SCIENTIFIC ABSTRACT SHEIKOVA, G. - SHEINKER, I.G.

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SCIENTIFIC ABSTRACT
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.0HEIKOFVA G - GEORGIEVA, J. ...... t. ! I Actinomycetes-aritagonists isolated from Bulgarian soils. Folia microbiol. 8 no.5:308-312 163. 1. Research Institute of Pharmaceutical Chemistry, Sofia. (ACTINOWCETES) (PLANTS., MEDICINAL) (SOIL MICROBIOLOGY) UCktG101A, J.; SHEIKOVA, G. Vitamin B12 formation from various actinomycetes isolated f-r-om Bul.~7ari,-.n -ils, Folia microbiol. 8 no.5.-322-324 163- 1. Research Institute of Pharmaceutical Chemistry, Sofia. (VITAMIN B 12) (ACTINOMYGETES) ?SOIL MIGROBIOLO(' Y) (METABOLISM) J411 . .7 -1 . ~ .- 1 -~- I . .1; . * , ~!-. . -. 1. - i ~ , ~ -r") t i " 7! - ~ . . I : ,-SHEIIjL_A.A. _CS ttyvkar) I , I Historical evaluation of the psychological conceptions.. Vop. paikhol. 6 no-5:133-137 S-0 16o. (km 13:11) (2ange, Nikolai Nikolaevich, 1858-1921) SHEIN, A.A. V.M. Bekhterev as a representative of materialistic psychology. Vop. psikhol. 9 no.5:152-11,:8 S-0 163. (MIRA 17:2) 1. Pedagogicheskiy institut. Syktyvkar. SHEIN, A.A. Perrovich Konaki,l), 1884-1941 as a psychologist. Vop. palkhol. 10 no.3:29-39 my-le 164. (MIM 17; 9) 1. K,-~Tpl pedagogichaskly institut, SyktTvkiLr. SIT T 7 c If ear 165. instit,,4, c:he ski, S C n .3 ring ~3;3 S-0 tv, + j- ~ Cl 1.92z0 -1/6 -2/G,-Cz,/CQ2/Gl2/Q25 L .1ack'-C unit '..'a ;:,C-z;on:l-orq n C- 1" _4 5, no Z!- 2. o-' rosonz~.t-ors a u r:-aa 11 yuc; oeL i---, ;:ia _--,.e uld o r., f;" z'--) C~. CL-n in -t:1(-. pate-;.-It of li--~. C! S -C, e scr--::,,s to offcr possibii1ties. izi 1. 1 is is in the slhane of 1 4, cour-'-~~;,.tes is described by: Cos y)sin(..-- + y)'; !~L 1/ 6 o~ U, I. i Q ;;'-f t ,, c . cc lu at iolz~ for i-Lis Cylindric a 1 cz,.n bc fou.,-! co.-.i~3arativcly easily but clictermination of co,.iz~ L L ant in I-acso cquat4oa!.; Icads to an -,-ifinkte w!'Ose :)ara-metors aro defi I . 171_1 -rLec- oy .I~Iizions Q:i t7:(-. rcson-a-zor wzlls. CO 7 :L7-. a c c C. I -. is sufficient to tal:c Inzo account Qnly t1e::-".";~ Of Tac imoortant ,,a Z. w-1 et cr 1-11liz colwistin~, of )crdqnt-s_'ia.)ed rosonators are -roc:-LICicies. 'I'liese Lazi be determined from '-2c c z; -.D 1-:. c ccon(litio:a z)f -tlie systern: + yr = 0 (7) I- Y of the ii1teraction at the a rcsonator, and Of t1le resoliator a-, r = a tl--e resornant frec:-,,,ciicies rc~:;Onatorz are uctc;-r~:iincd and t:io results -)eriul , zi C(: r Tliese are co,.,.varcd slom-c- C,-t 1 s/alli/62/005/002/012/0_25 L '192/ E3 3 2 .-"or -:aodc "']e discre-)ancy C. -nc rcs~_-_'Its c:ocs not c--ceed .0t -for t~lo S ccond C, A c) e c --cl c is o th e Lz aod y c -n I c o 17 f027 t. S a::'. C M Od C:~; r, Zl SZa:1-dard iz: un1y C. The resonators avc 0 val-.ta.-C t:~at -6-~c sc,:)ara-6-on O-r, ~"le r equ enc i C's t:ic a nci~:Ibourin,_,- ,.lode is -2-cater tlaan t.iat -C -, Z-Csonalor __C.CZOZ' raic", iz; clue zc, izs Iaz.~;c v 0 1 u:. r f ac Z-1.0 1 f _J _- u r 0 S . :,-osuk-A'crStvcn-.I-ry univorsitet a r :,D,.r State University) PERFSHChENKO, A.I.; SHEIN, A.G. Magnetron-type, anode block with resonators with elliptical cross nection. I;v. vys. ucfleb. zav.; radiofiz. 6 no.1jI19-125 16). " - (MIRA 16:1) - ,1. Kharlkovskiy gosudarstvennyy uaiversitet. (Electric resonators) (Magnetrons) (microwaves) L 18390-63 W51 ACCP,SSION NR: AP3003730 S/0109/63/008/007/1274/1276 .q. ATITHOR, Tereshchenko, A. I.; Shein, A. G. TITLE: Effect of resonator cross section shape on the characteristics of magnetron type anode units SOURCE: Radiotekhnika i elektronika, v. 8, no. 7, 1963, IZ74-1276 TOPIC TAGSt resonator, magnetron anode ABSTRACT. Theoretical and experimental investigation of the following resonatdr types is reported: slot, hole-and-slot. paddle, drop-shaped, and elliptical. 'By solving a planar isoperimetric problem and by using the method of conforrnaL mapping, optimum shape of the resonaror is found, and the practical shapes are compalred with it. The conclusion is offered that using near-optimum resonators (drop-shaped and elliptical) enhances magnetron-oscillation stability and separa.- tion of frequencies; the latter fact may permit relinquishing magnetron strips m Car(I 1/2 I L 18390-63 ACCESSION NR: AP3003730 some cases. Orig. art. has: 2 figures, 3 formulas, and 1 table. ASSOCIATION: none SUBMITTED: 24Nov6Z SU13 CODE: GE DATE ACQ: 02Aug63 NO REF SOV; 003 MNCL: 00 OTHER: 002 D - Card Z/2 - LYAPUr:GV, N--V-;_SK61N, A.G.; TEUSHCHENKO, A.I. Calculation or nonuniformities in waveguides using the Lorent7 lemma. Izv. vys. ucheb. zav.; radiotekh. 8 no.1:11-17 Ja-F 165. (WRA 18:5) L 008143-66 Zv1T(l)/EEC,-4/EWA(h) ACCESSION NR: AP5015809 UR/0109/65/010/006/1029/1037 621-385.6-032.266:621-372.8 AUTHdR: Tereshchenko, A. I.; Shein, A. G, TITLEi Septate waveguide of cross-shaped cross-section as a delay system SOURCE: Radiotekhnica i elektronika, v. 10, no. 6, 1965, 1029-1037 T-OPIC TAGS: se_.tate waveguide, cross shaped waveguide, delay system 25~ ABSTRACT:*A cro6s-shaped waveguide,'see Enclosure 1, potentially suitab-e for high-~ power TW tubes is considered. A dispersion equation descr!bing the cross-shaped- waveguide delay system is developed for cophasal LE-modes, 'by the method of joining the fields at ooundaries of sinple regions. A formula for the system coupling resistance is derived. The dispersion characteristics and the coupling resistanen were numerically calculated on a "Minsk-14't computer; the system has positive.dispersion at the fundamental harmonic. Both theoretical and experimental:,---- Yes results indicate that the cross-shaped delay line has a number of advantag a rather wide passband (as compared to the clover-leaf and rectangular septate i waveguides) and a high coupling resistance (1500--2000 ohms at P D = 2jr/6 and 60 D Also the experiments have confirmed the validity,of --70.ohms at Card L OO8h3-66 ACCESSION NRt AP5015809 X. 32 formulas, and I t.