SCIENTIFIC ABSTRACT SPACINSKY, S. - SPACU, G.

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CIA-RDP86-00513R001652620019-9
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100
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December 31, 1967
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SCIENTIFIC ABSTRACT
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RUBESKA, Ivan; SPACKOVA, Alena; ZENLICKA, -Tan - ~! ;4 ~ 1~;: I . 1 , - ,I - -'. - - . ~ - ii , . ; m, , ~ i : - ~ . : ''; -~l! ~ Z, :z ~: - , .. ~, :. : - : - - I ! ~ 1. ~ : ~~! : I . :~ 1. , -~ I :. 1, 1 1 , I I ~ ~ 11' 1 .1 -- j i ~ ~: ,4Z Praguse ?aeogiv or,) Firi-rolat!'i a 1~1 i, Vrl *111, Vo 2, -Copyright& -I'0lAPhW hauum. Of the Cnschomlwak Aca4v - once@ fttelstvi Ces%oaltmerie;&& ak&Ae-- my of s i tNakl. 1. -Estimating the Vollme of Ihe individut. I fiimeral a in :Bar-andistaza Oret'" Otto Pp 121-129. 2. -Re-arks -on: the ~Piftd dilts rq~of thi I;p 13 C-1,31. 1. -rlim-ralca of ClAmium in a VO Pa Nposite in I.Orth Viet- =.. :donsk J~HAII of.thc Cz-3 zvolarch 2rstitute (Vst.27 pro "4-,zk= rud). E-LLPAOI pr 1-52-l'o2. 4. "New Finds of 7haetonallur D=twval,~s (Ncval-. !E90)In the 3arramdlen,= moar.todcnlcm,," i1ri.L11:2, ;P 13,~_144. -Zowirk~ on the Algonquin Yor.-,.tion o, he Northern For- %'-On 0" t%" Vltuvs-Z Avel P.Q.HLICKI pp 145- 157, 6. nocal Spe opgrachic ltt:roanallyvis f ~I!zeralotical _tI :van riximn and IonbL 3N.L:i.W;. of a Central Gaolor_ L r~dni .1 V-11-1 _i Cal rnws a -Icky) , 2r",naj p-~ 15c - 7. on the ;Iozrdei~ tttween the 11..'tddle and Uojer Do. vomlwx Ia 'he 1.4chamtrm 'laanive." TAUG.L% ana 21we'. 101MICE; pp 165-175, 6. "Vessiliud Coaim taxat *,Ieu:. !IrtnIc"g Moruvia," juroolov _TYRA= of the Central Go.~Io~.~tc&2 Inatit-ate, rrLru!i r P lc-la5. P 9. "Zoolorj and Salanolos~y," ro=pd 3=3; pp 10. "Bacteris in the Mcent Sea Sed~Lv!rjts#" " denjk rLr:UL; PP IM-192. 11. "Idjustment of Comp%rr.*I,:e Bpectr-.ia Tablec for Another Type of spectrorraph t:sinj- the ~_xwnpls of Zalinin'a Atl&m for the Q-24 3pectrorrmph," Ardolf iLC32; pp IS3- 194. 12. ':;ote on the Yvl'-Ow Eclybdic Ochre -rem I:rupka in Bohe- eia," Prsntia�*A !;BM of 'he N.Lneralogleal Irtititute, ee,UMverallmy NilliRc2~.iZI-T I:azlcva Un!.,,,Qr- 1/2 SPACKM, Alena,, dr. (Preha I. Hmdebni 9, Czechoslovakia);~ KR---JCI, E., SPACKOVA, A.; Balneological Institute of Karls Univer:sity, ?rague and Ce-_6E_ralGe616`gica1 Institute, -Prague, CSSR [origizial language vers.on not given] "Determination of Gold in Various Solvents by Spectrography Budapest, Acta Chimica Academiae Scientiarm Hungaric V01 38. No 2,~ 1963p9 ae pagges 103-113. Absi"*ract: [Ge-,man article, authors' Enalish summa Two ~methods have been ry] developed for the spectrographic determination of minute amounts of gold in various liquid, mainly serum and urine samples. The:r first method is based on the analysis of the ash obtained by combustion of the aaziple*. The second method measures the amount of gold in the biologicalliquidi dropped on'~th6 ,-ra-chite electrodes, by direct spectrography. This latter ~io~edu:~e is- es_~ pecially suitable for routine serial analyses. 4 Easteim Euribpean,refeir'encies. Cpa 'j :If; . i 'bt, -19L-A i~ T,-; f3itc! ~fuqtjl- the:::' Id arg-ik4~d widi.!-:! InLI gia scti'4t:~ bf tAI6,;; P61nt ~~ k' lies Iii i R a s Jr o~1 V1 VA ANJ 71 ji" - url al". tj it li~i*w' out &1ito (maim., lip 15 7 -PharmaCol.'236 I'ul i: bo -sts at rw i h cc, es7' of t C. rts .6f, tt t-, - 11 - kx lie i or I;sp; Tlk~ Tk~ Tq~ Al 71 11, it: .:fD MiUlV b 4_07i_ _00 i i d- % OT, au8IF w OS A Igo Akh f~_v criat., (it ~6_0_ 1 13, lot loll 00 00 IS, 0 001 13 Mr. AiAml 00 ME -2111 -rL "t 4i1 L~&L Lnn&TM ammormovi %low siv,431'. vim. **"&ft. IV M. Is sa a u 0AT III ap; .41:;&* we 6, Rai w1lum 00 0 O.'A 0 M 01 0 0 0 0 v .0i 0 *Is wo'' 0 0 s,00 0 A-0 0 0 0 0 41 0 9 9 9 0 0 JIVI 11 F I-- ~ A $ 4 3 4 1 8 - 0 11 11 Ij U Is 10 17 4 11 Bill 12 A It 3 )1 V is )p X 31 U U Id 'a Is I? M n do I I f f, ki I I jt L j I . 4 , &I U L1 A- a -E . , , _ s__ , A ..CKM(t .-o -.0-twt,ti. .Mt. 00 00 A stedy of the ossWiss c*PMWI thIDIMMAI&S of aMmonium, "ssitue. sad sodium G.SPACUAXD1.G,MLuGvLxsctj. Bid. s-c. tninrr Cluj 5, M-107(IMA-The autbon 04 ObItoWe-the existence a( T empils. of X114 Cu thij~ulfatr~, Mcthods of prepn-!and 00 prownies of 5 of then are given: (1) 101AV60drICN1,O)i f1:0. yellow cn-tt. ni- white sumphow, (2) white cryo. (31 00 white cryst., (4) vibite cry~tp, lA) jCu(!YN),j(N1JJ,,- 00 2NIIaCJO*. white ciryst. potenti"lintUit/ -00 titration curves. Fvidtucc was alto obtained froax potentioxnetric ritrutions lot th'! 00 existence of 2 other couspils., one a brown-violet in color and the otherWar but the Ciall- 00, data on their c,)mpn. were that they coatsiiwd~ within the mol.. mew Nit. thkwuMatc .00 lol to the conclusion than compd. (1). Study tit the uWation rroction Cu + 2S)s 00 13. thatcupric solm of lowey conen- than 131 react With thk-UlfAte -Io, i)f the same votien. 