SCIENTIFIC ABSTRACT SHAGEYEV, Z. A. - SHAGINA, L. N.

• Document Type: CREST
• Collection: Scientific Abstracts
• Document Number (FOIA) /ESDN (CREST): CIA-RDP86-00513R001548520013-2
• Release Decision: RIF
• Original Classification: S
• Document Page Count: 100
• Document Creation Date: November 2, 2016
• Document Release Date: August 9, 2001
• Sequence Number: 13
• Publication Date: December 31, 1967
• Content Type: SCIENTIFIC ABSTRACT

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SHAGEYEEV, Z. A.
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LAWMT1YEV, V.I. Prinimal.-I uchastiye-. POLISHINSKIY, V.V.,,starshiy
nauchnyy sotrudn!k; AKOPOVA, A.A.,, starshiy nauobnyy sotrudnik:
SHAYKHUTDINOVA, L.K.; in21.; ~M ~.A.; lnzh.; TUMMOVA,
A.M-, preparatori STAROSTIN. P.A. BALANH(FOVJI A.P.J4
motorist; ARTEMliEV, V.G., motori'st.
Using the heai7 residual fractions of Tatar sour crudwas a
fuel for gas turbines. Nefreper. i neftekh-Lm. no.4.927-3/4. 163
(MIRA 17:7)
1. Tatarskiy neft7anoy naucbno-issiedovatellskiy institut.

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VOYTSEKHOVSKIY., N. K. . inzh. ; SFIAGIAKIMEDOV, It. S. , inzh.; BEKUSHEV, V. L
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L 13092-M EWT(IVER(MVEWP(d) TJP(C)/RPL WW16GI
ACC NR: AP6002076 100 URCE CODE: UR/0204/65/'005/006/09:04/0908 s
amanova,~ I
Mazitova, F. N.; Ryzhmanov, Yue M.;~Shagidullin,:O.' P.,,L A~ ~4!I~
ORG: Institute of Organic Chemistry.AH SSSR itd rganicheskoy;:khimii
(Insti, ~., it o : ~T ~
~AN SSSR) P hyRi _MA~j~R izansk Z o
Institute ofKqKM., iy f ik,
;tekhnicheskiy institut AN SSSR)
TITLE: The EPR method of investigating the mechanism ofantioxi-dant action:
.SOURCE: Neftekhimiya, v. 5, no. 6, 1965, 904-908
TOPIC TAGS: EPR, free, radical, oxidation,-inhib~~iong b nZ03r].
!peroxide, EPR spectrum, spectrometer, C.:6
'ABSTRACT: Oxidation of the methyl ester of o-amin 'but 1 no
qiR7-,Le rt by b4nzoyl
SolUt,
:peroxide was studied in anhydrous benzene on at room'land slightly above,room
'temperatures using EPR technique for characterization of the intervediate products.
!The object of the work was to study antioxidant action in t`he methyl esters of o-
EPR:spectra were taken at room temperature!using:a:PE-
were~:
g1301 radiospectrometer. The ester to peroxide molar ratiL and
2:5~
Card 1/3 L-~~-UDC-:-~ 5112.943.1"; 38.

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AUT!"OR:
-Shag-idullin, R. R.
30v/48-22-9-17/40
TITLE: ;1~ration Spectra of Some Organophosp,horus- Compounds
(Kolebatellnyye spek.try.nekotorykh fosfororganic"neskikh
soyedinenly)
PERTODICAL: izvestiya Akademii nauk SSSR, Seriya fizicheskaya,
1958,
-
Vol 22, ITr 9, PP 1079 -:1o82 (USSR)
ABSTRACT: The study of the vibration spectra oflorganophosphorus
compounds revealed that the presence of a number
of atom groups in the molecules-is accompanied by the
,occurrence of characteristic frequencies in the-spectrum,
of infrared absorption and in that of,combination
disDersion (Refs 1-5). The author attempted to
characterize specific atom groups by their'spectral
data and thus to estimate the structure of new organo-
phosphorus compounds. The diversified~:studies initiated in
-K-lzan' under the supervision of A.Ye-and.B.A.Arbuzov
,
both Members, Academy of Sciences,,USSR, covered the
,
synthesis and the investigation of these organophosphorus
compoulids. The Raman spectra and the s;pectra of infra-
Card 113 red absorption of 11 liquid substances were recorded.

714,J-22-9-1714'i
7-ibration Spectra of Some Organophonphorus Cor,11-'rlindl:-1 30
These substances were synthetized by P.I.Alimov, N.P.
Grechkin and 0.11. Fedorova, Scientific Collaborators
of the Kazan' Branch, AS USSR. According to the
method of their preparation and according to.their
structure they can becategorized in two series. Sub.stance
1 is specified by this formula:
CH
/12
C2H5 OP N\
CH
2 2
It was found that the-infrared spectrum of this
compound varies with,time. The equip!-~ient used in the
'h C>
experiments and (.-e method of investigation was described
already earlier (Reff's 6,7). This paper.only,contai-ns
the infrared sDectrograms and the characteristic frequencies
found (Table).-There are I figure, 1 tablel and 12
references, 7 of which are Soviet.
Card 2/3

1 1 z 1 ;I t . . ~,!O 1~I I -
I i . . .
; i i Ili- itllii- ~ III 11 1.;;;!