-Lle. I formulas. Orig. art. has. 4 f-*Fures ASSOCIATION: none -~Wk: EC SUBMITTED: 06Apr64 ENCL:'Ol SUE, NO REF SOV: 006 OTHER: 004 Icard2/3-- ACCESSION NR: AP5015809 4 ITF Card 3/3 ENCLOSURE: C~-oss-shaped ser a-z.- waveguide as a delay system __L_ 17546,66___ A=MrIM6000519 SOURCE CODE: UR/014Z/69/00,'4/005/053ii/(1.5,i4 'AUTHOR: Tereshchenkci, A. I.; Shein, A. G. .................. 1ORG: none ITITLE: DiApersion equations of toroids formed from septate rectangular waveguides URCE: IVUZ. Radiotekhnika, v. 8, no. 5, 1965, 538-544 TOPIC TAGS: rectangular waveguide, delay system ABSTRACT: By applying a fidld-joining method to the boundaries of simple regions, a-, dispersion equation is develope for a delay system (toroid) I formed by bending a rectangular! septate waveguide in the TE- I it plane. The dispersion equation for a waveguide bent in the E-plane (see Fig. la) has been @ developed elsewhere. The a problem of propagation of co- phasal LE-modes in the TE- Fig. I Fig. Z plane-bent waveguide (Fig. 1b) Card_ I /Z , - UDC: 6ZL 572.85 L 1754646 'ACC MR: AP6000519 is solved by subdividing the system into interaction space I and resonator -regions 2 and 3 (Fig. 2). The final dispersion equation is given in this form: IN Ct9 IN ( - )I_ 1-1- V. cjg,,t~ By using this equation with certain Ig a = I (sin M11) XMI approximations, the dispersion character- 0 istics of the TE-plane-bent waveguide M, 0, - as - w2p"".)- X" p2, toroid are calculated, and it is. shown that Isuch a toroid has positive dispersion at the fundamental spatial harmonic in the first ~.ransparent zone. Orig. art. has: 3 figures, 28 formulas, and I'table. UB C DE: 09 SUBM DATE. 29Jul63 ORIG REF: 007. 3HEIN, Ariatol~,y Ivanovich; NIGE"Y, Fedor I-lefodlyevich; REL-NIKOV,Yu., ~ .. I - - ---- Karatau. Alum-Ata, lzd-vo Kazakhstan, 1965. 81 p (141RA 1Q) KHORBENKO, Ivan Grigorlyevich; SHEIN, A.S., doktor fiz.-mat. nauk, retsenzent; ANTONOVA, S.D., red. [In the world of inaudible sounds] V mire neslyshimykh zvukov4 I ookva, Mdjhinoolroenie, 10,64. 120 p, (MIPA 17:4) M SHEIN, A.V.; GUTIN, N.D.; VERSHININA, A.I. At the Central Complex Laboratory of the Ural Geological Administra- tion. Zav.lab. 28 no.8:1013-1014 62. (PURA 15:11) (Ural Mountain region--Chemical laboratories) (Minerals-Analysis) s D. V. f)f Tionferrous me-w~-, afid [-,rofitable- O'L* pro~~an.ion. Gor. rio.1:28-31 Ja ' 0'/~. (It-'PLA 17:3) 1. Lrpravleniy-- '~oz;Loch-ni--.Kazak-h~-t;~,,nskogo akruga --osudars tire rrogo kc.z;dtf,,t,a firi :'jni.rtrov Kazakliskoy SSR pc nadzoru za .)a,ny,,q veder.; p~or.-y-jiJi--n-nooti gornorm nadzor~.. KOX-07, V.~., inzh.; POLYATIE, M.A., lnzh. At, -nining enteiTrises of eastem Kazakhstan. Bezop. truda -,r -,,rom. 8 no.9-.30-31 S 161, (MIPA lgal) Upravleniye llostocbno-Kazakhstfaiskogo okruga Goaudar-stven, rot~o, komateta ;)r-- Sovete Ifin-istrov Kazakhskcy SSR po nadzcT-,l 2; ' -,redeniyem rabot v promyshleprosti i gornomi newd- a bezopasnim SUIUURETS&U, V. - M. I kand. tekhn. nauk; SHLU, L1140t insh.; TASILBKO, T. Pay inzh.; DRANITSYN, TO. z., Inzh.; OTA=WUH AVY A. S.2 nauchnyy Gotrudnik Role of wetting and the moisture regime of coal in the jamr1f. UgolF Ukr. 7 no.4t42-43 Ap 163. (MIRA 16:4) 2. Institut gornogo dela All UkrSSR (for Sabare-vskiy, Shein, Tasilenko, Dranitsyn). (coal mines and mining) (Mine dusts-Prevention) SHEI1,11, N.I. _ Handle for cranking elevators. Sbor. rats. predl. vnedr. v proizv. no.2:17-18 t61. (14IRA 14:7) 1. Nizhne-Tagillskiy metallurgicheskiy kombinat, Vysokogorskoye rudouprav-leniye. (Elevators--Maintenance and repair) KUDRITSKIY, i-.-, VOLKCjV A - FOGEP Z.; PODOBED, Yu.; TITOV, A.; SHEIN, R.; I-ITSITTI'S, Ya. ru,*Itisy J.1; 0STROVUETS, V.; SEMENTSOV, Spc-ci)OAzatior; is indispensable. Tekh. est. no.4:22-23 Ap 165. (MIRA 18:6) 1. Spetsiallnoye khudozhestvenno-konstruktorskoye byuro Kiyevskogo ~;oveta narodnogo khozyaystva (for Kudritski-y, Volkov, Fogel'). 2. Spetsiallnoye khudozhestvenno-konstruktorskoye byuro Soveta narodnogo khozyaystva Moskovskogo gorodskogo ekonomicheskogo rayona (for Podobed). 3. Spetsiallnoye khudozhestvermo-konstruktorskoye byuro Soveta narodnogo khozyaystva Leningradskogo ekonomicheskogo rayona (for Titov). 4. Spetsiallnoye khudozhestvenno-konstruktor- skoye byuro Sredne-Urallskogo sov-ta narodnogo khozyaystva (for Sheini. 1q. Spetsiallnoye khudozhestvenno-konst--uktorskoye byuro So-~,eta narodnogo khozyaystva Latviyskoy SSR (for Litsitis, Ostro- venets, Sementsov). ,~HEIN, R., A ~ Artiat in a design office, Mashinostroitall no-10.41D-41 0 ; 62, (m I T'l v -# 10 (Art and industry,) SHEIN, V.A.; BELOV, V.P. Some means for lowering the expenditure of time and materials in lost circulation. Izv. vys. ucheb. zav.; neft' i gaz 5 no.6: 111-114 162. (KRA 16:5) 1. Kuybysbevskiy industriallnyy institut imeni V.V.Kuybypheva. (Oil well drilling fluids) (Plastics) F&~L(wmirilng the ccnnolida~.ed capital investment indi--es in oil ;fi,~ 1, --1 j .Nefteprom. delo no. 3:25-27 164. ('-IIRA 17:5) -n-nodari3kij fillul V:.wsoyuznogo neCtagazuvogo muudlno- is,~IedovaLellskogc instituta i Gosudarstvenny-j institut po ;~roy,~kLirovanlyiz predpriyatiy neftyanoy prorayahlennosti '.. C -~tochnvkh i yuzhnykh rayonov SSSR. EYEV.- V~ Me t-hr.d for the owunarat, tre techninal-econom--'n evailua, r4c-aa mt---thads of floodirg. Nefteprom. dsio rtj,,.3,~3G-34 'c 5. 