041 to form exclusively the tctrathitinate according to the eqtutiov: 2Cu-' + 2$A-- ' coo - 2Cu + For higher omens. 5 is pptd. and the other products nlosidation 004 art- furnied. It w4f; not dctd. whether thew. product of osidatwit wrrj~ fortned hy the zoo l method for the dctn. of Cu can be ba-A-d on the forniation #4 the first 2 comp4s, For al concus. 0.01 to 0.2 J1 the titration ends with the fortuation of and forconcns. 0.5 to 1.0 Mitendswith the hAmation of thecufupd. JCu,(.,t01).j(1.,If,4 -91 * Vol , 1 t 7 ia.0 *0 7" 94i A 1 6 - S L AaEtALL1Jf'4K#L LITERM,41C CLASUMATICid El Ito U t, id a ir it a it a tt it at ) aOt 11 iiio ni x4 ' ' " 0 a00 00 0,00000 0 0 0 a 0 0 0 0 0 0 m L. -0 4, 0.-0 0 o 4 a 0 0 6 0 o 00 I; . * ale 000 &m 0*40fougs bm"I OOA it OW lb W [NI NI; -A ~,A -Z "so= seat 4om.m, 06AAR jig J, it, Al i di, i wo;-a - "a ! ! 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( vl' ro'll 41. 11 , 1, Il / ii l l j- 1 0 k J'N Ii "If 1 . 6. 23-111 MilikIlAill . I i o f i ~ 00 r.-Ill ol.it'-pil o t it- pleviol is Work luut led to the i..ulatjott of tile L, new dtige. Alonti,iVA. - eo$). And I'%jg(SC'Vj.'Icr CH&I ("llere ell - ethyleloor'' liAiiaw)l 'p,-1, ' ' .00 so fwul.iti"o of tile itionn IAjr(SCN),I la Cm plaox- only in thr pre,%ener of is Loitc ciltv'!; 11 4 ully u%t,h-r t1jrC coli'liti"j, to tile looloolen xp- oul plue In the 4 00 wlo .4 Corys141%. Under the IlAnic Ow v%,loIW [ . A SCNIII- -00 *0 It --kN11.1.10 ba. 1~o Jq~jjljt-d 'I'lic luMmittE holvit A140 liecil prepd I * ' Z Ill- 40 ,, ro, 1k OC-N). ~r cloth. 111IC(SkN ! 0 . 00 r fig ICo ell, Oil (1, 0). ny dwbic tiorworripul. ill;l(l. $0111 , llvt~t;Cll prev! Utul Y so l ' iwilird unions anti fttions, th 1011.1wring datable a int-4, ~~Wrr I '11111 % l fills to "1111111ex =so 00 jitionsof CrIuve been pftpl.: 1Cr(,;CNWYZucn,4IcruW . I., %*)tl- ' n t N (Cr(SC. zoo 00 10, o:116 Clut. (11 M. 1c, (Sc Ico no, 1Cr C N SCS )j ~Iixi NI zoo 0 ' I V "A"4 NIf. . S 0 (Cif ornil. Cr Wit ell.l. V Cr C., It, CQ SOC Ica Tilt Cf. I 11, 2). Cf ICr roil. All, P" 00 tIl'- f0 Ihe .tili h.wilig anii'll. illwill. waq "tablished-, [M SCN W. I swt I%Io(1;CN1 j ICu ell I%fn(hL%i)T'1ICl I ) ) je . , . I elis)211,1 land -NNOWN"d Ni I rlW'wVfCIwVjwI. Theirvoloor dorlotrulto Oil flint of tile affilph-li Cation "'wd. 4illet tilt Mn i,oillpli-I Cyanair Is "llor6w, I'AtTO i t 00 00 00 .1lAtIL"Ll"" livio.tLitl it ' '2A '-I~ W a n I-s 3 is or u to it -4 . ; 0 0 00 00.0 0 1 000 9 0 oleo 0 0 0 000 0: 0 o 00 4 L a A 6, a a a a 9 9 0 0 0 0 0 0 0 0 0 0 0 0 0 0 goo 4 1 1 1 A 9 IQ it 11 If 14 1) 16 if is x if J7 a A b is v- a N 11 1 is 11 U U 14 is Al It 0 91 It if III or* - -C` --L [0003 A A a r -a-L P L M I I I A.-X. P- a a I I V -T-- L A ... A. , . $-A a. r 0 A 4040 41 00 00 this an-alievo 4cwtips",Ilid In tho illinse of the Campion i7, q 00 ifetwI, Ossi 5. 411" 414 111-11) let at). M.111 of vonspiv% ItIhiryalinle callon. Ity 44 O.WiIjArst 61141001"s; 00 st A* objrCt wM% the (IvvT1WIMWnt of fraffroth which might 1W ussrel its All" anti the Mol "ILthe tjjwlj~ ciwnpkx thiticyanate Issas which exist In oq. v 00 #Jds Ile amminv% which ran Ise tistrived front t". The asmainvo towdarct NI en, 00 00 cit-21ljO. 1,14 en. J(Wh)g. jZn ens,101.2111.0, JCu en.11W. lCo tn,jCIl:IlItO awl 101 en, A. Ch: en - ethylesirdianxim. Ttwir reilctionts by double decatopes. with alliall Metal ilkk4 0 -00 of t he coc"Illex thitwYanstra of As. Zn, Cd. He, Cy and Ni. were Alet&; N64 all al ~ the 00 jll, WVrr&i CiWUIIIV]t thiAMY1411,011C its"M Of kWh Of tlWQk- eltownts weft Poll. in aq. Idja,~ &.4 III asn"lln..., A he lollowind fww etwolvIll, living Ohio*' that we" obtflif" ON on, roe 11. time trithstril. swirlslar 00 1 C(t %%'.%). 1. INA vi. tirt, orivalar err-OnIq j IM *I#, ill let CAIS) CIV4AI%, I(*- CIIIII/oWNS).1, $native, 11 IZOO owl 111val wbilt.; flialaVi, Cly'l. lipt t C"I"', t,: 161 raillild(C'NS141. white P114". 161. re. IL00, lipt.; 90 %If I.P. (if ("VS).j. flast-vitsirt. cryst. 1.,.Cr age ~ Cdeped it W l.white1jit., j1(#e%~jjMj( QN).l.whitr.acirislarcrystak; Witstall no 4j ale 11K(C' 0 V.S 00 i4 for ftlat ve Ylitalq; J(`W rxt6jCXCNS6h, mauvv, cr"t, iscantlet: ((W rail,1117're 00 0 t CS-IN I., ft"t. Amy, cryst. 11pt.. VIA too, I f%W' kiiI.Wid Ilpt. .Thew mal II"I'l: see (.Vl IN j arr usually Sol, In acettIne and Py- -~Iut infrequently %a In the Istual tv's lsolve'rib. OWL. filter. a1c, and bvnzvllv~ R, S 1.1111111,40D e ~-1000: 1111114111 too 16: too if *1,L3, at Q ~j st jLo to it it 10 at' a a It' ti It as F j an t 0 goo 0 go 0000 00 4 0 * 00 0 0 :0 41 0o 0 0 4 so 0 go 0900 0 0 q go 00 0, of 0 0 ~Ilf WOW -4 1 gogww*n&w IPFV b u SAY 10 - a 0-0 -6, 0- 0 -0- 0 0 0 V, W*19L a fW; *I a 0 A*& .0 g 3 q7V i64,we 064 Q~ 0 1 W 0 0 0 i 4 ' 00 0 t 0 0 oil 0-0 0 o 0 0 0 Pw a I a I c 0 0 r, 0 ~4t; L a v ~ . a w 6 Nola on wo.1ma $1 k I k AT s T"s it cm AT s , 1 T &00 3op IL11"M LIFTY toot &Z 3no C~C&z V vwm off. -Tdd~LS .044 - 74 ~L--;- Vogul lWN9VM11VLJ- V I 1 9 It V F Fee at 00 Vt IL 00 eel 00 00 00 00 A 17. 