8(2) SOV/32-25-3-48/62
AUTHORS: Kashayev, S. Kh. G., Le, B., Shagidullinv*,Ro R.
TITLE: On the Methods of Producing and Evaluating Raman~Spectra
(K tekhnike polucheniya i obrabotki spektrov kombinatsionnogo
rasseyaniya)
PERIODICAL: Zavodskaya Laboratoriya, 1959, Vol 25, Nr~3, pp 368-369 .(USSR)
ABSTRACT: Some innovations in the analysis methods of gasolin fractions
as to their hydrocarbon composition by m
e~kns of :the home-produced
.
unit consisting of a spectrograph ISP-51,:,'a comparator IZA-2y~ and
a microphotometer MF-2 are described. Analyses~vOere carried out
according to the methods proposed by the Fizicheskiy institut
Institut organicheskoy khimii AN SSSR (t-1-hysics', Institute and
Institute of Organic ChemistryAS USSR). qonsidering the,
recommendations of Ref 21 the Hg lamp EP S-102'was connected,
via an electron stabilizer SN-2 and compensator LATR-1.:The
diaphragm according to Gartman was exchanged and thus a
sharper spectrum obtained. The position of the'objective.was
altered according to the stage of the analysis. In order to
reach the maximum intensity of the spectru:m without using too
many vessels, a paper sheath (Fig 1) was made and used.
Card 1/2 In order to be able to use films of smalle~r size than UA. b0 IX9
MIT Prili 0"11 011

SOV/32 25-3-48/62
On the Methods of Producing and r,,valunting Raman Spectra
an insert to the box was made (Fig 2). A small device (Fig:3):
was designed to.facilitate the working with substances
containing fluorescent admixtures. An instrumeni(Fig 4) made
of brass foil was used for entering signs on the film. In
order to facilitate the visual photometric'evaluation a
comparison with an iron spectrum is recommended.
There are 4 figures and 2 Soviet references.
ASSOCIATION: Laboratoriya fiziko-khimicheskikh metodov issledovaniya
Kazanskogo filiala Akademii nauk SSSR
,(Laboratory for Physico-chemical Investigation.Mathods of
the Kazan~.Branch of the Academy of Sciences,USSR)
Card 2/2

M65
S/062/60/000/012/004/020
31BQ55
AUTHORS: Grechkin, N. P. and Shagidullin, R. R...''
0 Mine Derivatives.
TITLE: Or-anophosphorus Compounds of Ethylen;
Communication III. Addition of Acids to the'Amides of
Phosphinic Acids 11111ith Ethylenimine
PERIODICAL: Izvestiya Akademii nauk SSSR. Otdeleniye khimicheskikh naulf,
1960, Ito. 12, pp. 2135-2139
TEXT: The pregent publication gives the results obtained in the N-di:ethyl-
phosphonaminoethylation (the term used by the authors) Of carboxylic acids.
The authors apply this term to all reactions in which the.amides of:phos--
phinic acids with ethylenimine add to a number of com pound's under cleav-a~e
of the ethylenimine ring, as shown in Refs. 1 and 2-1 By this reaction, addi-
tion products of diethyl phosphinic acid ethyleneam ide and several carboxylic
acids iere obtained (Table). All the esters listed in the,table werepre-
pared similarly, equimolar amounts of diethyl phosphinic acid ethyleneamide
and the acid were heated at 110-120 0 C in sealed tubes I. for :6-7 h. Af ter dis-
tilling twice, the pure product separated. To establish the: structure of the
Card 1/3

87165
Organophosphorus Compounds of Ethylenimine S/062 / 601,000 10 1 2j,-"'o)4
jU2
Derivatives. Communication III. Addition of B013/ 13055
Acids to the Amides of Phosphinic Acids With
Ethylenimine
compounds obtained, the authors evaluated the infrared.absorption spectra
of the reaction products of diethylDhosphinic acid ethyleneamide and,acetic-
respectively propionic acid. Diethyl phosph.1-nic acid ethyl a.mide~was used
as model substance. The spectra were run on a HKC--12 (,IKS-12) spectrometer
with adjustable slit width using a NaCl prism in the 700-2400 cm-1 region
and a LiF prism in the 2300-3600 cm-1 region. The spectra of-the three
above-mentioned compounds in the 2300-36oo cm-Tregion are shown in Fig. 1.
(C R PNH 2a) H PNH_CH CH OCOCH or:
2 50)211 C2H5 (C2 50)2 2- 2 3
ZCH 2- CH2OH
2b) (C H O)gPN,\ 3a) (C Ef ITH-CH CH.-OCOCOH -CH or
2 5 C-CH 2 50)2P 2 2 3
0 3
0
CH CH OH
2 2_~
3b) (C 111 P--N
2 5.J)211
cc,[ CET
2 3
Card 2/3

87165
'3
Organophosphorus Compound;- of Ethy-lenimine S.,/062/~O '00,6/012/004/0201
Derivatives. Communication III. Addition of B013/BO55
ficids to the Amide:~ of Phospbinic Acids With
Ethylenimine
The infrared spectra indicate the )resence of intermol,ecular hydrogen bonds
between the nitrogen of the amide :,rroup anti the oxygen atoras of the Dhos-
phone group (P-0) and the other gronp (C.0)- The SLY-LIC ture of the imbstatwa
obtained by the xtion of diethyl phosphonic acid on diethyl. phosphinic acid
ethylene amide is still unclear. The study is, being continued. There are
1 figure, 1 table, and 6 references: 3 Soviet and 3 US.,
ASSOCIATION: Khimicheskiy institut Kazanskogo filialA All SSSF
(Chemical Irstitute ofthe Kazan' Branch of the AS USSR
SUBMITTED; June 19, 10,59
Card 3/3
11111 1T7, _."i, IH'

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aVd-5816V=1bo i io%/ 120
A160/A161
AUMORS: nagidullin, R.-R.,.Greahkin, N. P.
T-rff Y. - ~ftbratlorraf spectra of zome diethylene amides of
ELikylthiobhosphoric acidz
PERIODICAL: 1~efer&ti'vn~y zlVdimiil, Plzlka~ no.. 1, 1963, 23, abstt%dt W-156
(In collection- "Kh1mlya I 'PriatenehiYe ?osrororgan' ~Da~inenljw.
M., AN ';SSR, 1962, 112 - 115)
TEXT:~ The infrared absorption spectra and the Haman~zpeclra of: ii nu&et- at
new d iethlene amideu of a141thiophosphoric aoids wore ifiva'stigAt4d'; A is ahd&
that the pulsation vibratibna of the ethylenimine ring in Ithe pr'66bfibe 0k ~fiba--
phorus appear to be adequaiely chardateristic by their freq;uerla~ and M+enalti,
and that the corresponding lines and tands, which clearly appear, in the infrared
spectra, may serve as a good analytic indication, th the region'of W 01W-1
vibrations oF the C - N bonds at thering are anIfested. A strong Infrared. ab-,
sorption was observed In the region of c930 am T. is identified-with-en asy*-
(jAM 1/2