1~ Krasnodarskiy flllal Vseqoyuznogo nef tegs-zovozo naucl-t-i-l- watellskiy Inst! tuta i Gosudarstveninyy insi,4tuf, ed( pr3yelk,lirovaniyu I issi-iRwatel-e-kin rabo,.,im neftedotT-varv5~ichJy --,ostochrykh rayurlov strany. "i,11/4c- ,kUTHORS: 6. L. S-1-'n, HTLE": in'n-,isity of i~arth-u,"-s Basedon :)F--,,a So-eLetFarEast- k~ 4" P'. - era ~_n~l Con--inen-tal) S,~,-T_ions of U6SR FEIRIODICAL, A,::aaem: i naur-I SSSR~ ~--~Ofizi-_,_esI~aya. 1 plate kUSSR~ 3A r p + MI for-i:i; la M -A a :aean ra"-e of v;here t:j fUl,..,~rjo.,j ~Lecr;,ase of -he Ground displa-a-taent uli~3-ance saz, -_Lmrirical y, der-a- t9 A~ 1 - 2c, - 1 - g2 5 16 < 100' _.e reunions extending from the Caucasus ro +-he Middle Azia (ZS, - epicentric disr-ance). T-,---e Tesul,,-s of calcula- tions ,vith + 0.25 accurac-,, are tabulaz;ed in Tab 1. .-.-.he followiflEr data are included- Colu.T--, 1 - date; - time of eart-I-quake; 31 and 4 - their co-ordina~eSi - -e~~-ion-. Mjean; number of st-arions taking n S to 14 - 6" part i determination of fAmear ~Istati,)n Mmean; 15 - mean 6M. The results cf calcula 0 --:, M ig AF.E/ACc., dezermined Far East - MCOI)tljilllental 'i-Gy of E~jrth;,uaa,~S based on Joviet Far Eastern and uf OSSR scime of i.-,'.-e Fa-y- sta~ior-- I -:J,-,,E- 1 r- D-Lo-c- 1 to 4. This he I., -LO i y PAL 1~1 C) (Tab 2) Fi~- on cf M- Ni -- f"I". ,, o ni, il~-ere ar-e 2 iGures, -L'c-.- a.,~ Sc-vi~,'- Freacll- and 2 En-I S - I CL , A i A I(-J-11 A. -ai c!,,rii y a ~aa u ~%- 6 kSSR ~ I n s t, i tu t f ii2" h (AS USSR. I.- Pfl.-~-sics :)f 1~ar-, J 10, SHEIN, V.B. ~-rm,) Pickup of the humidity of air. Fiz.v shkole 22 no.5s78 S-0 162. (NM 15:12) (Hy,grometry) KTJZNETSOV, German Ivanovich; FAYN, Genrikh Moiseyevich; SHTMIBUH-G, Valentin Fedorovich; SHEINA, Antonina Aleksandrovna; MIMMEV, R.I., red. (Drilling pipes from light alloys3 Burillnye truby iz leg- kikh splavov. Kuibshev, Kuibyshevskoe knizhnoe izd-vo, 1964. 51 P. (MIRA 17:12) I w 1, .11.9 . '. ~~ ! , - 1 , , , - . - . - , 1'~ , .. , - - = - , -- -,, . .- . , I . .. 'i . . i - I :. ~ -- ~ l.. - - -,:.- 16.,!, 1 1 1 r-: . ,.,I a I experimen' a I data cn trip use of a] tranound In bronchial Trudy TSIU 77:8-13 165. (?MRA 18:9) 1. Karedra fizioterapli. Nwr.., dotsent A..". Spe--nskiy) i IV ~a`e-dru terapit (zav chlon~korreipondent AW! '--" -roC. P.I. TSPntratnogn, In3tit--i"a upov,~~rshenstvovaniya vrachey. SHEIXA,-A.N. Ultrasound and the treatment of bronchial asthma. Trudy TSIU 72: 45-49 '64. (MIRA 18:11) 1. Kafedra fizicheskoy terapii (zav. - dotsent A.P. Speranskiy), i IV kafedra terapii (zav. chlen-korrespondent AMN SSSR - prof. PaI. Yegorov) TSentrallnogo instituts, usovershenstvovaniya vrachey. USUVSKAYA, R.M.- SHEINA., A,N, Zffec~~ of altrasound on the tonus of *a-onctfal mu-szulatlirp- and hemody-namic indicesv experimental studies. Trudy TSIU 72.z 50-54 164. (MTRA 18:11) 1. 13 kafedra terapil chlen-korrespondent AMN -SSSR, p-rof. P.I. Yegorov), 1 k-afedra fiz:Lcheskoy terapii (zav. - dotsent -4 A.P. Speranskiy) Menti-allnogo, Instituta usoverabew3tvoranlya waclit"fo - SHEIILk, A,K., dotsent Use of 11pocalne in acute and chronic dAseases of the liver and the billary tract. Vrach. delo no.2:48-53 F 161. (MIRA 14:3) 1. Kafedra terapii (zav. - prof. G.I.Burchinskiy) stomatologicheskogo faIkul'teta Kiyevskogo meditsinskogo instituta. (LIVER-DISEASES) (BILMY TRACT-DISEASES) (LIPOCAIG) Ye.", Probc.-Lonns ctateriidnat-lon f 7a.3tr-.c c y 'I i ty glo~!sod . ia Vrach. delo :10.0':45--47 Je -'61. 15: 1) 1. Kafedra terapcv-ticl-,es,:cor stomatoiccii (zaw--iu-,-.is*hc',-dy - prof. i.0, IqV4 k) , kafedra tciraiAi (zavudu sto,~:ia'L,olc):-~-~-(--hes.-ogo ' kul ota i fa :a 'fe,F; Shamray) llipvokagc !,,ieditsjls:c"o SHEINA. A.K.. dotsent ~ - --- - - - - --- Clinical observations of the action of phthivazide in Botkin's disease. Vrach.delo no.8:72-75 Ag 162. (MIW. 15-11) 1. Kafedra terapii (zav. - prof. G.I.BUrchinskiy) stomatologi- cheskogo fakallteta Kiyevskogo meditsinskogo instituta. (HEPATITIS, INFECTIOUS) (PHTHIVAZIDE) AFANASIYEV, G.D.; BORISEVICII, I.V.; SHANIN, L.L.; SHEINA, I.P. Cases of Ar and K nonequi-librium relations in biotites in connection with the creation of geological time scale in the absolute chronology. Izv.AN SSSR.Ser.geol. 28 no.1219-45 Ja 163. (KIRA 16:2) 1. Institut geologii rudrqkh mestorozhdeniy, petrografii, mineralogii i geokhimij AN SSSR, Moskva. (Potassium-argon dating) SHEINA, Klavd1ya Petrovna; YAKOVLEV, Mitrofan Fedorovich; ----------TUBOI.ITSEV, M.', red.; F(-'/J1AffEBKINA, M., tekhn. red, [Taking care of the most important] V zabote o glavnom, MoskvaV Mosk. rabochii, i963. 109 p. (miRA 16:9) (Moscow Province-Efficiency, Industrial) DRYNOVA, I.A.; KORSHUN, L.L.;,SHEINA, L.A.; SHUBINA, I.I. Use of flat lacquers for furniture finisbing. De~-.prom, 10 - no.11:9-10 N 161. O-ERA 14-10) (lacquers and lacquering) (Furniture industry) ACCESSIO14 ~;T~: AP4044276 S/0192/64/005/004/0583/o589 AUTHO It 9 1".11--rtsove P. V. ; Klevtp3ova, R. F. Sheina, L, P. TITLI:t Cryntalline yttrium hydroxides SOURCE: ','~-iurna) -icrukturnoy khLmii, v. 5. no. 4, 1964, 583-589 TOPIC TAGS; yttriur. hydroxide, yttrtum monohydroxide, sIngle crystal' growrh, hydrothermal crv!;t-ql growth, forrite crystal growth, single crvstal structure A 3 S -1, RA If"T ral-'s-paren t Colo r1es j cryG ta 11 111 --- 10inge s previous ly ob~- !;erved t'le -D-Uiduct5 of hydrothermal synthests of yttriur. ferrit-e rrvstais hivve been -'dcntLfied as yttrius, ides, YO011 and e!11) Thic f-,--yf3tal structure oE these lhydvoxiden wa,3 studied gonlo- ri e. !-. i: 1. 1 vand by x-ray diffraction, chemical analysis3and other !