00 ir 00 90 I 8 d I I r R I a 1 9 W x IN it .1 $ f a v 11 a a w 'm In to a a 11 w Hann9 9 a " W w W 11 a - A ' I L i. L - - -- - - - - - - A 0 L a J I r. IF It 16 For to W JO n 14 is )I ja 20 jall 12A1 jib JL j a 14 j, 2 8 1 s IF 4 , -,, I AA N lE _y I I V.0m misk"IL V1. G. t AJjL~,Aj#R' .40 A now claw 91 Ommbws--OWPIO -k-0 - C.61I.MACAROVIC11. str don-moctiUd"(Py - pyfidine. TIM - tolitlinc, phyd Is- phenyl, xlq ci)ln ; 4j . j)w J,, jjji new l hytirmijw): jCd1W41Py6j(.%CN), frous lCdl'fidl SrCN), awl PY i's WT, tibelf; 17P1' 1 MxTAdpy.j(sFCv), (ruin 7WdPv,)(SrCN)i Will IZFFI - a (WAARSOCA"All it i h 0 e a n t ; ;KtAltilir Insminst without flanoor. d, 1, loll C41 NCN)V; Izo Atroorb 1f(IVFWAM .00 400 06 A 00 :;0 0 Age A%.-SLA ITALLUFtGKAL LITEN&Tt;*t CLASSIFICIATICS1 ow 4 all Srafla) -iv Q*( T-- L0 a to ZW to (11, of K If It W PE or It At it S a If 0 0 000 00 0 00 0 0 09 * 0 0 0 0 0 0 - 0 Oro 0 000 00, 0 IQ 11 9 ti w I a 7 4 vp nits u1111 Im h -W -* -W A V gal Gel -IT l S o I assosca, -s"ALLMOWAL it ;No- $"as& gem SMA&V owl / 2e -- - - - m Mae foam dw a" sit qr r y w u a 0 ; wo O rr k a, - a ;-4 41 i % 9 a 0 3 ~! I, * 1, ~L, o -0;.c~1 e-.06*90004,0,0WO-4 o 64 0 0.0 0 oio 0 0 0 T ' ~ _WkW 010 6 ois, e a e M 4 0 0 0 o o 11 It 1, is is it it it 10 11 11 .4 is a is IT x A 11 if l: At m 0 U v lot is t it U of 0 a A -f-'f --ii -n--" L .4 to if Q 9- L L-PA ix W It to 11,t 1,0 0 The class ol ammines rit tiollocy"ates with bestaidive and tolidin IV G; 'SPUCIS 00 moil C. (.It. Mactitsiici. Iffid. sec. i1ji.4 Chwj 7. --,:.-7 17CIRU). c(, I as Itruddhir and ttilislatic ilcrivs. Lilco. M.C11, Mo.zitallil NIX i.oo 00 1 hey Acre isylithmi'mil by usinK ale. boins. of the mittituctiti. Ali allf. soln.'of Ni-: t.NU,),AIi.0 unit KCNSon treatinent with heruldine (11-1) yieldi I.NiItISUI.0M.SCNj- - % 11.0, is firre x a 1, 2, 3 or 4 acanditti; Ito I lie coutlithmil tit (it yint. ~i I'M I Idt I ($M, "a% obtakard by holding lite ituatilfial at 75' ulf VA. Cd(SCN)' &0 jSCN)l. minpirtely anhyd, I Zu Bill (I l,O) i1 (SCIS01. and theAl 'I lyd. -4LIt 90 was obta,ined. In all thc~jxbovc coii I, be 04 tm~upici 2 ccWxdination puMcitim. In the Nfg com;Wds. 00 06 1.%I9IId40IzO)2J(SC.N)s arld the base occupic4 a siosj;k cowilinatillra I-itimi. The compil. cortill. two molo. of 11,0 can Lie Irk for d4yiijit coni-ict with Joyriding. with 1141 change, but the anhyd. forrit atki-s two tizolit. oil pyrldine. A iiinilir 06 -ries of hilidilic prelml, with file cAciftititill of lite Mg cortilml. lti'thi:w =00 the lia-c occupics a single cuortlimation poinion. slid the 11.0 k utote loo,,cly butind 00 than in tilt: Corresponding bviiiiiiiiecoulpds. None of lite comptis. Is W. in cold Ilio, -.00 69 and all are ifecumpowd bY IlUL lf%O. 110,it of 111011 tire Nil. Ill 131011 and NItICO, mad all tire .4. in UNA CIIC4 anif C,11s. The SCS CU111141. do, Stuvastre ill all 1. 00 haiimir -Aith the SA,CX comp&. [tilt tire, on tilt' Whole. Aillitilf. C. It. 11. jefftvyi A S it A .1 i'ALLUROCAL L L AO itit.l I A~ 5 IF U t%AV :,t 5 CW a ~ 16: - I or )it 5 Al 'a :$ Ap It 17 tv 11 v #4 a It for 91 K ri M it a M10 n 1, X4 f. 0 0 0 t, a 9 0 0 6 0-0 0,0 0 0 9 0 0 0 0 0 io 00.00 O'o 0 6 0 0': N 0 00 0 0 oi 0 a A J oo Go of 00 of so 00 00 roe Cog *OJ -!Do boo t:oe ASM.SLA METALLURGICAL LITINAUM CLASWICATIMS age. It" 00"Anv 911300a wal a.. out 0-4 U 0 10 is a In IN 19 1 FA v 0 0 0 Lf 0 4 a a 0 000 00 00, 0 9 0 0- 0 0-0000 00 :16 lei 0 0 000000 000 0 0000 0 0 00OV-0,we a 00 15 -fit 00410411000000 00 019 W 11 V U M 13 14 11 A-IN a so a M ~jl to i1 31 D JA is 36 IF jr 0 a A; A --A I v A X _- AA -4 1-1. ___L~ c# illIA lop 11111 It ~.N.pf 0 FOA 0 is *0 00 00 ;7 coo 00. see T-T ,NNW IL J IL, aeo see moo its-ILA WITALUMCIC.L LITIO&TWE CLASIVICATOOM 01G.1 $1,14ill. A' F- 0 W. 1A FAA9 It rw *I I cl 6 19 11 03 It a I I of lot it a r9 *,Q - - - - - - - - - - - - - - - - - - I ; 141 Z 'it I ,m It 0 11 a a a 4, a a 9 8 v 9 1 6 a 9 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0; Gilo 0 0 o a 00 00 4 o 0 11 11 u bi is k it w to N 41 41 a 85 r*00003 00 -00 Reftselonwirk mlisdy tal the fam4140". In 44"s liolit. Joe of a Ord" Of d*N4mNwdG blOw"a, ciollod 1-00 INA, K -A ifilak ~i il"Wroll aq. ,131b. knultdiubw two6shm NAVCUW nig to the I,j% toll kmalftfs., Killgel.1- N'1411140.1; rml,,wSCN)j. KtjllC(Cri jNlyl- KIMI(Oll, N11 114 0 The ~wk iq 1whij, cpolijilled. J, 0 g j too .00 IMP tsoo AS.-IL 4 401ALLLIKE,K41. 4.111PATUdif CL.WFKAMN l1w, 6 Use A. 0.0., .11 1 it jim 0. I as t, V, 4; :11 PA IV It let it Igo go 00 *is 04 0 0 0 o 0 OT ~o goo 0 go 0 0 0 0 000 6 i0 Wo 0 01 00 00 0 * of Go 00 004 09-3 00 13 Od 0 w no., a I I L A MULLUKKAL LITINATUM 3w 111hallve W A -00 ~$ is .00 Ak 400 see go ago WOW4 m NO coo i. f. .4~ gK 0 bdffg *goo see moo Wool MVMA"W low w NO boo a --w -v im A, 10 "1; O'~d a I W~ 0 9 dj 4 2. g V-dft 10~04: U0 0 0 0 0 0 0 0 0 0000 0 a 0 1, 4900 le 40 0 0 a4*4 Go le 0, i~o 0 a 0 0 0 0 0 0 0 0 0 0 0000 OLO to 0 00 00 0 0 00:910 0000 0001' M) g) im a ej a - - - X 31 2 13 Jd X Is 0 X X 4 41 42 43 Ad 4 SIT ANO 44kcal log ifto 4 too cootes FWfU9& AND P900#414S -011 sea ~ r 00 do l ; , 66 000 coo M CLANINWAIM m!" we* 83&111 40 OW Lit 0 loop U. AN a 1 w a 9 2 a 31 IF ~A 00.0 0 0 0 0, Vo fe 9 0 0 w - W. -..