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S/051/62 1.5/002/0.03/o14
E032/_E314
AUTHORS: Gariflyanov, N.S., Danilova, A.V. and
ShaZidullin, -P,.P,.-
TITLE: -par-amaGnetic resonance and absorp'tion
spectra in, the visible region of alcohol And glyccrin~
solutions of Ti
PERIODICAL: Optika i spektroskopiya, v. 13, no. 1962,
212 - 215
T ZXT A study-,.is reported of EPR lines of the green and
violet modificatiod5 of TiCl .1-1 0 solutions. Glycerin and
absolute alcohols *(~? ethyl, ei'hyi and isopropyl).:i-rere Ius ed as
the solvents. The 'specimens were rapidly sealed in thin -lass
+++
capillaries since alcohol solutions of Ti salts were found
t6 be unstable and oxidized to Ti Measurements were carried
out at, N1 = 9320 ',Nlc/s using.the standard radios pectrom et er
-1301 (RE-1301) at 400, -995 and 77 OX. The line 'width 6H was
daterm3'-ned as the distance between the maximum and minimum of the
first derivative of the absorption curve. The'results of line-
wid-h measurements and 'he spectroscopic splitting factor at
Card.1/5

S/051/62/013/002/003/014
Electron paramagnetic .... E032/r314
T = 295 .0K are given in Table 1. The intensity ..o f. the EPR lines
in liquid violet glycerin and alcohol solutions 'is very 101-T
compared with the intensity due to green glycerin solutions. It
lere:Cor-e considered that the EPR lines of liquid violet
.is t1
solutions are exclusively due to a small amount of green
asymmetric complexes of the form:
+
Ti (CH 01.1) LTi (C H OH) C1
3 4C'~21'; 1T't'P50H)4Cj-2)+; 3 7 4
and iLC3H (OH) I cinj+
IT 5 31
In supercooled alcohol and glycerin violet'soltit:ions.of Ti -there
is a -large low-synmetry field component due to particles in
the second coordination Sphere (the motion is frozen). For t'his
reason, in the super-cooled state each paramagnetic Ti +++ ion:
in violet solutions contributes to the intensity of the SPR lines.
At room temperature, on the other 11tand, owing to the ion,(- spin
lattice relaxation time, Ti +++ does not significantly contributed
%1o tile intensity of the EPR lines. As the roo;iv:teimperature is
Card 2/5
1;-!'; H!!T

Electron natic
,)arama,-,, E052/E3111
a-)oroaIched 'fields at the
6.1e colnpa,2nt of low-symmetry electric
TI ion t ends to average out and electron paramarnetic
absorption is ali;iost entirely due to green asyi-iii:ietric cocaple-xes.
T:iis 2henomeno has been used to determine the..percenta--e concen-
~ration 0-,
L j. Zree-n compl exes in violet solutioiis on, t1ye- nature of
the solvent, and the results are Ziven in I~able 2-, The',asswued
was Lhen ChCGIced by carrying out -spectroscopic absor-,
Dtio-n measurements t1he CL~- 2"M (SF-2M)
It- was found that the absorption spectra in the irisiblo ra~,io
are in _rood agreciaent with the above interpretation of th e
EPR spectra. There are 2 tables.
SUBj,,AIITTED: June 9, 1961
Card 315

S/051/62/015/002/005/011,
Electron paramagnetic .... E032/E311,
Table 1: X ey 1 Concentration, inole/litre;
2 611, Oe; 5 S-factor; Violet solution
of TiCl H 20 in methyl alcohol;
5 - Violet solution in e-thyl alcoliol;
6 - Violet solution in isopropyl alcohol;
T
7,- Glycerin violet solution of Tici H 0
8 - Green glycerin solution Of TiCi F. 0
3 2~
Table 2: Violet-solution Percentage concentk-ation
TiCl H 0, 1 mole/litre of the "green modif ica tion"
3 2
Me thyl alcohol
Glycerin 7
Ethyl alcohol
Isopropyl alcohol
Card 4,15

Electron paramagnetic ... C032 /E514
QD r
P
arl ;Ipr. 1 4
U-011TO C] 'ItTpa

411 apcr. "aimp
17
Table 1:
II~~OJIOToowit pacTuop TiCl 11 0
3 2
0. 5 10+2 1*15-24-0,102
B 'MM1,10HOM CL111111TO O-TH 10::2 1.9524-0.002
2 51 + 2 1.95:3) + 0.002 0.06 10+ 2 11.95210.002
t -40, 2 1.953+0.002
0.5 15+2 1.953+0.002 1"Imlep aTIODIAR q'.10.-,OTO1Iuii
0.25 25 -- 2 i.95370,002
0.12 24+2 1 1.9.53;:0.002 pao-mop TiC1,11.0
0.06 2172
1 1.953--1-0.002 2 45
0.03 2 +2 1.953+0.009
3 1 43-;-2
- 0.5 39 2
0.25 .39 2
-
G, ID110.10TOAHArt PlICTROP D OTTMOBOM 0.12 4L+
2
CUUPTO 0.06 41 +2
2 184-2 Loio+0.001) 0.03 4242
0.5
1512 Lqi
oto.oo-,
2115 M+ 2 1.950 0.002
0.12 IOT2 t.9.9010.002 - TiGlafiiO
0.06 11+2 1.950+0.002
0.2 39-1 2
-
-
~
it
2

(DITOdICTOBTA POICT11op
-0.05
31
+2
B 113OPPOM1.710DOM CLIJIPTO 0.02 37 -2
1.5 2" 2 1952+0 009 0.01 37 2
0.005 37 2
Card 5/5 0.5 1-952-~ 0.002
77 777! 1 71-M.-IT-1zi. I I Elf H F~ Ir III I "1 11 J1, lit