%c t 1--!" T',-,e r~,Cudy Was considered necessary Fur better understanding --Equillbvia and chemical ' reactioris in hydrothermal systems. rhe Y(~ev -,,ad Y,~011111, singt,!3 cryataIg used: 11-n. the study were synthesized lit 1-11d i-C villa I condltion:s frorp. either Y~03-'Fa203-Ii2O-NaOll or Y203- u" Most of the N00111 single cry.,4tals were In the form C A CC E S S I f'!,' A P4 4 4- 2 7 0 0 9 Ilex a a I I; -17t, be I ong in i; to the rpr i -4rnat Lc c I ar a of tile mono cl In ic cry s It a L i~ys teu-i and to tile P2 I /m q nace I, roup. Typical Y(f)11)3 single cry,;Lal-i wcro. oced"e-shaped, I cin x ;t,0.6 min, belonging to the hex.)- gonal and co tile! 116j/m spat:,-, group. Dimensions of Lite. untt cell le!--ermined for both hydroxides. 'File piezoelectric affect wns vot tl,:~tet-.ted in freghl" prepared Y0011. or Y(Oll), cry.3tal!" 71 h C x- ray (I 1"af-,t ioli pat te rn,-~ Y (011) ,A cry s ta In were found to be Simi I ar to those. M OR,' were 11 '-.q La , Nd , Sm, Gd , or. Er It was concluded tha t V'I 1 Y two cry-'~ al I ifte Phases--y (011) 3 ane YeaO.11-are f o rmed, ind iv id ually or s1multaneously, in tile Y203-1120-tia" syaLeifi belov 600C. Orig. art, has 2 figures and ) tableg, ASSOCIATIONz lnSLituc neorganicheakoy khimii 50 AN SSSRp Novosibirsk (institute of Inorganic Cheniitry, 50 AN SSSR) SUBMITTEDi 11ju163 ENC114 *0 00 NO REr SOV: -004 GTH K R t006 SUB CODEt S 5, lc Car-j 2/2 L 60923 (m)/EW I.D(t* (b) 1JP(c) -65 EwT(1)/EwT j/T/E11G(b)_2/EWP ACCESSION NR: AP5018925 UR/0363/65/001/006/0912/0917 546.65-36:548.19 .2`1 AUTHOR: Klevtsov, P. V.; She4qq, Lo P. TITLE- Hydrothermal synthesis and ystal structure of rare earth hydroxides _5~r SOURCE: AN SSSR., Izvestiya. Neorganicheskiye materialy, v. 1, no. 6, 1965, 912-917 TOPIC TAGS: rare ..earth hydroxide, hydrothermal synthesis, crystal structure ABSTRACT: Rare earth hydroxides of the composition M(OH)3 for elements.from La to Th and of the composition MOOH for elements from Nd to Lu were synthesized in aqueous NaOH solutions by'the hydrothernu-3. aiethodo. The N(OR)3 comPounds are stable at a lower temperature than MOOH. The temperature of the M(OH) j -.4 HOOH transformation decreases with increasing atomic number of the rare earth'element,'.- _j600C for Nd to 120C for Yb. -ray diffraction studies showed that all of from > X the s hesized trihydroxides have a UClj_type structure, and that the mono-' ynt hydroxides have a YOOH-type structure. Ne lattice constants of all the compoundsf-~"- are tabulated. In both the mo-.qo- and trihydroxides, the unit lattice parameters decrease as the elements become heavier; this is due to the lanthanide.c6ntraq- -J, on# "The authors thank F. A, Brusentsev and A. N.-Rebenko for assistanaa -at" L 1t,63620-65 -EEC (b) ,2ZW (I) IZW(~)/DIR~W/T/Wkt,*~. Pi~~-4 Vjp/ ACCEMON NR: AP5016921 UR/ 0192/65/006/003/0469/0471' 548.736 b ;AUTHOR: IGevtsov, P.V.; IGevtsova, R. F. Sheina~, 4 P TITLE: Crystalline yttrium hydroxychloride 4. SOURCE: Zhurnal strukturn 1965 469 471 khImfi, v. 6, no. 3, TOPIC TAGS: yttrium compound, yttrium hydroxychlorlde, crystal structure ABSTRACT: The chemical composition of crys talline yttrium. hydroxychloride was de- termined. Chemical analysis gave the foHowing results (in wt. %): -k3+ 54. 8; Cl-, 22. 0; H20 + HC11 31.3. Infrared spectra showed the absence -of water of crystallization and the 1 presence of hydroxyl groups. The results of the chemical analysis led to the formula Y(OH)gCl, which was confirmed by an x-ray structural study. The compound be-longs to thel rhombic system; Its Laue class Is D2h - myrim; the unit cell parameters are: a = 6.21 + 0. 03 - A) b = 12. 54 + Oi, 06 A, c = 3. 62 + 0. 02 A. The average density of the crystals measured by the fSotatton method Is 3._71 g/cm3; hence.. the unit cell contains four formi units Y(0142CI (the x-ray density to 3.73 g/cm3) X-ray powder diagiams of the Y(OH)2161. crystals were also studied. Orig. art. hu: 1 table. I Card 1/2 KIXVTSOVt F.V.j -6BETNAt I-,P- I ,hermcgraph!c and X-ray diffraction study of cz-(StAlline hydroxIdes of rhre-earth elements and yttrium. I%v. AN SS~ ,zP. horgo mat* I ncol2if'219-2226 D 165. (M.111.k 1. institut neozgitn~cnesl(cy khIn!I Slb!rokcgo otdc1naiya ON to. SO R a 5 ~'LIOO A I.-2H 13 1 IS Gailay, Z :1 - Aand Shei na, 'N - :T 3 106 Y3,1 4 7 T 1T L-" Amperometric titration of vanadium. and uraniu;;. trivalent titanium 1ELIODICAL: Zhurnal analiticheskoy khimi-J, v. 16, no. 6, 19061, 7o6-73~; TEXT: The authors were the first to use comDounds of trivalent titaniljz as reagents in am.-perometric titrations. it had been -found earlier that trivalent titanium oxidized on a rotating platinum microelectrode in the potential range 0.4-0.9 V, with the diffusion current being proporti 0 nal V~ to the titanium concentration (Ref. 4: Peshkova V. I'M, Gallay Z. A., Vestnik MGU, ser. fiz., mat. i estestv. nauk, no. 10, 73 (1954)). Because of this valuable property and owing to the fact that trivalent titaniuE ~s a sufficiently strong reducing agent (E0 TiIV/TJIII = -0.04 v) Jt can be used for titrimetric determination of hexavaleni uranium t' w 7 '2 + , IV (~o '; 07 /U +0.407 v), tietravalent and ventavalent vanadium in -ure salts and in the -,,resence of tetravalent titanium. T--e exzeriments -.iere Card 1P 29526 S/C 7 5/6 1 /01 6/006,41CC z/ 0 Cr'_ kmi)eror netric titration of 06/~O 47 -ade ir n a visual polarograph with an M-21 (M-21) galvanometer (max4mu:~ sensitivity 2.4-10-9 a/mm/m). A rotating platinum microelectrode o. lenCth was used as indicatur electrode, and a saturated calomel electrode as reference electrode. The rea~~ent solution was obtained adequate dilutiun of a 1c6 TiCl-, S01WAOI" Vlit;~~ ITC1 (I or d ~[ H-,SC- 4 -it can be store--- fk~r in dark. glass vesFjels. All experiments were in :iitro~_en atmcs.