- - - ; 0 * 0 V31 10 IS M11 N P 6 it 41 Of M 0 11-4 L, 4CC U o AA 90 A A ;_e0 Its 441,001,0~ Old a 4 d w m d kiamm"a a i mm Mid, j,h M. NOW.-A con.: 00 a be 60098* 2404Y MAN. amtg. 2 qwto (cf. C. A. "140. Amp) love The InIbmime 0 - . R Imill, Ifftf fir jCdCIjNI: ICuCIjcjI o, - Imuct C4 b C .06 0 1 .-I L Ctl(, %0 or i . ei. us .. jIjCjjCj !~ ICSC"IBM OWL INGCJ. Ca; 4)11 - . I L KI: 1010400OUN: 1AI(MJ 1K I , 0 11 # ; IFVCLIK: j"aC%JK,; (C4,kIK; -d In. nw fomming wesno Iti, ll;j ilimber.4w,jr, "Mill CW1s; OW kk3 + KCI, fiti, ni.A. vi of C-h Cowtiturat a rm witb bvw O k 0 : t ulto t w pff imv.~j d The w"Wt!% we givtn fm 37 exlenjilm t&tjIjt% "d w dow".i; Victor JIjCk�L J be a ' PIP tv IP to a 09 t 0 j~ j_- ~__j MAD n 0 0 0000 0 0 0 0 goo 0 0 S 0 0 OL 0 ' 0 00 0 0 0 00 0 0 6 0 0 0, 0 0is a * 0 0 0 '0 9 0 0 9 0 000 0 f 0 0 0 0 0 o 0 0 00 A 0 0 00 0 0 0 0 0 t 21416 AA to twill) 13 u 11 14; It JL-.x f_Q -4 Mil 14X MLF 181114 41 0#1 At-1- Oq .O# 6 00 0 00 00 00 00 HI 00 a 00 ff 004 00 211" WAIL eii Mioii- TOmd-do .NOW gw 11a0bo" amd 000 Go ma C. Gb. MwmovkJ (ASSIC $-- 861416 Clojit 'm . a ink U& I. 1422-1m)-m-Tbe M201had d 0 - I s " 0 11'W T IIIIMO 0 6 t 11 GeV . 01 O III 111 . th. Za by S&MIUM ti fikm" of - "wot put of up Ob" 08, lif NHCN8 grM AjNO. 41br ii-WhIllotim 01 U"'.1""O' go" oa -A. P. Aloe, age 1111TALLUISICAL Lfftf&TMW CLOSWIC&TOR I low oftifte, 11 moo ."M i'llow) .1p mkv dot 811"JI09 ji door a" &$I u a, A. I 0 :i 0411111111000009-40411111100 0 0, W* 0:0~ 00;00:000 log : t s 0 0 0 0 0 0 0 0 0,01Wwollio 0 0 00,60 W 0 v 0o 4 .00 -00 00 12,// -a. Vdmmwo ml&d aw ft ftbm"li 0; C. Abo.. [wrld: 00 x V. Arnwam (BEL &r. +ink CSO, UK IL $06-21 aw -00 -Tbe w Od ~Mbbe im Kcsowtbad of seem; go C to] a Ni KCN, mWim cmwm pyo Omwe this to toil S E~rlb .=. 002 + Py+ .00 ht vic&t pvcipk"e i" HI jK"FWXcl,%)l-wd dw Oft4ribm" &ON&M is VZOM 11 ~~Oja KtN+to' f0m INneikio am Orm for c evilmatim o( Mi by brA a dketa mad an: indim4 nwt . thm. u~j twit* a avamtkm cmtainino 20 pm. or Kc.-,q "A 11) re- of pm',Iine prr coo zoo go. lie* see I S L A .41ALLURCICAL LITIOATURt CLAVVICATMN x IC31 03-LMV t %ftgqv~ 40, Aill"Pt Ca 00. ISJ - -1 --1 -;=-g- -1-T- f L 'a T, EA AR L 1 0 fm 0 O.'s I W, of 0 a 3 u V, 40 '0 Is it a AL No I not mall, its dL 00 3 ato.116& 40 0 0 0 a db a a a r I s is it u uu IsWull too It t US a jolt i1,= 3435JOI73600 41 90&4 k m I x f T P~L - I it is? ANC ?No 041mrs -140 640111 Ml I, 040cls"s 00. py0*10roll "Dr. A &W so" ION pm-u and Ch. Marsturld (not. (11"j. IIKL16 (2). 24:i-258t' ru.. ' 27. (4). WA).- Ink, two bw&Lrn pmr nopft4iv "IV equal fluantifird Q#' 14) 15 of Ilk' PA,Iutk d i i " m un " exom nat on and of 1~ rd .4wgioj. To -ach ^41(111.5 C"1.3 of nw. Agitate .~ alclolmlic sulwtim a(dirmthy%lynxi thr FKA116111 and thell &41 (112 cm.2 od' 1% iJcw&Aic mabdion of Immakfine or tolidine. Athm to �(WW for a mints" am thm mmpam. ~ TIw colmor obtain"i with "Wine in dreprr than IUJ with benjklimr.: j jw wtwjjyikv jA I to 6 alkut I4.0(ks.(K* -Mr. A. C. -N. 69TALLWGCAL 4m 143040 mirmw cot 1ALM609 ircolt a.* tg 00,0 0 v Owa If ~,W~5M a I ll~ T! a 41 0 we e 0. 0 0 0 0 0 *.* 0,0 0 :1 db a db 0 111 0 0 0 1 0 0.0 0 Ot* 0 wi* 0 A I$ H If if if ""'I "I A v a it 00 009 off 000 008 us".: *so Gm owl goo 00 a - =00 42 go 0 gos woo 43 see 2i go SLA MdTALLU*GKAL LIMMUlt CL4SIWCCATICO lam 7 I low ball IN &L tdicaa 41F a-, I-C I A 91 m L t a 10 9 A -a ~l 0 1 ~DIU 11 A~V go it In 0 w a a w a 't It WA 00 0000 0 *1 6 0 0 0 0 0;* 0 Or 0 0 6,0 0 1e0 '00 o 0 0 'a a 0 - - - -j j j ; j i ; 60666 6 j 0 * 0 e 00 ;!1 2 1 4 s 4 1 1 9 a ifu IN u is 16 ty 0 A r !!1 103-10 me 411-v it x a v7 a a 1-a it P-0- a I PNOMW AND POC"*1141 MDIN 00 c go got HMO T, Amwum~pw. -0 003 kc~ aim 6Raw eow Sm. 5 00% a I I L 4, !11 91cm. ox It X-1 541,24W.A. Q.V Oat MINI -at v %s7 M a u : AV 00 Is W4 04 is a aa a wft a 4 1 a 0 ofee 0090 0000 0 0 * 0 it v x ]"LA I AD It It a 9 is If V 20 20 m If v u id b IS It 31 ifa #1 4) If I It L I AA #A CA IV U I t I ) 4 111 01 A. -tL--J-.L 1. A -A F v A I it 00 00 -O"O."'S go 09 .00 go uf Z.aptul.(.Ar"i 100,21-71 fi"I~ fu3".J.- reactims tied is SO,-- A. 2 Ag Ag:1-J),, ;P~pfe_ %rut U1111- oxidation (d the SOS- - Off- w"Ik i~ rwri'A out 96 00 Ax,,%(), frmn I~issjt 1,4 ca. the titruticul i. varrj~'j ~'Iit its 00 the ptr~lwc (it Sk.. Thc it. tj'Imi wreft it 'A ifir fif Ag all. the C.11-mr4d v14T(Itxlc is ItIca.liml. W. I'. ill. see see 7 TLARE CL* IF)WIC" A IC L LI EN ".own Itu I 101 00 *0 so a 9 0 0 0 00 a 0 4 w 0 0 0 04 0. 