara Valeriariovna; WWIROTA,

!:'I'!* I 'I I 11-U-7FFTF777777"7'~IT

DOBYCHIII, B.D., prof., red.; KAZANTSEV, Apollinariy Innokentlyevich,
prof., doktor med.nauk, red.; SHAFIROVA, A.S., red.; KARASI.
V.D., tekhn.red.
ECollected papers on the structure of the peripheralnervous
system] Sbornik nauchnykh rabot po izueheniiii struktury
perifericheakoi nerv oi siBtemy. Pod red. B.D.Bobychina i
A.I.Ks zantseva. Irkutsk, 1959. 189 p. (MIRA 14:2)
1. Vsesoyuznoye nauchnoye obshchestvo anatomov. gistologov i
embriologov. 2. ZoveduyuBhchiy kafedroy normallnoy anatomil
Irkutakogo meditsinskogo institute (for Kazantsev)e
(MVES, MIFEM")

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ACC NRt Ap6036898 SOUkdCC6DE'.--tJlfl62~16-16~6-1066/'Oii/004-3-/0045
1AUtiOR: Antsiferov, V. N. (Perm'); Sh.afit, 1. A. (Perm')
0 G: none
TITLE: Investigation of the technological characteristics of,W-Ni-Cu alloys
dispersion strengthened with zirconium dioxide
SOURCE: Poroshkovaya metallurgiya, no. 11, 1966, 43-45
TOPIC TAGS: sintered alloy, tungsten nickel alloy, copper containing alloy,
zirconium dioxide containing alloy, alloy sintering, alloy density
ABSTRACT: The effect of the additionof 0.01-0.4% Ni, 0.1-40% ZrO2 and 0-15% Cu on
the density of sintered tungsten-base alloys has been investigated.. Alloy powders
were compacted under a hydrostatic pressure of 1100 atm, sintered at 235-1265C in a
hydrogen atmosphere for I hr and at 1785 1 10K for.2 hr, and furnace cooled.
Increasing the nickel content to 0.4% increased the density of sintered compacts from
79% for unalloyed tungsten to 91.1%. Further experiments were made with W-0.41 Ni
base alloys. Additions of up to 3% Zr increased the density of sintered W-0-0.4% Ni
?2
alloy to 96%. With further increases in the ZrO content, the density gradually
decreased, and at a Zr02 content of 10% became equal to the density of the initial
W-0.4% Ni. alloy. Small copper additions (up to 3%) slightly-increased the density of
W-0.4%Ni-10% Zr02 alloys, but larger additions decreased-it below that of the initial
Card 1/2
AP6036898.
w-0.4% Ni-10% ZrOZ alloy. The obtained results showed that W-Ni_Cu_ZrO2 alloys
sintered at 1785K in hydrogen have high density and can be used as structural.
materials. Orig. art. has: 4 figures. EMS]
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YUSHCHMO, N.R., doktor tekhn. nauk prof'.; MIDITEVICH, L.N., kand. tekhn.

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USSR&-hemistry Wtal-,Hydride~ 21, -'Jun'~ 51
Kift6 C 0 the Reaction 'of. Calcium With T~dli;6--
gen, V4~ A. Shushunov, A. 1. Shafiyev, Sci Res
Inst Cheii, Gor~kiy State U, U.
"Doic Ah Nauk SSSR" Vol I=IIIJ, No 6, pp. 1181-
1n previcu~-, ;,)hases of the investigation, which
deals ~reac tions of me tals with
gases and. of a"I'loys v-ith alkyl halide vaporsj
existence of zone in which temp dependence of
reaction rate does riot follow Arrhenius' law has
been eLtabl:~shed. Wben layer of CaH2 reaches
184 T20
USSR/Chemistry - 14--tal Hydrides 21 Jun 51
(Contd)
certain thickness in reaction of Ca with H2, d if -
fusion of H2 Throug)a the layer becomes slower
than chem conversion at Ca surface. At higher
temps, -rate of reaction is again detd by kinetics
of chei-,i process. Arrhenius7 law is applicable in
entire range investigated, up to decompn t-re of
CELH2.
184T2 0

'
-

:A.
calci"n hydride. :
at the formation of
and zA, 1. Shafiev (St
'