~.here. The concentration of the reafEent S,;lutiull was ascertained by potentiometric or amperometric titration with -a standard solution oi.' potassium bichromate. When,--' 0.5 sulfuric acid is used as a medium, pentavalent ;anadium is quantitatively reduced to trivalent vanadium by trivalent titanium. In a 0.1 Y, sodium tartrate solution (PI, 5.9) as a mediumn, vanadium is only reduced to tetravalent vanadium. Solutions of comPound3 cf trivalent titanium can be used as a ::lediii,r. 'or The amperoi.,,etric titration of tetravalent vanadium boTh in -,-,ure salts and i!l ~he Drese:ice of considerable amounts of Cr(III)P .1,Tn(II), and TJ~TTr' 10 :T H_,S0. (Table 1). Hexavalent uraniurn is only slowly reduced trivalent. t.itaniur::. Reduction is accelerai-ed by addition of ::yr:,- ~,nos:)horlc acid or 1cw a7.3-ants cf SnCl,. Ye. R. 'Niko'layeva and Yu. I. .4 C . i 16 IOC6,'C C I ~CC6 S !C751161 i l C) III, Am,perometric titration of ... B 0 B147 discovered tliat -iddition of pyrn-phospho-ir "!C"O 111-,='-'-15~11 valuo )f :';' _, 1,1, fl-01,1 0.4 to 0.(). Wilrtl-.~ -,01-r- ,T),,,- i-ophes p-1-1- orli c T ~.Cid for:;1 a cjmpley compound , tetravalent titanium arid, thus , lowers t.,.-2 redr~x ,,otetitial of the system Ti(IV)/Ti(III) .Addition of 0.2-0.3 milli- I e 1 o f 5 0,; 1 , i0in 1 N 11 so as a medium made it 'possible to cc~nduct 1 7 2 11, a-~ipe--onictric titration at E =0.8 it. The error of determination of ~ 'I -j -a:- Cf Tr docs nor exceed 1 .3 Thus , uranium can be ji--.-antitatively -1- 4, e r!~ i i n ~-: d-,I tile presence of considerable amounts of tetraval-it t.3tanium, (u!- to a ratio U : Ti = 1 100) in 1 11 H2SO4 as a medium if the solution to be titrated contains 1 milliliter of 5C~' PYro-jhost)hcric acid -/V1 0 per 10' r.-;illiliters of solution. Deflection of 'the galvanometer is -;~-.--istered "0' seconds after addition of the reaGent solution. There are -1 ft,--ure, 2 tables, and 7 references: 5 Soviet and 2 non-Soviet. The reference zo the -.--nL~lish-lanouage publication reads as follows.- ;'~-,nrixcn S.. j. ALI. Chf--,.m. Soc., 45, 2013 (1023)- Card 3 A 29526 A-miperoric t rLc tiltrat ion of BI 06/ i31 47 A6 S T j,'; I T 1~ '7oskovskiy gosudarstvenniW universitet ira. V. Lomonosova State University imeni I.T. V . T ~ o ri. 0 p, C, ,M,ii:*i','T:--,): October 6, 1960 Table 1 of vanadium in the presence cf foreian e 1 n t s 10 INT ~T QO, P's a medium. 2 I-c,7cr a' (1 for-24!~n el%,ments, (2) V, mL--; (3" taken; g: Orrc-r, CZ) V. AW 02 V. NJ rIOCTOVOTHIRE OW116Kl HOCTOPOIlInfe - - 3 - B3JTrO ~ 7 M w 6 0'4 0'45 -2'0 -100 0,68 0,63 -7,0 1,39 38 -0,7 TOV 60 2,00 2,06 3,0 Crl+ to 0, 92 0,91 -i,o - 60 1,()0 1,02 2,C) _J00 0,92 0,89 -3,0 -104 1,()0 1,04 4.0 I-In'+ 50 0,68 0,67 -1,11, C-aa-d ALIMARINY I.P., GALLAT, Z.A.-, SHEINA, N.M.; HODIONOV4, T.V. I Current-voltage characteristics of N-benzoylphenylhydroxylamine solutions. Izv.AN SSSR.Otd.kh-im.nauk- no.3.'567-569 Yr 163. (MIRA 16:4) 1. Moskovsk-ily gosudarstvennyy universitet im. M.V.Lomonosova. (Benzohydroxamic a0A) (Reduction, Electrolytic) GIALI,AY, Z.A.; ALIMAHIN, I. F.; SHEINA, N.M. Voltanmetric study of benzoh.,,rdroxamic acid solutions. Izv. AN SSSR. Ser. k-him. no.11.2050-2051 N '63. (NI-PA 17:1) 1. Yoskovskiy gosudarstvennyv universitet imeni M.V. Lomonosova. GALLAY, Z.A.; A-11MAIRIN, I-r.; SHEINA, N.M. Use of N-benzoylphenv"',ydroxylamine for the amparometric titration of titanium, zirconium, gallium, and scandium. Zhur. anal.khim. 18 no.12:141142-1446 D 163. (MIRA 17:4) 1. Moskovskiy gosudarstvenn~7 universitet imeni Lomonosova. 164 L 14686-66 '.'P(e )/F1VT(m)/ETC(f )/E',VG(m)/T/wp,'-_, ACC NR: AP6005881 CA) SOURCE CODE: UR/0075/65/020/OIOA093/10 6 AUTHOR: Gallay, Z. A.; Sheina, N. M.; Alimarin, I. P. ORG: Moscow State-University im. M. V. Lomonosov (Moskovskiy gosudrastvennyy uni- versitet) TITLE: Amperometr,c determination of_j~alli in gallium arsenide' and phosphide SOURCE: Zhurnal analiticheskoy khimii, v. 20, no. 10, 1965, 1093-1096 TOPIC TAGS: gallium arsenide, phosphide, amperometric titration, gallium, arsenic,. graphite microelectrode, electrolyte %J(M avqece 0RCLr04keIr'%Sti(.!. ABSTRACT: The applicability of the amperometric method to the determination of GaAs and GaP in samples of minimum possible weight was studied using a rotating graphite microelectrode and the reagent U-benzoylphenylhydroxylamine (N-BPHA) for the ampero- metric titration of gallium. A preliminary study of the volt-ampere characteristics of N-BPHA on a graphite electrode was made; oxidation waves of N-BPHA were obtain- ed, and the dependence of EY2 on the hydrogen ion concentration was determined. For acid background electrolytes, the diffusion current was found to be proportional to Card 1/2 UDC:, 543.24 2- __ L 14686-66 ACC NR: AP6005881 concentrations up to 1.10-3 M N-BPHA, and the oxidation current of N-BPHA was found to be much more stable on a graphite electrode than on a platinum electrode. Gal- lium was determined by means of the oxidation current of N-BPHA at pH 3 byK:mpero- metric titration in the presence of arsenic (III), at a graphite electrode po* tentia of 1.1 V. The accuracy of the determination is high up to a Ga/As ratio of 1/1.5. Arsenic (III) was determined in the presence of gallium by amperometric titration with potassium bromate. In the case of the semiconductor GaP, gallium was determin- ed with sufficient accuravj up to a Ga/P ratio of 1/1.5. Orig. art. has: I figure, 5 tables. SUB CODE: 07/ SUBM DATE: 270ct64/ ORIG REF: 004/ OTH REr: ooo Card 2/2. GORTINSKAYAq T.V.; SHEINA, N.P.; SHCHUKINA, M.N. Determ-inati;n- 'ofpAthe dissclution properties and the mechanical hardness of tablets. Materials for the 9th edition of the State Pharmacornia. of the U.S.S.R. Med prom. 14 no.9:15-23 S*160. (MM 1, jTABLETS (MEDIGM)) (DRUG INDUSTRY-ZQUIPI~MTT AND SUPPLIES) GORTINSKAYA, T.V.; SHERIA, N.P.; SHCHUKINA, M.N. Some derivatives of 3-mothoxy-6-(sulfani.