0 0 0 p - 0 066 06 see* 90000010 0 0 C4 G ~; : 21 ~ ~9*0 __ ;0 CC 0000 0001WO*~1,60 Ole *00:,% 090040,6 0000 0 00 00 090006066 0 in 17 IF a III 111 0 _jn 6 fv;~ mo,% L a aas I w o IF a If 0 at a a a WIS &V IS am 41. ilobtat Geou-S 04 Or loftwo, NL 00 n 00 low" PO 00 C, 00 OW -Wo p 00 -v Oft lkwas" -Gqk--("O 'got :0 I lul "Alwx '01M) L 0 is 41,0L 00 40- ir 00 941090 oil 0.%, 111 r V ft 11 well I - - - - - - - - - - 0 Ir w San Is 0 b IF a a a 41 a a A :6 C 0 a's a AL L ~* 0 0 P9 IN 1 7 W -W2 r f b I & ..go F. rAours VID tfftg. 300 No ST" CODM I - - - ..ifa.Ls Met$ VII-asT 0 IMM , 71 s c Sign P 8 O eo~ ~WA so- 4$" v -- s so. swomm, : d ee 0o 0o 00 go o* 00 0e MAT-P-1-Tf T go 00 0 -0 *~; : 0 0 0 0 0 0 a 0 . I i id'i 4 if 11 11 w ti It --mrsus M-0 Olocof; bit Iwo 36m b~v 14046 41 Quad ~tt. w moo- -0 06 06 400 or*d A a 1 17a so ! C1 JIM. t (3), and C. Vh. MacatOvici (Hod. c0 are I im'I -In 6 Part of the wintion Ni Out . - )~~ in all after prWipiwian M [COV)~JOCNh MW ' low s EW: t ,,art of the "Ution, the 'XI oont-I is bv Pirsilick & ltlet so the C, ,Rint mn be ralmilated-1). S.: A S a. I L A WTALLURGIC&L LITIOIAT. C L 1104% 03) $)1 cot q- 41, ~i_; u 1111910,11; it4 40 ill o , - -I Af 0 A a .7 am 0 0 0 i 2e ; 9-lLA 0-0 0 0 0 0 0 o 0 0 a 0,0 0 0,0. Too 0 0.6'0 0, W .0 0,04 016-0 die - - - - W - - - - - - - - - - - - - - --- w W w w W W f, 4 a A k- . . is u ts 16 , o 4 s ' " I I A 9 A A -A- . J- A 4 OOA t go i god a m. low. 1. Nov, -00 .00 goo OOJ OV Ice '020; fQ4 (Ni GOO and F. R. woo n see n ow 61"s I" ~"Amw t; samw .10 go. ow 68&A11 m wo got u 0 L 9 a Im 0 0 6 1~6 0 0: A 0 3 L ~ 0 0 l 10 0 a oo o O n : 0 0 0 O e 0 0 0 O~o . a 0 a qp a v III v u 9 w 9 " IT w w v v w IF - - wl ~~ 0 IT I I L a 0 0 A is, 1,10 Abo IT. colates oloctists A.0 P26"alles mots sit -oil , 00 oo -00 pt god 1 P. Vr 00 now Id + GO 1 00 so* -so 1 Wes MITAL fit,, Wong -4 I Islasa wit mv 41" - -_ u 11 &&wodl we -4 0 o * 0 0 00 0 0 to 0 0 0 40 0 00 :ie 04 0 0 WAS 0. : 0We 0 010000 00 so 000 .. I I I I to I I . I . . 1 '4 0 ~o 0 0 a 0 ojo 0 64 0 0 40' a * off of food oo:,::, Ooo - is 14 it It J, ! U: a 14 is h r .1 jV A 11 U AA Id y . 11 1. it. It L, is #4 iu 81 U .1 44 43"10 I 700 l : p r "is- '-t go A oo go : -00 00 of w stansous too with Patois-; 0 or ,V"m and ' C. DrAsulk-wis Bull, sign iodaft, 0, 5 ;& 4 , iv -20. !Nis. t-41, i I 00 Z of Sewl. In I -!,I N lict wete IttrAted ; Illmet N, with 0.01 M KIL.. Atmut D5 mig. WuS J~(C*Cnt 00 J; and the total vol. wu about 40 nil, at Ow clul of tile ilm, The values affircrol within 0-41 fl"; L of Ifir ; - - m ll m; f $ f I d 1 I 4 o , illio i(II I 'e 11, h Is 0141 actilry II ..k eq, 111 00 c The! Method wits itlioll hi 1110 pro,ft-11'.0 .'f "dwr VIVIllo-Olp. s W r If 1 d i allo f I lik t l is 04 . . ~ o w t" n n . e y y ZOO If zo 0 d Z;~ of 60 A SO-)L 4 OffALLV6KAL UTERAII,4t CLAWFICATIC6 ww S -7 Ile ell Z., 7;ir. U S AV *3 JLS'; i't ol. 0 4 Q It Is I ~,oo 146 00 0 0 to 0 ;0 0 o 0000 V 0 09 0 0 0 g 0 e ft 0 0 * 0 0 ' 0 0 "O' 0 0 0 06 0 ~0 O i '10 W V IF W q? W IF V U 0 0 41 O A 0 P 0 0 * 0 * 0 W W V A If A 1 K It t; M 11 - CX W tj i It #I I a I . 1 , Its 4. 00 4 of tke stannous Ion with alkali pOtn&Otamjnj is 0 0.- H.H. li~j. "dd. r'skWj iiiii %o. S -00 I 61111 titrations dtocribed ;iWe made with 2tyltfux- (),1)3 ~411 -00 snCI, in 1 1-2 N FICI and one Of Is in YO which w1V 0 S In 11 aad 6 M in KI. , A i ntwured.vig. of the SnCls 00 8: %oln. '0-10.01 mi.) was full i nto an C%cT*4 of Jt Natill h 00 and tittated In an 51m. of - e No with the Is --kthl- T amial i th ll i i e ca onittr n or" followed "ent y titratiow Under the atsove cmaditions. N2,Sttth 1.4 fornird y f react.,; with the N&IO (fostutd by the. action ot It ' h The Nx&O. and Nal. on N&OH) stud tbt products arc 00 jt~ , equivs. of So Wal Is are the same as it the reaction V4 qj pla in an acid asto. The max. error in 13 titratiOM4. C 000 elskit all the potentionsIetcr readings are given, To" I. 00 j: 624 ml. used in place of 4.6&4 m). cased. About 4) 4 . tnin. was required for a titration. w.T. it. 00 woo coo TO PO--* 0 CL-SSIFIC.M. ;,JaL ' Is or .'A S V It It nn t 0 00 0: 0 0 00 0 0-6 0 000 00 0 - 0 0 Ion 4 is 0 0 0 0 &'40 00 0 0 0600 '60 0 0 0 0:0 00 of 0 0 a az,* Nis m visplil oil mis Ir m to if If 4.1 it w 941-1 00 go .00 so Ild UiB 1101 00 two m OW .00 Kee *(CW d 0: A, 4!HP POP Op 0 &aim A in hi* dmw In sdm*m y 10"Wg Omar Twilms ode- mlhm~ tell wit A too zwo IB An, XoO NO 4116 :1, if W @a. bw imp too A A OCIALLUR(MAL tittlialtAt CLASUFKAT.00. T 9 1 V 11A W a 7 g u Vt A. 10 14 7 0 9 0 0 0 0 1: is 1, '? is to 0 0 0 0 4) a 0 zi . . . . . I . . -I,.. L L to to P q st jj X~; jl 2) 24 a 20 AZP 9 11 U to V to AC. $1 #1 00 1. AA U ~M W ix o.j 00 - of .-fop 'to taws Colu- Tht WtiCS Of PYnd-9 and of awinosia'os Pltl MiMas Contaislat bontiollse., C Sports awl C. Ch. -41 "(tjXj1)j. Slacniuvici, 11vi. .4i;tv. v ;. I'loWfe0j, 9~.. -A BY utilizatitm ovi 1eme, th aojfV:~t it Is P044ilde tf~ Iffri.