S/08 1/62/000/021/004/o65
B1 68/B101:
AUTHOR; Shagidulling R. R.
TITLE: A study of intensities in the Raman spectra of-
ethyleneamides of dialkyl phosphoric acids
PERIODICAL: Referativnyy zhurnal.-. Khimiya, no. .21, 1.962, 15, abstract
21B70 (In collection: Materialy 1-y Konfeirentsii m6lodykh i
nauchn. rabotn. g. Kazani, 19599' Sekts. khim. ka.zan', 196,0,:
137-140)
M
TEXT: The author measured the molecular integral intensities W,.) of the
12566-1280 cm- 1 line of pulsation oscillation of the ethylenimine ring in
Raman spectra of the dialkyl phosphoric acid ethyleneam'ide series. Re
M
found that the values of I I for one ethylenimine ring varied little in. the
.series of compounds investigated, and notes that such rings1bonded to,t.he,
phosphorus., atOM interact little with one another or with the ~alkyl group.
The presence of a P=O bond leads to a certain increase:~in ? 'as well as a:
shift of freqpencies. A P-S bond in a similar position shoIwa no such
influence. Abstracter's note: Complete translation.-i,
CELrd 1/1

- ------------ ---
SHAGIDULLIH GT--CHKIN, N.P.
"Oscilla y spectra of certain diethylonewdde3 of alk~rlthiophosphorie acids.
tor,
,y :Far Afl-~-l Ac--,kd
Alection of ~At t"tt 1 -i" 7,
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lou. lml~rllll,
SHAGIDULLIN, R.J1,; SATTAROVA, F.K.; TROYEPOLISKAYA, T.V.; KITAYFV, Yu.P.
~
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L 46322-66 EWT(M)/FWP(J) RM
ACC NR: AP5025128 679/66/035/016/1811/1814
SOURCE CODE: UR/O
AUTHOR: TsIvunin, V. S..
Gillm Kamay; Shagidullin, R. R.; KbLisamutdinova R Sh
ORG: none
TITLE: CondensatIJ reaction of dlethyl(diphenyl)chlorophosphineI With a, 6--dIchloroet4ylal1qV
ethers
SOURCE: Zhurnal obshchey khImiL. v. 35, no. 10, 1965, 1811-1814:
TOPIC TAGS: condensation reaction, other. chemical reaction. /)I rrH P"P'VY
ABSTRACT: Diethyl- and diphenylchlorophosphine formed with a, 8-dichloroethylbutyl ether
a coniple4as expected from their reaction with a --chloroethylalkyl ether, but hydrolysis or
alcoholysis of the reaction product was followed by dehydrochlorination to give diethyl- and
diphenyl- a -butoxyvinylphosphine oxide, respectively. Similarly, complex, formation of
diphenylchlorophosphine with a -chloroethyl- 0--chloroethyl ether'alcoholysis and thermal i
dellydrochlorination during distillatlon produced d1phenyl-a -vinyloxyethylphosphine oxide.
Hydrolysis of diethyl- 6-butoxyvinylphosphine oxide gave diethylacetylphosphine oxide, and
Infrared spectroscopy of the latter Indicated Its enol-ketol tautomerism. The starting com-
pounds reacted under cooling in a C02 atmosphere at OOC to give viscous complexes, and
Lcard 1/2 UDC: 546.1854547.431.4:541.49
iq

a

-L toj163-6Z E7wT(m)/EwP(,j)/P,,wP(t)/ET;- ijp(c) 4 1 =31 1=---
ACC NRt SOURCE CODE: UR70062166700070067
SHA:GIDULLIN H* CHERNOVA, A. V.. is B. A.
FUDOVIK A.'W.
institute of OrgaXdc and Physical Chemistr ni A* E. Ac $IV Of
y ime ade
Sciences USSR (Instiutt organichaskoy i fizicheskoy khirdi AN SSSR)
I-Question of Pon4ugation with*Participation of the Phosphorus Atoze
Moscow, Izvestiya Akademii Nauk SSSR, Seriya Khimicheakaya No 6 1966)
P -1124
1123
p
_Qstract- The ultraviolet and infrared absorption spectra anal, Raman spectra of,
O(B) 0
compoun ds containing a diene group with substituents -P and were
OR) OR
nvestigated in comparison vith isoprene. In the case of a-teftdnal situatioul
of the slabstituents, a bat-hochromic shift of the absorption maximum in the.
ultraviolet 5pectriAm and a sharp increase in the intensit of the bands in
y
zhe infrared spectrum end lines in the Raman spectrum of the valence vibra-
tions of the C=C bonds is observed. These signs of conjugation are more pro-
nounced for the carbonyl substituent. In the cane of side substitution by
0
P.;two~ -P greups, the opposite picture. is observed: hypsochmmic: shift, in
2
1/2
Card UDC: %146 +;66l.7i8a
13

L
ACC NR: AP7000737
th,e ulti-aviolet spectrum, decrease in intensities in the inf Irared and Raman.
spectra, indicating a decrease in the conjugation between the two C-c bonds,
probably due to competition by the phosphorus portions of the molecule. Pre-:.
-liminai-f resultslo4 the intensities of the bands of the NO iind P=
_bpnds
indicate the participation of these bonds in conjugation,. Orig. art.-has-,
2 formalase ~fTPRSI 37,02f
TOFICLTAGS: UV spectrum,*IR Upectrum, Raman spectrum,-chemical bonding, chendcal.
valence
,SUB CODE-:. 07' SM DATE: 1711ar66

-L - 7,1 2 1J
SOURCE CODE: UR/0079/66/036tOO /028~762T6
ACC NR: AP60227983
AUTHOR: Khayrullin, V. K.; Shagidullin, R. R.
ORG: Institute of Organic Chemistry, AN SSSRL'k~iani (Institut organic eskoy khimii
AN SSSR)'---
TITLE: Reaction of chlorides of trivalent phosphorus acid with conjugated'systems.
I. Reaction of ethy1dichlorophosphine th alpha,beta-unsaturated:a-cids-
V.
SOURCE: Zhurnal obshchey khimii, 3 , no. 2, 1966, 289-296
TOPIC TAGS: organic phosphorus compound, chlorinated organic compound, conjugate
bond system, IR spectrum, molecular structure, condensation reaction, alkylphosphine
AB5TRACT. A simple method was developod for producing chlorides of 4-oxo-4-
chloi-o-4-phosphocarboxylic acids, and a reaction scheme wa 's proposed. Ten
derivatives of 4-oxo-4-hydro.Mr-4-phosphocarboxylic acids were produced from
such starting materials as othy1dichloropho-aphine and p~enyldichlorophosphlnw
with acrylic and methacrylic acids. The structures of the condensation .
products of othyldichloropho6phine with alphatbota-meaturated acids and of
the products of further conversion of those reaction products wwo confirsed
by studies of their infrared spectra. Orig. art. has: I figure. and 2 tables.
SUB CODE: 07 SUB14 DATE: 116Nov64 ORIG REF: 005 OTH REF:- 002
547.468.1*
C rd
11 H ii i 1111 1'~.