-lamido)-pyridazine. Mod. prom. 14 no.9:23-25 S 160. (MIRA 13:9) 1. Vsesoyuznyy nauchno-issledovatellskiy khimiko-farmatsevticheskiy institut imeni S. OrdzhonlAlidze. (PYWAZlITE) L 14839-65 EWM1M(k)1EWW18WP(J)1AW(0 Pc44/Pz-6 UP (0- AFM W AT/RM ACCESSION NR: AP4048434- S/0181/64/066/0,11/U74/3475 AUTHORS: Avdeyenko, A. A.; lgaboyycin, Yu. V.; Sheina, S. P. TI TLE: Effect of external field on the:spectrum of the imomo- geneous 2hot conductivity in pyre~ie single crystals SOURCE: Fizika tverdogo tela, v. 61 no. 11, 1964, 3474-3475 TOPIC TAGS: photoconductivity measurement, carrier recombination, i carrier lifetime ABSTRACT: To trace the influence of an-external field on the spec-- tral curve of the photocurrent of a layer-type photocell (in which the illumination passes through a transparent'blectrode along the applied field), the authors used sing.le-cxystal pyrene.purified by- sublimation, a DMR-4 double monochromator,,a DKSSh;;-200 electronically' stabilized xenon lamp, and a Ul-2 electrometric amplifier. The re- sults indicate that at low fields; there is only weak separation of Card 1/2 L 14839-65 ACCESSION NR: AP4048434 ;.the charges and their recombination rate in high if their d ensity in, ,...the generation region is high. The anticorrelation between the, :.photoconductivity and absorptJon spectra in weak fields is attributed~ _to the decrease in the carrier lifetime in the region of strong ab- sorption. Favoring this conclusion is also the behavior of the soe-0- tral curve when the illumination is applied from the sideof the negative electrode, where the field has. a smaller effect, because .the drift mobility of the electrons in pyrene is much smaller than :the drift mobility of the holes. "The authors thank V. V. YeKemenko for a discussion." Orig. art. has: 1 figure. ASSOCIATION: Fiziko-tekhnicheskiy institut nizkikh temperature AN UkrSSR, Khar1kov (Physicotechnical Institute of Low Temperatures, 'AN UkrSSR) SUBMITTED: 09Jun64 ENCL: 00 SUB CODE: SS, OP NR REF SOV: 003 08 OTHER: 0 Card 2/2 ',!J 7 k i k, teineratur Ail S/141/61/0o4/oo6/033/017 F192/E382 AUTHORS: Peskovatskiy, S.A. and Sheina, T.G. TITLE: Measurement of the permittivity of small samples at UHF P.,'-JUOUICAL: Izvestiya vysshikh uchebnylth zavedeniy, Radiofizilca, v. 4, no. 6, 1961, 1099 - 1103 TLXT: The paper was read at the conference of MV and SSO 55SR for radio-electronics, Khar1kov, 196o. The possibility of measuring the permittivity c of very small samples, such that the maximum dimension of the sample 2a is . '. much less than the wavelength X , is of considerable practical. interest. For a sample having the form of an ellipsoid of 1-J- revolution situated in an electric field E 0 which is parallel to the longer axis a of the sample, the frequency deviation in the measuring resonator is expressed by (Ref. 5 - A.L. Mikaelyan - Radiotekhnika, 10, 1, 23, 1956): Card VaK s/i4i/61/o04/006/013/017 !-leasurement of .... E192/E,382 __f2 F, 2 (2) f ) V where ~c C/60 - 1, c0 is the permittivity of the medium in which the sample is situated,and v xs the volume of the sample. The remaining symbols in Eq. (2) are defined by: A- P F E2 -C)2 [-' In 2 (C,/a)2 I - -(-c 2 Card 2/0 'it-asur(.!ment of ~-l 9 2/ F-3 8 2 wh er eo .1 ~ c/a< Iand the quantity R cati be expresssk-d hv R 0 03 , oe.46(c/a) - 0 1 (c/a) (3a~ where c is the small axis of the ellipsoid. On the basis of the above equations it is shown that the real and the imag-inarv components of C can be expressed by F/2TJ R 2 + RNs Q F C Where I/Q. J/Q OE 1/Q 0 ,where QO. and Q0 a r e t h e Card 3/6 _-., 3 ',.~ S/14.1/61/oo4/006/013/017 ,qp,asurement of E. 19 2 / F3 8 2' qt1a.11ty fjjct(,)rs of' the I esoriaLor with and wit,hout the samplf, 1-especttvel.y ihe parameter R can be determined graphically (F iT., I ~ It is shown by analyzing the measurement conditions Uia~ tho main error in measuring e- is due to the deviatiou of [lie sample from its ellipsoidal form. On the other hand the error in the measurement of C 11 is primarily due to the error in determining the quality factor of the resonator without load The errors in measuring e' were investigated experi mentally vriLh parallelopiped samples of identical weight. )I was found that for the cylindrical samples the measurement frrnr of E did not exceed 10%_ On the other hand. when compared with the waveguide method of measurement, thf: above imall z;ainrli~ 4nethod resulted in a discrepancy of not more than Ito,` I t ),7 thereCore concluded that the small-sample method can be used SU(ILessfully for the measurement of c the horrors of measure-, inent are- comparable uri.th those of the waveguide method 0; the small -sample method has the advantage that vcr-Y 1 ~iampLes ran bo employed and that interpretation of tt- ~e- ,ult5 i!- riot morr complex than that in the othet mpthod!~ s/14l/6l/oo4/oo6/oj-)/OJL7 Meaauremezit of .... B192/r, 382 The authors express their gratitude to A.N. Chernets for valuable; advico and for his interest in this work. Ther-t- are I figure, 3 tables and 7 references: 5 Soviet-bloc aud 2 iiori-Soviet-bloc. The tiro English-language references mentioned are: Ref. 4 - H.B.G. Casimir - Phys. Res. Rep., 6, 16,-,, ig5i; Ref- 7 - L.C. Maier, J.C. Slater, J. Appl, Phys.t 23, 68, 1952. .AS_--,OC1.,'%TIoN: Institut radiofizikirelektroniki AN UkrSS11 (Institute of Radiophysics and Electronics of the AS UlcrSSR) SUB'MITFED: Febrijary 3, 1961 Card 5/# ; 2 817 6 s/iq0/61/003/Q40/Cj04/O1.9 B" 30/B 110 AUTHORS~ Kc-rshak, V, V- Krcngauz, Ye,,S ; Sheina; V Ye TITLE~' Stud;.es in the field of coordination polymers V- Synthesi; of coordination polymers of some b1s-.