- pyrillita, (PY) and atnutimia x4ld%lixoducts It."Is k"1111111A CO, Zoo and Cot b,"Zioline ( Rrd) , divid". Cwi,.- 'Illy 1111), !I,y (11), C,IC6.lAxd.- Got JCdH,d(XH.),jCl, M. jZnBtd(XII,),jCI, (M. fjFdCj,) to. PyTidju,. r,_ direct adoln. (of the dry (metal Sultot in a (1hplactment of the Rzd toy the pyritline. I lie j direct a Id of aluma"IM to a mclal H1110, rtmen'. a cvml-~ 00 pleir rvm;xl. wilb six viols. of slit Alldrd; howevk lose-i four mols. of N11i tesdily anti in the cast it( CK1,- B'd + (INIf, the prnoluct decclutpotieq, owing to uxida- 00 j tion. Addn. of Nil, in ale. or stirring of the anutu"tia Ado. product in ale displacv-4'the betuidine. The vow 00 com". prove 11;at Hzd polssmws two cfx3rdinal ion =00 R. F. Dere go ;Oo :zO A~ O:Jl a ASN.SLA .[TALtL.FrKAL LITERATURE CLASSIFKATION . ..... .... V -c'-43DI -4 -7.4"'i "llia v tv ty to vp et K gi w st Pr rt it or x mLD n t :iol 0 so 000 0 0 0 * 0 0 09 0 * 000000 0 So 90 0 00 100499 1 '!~ . , 0 Wo 0 - 0' 0 0 000 000009 go so 000000 0 0 G~o 0 tn 0 ~:, 0 : : Is We 0 0 0 0 0 0 0 0 0 11 U u Isis us? Mits -1 44 a 46 4;4 0 gall I I A I a 4 a V Al a A AA-MAL 14C~ 141, 00 A[ Recis"s A.t. to(Ifleflis ~.tjls 00 00 SAM. ~G.ArAcu smil A. Por Sm. lee 00 MI. 190. 9. 31YT-.317),-NLY Uma spk4am of 1.2%;sims of 00 awl pptn. with NOW kh" -,Su4'1OHA1 (11; ims ub"ined. re go cumplmand No Y- 00 Z whit* arvab in *bmare of acid. v4pburs. Aq. solls"s aft 4&bb in preerner of excem of N&,14, mes, zoo mg Omi Dibrius 18 [Ve ill 1Wt sea up. . ZOE miction of amwm L14 4)f:(Ij tile 004 w am& have been 63110 NI 00- lee 0 -4 0 12*06j; c" s *-.J~ ago lee 4 lee MIS& S L .11.1~~RCPCAL UIRMATLOOF CLASSAPICATPOW Kit I A a: 3 u 1113 'Is to tvewit ma, sa qt Ruit it u V, --s a -i F7i,7,,ff 1* ge 1g, 414 : too Ok~oolloeoooooooo*oeoo.ooo~ooio*:** ei*00*60.0 00' 40 1 0 hit lei*u 00 0 0040060115, 0 " gg A to a 00 as deftnubmim d miss Sravv mA IL,VA*ou (Rol. 8qv.,,4.a pjinl ANO ... L ifi p" 00 IWN,)I'OA oil Volbwd'sp amithod. TU meuM is mpid OW ace We, 0. J. W. 10# ::go fte, -ITALLURGICAL LITERATUOF CLAS111FICATION ci U T6 &V -0 Ls iT--j 0 IFI d .1 it 7 IVCVIV~061 RX NEW KU rf It- 4*ADa 41 1: s 0 00 0*000000000, t ~ 1000 00 1:40: Oo 00 00 0 0 0 o 0 o 0 o 0 o ogee 0 0 0 0 1;0 o 9 its 1 -1 I I 1 Ku l . 1 a iv a ~ - , , , -,4- 7 ISLAM* IgR oftepp. - 3.0-4ho 0 coo *9 POIXIS"s Me "Optaftel M"K gal 41A "d law, JIM 4b 13 A.91 22 go 77. - AS&-SLS .:4v ll*" filmoll" o i;; OWN ~vpftmv p"[ elisp do -am al to"" f =u As u b At ; 0 a :9 !3; W, a 9 0, w! 0 . : 000-0000000.000, 000:0,000*0.000~4 : 4ft*000 0000000: I t li l ~ wo 0:0,0 0 0.0.0 0~0* o 04 0 olto 0 *1 i* 0 .0 0 O'l, 0 a A db go 0 0 0 o ; 0 o go 0 004 00000,000006000OW6*066 *I* * 0 0 0 0.0 0 0 0 0 0 0, 1000 000 1 j: 1V I u . C V fl, 6 , 1, T LOW b v x if 4 41 4: 41 ! b _ $4 Is: W71, It. f~ Vf;~ din -0 Ve 1004 00, 00, 0a aw dmmpl~ so p Zw caj 00 00 Al pw 00 oil 0, 7.U"lc 59 -as 00 00 VMW_ 00 00 go -fir 00 00 e go 7~ i!~ 00 T~M 00-L v r i-f"'i, it tit i,I m 11 n m jj 4. 11 11 U a a $I v a nr a IS( M$I 1; 16 10 00 0 0 00 0 0 0 * 0 0 0 0 0 14 1 4 0 0 a Ole WOO6 Ole lose a,* 0 0-006000.004::r N, 0. 40 ~ is, . .0 40 0 W a 11 ii 9 It m b v a It a As 42 43 60 al a VC D of 4 0 pu a S w if CIA, AT u n I Lie; 41. Mot. 004 It r 009 (0 pulaq il-H -A -a 'own,, ^so 4 0%,10 0-- MO. so-- -so so. jp 00 -V pm P Awn 00 goo so so 00- s0.. ----- -- v 04 0 0 1 - -- , I ~!' !", !` . - 'a too 0 a U 41- -, M, ilm , , , f ~~ND a A . a . - I . ~ I . I I . I . . I ~ . .. 1 11 1 -11 v qw. mt '11i'lp `tlp V m " - , " - , - , - - - - - - - - a IW 0 0 0 0 0 0 0 if 0 0 0 0 0 a 6 0 a ~41 0 0 0 0 w a I v it rl 11 14 is )G V it 12 a 34 4 34 g- 031 o- c v j #3 f. fkR e~yt*j 40 '00 so a. DOTAL -Amd. 00 8 00 Vo. 00 00 the drmtw" 1). It. Vo too A S. I L A 00 tALLtl"CKAL tiffs.swt CIASW WATION 8111113M.C. bill it bw cp it lp 0 a a 21 a pi 'r or $A I 1 0 FW 0 V~l 114, 0: 5 Al4 3 1 a is I a a; a 0 0 0,41 0 0 wo 0 0 1.0 lo 0-0.014 T 0: 0 0 0 0 0 *eel'*' 111 16 1? it; of I a it 13 14 )1 it Lr n p $I a, v f Is - 1~ 1 . ... a r ~ Q . 4 r a 4 4 6 60. 06cct list a Pat-re a lit I..Ot. ill AOC i its beg led* I ad C. IIIII&.11J.- Asoot: Aid. .1 111061i~ ' 90. 22. mm-am dill soft or 00 low 00a mo too a* Avw vm~ its =00 moo i4 bqp VINANY at 4"Of f0. PMMM 10 ILILT. me --I L -."-IAL UMOICAL see u It AV is A As a 09 a a It a z 000000 see 0 0 0 go 00 0 000000000 0 066 41 0; 0 0 tolo 0 0 ALOW00*00 000 0 0 0 00 . - , ~ . - . - . 1, 0 ., " ft III M 111 44 CI 4. & 6 0o A M AND IND-t -41 oo I A 91A 4 00 Al 0 All- 40 90,3 Ode as so 9 Dow 11"Ill V0.4mv V I&A IAI S 0 ftd :0 0 p a A, --L,[; a 111 0 Ic IT, a I VA 0.0 0 Wo. a 0 6is 0, 0 0 Wa *00 AD G!* 0 0 11P1 ; 5 dW4PW 1 - .1 ~. - -- - - - - - - - A lk L JL -4-.A- L-L a N P-4 x 1 A AA _VA ' '4 tav. , ~ - - . , i 1 . 1 's-Ims 4w 0.0pow tit -lee 00 116410? sum a ai~- 7 M A l1w lummima mmq&a Sdb doubts dKenjo, * (16"L A r0 f 400 r - % %h 46 c (~Smi A" 14 w . go w461(3Df%6,f kw=)461 ~ F.J. fl-.