L 06529-67 EWT(m) EWP(i) RM
ACC NR; A
P7 6 SOUNC CODZ: Ur~./0062/66/000/005/0839/084--'
NURENDINOV) I. A.0 PHAG;WJLLIN, R. R., SHAMOIUN, Yu- Ya.) GMEMM, N. F
Institute of Organic Chemistry., Academy of Sciences.USSR, Kazan, (Institlit
organicheSkoy--M= An 553H)
"Amides of Phenylvinylphorphinic Acid"
Moscow, Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, No.5, 1966P pp 839-.
843
Abstract: Amides of phenylvinylphosphinic acid were produced by reaction of
the acid with the amine- The ethyleneimide of phenyl-beta-chloroethylphosphinic
acid was produced by reaction of phenyl-beta-chloroethylphosphinic acid chloride
'with ethyleneimine in the presence of triethylam~ne as a hydrogen chloride
e
acceptor, in an unsuccessful attempt to produce the ethyleneimid of phenyl-
beta-ethyleneiminoethylphosphinic acid., The infrared spectra of the'substances
obtained were studied. The presence of ppi- conjugation in the systems con-
dpi
sidered was hypothes#ed on the basis of the frequencies of the NO and C--C
groups. The rate of inversion of nitrogen in ethyleneimides of phenylvinyl-
phosphinic and phenyl-beta-chloroethylphos rding.
... phinic acids is very hig4 aceq.
tQ the Droton magnetic resonance-dat.a. Orig. art. has: 2 figures and 2 tables.-
lip
TOPIC TAGS: organic amide, vinyl compound, phosphinic acid
.SUB CON: 07./ SUBM DATE: 28 Dec 63 ORIG RCF: 004 OTH RCF: 003
Card UDC: 543.422:542.95~ .1:661,718.
........... '1~. -

AX NR; AP6031389 SOURCE CODE: UR/0079/66/036/009/1670/1672
AUTHOR: Catilov,.Yu. F.; Kamay, G. Kh.; Shagidullin, R. R.
!ORG- Kazan Stite:Pedagogical Institute (Kazanskiy gosudarstvennyy
i instiLut);.,
~Institute of Organic and Physical Chemistry im. A. Ye. Arbuzov, Academy~of Sciences-
iSSSR, Kazan (Institut organicheskoy i fizicheskoy khimii Akademii nauk SSSR)
ITITLE: Rearrangement of some dialkylarylarsine sulfides into the.corresponding
lalkyl alkylarylalkylmercaptoarsines
!SOURCE: Zhurnal obshchey khimii, v. 36, no. 9,-1966, 167o-1672
iTOPIC TAGS: fungicide, dialkylarylarsine suifide, alkylalkylaryl,: alkylmerca toarsine,~-
P
sulfide, mercaptan, phenyl compound
ABSTRACT: To obtain new fungicides, rearrangement of some' dialkylarylarsine
-sulfides Alk (Ar)As-S was studied. Diethylphenylaraini sulfide.
2
on heating in a sealed tube for 7 hr at 240% undergoes re-
jil"ngement:
C 11 C it
2 5 2
As-C,H6 --- As-SC211r,
C,1f,>
Card 1/2 UDC; 542.952.1;546.221.19

ACC NR: AP7013133 SOURCE CODE: UR'0062,66 000 0091'1543,15L6
AUTHOR: Shagidullin, R. R.; Chadayeva, N. A.; Zarubina, N. I.; Kamay, G. MI.
ORG: Chemical Institute im. A. Ye. Arbuzov, AIN SSSR (Mimicheskiy Institut
AN SSS R)
TITLE: Vibrational spectra of organoarsenic conpounds. Conz~unication 4.
Infrared spectra and stru~ctuire of cyclic arsenic-containing Oerivatives of
pentaerythritol
SOURCZ:
SSSR. Izvestiya. Serlya khinicheskaya, no. 9, 19;66~ 15L :3-1546
TOPIC TAGS: organic arsenic compound.IR absorption spectximal, IR-spectrum,
pentaerythritol
SUB CODE: 07
In A- imhtim Iiation of earller~':C2ivestigatfons,' t1ii":[nf-jaiiid absorption
ABSTRACT:
spectra of seven cyclic derlivatives of arsenous.. alky;arsinous, and arylarm.
sinous acids with pentaerythritol, werd obtained and interpreted.~ Spectra are
cited for: 110 N V
) OH)1,; 2) P(OCK2) CH20H; 3) As(OCH2) CCa2OAs
1
C (CE~2 3C 3 CCH20d; 4).As (OC~2 3 1%0.0 V;
-5) As(Oci~) CC%OAs(C2H 6) As(CCR2) CCH,_,OAsPbo;,7) C2K AS(OCF2)2C (CH20) AsC
3 5 2 3 - U_ ~5 2 05;
Cardl!2 LT-D-:--543.422-+547.242+547.4n~7.1.1 r - I -, ~
...... 0733 ~082.1
-77T F-,

ACC NR-. AP7013145 SOURCE CODE: UR/0079/66/036/011/193711191)1
AUTHOR,: Miarrasova, F. M.; I(amay, Gill in;"'Shagidullin, R. R.
ORG: Vazanl Cherlicotechnolo.-ical Institute- imeni S. M. Kirov (Kazanskiy
khiniko-tokhnologichaskiy institut)
TITLE: Action of carbon tetrachloride and chloral an alkyl esters,~of di-(p-tolyl--
phosphinous acid
SOURCE: Zhurnal obshchey khinii, V. 36, no. 11, 1966, 1987-1991
'D)PIC TAGS:. carbon tetrachloride, ester, phosphinic acld~, organic phosphorus
compound
SUB CODE: 07
sized and
ABS TRACT: New al'syl esters of di-p-tolylphosphinous acid were synthe
ous alid were found to
characterized. These alkyl. esters of di-p-tolylphosphin C
with carbon tetrachloride, liberating the alkyl chloride 'and forming di7p-
tolyltric',iloromethylphosphine oxide in 53-78%o yields. Tne esters also reacted
readily with chloral, liberating the alkyl chloride and forming the beta,beta,-
infrar
..4ichlorovinyl ester of di-p-tolylphosphiAc acid. The ed,specra of some
'Orlj;. art. has: 1 figure, I
of the reaction products are cited and analyzed.
fornula and 1'-tab le. PPRS-. 40,31g
Card UK: 547.588.1~
-7
09330
11': PH) 11. IFIFFF~ =j71- 'IM