*',-diketones) PERIODICAL: Vysokomolekulyarnyye soyedineniya, v. 3, n,-~ 10- iq6i, 1456 '46,, TEXT~ The authcrs synthesized aliphatic bis-(P-diketones), 1;112,2- telraa~;etyl ethane (1), adipyl- (II), and sebacyl diacetophenone (III), and prepared and studied their metal polymers, They prepared I from a suspension of 0.5-mole Na-acetyl acetonate in ether by adding a solution of 0,-5 mole iodine in ether at room temperature under vigorous stirring, The melt:ing point was ',85-1860C, the yield 27-30%, 11 and III were Prepared a-:,,~,,crding to V. V Korshak et al. (Vysokomolek- soyed 17064, 1959). The me-Lting point of III was 1081,109,5 0C (Yield 20-22%) The metal polymers cf the bis-(P.,diketones) produced were prepared by 3-hr heating in a va;,.uum -3f 2-4 mm Hg of their equimclecular mixture with the Card 1/4 M 76 S/-,g 6 -. /o0 -3 '0 1 O/co ~,/C- i Studiec ~n t?,e faeld c-f oordi-na-.ion B130%1110 )/ respective Me-acety! acetonate at 150-2100 C until no acetyl acetone was set frer- To remove the remaining acetyl acetone, the resulting product was rreated with hot water, boiled in alcohol, washed with ether and dz,ied to ~~onstant weight. The ,opper derivatives were obtained by react_,L~jn of the diketones with copper a--etate in an alcohol solution it vas found that I with Be-, Ni~-j Co-, and Znr-acetyl acetonates formed norifusi.ble powders which were unioluble in ordinary organic solvents and hau a high decomposition temperature. I formed no coordination compounds ,with Mn and Cd The ;hemical analysis showed that the composition of the re,2uiting metal ccmpcuAids corresponded to the theoretical values Also the metallic deri-atives of II and III constituted colored powder~i The Be -derivatives -of III, and the Be.-, Zn.- , and Cd-derivatives of II, are 5cluble in ~_hloroform, tetrachloro ethane, dioxane, bromo benzene, and dimethyi. formamide ', the Ni- and Co-deri,,ratives only in dimethyl formamide and dioxane The peculiarities of these compounds are explained according to Hammcnd Borduin, and Guter (see below '), In the interaction between tetraacetyi ethane and the metal ions. a coordination binding of the meta'J. taKe3 P-,aLp- between the keto groups of adjacent mclecules c--P tr Card 2/4 2 81; 7 6 S/19 61/003/010/004/019 Studic-s iii the field of coordination ... Bi 5OY31 10 bil-"Jinp ~;gent (rig. 1). In II, ani particularly in III, the formation of closed, monomeric complexes is probable because of the presence of a flexible- meti.3'lene chain (Fig. 2). rhere are 2 figurem, ' tablea, and 6 retf-,~rences: 9 Soviet and 4 non-Soviet. The four referendes to English- lan,luap,e publications re?d as followei R. G. Charles, Organic Syntheses, T `~ .a,-1, 1959; G. S. Hammond, W. G. Borduin, G. A. Guter, J. Amer. Chem. 500. , 51 , AbC2, 1959; G. A. Gauter, G. S. Hammond, J. Amer. Chem. Soc. _, 4606, 1q5); G. J. Buller,) Acta crystallofgr., Li U 12t 703, 1959- AS S , OC !AT i .) 1; 1Institut elementoorganicheskikh soyedineniy AN SSSR (Institute of Elemental Or&nnic Compound-, AS) UISSR) 1960 EUB"ITTED: Outobor 25, 1. i:'J)d,_~l cof a 1,1,2,2-tetraacetylenu etlhan,? cor.,ple:. j;ith neta-I, 0 --hydroc.:'ni, -)-- oxyCen, metql. 2. of a st~buc-l di.~.,cptorlhpnone coiu-Llex wit.r. metal. Desi -.,ations as ir. F; .7- 1YIN19 5 0 951 q 7 C inva!"- r o t~her 2S, _L'a-nt~ 0 t ca 0 -rT -7, , ~ I ; 1, _-_ -- _ ;' , - u Z' y C'3 su" - - " r c e S J-Y ~jQ S ts -~C'a -7 0 ____--ed ue 0e r ~U' - Z: Su- - e -.- e Is 2 od 0- J'j ' Lz.- e ... U 0 1- e Ic., s ly t and S'i a i.' -a, d 0 71 zD t "a:. va- r 0 0 n" U!"z" 2d the or G ad E., 75 e -'a. T,~ L 4 t t i vi ty C and 'an.-ens ol' - . ~ - Z, " - r. = -- ;?,./ -. IN --e s -a r We- V e o f 2 G C) .2 27" vi 0 1 -, sY ven. The 0 r, r o n :)du cl CY pc ~- f turbe ~ac' ~Or O~ 171 lr- 4 --y )" a'n Vl~ 79 kw; ~2-L L 22651-65 EVIT (m) /ZpF (c 1EM?j Pc-4/Pr-4 RM/MLX ACCESSION NR: AT6002130. S/0000/04/000/000/0173/0177 AUTHOR: Korshak, V. V.', Kpongauz, Ye. G Sheina, V. Ye. Vasnev, V. TITLE: Synthesis of bis-(beta-diketones) SOURCE: AN SBSR. Institut neftekh1micheskogo sinteza. Sintez i svoystva monomerov (The synfhesin and propekffe-B7oT-xg,57Ed--me-rs~.-'Iffo-o-edW, Izd-vo Nauka, 1964, 173-177 TOPIC TAGS: diketone synthesis, beta-diketone, aromatic, diketone, diketone polymeri- zation, organometallic complex, boron trifluoride,' acetoacetylation A13STRACT: A direct method has been developed for preparing aromatic bis-(6-dike- tones) which can be polymerized to give coordination-bonded metal complexes, and a re-b action mechanism for the ketone synthesis has been proposed. The aromatic compounds. are acetoacetylated in the presenct: of boron trifluoride with acetic' anhydride. 4,4 a'- (acetoaceLyl)diphenylox1de was derived fiom diphenyloxide as shown by the following equation: 0-0 + (Clico).0 -"y. C112co- COM, are cllscoclhco-.~e--~- ard 1/2 0-jD-C0CHt=ff. C L 22651-65 ACCESSION NR: AT5002130 and by similar reactions the 4,4-bis-(acetoacetyl)- derivatives of diphe4ylmethane, di. phenylethane, and of the diphenyl eMers of ethylene- and diethylene glycol were obtained. The best results were obtained when boron trifluoride.was rapidly added to the reaction system and this effect was shown to be related to the proposed reaction mechanism. Diacetylated ketones formed by the first reaction step are further acetylated either by direct C-acetylation, or via O-acetylation of diketones and subsequent C-acetylation of the ester formed with the enol of the diketones. The first -route is exclusive during the initial reaction period, while the second can become dominant a's the acid concentration increases. Infrared analysis showed that only p-derivatives are formed and that the bis-(6-diketones) exist only in their enol. form. Their reaction, either in the melt with acetylacetonates or In -solution with Me acetates of Be, Cu, M, Zn, Mn, Co and Cd yielded coordination chain polyme v:ce colored- and infusible* 0= which were higb? powders which were insoluble in: i olegido. so-tv-0,6t j-4-200400C.