~ j lee 00 S MS L A211T.LLURSSEAL U11241WIN CLASUPKAXICU SO.In', 'loo Sn') 4-1 willpic"I 611111dw - u 9 AV ND Is mot ng*1W of Ic a K me -1 i7) 4 9041immM w cp to it i Ito T? ~Ns 1-0 004 000 PROM 00.0 00 : 0 111s" 00 SJH MAC. Do 2L I- C. HC1 is trwaW W" I by HW + 31' - of and sher 3 M6. tim oev imuT with 0-1 nn" Any Anul F N Dom ;j: nf man AID ]$At list 30104041 4azalud ilk .... ...... r-0 9 "Cocarq$ .01. Ott iWOM minim im of C p abu (OWL Amd. - I& .00 wt. of KI -1pnA miiiiiiatbel -4- + HiM I, + w 00 ro waftd in an sta. QUI ~1 .. &n iMmim' of the toW See BOW LAT1441kM CL"WKAVMM soft Wool -4 S183003 .10 GOV Got Alin ims 411111 dw!gw.! All u 9 AV 00 It T I I 1 0 a a a a 01 'a it 4, 0 It 0 0 0 00000 0 0 40 0 o IS 0 a 0, 0 o 0 0 -0,00 0 0~6' L 0 o oI ! 0 0 Off - - Wo Olga 0 0 0 0 4 O"Al 0 4 e 9 6 0 0.070/'' MIME Nis 0 0 0 0 4 a 0 0 0 a 1 a v Ic f I ! at is U is 4 ir to 14 1 11 3 It A r N il A [I V 11 U 15 k ;4 r.C 41 U j A J A _u U; t.-U A-1- -AA:-m -%,.M (t I -4 Comtributim to fit Comeww"i of hetairopolyadda 1 00 A new dam o( anaWnes, The pbompbo6ed-tumoute r, c and V. Xkotw-wu. HiM. sect. 1.00 Complex 00 16- -00 tion of itirthcul (it prepa. and &FIXIFIlif Of ICO Vn,(-NOJh1f- -00 SILO let( N IfshSCS1 MI POV100.1. I A 1130 .161110, so (CrenjJ3104 A. A. Vermin A 00 -49 14 HIT it It it it at aLo 1) 1 :1.6 0 0 0 9 0 0 0 * 00 0 0 0 0 0 ip '9-0)p 0 0,0 001 O-Le 0 0_000000000,00000 0 0:~OA 4 0 0 0,0 w 0 !0, 0, 0 0 ~ 0; 0 4 I's 0 0 to 0 0 a 0 .0.0 0 4 0 0 0 d. 0 0 0 I I I V it 11 ?1 it 0 If It fie it 0 h ~17 a to a is V Is It 7 as of 1) a 34 it u I' is it a 41 a 41 Id u 0 1, 6 _6 4 1. a it r 9 4 1 uI ?'A. ALA a m Op it i' I . 0 0 . # at I., - 1- -.4.1 .0 Go 0 00 00 -00 00 b'' 0* rot o0 A Two Dqw COw4&md*--WAvar diallium PbOmWitato *",1 .00 I,. S Suva( tb&Wum Mwoo 00 a _49 4 fv 3ri. dmid. rommialme' p 4 Ndn. of i 00 12"M in 40 ce, 11M and Wil Jr. its -64 t- Ilp was istlilcil with aitilAt~ml H 4.411. itf kG1 jtj:.'1?cc.Hj0. 1,hr ppt, wastmio Jill alc~ and vilirr ha,l 00 1 tic vtonpri. Ax,111", Sisnilarlytuaw-In.oftlAg. Naill-, oo ii- and t',M g. TIOAe in 211 cc. 11,4) A,O, 7 11,0 in 40 cr, 11,0 a, m Iw tant t" h't-.1 talw'd IVAK 00 a: It i A 'Inglitly 111"1c 1111611 1,111lut lite I-kiliNt 4-mlimm, tit, ppitt, i% qu4nt. L C. L" 00 00 COO C:46 see Of 4se *0 4%-%kk OtTALLtiPrKAL LITFIATLAE CLAIIWICATICo 00 C., Q" XOO Rt, Jr. 0 W7, 0 it a t a K ft it it a, W n I to I Ai 0 3 oo' 77 0 0 0 0 000 0 0 00 o 0 0 0 00 a 0 ei 0 0,0 0 0 0 4j o' 6 00 0 0 it 0 0 0 0 & 0 0 0 0 0 0 6 * 0 0 00 0 0 0 0 o'0 a 0 * o It * 0 0. 0 0 if 1) 11 u it Id 1 4 A 111 Of 49 .1 41 AJ AS: A AL T*, a 1- 4 lk i . 1 0 0 it I I abil ttr 64A It on. 1.111tot - It., 14"01 :1, 00 a -0-0 00 00 CIA" of Ammin" with 541jidroxyluis:klise and 5.7-di- bromik4-hydrozyquisit"C' G. %Ipacu and C. Gh. Ma- 00 HikuslIvi. I-it) S -00 -so 00 1 till were pirtkif, ill Allich I And 11 were unions: 00 It, -00 411,0, to. -00 00 (Coen.j(OCf"$'V)..flHkiO. 400 o )C.11'N ji,211m, 4110, 00 it, jCojnjt(OCs11.Hr1N)1' Ic" see 0001 ~cr crul(CICABrOK)II. jcr(cO(iq1J0j16HOc^HflNj1. coo 00 1criallupyrinc 141 (OCJ1,HrjN)., JCr(XH.)sj(OC.If.- =00 00 V11 firN i,. Similar ctxtnpds. of Cd, Zu unit Cli could not be juvIA. numunuch as I And 11 Ikeestne part. of the catiun. I Ike gmt-ral inelhoil for preps. the Above complis. ccknsi~tIk "I filing a di). *411-A t1m K ~~klt of I or H to a dil. 1"u.'A =90 00 A, Ill., 'Offf,pniding chloridie Air nitrate. C. IA) Ck"o 00 I rots X06 Do ZOO W _ AS-ILA s(TAWAIGKIL LITEP-1441 Ct.SSiMiTmk most i0 S t ire 0 Ik~ to n It 44 1111 it R 0 it A* I so 0 0 0000000000 0104 Ois 0:0 0 0 0 0 0 0 loo i 60 00-0 0 0 00 0 0 0. 0 0 0 0 *so o- is 0 0 0:0 i O's 0 O's 0 9; W!6 a **else 0,1 III F A flimlirmt 1 1 00 A 00 Arc WWWAka W a -00 go' ii~69AGO&WM OWL Amid'. I MI. 460jainiig: an ez~ of TWAo or of 0 IF ~WMWL it WaWw"d obi woulms WMAM slez j 4#0 00 T~~U;M~am abbiod wo a- is" -lbmw ad-i Au do is VON"= 0* oj~ ow;, *rs" oov I tT.LLUIIC-IClL LITEII.Tbff CLISUP)CITICX ... ... . ..... 00 too &V Ll 0 (*It Ira 19st rrff; 11t; .4 W~o 000*0*700 09 900 0000 00000*00, 40 a 0.0 0 0 0 0 0 0 0 0,0 0 0.0 0 a O'l: A 0 0 6 0 0 a 0 0 0 6 0 0 a 6 0 9 0 & 0 0 0 0, 0 0 0 0 0 0 6 Id J7 A, it 1) m w 0 T U L. L - M0 t I A ... . ..... . . 00 0.0cit"I .40 "WercefIfs 'W4. 00 -00 C"Wmion 0 bVivr"My"We. M. "llibe pht"0~40-1, i and V. Nicolvica.u. Bull. jw). set. futfal. taxotall.W4 3.3-7-400040)(in Prowh)t d. Ci it. 34, 00 tionls for the prefsp. ul MAIL -00 nee Clio Ill) Ally 11'(W101), 1.211.0 121C K.Nifi il 0 M? i Of =00 00 v A. A. Vcru,,n 00 gas coo see. go* he !~TALL!~M~~& LIT94A too M. Qvc a" 92- &%1 S Moog A, r Is 0 U OF IV It It OF 49 K K tf It it K "a n Is 00 0 00 0 6 0 0 0* 0'0 &'0 * 0 00 0 0 a :11 01 ~o a 0 4 0 a 0 0 * * a 0 0 a 0 a a F10 6 6 0 0 0 0 0 0 0 0 0 0 4 0 0 41 0 1lei ?o it D 16 Z) AbJ1 12 13 MII it A I-L 00 4 -9-tAkc -?ho th-(*Dt RI 040MItt APO PRCPlat4l -Drx -,LgAL-- -f CIA-. s mezz 0" . W4 11. ~'Tolchemcm~ Ull. fill= AMMIATU CW 00" ame a. 400t. *al. acvA. mpudso 25, b1&20(14,43)0 'Aiiii) l cielio zemii.