2776?-66 1 EWT(M)/EWP(J) RM
SOURCE CODE: LTB/0979/65TO357011/1993/199,
AUTHOR: Kharrasovat F. M.j KamaYj Gq1-Sha91dU11in#,R6:R~
a a a
ORG: Kazan' Chemicotechnological Institute im. S M. Kirov (K z'n kly-khimikd
tekhnologicheskiy institut)
A
TITLE: Effect of carbon tetrachloride and chloral.on al~nl esiieis~of P-bromorthenyl.
phosphinous acid
SOURCE: Zhurnal Ishchey khimlif v. 35P noi 110 1965, !"3-199k
TOPIG TAGS: carbon tetrachloride, esters organic synth tie pr:c6ss, phosphinic~
acid brominated organic compound
SThACT: - A series of esters of p-broioph ea
AD enylphosph1noub,'scid;'were synthesiz.
studied. w4eri"
As representatives of trivalent phoaphoru vatives, the!esters:
react with carbon tetrachloride tio,form. esters Of P-bro~6plieny:ltricblc)rom~thyl-
~pbosphinlc acid, which are thermally unstable compounda.!~ 11
ne. eaction, of;esters:
of p-bromophpnylpboBp4inoua acid with oblor 1 proceeds ieadily;,,*ith liberation
of alkyl. chloride and formation of the corresponding mixed alijl4eta,beta-
dicblorovinyl esters of p-bromophenylphoapb~inic said. 1~ constr'sat to the
:triehloromethylphosphinic.derivatives, :t-he,beta,bete-dichlorovinyl:eoteri3 of
ip-bromophenylphoophinte acid a
re extremely stable cowpoin~6: distilling 'Without,
:signs of decomposition and tolerating atorskeAn se&led*,8'M'P'0ule'9';i iurrarLid
spectra are cited for four or the reaction products , Ori'g'.'! arb.~: has - 1 rL tables
- Agwor-,
j
007 OTH BEE 001
SUB C9DE: SUBM DATE: 3OOct64 ORIG REF: 4
Card
547
UC 46,183,325
7
--flT-rd" 171 I'I'l

27763- 6 EwT. (m) /Fwp (I gM
NR-c Wf6518505 SOURCE CODE: tIR/0079/65/035/onA998/2001
AUTHO71.- Tsivunin, V. S.; Kamay, G:j S hagidullin j, R. R. XhIsamuidin'ova, R, Sh.:~
ORG: none
TITLE- Condensation of,di6thyl-.and diphenylchlorophosphi~e~wii.h'~alpha-chl6roalde~r,.ea:,,,!'
SOURCE: Zhurnal obshchey khimii, v. 35, no. 11, 1965' 1998-260r:
TOPIC TAGSt condensation reactionj aldehydel chlorinated organlb~co Iinpoundl-::orginic
phosphorus compound
ABSTRACT: Diethyl(and diphenyl)ehlorophosphines vere~fowdlto forwComp exes V1th
alpha-ch'loroaldehydes. The reaction proceeded exothirmel ewthe',eomponents_~
were mixed in bulk or in an inert solvent (diethyl ether)~Oxidis'and thlocildes
Of diethyl(diphenyl)-alpho-bydroxy-bets-chloro-(betajbetaji~~i~-til'~blam)-.
ethylpboophines were Isolated by decomposing.the comple"441th;ii~dbois or bydr
090
sulfide, respectively. -The condensation of secondary chlci6pboi~hinez vith chloro-
osposition lezii* or
aldehydes, folloved by nucleopbille dee of tbq:io* Ith va"r
Alcohols to recommended as a nevp comperattiely simple 1001070-aff-,#rbdualm - oxides
;of dlelkyl(or di I)-~lpbs-bydroxyetbylphosphI=s* Orig,,~~mdt.~ has:1 f igure and
-6- as~5
02,
004/. 0h1;REF:' 0
SUB CODE. 07/ SUBM DATE: 17Dec64 ORIG REF.
UM 546 185/54~i"6.ii~4"
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J1 163.
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1. Iz kafedry detskikh infektsiy (zav.- prof..N.P. Kudrya-,rtseva)
Kazanskogo meditsinskogo inntituta.

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Is - I. 'At"&-_l% on
work and %dti=te state of steal r_.._. or
industrial blldi.g.' (session rx) : A.
PERO, 0. Ylk. - *Research on the concrete
strength theary, (Bastion rl) - I
MGMMV (rQU) Jprabobly NL%ol W BO9dAWTyA,
my "tions
and WMW (fhu) - *Ge..ral m
adapted' In-now 'Instructions an desi
erection and molatenance of flat roof. in
the UWR' and the resuit of recent In,
tigatLan of flat roof structures In the
UWA, (S .. Ica vr)
Do S. R*ot f min-
lth`.ceef;e.t of
transverse forces" (Session t1)
GVZDE4 A. A., pmr. Dr. --pres,nt state
and PrObleas of dooLlp OCbuilding stractooW
Session 11)
GrIllafty F., Prof. - Rgt*m
~-PQMM ORPortezce* (Session ry),
ODnOWY, X- V-, and USMCN, 1% V. - 'llabl,,,,
of Joining hes-y Jaigntj In yr...t
dwalliag.' (s .. I_ ZV)
Prof. Dr.
No
9 and stiffness or reinforced coscreW
-.bar&* (Session XI)
OWSTAMCIN, V. I., p"r., Fresidant br assion rz,
also scheduled to prosent a psW I. *,St.
IX, title not 41"n. Member of ties shoeft"
Committee far the Caegmea,
MIMMA. Alakwy it., Pror: Dr. ;-&" or
co"Ma capacity of @IN* ad ~11. bw Us
sortbod- (Seenies 11) i,
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Getere,
Sol. Ovoomou rw DAUA&MO nwogmb, evouee, ad ftneensolle,
00011-3-ft, 144t) QoV Mp.