=--O(T02T7cf.,
31
26, (i
la order to study the range of tamp. (or which;there
neg. temp. coeff-far. the rate of the.heterageneaus cheni.
prcv-,;, the reaction of Ca with It was studied at 12(f-
5309. 1T4 reaction, forming' calciunt hydride,
occuls wiEho it aut ocjxtalys;s,~. and its rae

yaride layer. Pl,~;l
ent ~,n the mte of diffusion of If through the h
Tile detil. of the tPlop. delknileuce for the' reactiojl~ rate j., J~
,
Dtly IM for.' We
WI)s Wguificu
showed that Om temp. COW
Chem. stage of 016 p CeS3 than r - the diffusiou stage.,
r
u
f chem. Prawn; was 65M &at;/-
The activation energy
o
mole and for the diffusiurt process it was 15,000 cal./Inale.
tovnr Leach

w

allTI-ORS: Korshu-nov
1. A., fhai'Vey, A- 1- 78-1-17/43
,
TITLE: The Chemical State of Radiophosphorus-32 Formed in Some Targets, With
Neutron Irradiation (Khilnicheskoye sostoyariye radiofosforaw-32.- po=
luchayushchegosya v nekotorykh mishenyakh pri:obluchenii~ikh neytro-
nami).
PERIODICAL: Zhurnal Meorganicheskoy Khimii, 1958, Vol. 3,,vir 1, pp. 95-99
(USSR).
ABSTRACTj The above questions concerning radio-phosphorus in the moment of its
formation are neglected in spite of a thorough investigation of the
nuclear reactions of its production. The choice of the method of iso=
lation of any isotope whatever, especially -without carrier, depends,
however, on the chemical state of the isotope in the target. The che.
mical state of the developing radiophosphorus;for a number.of targets
various chemical and physical properties; CC1 S C12 , CHCI
with
4P 2
.
aC'2, etc. was i7esti-
0
, MIS, NH 4Cip M'gCl2' C
Na2SO 4' Na2so
Na2S2
1
,
3
3
c-ated in the present reFort. The separation 61f phosphorus in phosphate-
and phosphite-ions -was carried out according.to the methodics of refe=
Card 1/4 rence 14. The chemical state of-phosphorus-32, in CC14.,The authors prox-
I , ~j- =T.M.

The Chemical State of Radi-ophosphorus-32 Formed in Some Targets 78-1-17/43
With Neutton Irradiation.
ved that the whole radiophosphorus from rCl 4 cannot~be obtained by
ordinary extraction. This was only achieved by re-cooling in the
presence of elementary bromine or.chlorine under an HIM -solution or
of water. Table 1 shows the ratio between the~valence Rrms of radio=
phosphorus and the percentage of the non-extractible.part according
to the nature of the extrahent. During the formation of radiophospho=
rus it is adsorbed on the walls of the flask which contains CC14 . The
quantity adsorbed depends on the water-content in the target (table 2)._
It hence results that radiophosphorusiwith large quantities, of1water
(lo ml) especially with acidifying and agitating passes almost comple-
tely over to the water layer. 'Kith an higher water-~content
of CC14~ the
adsorption of the formed radiophosphorus increases,substantially-. The
chemical state of the radiophosphorus formed .in 001 is: influenced by-
:4
water, gaseous ammonia, chlorine and acetone,: if they are added prior
to irradiation. The oxygen dissolved in CC1 4 doeshot have this effect.
The duration of the irradiation favors the formation,of the pentavalent
radiophosphorus (table 5). Table 3 shows that!the water-content of the.
substance of the target favors the stabilization of. the radiophosphorus
Card 2/4 in trivalent state. The formed "hot" radiophosphorus- atom can consequent=

The Chemical State of Radiophosphorus"32 Formed in Some Targets -7871-17/43~
With Neutron Irradiation.
ly form various chemical compounds after the loss of~a substantial
part-of its kinetic energy-. If free chlorine is present in the tar-~
get,.considerable quantities of PC1 5 are formed. Part.of the phos.-
~phorus atoms remains in-elementary statelor forms non-extractable
compounds by means of water. The valency-stabe-~of radiophosphorits
is changed during its extraction. The chemical'state of phosphorus-.,
32 in other targets. Radiophosphorus forms PSC1 2 in a ta rget of
5 C1 withand-w=iout the addition of carriers-. The chemical state
2 2
of radiaphosphorus in targets of.anorganic salts containing both sula
fur and chlorine depends on the oxidative.;-reductive properties of the
respective compound,,on the presence of the crystallization water and
the thermal treatment prior to and after irradiation.,Table 6 contains
test~-results on-the dependence of the valency-state of the forming
radiophosphorus orr the chemical nature of the substance of the taraet
of the crystallization-water contained therein~.and of the mentioned
treatment. Radiophosphorus forms, together with higher oxidized sub-
stances, less oxidized compounds!- in compounds with reducing proper-_
ties:. Water favors the formation of higher oxidized compouncLs. The
Card 3/4 thermal treatment of the target after its irradiation with neutrons
VI