--Orig CZ has: 11 formulas. ASSOCIATION. None SUBMITTED: 30Jul64 ENCL: 00 BUD 00DE.. 0C clc;.. NO REF SOV: 006 OTHER: 010 Card 2/2 ~ -- . Usin-~r eleL:~I-rodi al-- ~ ~- fo . jt,-,dvi.PZ bleached --ocks. `r,,~dv Gor.- ,i S I - - I Z-10 01 -inst LKICI-, SSS~-, r-C. -2:153-1159 15c'. (T- ~'- 14,:2 ) (i dme-ralo-ical chemistry) iiurliriskiy porous silic~~ou* rocKs :,I;s ausorben-E. TrudY -Jror.- inst. Uio'.'ilf SS611 no. )5:277-289 '60. (H UiA 1l; : 1) (Kurlinskiy region (Sverillovith- Prov i tire)-- Rocks, "Aliceaus) (Am3orbents) kand.khimicheskikh nauk Study ano salection of wetting agents for coals of Yegorshino District by use of the method of capillary absorption. Sbor. rab. po silik. no.2:29-39 160. (MIRA 140) 1. Gorno-geologicheskiy institut Urallskogo filiala All SSSR. (MINE DUSTS) (WETTING AGENTS) ~_SUINA, Z.G. -, karid.khimicheskikh nauk; PONOMAREYA,. L,,K. Study of the kinetics of wetting dust from quartz-bearJ-ng rocks by means of capillary absorption. Sbor, rab. po silik, no.2:115- 124 '60. (MIRA 14:3) 1, Gorno-geologicheskiy itistitut Ural'skogo filiala AN,5SSR. (MINE DUSTS) (WET',"ING AGENTS) WALUKRIN, G.A.; SHEINAY Z.G. Swulling as a diagnostic feature in determining the mineral composition of clays. Trudy Gor.-geol.inst. UFAN SSSR no-56:155-159 161. (MIRA 15:7) (Clay-Analysis) KOGHNEV, K.V., prof., doktor tekhn.nauk- SHk',LIX&,Z.G.-,_kand.khimicheskikh nauk; :L--== FEDOROVAI, G.G..' kand.khimicheskikh nauk Preventing dust formation and keeping down floating dust in the Korkino open-pit mine. Sbor. rab. yo silik. no.3:109-117 161. (NIRA 15:10) 1. Gorno-geologicheakiy instiTut Ural'skogo filiala AN SSSR. (Chelyabinsk Basin-YAne 6sts) KOCHNLV., K.V., prof., doktor tekhn.nauk; SHEINA, Z.G., kand.khim.nauk; FEDOROVAIT G.G., IQand.khim.nn,1k Wetting agents and siLline additives as means of control-ling the process of dust preAftbQ. Bor'ba s sil. 5:21-27 162. (MIRA 16:5) 1. Gorno-geologicheskiy institul Urallskogo filiala AN SSSR. (Mine dusta~-Prevention) -SHEINFAYN, R.Yu.; KRTIGLIKOVA, N.S.; STASI, O.P.; NEYMARK, I.Ye. Mebhanism of the formation of a porous silica gel struct-ure. Par'. 1: Effect of the acid treatment of hydrogel on the size and packing density of xerogel particles. Koll.zhur. 25 no.6:732-738 11-D 163. (MIRA 17:1) 1. istitut fizicheskoy khimii AN UkrSSR imeni Pisarzhevskogo, Kiyev. -SHEINKER, A.P.; ABKIN, A.D. Mechanism of radiation polymorization. Part 1: Mechanism of gamma- ray induced carbonium polymerization of isobutylene and styrene. Vysokom.soed. 3 no.5-.716-723 My 161. (MIRA 14:5) 1. Fiziko-khimicheskiy Institut imeni L.Ya.Karpova. (Polymers, Effect of radiatAdn on) (Propene) (Styrene) L 56540-65 ACCESSION NR: APS016786 (JR/0286/65/000/010/9119/0119 AUTHOR: Lefarov, A. Kh.-, Shei I G..X Girko, Mi-D.;.Gubitskiy, A. A. nker, I TITLE: A transmission. Class 63, No. 171278 SOURCE: Byulletent izobreteniy i tovarnykh znakov, no. 10, 1965, 119 ;TOPIC TAGS: transmission, engine equipment, clutchNI 'ABSTRACT: This Author's Certificate introduces: 1. A transmission designed prin- cipally for trucks and caterpillar tractcrs., Provisionlis made for shifting gears .without interrupting the power flow by using multidise friction clutches mounted oni ,rotating shafts. The unit contains an input shaft, two coaxial output shafts whichl bare joined by a differential and are parallel to the input shaft, and intermediate ishafts, one coaxial with the input shaft and one with the.output shaft. The trans-~ mission has relatively small overall dimemsions. The. first intermediate shaft, iwhich is not coaxial with the input shift., is hollow and encircles one of the output ishafts, which passes through it. This intermediate shaft has a multidise frictior-- .clutch mounted on it. The driven,elements of this clutch are connected to the dif-' Card 1/3 F. 1, 1 AP501678E KUN~~,.V, St.; SHEINKMAN, M., FURSEN(0, V. A method for 'the nont~ontact studies of the conductivity phenomena in the cadmium sulfide semiconductors. Izv fiz atom BAN 10 no.2:29-30' t62. TT 7 7 1 A C 'C N RAr6o1L8Q,'w- SOURCE CODE: GF.10030' 6/013/001/0025/0036 /6 AU'PHOR: Kor5unskayal N. E.; Markevich.,_I, V.; Sheinkman., Mo K, 7 ;7 3 ORG: Institute of Semiconductors., Academy of Sciences of the Ukrainian SSR, Kiev TITLE: PhotochAmical reactions in CdS single crystals at low temperatures SOURCE: Phyeica status solidi, 7. 13, no. 1, 1966, 25-36 TOPIC TAGS: photoconductivity, recombination reaction, electron trapping, low temperature ef feet, _capium sul f ide crystal I S=Msa~~ V I M ak;~ 8"Woor ABSTRACT: The investigation of glow curves under various illumina- tion conditions in cadmium sulfide single crystals (previously annealed at high temperatures) shows that the photochemical formation of new trapping centers arises at +20 to -100C. In the same temperature range, the new "sensitizing" recombination centers, having small capture cross sections for electrons, also arise due to the photo- Card 1/2 L 36260-66 ACC NR1 AP6oi8336 chemical reaction. This causes the photoconductivity to be Increased bY a facClor of 2 to 100. The investigation of the kinetics of trappings and recombination processes by various methods makes it possible to determine a number of parameters for the new trapping and recombina- tion centers. The authors thank Professor V. E. Lashkarev for his interest in this work and valuable discussions and Dr. W . Bqrchardt. and Dr, J. Voigt for helpful discussions. Orig. art. hast figures, 2 formulas, ana-1 table. (Based on authors' abstract) (NT] SUB CODEs 20/ SUBM DATE: 03Sep65/ ORIG REF: oo6/ oTH REF: ol Card 2/2