SHAGIN. Petr Pavlov.ich,_doktor tekhn.nauk; MOROZOV, A.P., na-achnvy red.;
SM, N.Ya., red.izd-va; VORONETSKAYI. L.V., tekhn.red.
(Static calculations of prefabricated frame-panel apartment
houses and public buildings) Staticheskii raschet abornykh
karkasno-panellnykh zhilykh i obshchestvennykh zdanii. Moslcva,
Goo.i2d-vo lit-ry po stroit., arkhitakture i stroit.materialam,
1959. 174 p. (MIRA-12:4)
1. Deystvitelinyy chlen Akademii stroitel'stva i arkhitektury
SSSR (for Morozov).
(Buildings, Prefabricated)

_;TAGj~~!__Petr Pavlovich, doktor tekhn. nauk; VASILIYEVf B.D.9 zasluzhennyy
_d~Y~-E411-ifauki-f-tekhniki RSFSR, doktor tekhn. nauk, prof., red.;
GRIGORIYEVA, I.B., red. izd-va; VOLCHOKt K.]K,p tekhno redo
[Stability of-frameless apartment houses made of precast elements on
highly or irregi'tlarly compressed Soils] Prochnost' i:u6toichivost'
beskarkasnykh zhilykh zdanii. iz sbormykh elementov na sillno i no-
ravnomerno szhimaeqrkh gruntakh. IAningrad, Gos.j izd-vo lit-ry po
stroit., arkhit., i stroit. materialam,, 1961. 119 po (MIRA 14:8)
1. Chlen-korrespondent Alspdemii stroitellitra arkhitektuIrjr SSSR
(for Vasillyev)
(Apartment houses) (Foundations)

J
LiA mut
SHA;3-1, `.;h. Y.- BD~
Ev
A i a JI 3 C', P, 4 a-d D NEPROVA 11.11,
'-~X),-a., A,
red i zd-va ~--!HZRY, A A I-eyb--, red.
LStabiilty of :-4 ~L~i-:ilingS or, sagging soils]
Prochnost' sbornykh zdanii na prosadocbmykh gr!intakh.
Leningrad, Go&qtroiizdat,,. 1963. 119 p. (MIRA 16.10)
1. Chlen-korrespondent ALadewill. stroitellstva arkhitektur7
SSSR (for Vasillyev).
(Buildings, Prefabricated)
4

ITHIN Iiiir P111 111' "1 llwdl'~i

lig I
-- - ---- ----
Wild[

8/920/61/136/004/Q26/026
B01.6/B075
AUTHORS: Stepanov, V. N. and Shagin, V. A.
TITLE: Kinds of Vertical Variation of Salinity in:Sea Water
PERIODICAL: Doklady Akademii nauk SSSR, 1961, Vold, 136,PNo. 4,
pp. 927-930
TEXT: The present paper deals with the classification of kinds according
to which the salinity of sea water varies with the depth'. For~this
pu nose, salinity has been measured on points that 'were rather evenly
distributed over the total area of the ocean. By comparing the curves of
vertical variation of salinity, the authors have found several similar;
regions. For each region, they calculated the mean values of salinity
(Table 1) and on the strength of these data they have plotted.curves
(Fig. 1). The authors distinguish a total of 7 kinds of vertical
variation of salinity, which are subdivided into 15,groups. B) Polar kind,
grouped into: 1) Arctic and 2) Antarctic. The 50-10.0 m thick surface layer
is considerably freshened. Salinity rapidly increases down to a depth of
Card 116

Kin ds of Vertical Variation of Salinity in S/0'20/61/136/oO4/026/026
Sea Water B0116/BO75
from 300-500 m and then remains almost unchanged. V) Subpolar kind,.
grouped into: 3) North-pacific; 4) Antarctic. Similar to.B; the
freshening influence of the surface layer, however,.extends to greater
depths due to the sinking of the water. Salinity increas E! s down to
1,500 - 2,000 m and then remains almost unchanged. G) Temperate subtropical
kind, grouped into: 5) Atlantic; 6) Indian; 7) North-pacific; and 8)
South-pacific. it appears in tropical and subtropical latitudes. It is
characterized by a high salinity on the surface and,~a freshened inter-
mediate layer. Salinity decreases rapidly with the depth; reaching its
minimum near the axis of the mentioned intermediate layer. A secondary,
lower maximum of salinity is found at a depth of 25PO-3000 mand a
secondary minimum on the sea bottom. D) Equatorial-tropical kindy grouped
into: 9) Atlantic; 10) Indian; 11) Pacific, differs from~G by a highly
saliferous layer immediately under the surface. In deeper layers, this
kind has several maxima and minima of salinity. Kinds B to D are widely
spread in the ocean, and are dependent on the climatic conditions
prevailing in the individual latitudinal zones (Fig.~,1).'The kinds,E, Zh,
and Z are only locally distributed.:E) North-atlantic kind, grouped-into:
Card 2/6
19111-1 R I T '11 f III

Kinds'of Vertical Variation of Salinity in S/020/61/136/004/026/026,
Sea Water B016/BQ75
12) Temperate-tropical; 13) Sub-boreal. It iq similar t~o~'mode G;:howe,ver,,,-..1.
salinity gradually decreases with the depth and then remains unchanged
from a depth of 1000 m down to the bottom of the sea. Zh) Circum-~
mediterranean kind, grouped into: 14) Atlantic; 15 Indian. The upper as
well as the medium depths exhibit high,salinity. Z Indomala an kind.~
Y
This is known in the northern part of the Indian Oqean.~ There, salinity
raDidly increases with the dlepth. There are 2 figures and 1 table.
ASSOCIATION:- Institut okeanologii Akademii nauk SSSR (Institute~of
Oceanology, Academy of Sciences USSR)
PRESENTED: June 20, 1960, by V. V. Shuleykin, Academician
SUBMITTED: June 19, 1960
I ill 11 lt"'Jil 1~:
!I ! ii H! N! 1:111 .11: I'MIA"M 11