.The Chemical State of Radiophosphorus-32 Formed in Some Targets; 7 B-LwI7/43
With Neutron Irradiation.
causes. the transition of radiophospherus in compounds: of higher va-
lency. The ultra-violet irradiation causes the formation of pentava-
lent phosphorus in CClh. Irradiations with- both garma and neutron
rays favor in both kinds of targets bhe formation of radiophosphorus.
of higher -.ralene~ex.
There are 6 tables, and 14 referencea, 9 of which are Slavic.
ASSOC iATION*GorJkiy;, SW* iffti-mrsf-ty-im U. -t.-1bb%rjpYxki't,' Chair f or Radio,-
chemistry (Gor kovs-kiy gosu~arstvennyy universiltet~ -1m. N. I. Loba=
chevskogo, kafedra radiokhimii).
SUBMITTEM. June 18, 1957.
AVAILABLE: Library of Congess.
Card 4/4

A JI
AUTHORS: Korshunov, I. A., Shafiyev, A. 1. 78-1-18/43
TITLE' The Methods of Isolation of Radiophosphorus FroaChlorine. and
Sulfur Containing Targets (Metody vydelpniya radilofosfora iz
misheney soderzhashchikh.khlor i seru).
PERIODICAL! Zhurnal meorganicheakoy Khimii, 1958P Vol. Nr 1, pp. 100-103
(USSR).
ABSTRACT: The problems of the isolation of radiophosphorus.without addition
-of carriers from targets, besides carborldisulfide, are neglected.
1 -0
Methods of Isolati n of radiophosphoruswithotit carrier from CC11.,
CHC13 , s2C12.0 tE4C1, MgCI-2, CaCl., Na 2SOW~ jja2S2 039 KCt'S and
other substances, as-targets, were investigated in the present re-
port. The isolation by means of an electric field (reference 1.5)
can be applied with the CS -target, but', not with the CC -targget.
2 14
The authors proved that the perfection of the isolation from CC14
by means of this method depends on the water content and that -it
increases from 25 to 5oO/o by,using acqu The saturation
eou's CC14
Card l/_T of the CC14 with elementary sulfur increases the precipitation of

The !-rethods of isolation. of Iladiorhosphoru-5 Frcn 78-1-18/43
Chlorine- and Sulf1jr Containing Targets.
radiophosphorus on the electrodes up to 75cl/o. The study of the
methods of adsorption of the extraction of the radiophos-phorlas.
fron Col 4 (table 1) shr.-r that silicagel is the best adsorbent.
Further, the adsorption of radiophosphorus on the walls of the
irradiation flask can be used for extractjoh, This is achieved
best, if, prior to -irradiation, 0.,6 to 0,8 ml. water per 1,0 li-
ter CCl 4 are added. Po to 9oo/o of radiophosphoru slare adsorbed
on the walls by agitating such.a target from time to time. Radio=
phosphorus can be extracted in a still simpler way by agitating
the target during.the irradiation and by adding lo to 2o ml water
per I liter CUL (approximately Q,oO/o radio--phosphorus). The di-
stilling of CC under a water layer, especially when beinr, acidi=
14
fied with FJIO and with a small- addition of,eblorine makes an 1000/0
3
isolation of the radiophosphorus possible.~it can be*obtained from
chloroform in a similar way. Radiophosphorus is obtained frorL su.1f ur
monochloride best by means of passing the target:through a coilxmn
of air-dried silicag
gel. Radiophosphorus is.desorbed from- thia by
Card 2/3 means of water acidified up to 95'/o. The mAhod~.of boiling with

The Methods of Isolation *of Radiophosphoras From 78-1-18/43
Ghlorine- and Sulfur Containing Tar-ets.
acidified water can be applied for the isolation of radiophosphorus
from sulfur irradiated with neutrons-, dissolved in.chloroform and
toluene. From salt solutions which served as targets-, radiophospho-
rus- is isolated best by adsorption on aluminuw~ or ferric hydroxide
on: difficulty soluble deposits of BaS04 and BaCroVas well as.of
aluminum oxide.
There are h tablesp and 21 references-, 13 of wh1ch are Slavir-
ASSOCIA.TIoN: -G6r'kiy SUte Uaiversity.im. N.I.,,-Lobachevskiy, Chair for Radio-
chemistry (Gorlkovskiy -QSUdarstvenr-,%rY Univ.ersitef, im. N. I.
Lobachevskogo, Kafpdra radiokhimii).
SUBMITTEDt June 18, 1957-
AVAILABLE: Library of Congress.
Card 313
1 U,

Gorlki-yj 1959, 13 pp (mfin of !Uigher Education USSR. Gorlkiy
State Univ L-i N.I. Lobachevsldy) 1,50 copies 3,31-59, 11-7)
9
',[.I f

d"IT III
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