-Z
m i00 m 200 500 M. S/020/61/136/004/026/026
B016/BO75
S. IIOJIFIPHWR THn 32.29 33.90, 31.52 34,77.
i. APKTIIIICCKUR nOqTHn 30.76, .33.54 31,0 3i'so
2. ANTaPKTHqeCKHR nOATUR 33.82 M.25 34.51 34. w
a. Cydnojlgpliuo THTI 33.23 33,57 34.03 34.32
3. CC6ePOTJIXOOKeaHcxHA nOATIM 32, 50 33,05 '33.77 34.15
4. AHTaPK'ritqeCKHfl noATun 33,OG &.00 M.20 3-S.40
r. YMCPCjjjjO-TpO"jf4eCKIjfl THn 35.25 35.10 35,02 31.6-,
5. A-raalIT119ECKHR noATun 35,07 35,64 35,29 MoO
G. IIIIAHACKHR noATun 35,53 35,15 33.37 35,00
7. CenepoTHXOOKeBHCKMA noATun M.46 34,52 34.41 3S,22
8. [O)KIIOTHXOCKeBIICXHII nOJETHIT 35.03 3j"os 34.98 34.U
A. .9KDATOPII3.MbHO-TPOnK4eCKHfi TIM 34.89 35.14 35,t3 34.77
9. ATjiaHTJ14eCKuR noXrlirl 35.09 35,il 35.22 34.74
10. IIIIAHACKlift nO;tTHn 35.10 35.Z5 35.20 34.90
ff. Timnoxenjimift r?oATun 34.40 35.01 MOO 34,66
E. CemepOaflTJTaIITH4"KHR TIOn 36.01 35.97 35,89 35,46
YMCPCIIRO-TPOnJl'l"lCllft nOATHn 3G.50 36.50 .36.40 35,75
13. CY66OPeaAbHUR VOXrNrl 35,30 35.20 35.tS 35,05
)K. npHcpemlf3CUFfOUOPCKHII THfl 36.00 35.06 .35,70, 35.35
j 14. ATJT4frTH4eCKMA noATtin 36.03 35,06 35.83 35.46
15. HHAHACKHlk noATisn

3. IIIIAO-SO.MaRCKlIft
M.50
31.85 35.05 35
.10
Card 4/6

00

000

00 0 .A
200

oo

M woo
3S.81 31.82 34.82. 34.a2 34.82 34.82 83. 62, 34'st
3A,03 31,05 34,05 34.05 34,95 A.95 34.95 (34.U5)
3!"6o 31,70 34.60 34.69 34.68 3t.68 ;34.68 34.67
31.45 34'5t 3A.59 34.G6 G4 .66 34.66 SA.70 34.70
31.32 M.40 M.51 34,60 34.62 34,62 34,72 34.r-
M.SS M.62 AM 310t 3S.70 34.00 34.67 34.67
31.1.5 MAS 3..G; 34.72 3S.76 M.77 31,74 31:r-
3$.39 3..48 M.77 3-i.B8 34.80 ss,60 34 75
3'.,Gt 3S.68 34.78 3A,83 3S.84 3.i,lt 31,75

R. 28

4,40

4,51

1.60

A.Gi
" _
34.6,
34.,G

1.66
31.43 .1s.42 34.55 34.61 31.67 24.69 34.71 34.70
W,.Go -34,77 34.80 3-S.80 34.80 34.79 .34.78
34.67 311.06 31.00 (34.94) 34.93 34.89 34.85

34,70
31.55
3S.75
34.80
34.80 34.80 34.80 .34,77
34.57 34.58 3i.Gt 31.G3 34.65 34.67 34.69 -34.71
35.11 35,0S 34,97 3..n6 34,03 M.93 34.93 SA.90
3.5.20 35,10 3:),00 35.00 34.95 34,95 34.95 -34,90
xi.m 3-11.92 34.90 3A.90 34.00 (34.QO) (34.90)
35.30 35.40 35.20 34.90 34.85 34.'85 -34.65 34.85
35A,8 35,33 35.01 34.83 3A.80 34,75 734.73 1 -
35.00 M.05
1 31,85 34.80 34.80 31.80 34.80 34.81)
S/020/61/136/004/026/026
B016/BO75'
Card 5/6

S/,.020/61/136/oO4/026/026
BG16[B075
180
60
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s/o65/62/000/010/003/004
E075/E.136
AUTHORS: Chertkov, Ya.B., Zrelov, V.N., Rybakovq K.V.*
Shagin,__V..M._, and Foihishenko, B.A.
TITLE: Characte .ristics of micro-impurities'in middle-
distillate fuels
PERIODICAL: Khimiya i tekhnologiya topliv i masel, noolo$ 1962,
56-59
TEXT: The authors investigated the nature~;of micro-impturities
in fuel TC -1 (TS-1) used in aviation gas-turbine engines..~The,
impurities in the fuels form through the intera ction of q1etal.
containing compounds with high m6lecular weightt'resinous compounds
and moisture. The metal-containing compounds originate from
corrosion of tanks and moving parts of various mechanisms, as.well
,as leaching of certain fillers from plastic materials. The
coarse particles of the impurities form mainly by ~.he:
agglomeration of finely dispersed material. -The formation of
particlis having the size of 0.1-1 micron is speeded up by
,increasing temperature, agitation and excessive; pressures.
Card 1/2

S/o65/62/000/010/003/oo4
Characteristics of micro-impurities..
E075/EJL36
The inorganic part of the impurities in fuel TS-1 contained 13-7N~
~of Fe after filtration through A filter with 7 micron pores
This indicated that Fe can be present in the fuels in a finely
divided state. The second most-abundant element in.the impurities
is Si. The organic part of the contaminants contained S and N,
the latter being present only in the organic part, whereas some
of tile sulphur was present also in the inorganic part of the
impurities. To avoid the contamination of the fuels it is
advisable to carry out systematic removal of moisture., prevent
the formation of high molecular weight resins and exclude metal
containing compounds.
There are 4 tables.
Card 2/2
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