~ 190, to so R i: 745; ef. C.A. 3b4521.-The &fffe%L0f' (ba im 9- 114%tt WN3 an (0a ta %) (t) bApaleldine) was latudled. I was ObtsUed so a blawk,ppt.' ty, RWV4 di sols. 1*0 7of bL The powd. coapd. was us" ropMedly with sibe. ale. aedfetherl it was dried at 1000 ad them troatal with lI miss of llqmlt'fiw jai W10 at sot 00 j ' 160 In a f4ensimeter. "we first lestbmiki at -769 ormle U" 4e a 10- **a, ammudate %d Sh a vwpw tems"M 4t_,15M ON& a& the f - sea of vudlar appealwasie. no -440 isotherm cormpods toii; ioijitien of a 6 -smoulate. At 10 thle doemp. "te & "Moll" is #*~610 to wd at this saw. decam. lilto 0 2-ammoslaU SUM0.40 T80., fttiiiim 76 04 mos lose a 1-~alats *3det& "w m& w., Ot Wq =146 8"ad i"Vikoei: oltak imen"Ing G MS. vol. of fibs Soma# We N2 Wia p6malts prowifta I no"" 7:~ a ~ eO cawaxes. fte 180the"m of uwlcm~u 012)-m system are awl4ir to tkjv~ ' ZzZ vote :d is of the ftj j*f%W We of the (Za ba 01 )-F3 W*U% but Sbe form is M"! l M th e oner & Sim; p"nm=sd the awdler the vD. or, the lieAll.ty at M3 wels' 'a Sks C014A 14. 1 L AAITALLIJOGICAL LITIOATUMI CLAIWIC470", ](14W ~com 11 will 411411 dd op,' III u 1, -0 '1 ; 1 00 000.0 '0:0 0 0 S640 0 Vv alt Jim 410 hock 91 go A the ink 0-01 A6 it P60A ilk;* I -CC. "k4lic fila a" ow m K so how 4191 a dlkvm. AfIrt I it jg4V, j A dif NMI 10 W. 40 OW W .-wM 11 m Wa6wi 1-2 JC1 arsti 3 4it. ;2!. HAQ~ m idded. u4 the aLmm K1% is I ' Ila. tatrov p4aft mehiesib wkb Cu it VaAn~ td. . c.A. ji,i Orr)- Cbeck sGrArm-art rvpmgd In toks 11bc "Ar4 cd the Tb(106)4 Im Will M Jao~ WUN Md. mit is cpaud a& 1h X 10-6. IL ~i ASINALS ftkI4tUVGK4L tWINNATURt CL*MOICATWX t So& T ZA I fu 0 ~HC 0 .1 0 21 1 9 It a. it ft 6C of 91 It K W: 4 IC119.4 a 'I Va 14 '64:6,44 0 0 0 *a- ttl see- rA The study uf the storwturv of pot"w"m "dillonlate. A nrw ela" of sointined The ho"hylifosmitinlomy. millingil, alid C. M'A'uh'wtk~~ ~t~miw. liinhart~t, Rimm-M.0-1cid. Not, Aplht'r mo*djrr. himj~ A' 1. -11 N194S).-Six tiew bevillydrip,ty. arillnumptinnines "r pTcr4l. ill prove thr rhviii, sinicturr of K11,14010.1 by IVI)LIcilig The K * With Co. Cr, Aliff CII of kil"wil "'.1stitilliow A 114). II,;'Co.(.I.."II,(-J, (Ind Mf 410111V QJ. In JI'D al rwito fritilf.: ill bill 110 lber 'Tfjlflp~ Willi ppill, if ill arid. %W% Ir V %I V MAW , 1111!I WISM Ills roplIM1263% mHawlall R." iij4vislowileam GX 0 -YL.j-j I AA A A ..L-& L 1 -.11. -4 0 00 09 A 96 #0 D. 01 if. G (Bukami, Unit, ) 00 a is I P. cf. CA 1 28. 00 0 !:1 ju of dtr' litr if Noveff Cc t a W, 00 umat'.41 Th If L4 actory but COW re"1116~could: be'ob fifterins. tained by pptg. In an aliquot lain of the and deta. the Clem loi- filtrate, adifin 0 'j() and titrating, the 11j)",t, K I and If,, d It th Xii-~,Oi- -rbe .4 0 PARIS were liti'l. pw 00 satisfactory. U1. p4"1101-trkway and the results were goal, jud. in, 2Z"I(IM).46"nshistims Cd J; dctd- by adding a jnown to, a, Kjo, L,' Him Th. can awe d d be .!Mx(,nt, To obtah, Cc); Ian ttg threxcess 0 a it E-6 11 nplete ppt.. Of the L "Y that tbc Solo. Should conjah, a,:. !1ast"i 0 z Of 2 reudts resiorted, one 6 d 111C an of her is about too hiSh. W.-T. flail as !ti Zoo 41 ago -4 x(TALLUP.GKAL LIMATUOF CLASSWICATICK 14"49 .7 t-j "I V of .3 a 3 10 9 NMI U It AV 03 Is ;p to pipip cric wit JIM lit(tt UN 0 isee 0 0 0 9 'Wso To * 0 0 0 0 0 0 Is o 0 0 0 0 0 0 4 i 931 A A 1 1.* It U It 4 13 11 11 to M X) I It Z, r I I L it n b, 25 36 :7 a .4 A; it u M J4 25 it 11 M )f & it At it 14 ag:o , t R~ I -A A 00 , ~ . - - - AND v;: r~ imp t NJ P*OCC--,#t A.!; Off"I"Iff -1511. -00 00 .45 -00 0 9 Ilitrastimmawark bu goo, Deterininsfift of I =*O 00 Simest o g (19VO; ef, C.A. 42. So Mi~%!Jrn sKa hic acid is trc-Atrd o its aciil,~In. with KIO. asul K1, it 6 oxidized to dchydro- 000, a-urbie acid by the I formed. 0"e nw1c of time w%-twhic. 09- acid reacts with one of 1. The cxct---.i I can be titriatc-1 zoo . x1tentiollictricAy withN;AtSA Join. W. T. 1611 00 goo zoo fTALl.U$rKA1. LITIEPAUoPt CLASSWICATION 0.0 Ut cft. AT -0 is a T An I I I nd, 0,; A, I ~1, j ty IT it A( K a ,A, 'S., a,, It x M* n 1 114 I i Fist im 2 A3 13 3 0 T 6 00010 0 9 00010 l 0 0 Os 0 0 so* 0 IS 90,41 0 000,000 0 0 0 0 * 0 0 IS ISO 0 090 00 00.0-0 0 -0 *:;1* a -0 0- 0, o "to 1 is: 00 a 0 1 :0 *,*I A/1 V. Os li%oj F m I 11 1 11.5 It. KNA). in P) tell. 11,0 J- I (C.Q.11,sbh[Co~ , IW %ta-itilt,41 fm MY111ill.. .41hi IN, I'l-In, I wn.h.A .4 lilt ...4.1 11 ~t 1. mill 411 ii'l .11 ;1 I.Wqln~ I m 'I' t, It a. 10i N IN YVI, is. 1: Colegirkir antisnany taitrat" Ill Q S send Dr- L 'i `L"Im" 11, i l n 11410 .11.1 (Ov, C. a 6'. 4k 1'.1 ills 'hi ml rtra 11 I nrlmrt,t. Rnn.1n. . Y " Papsul'Ifir Ramooli'le, flul. Moinj A. 1, 14:1 51i liti9j; If. Poid/. me a IdjiL. IV. Isimccentributioas to the study ,ewt see Iliad. ow-apost 27. 1:1.14C liM I 0t the structure of taftar elliatic! .1"'Abli'Awd Rep P.-Ph~' 1-111ftOl- "Os I-Irl"I it, Wdre- N$ Intor Or %lion'Mir /'I" R O'llse, f,~ (Alms. A. ell W.41.1 I Ile, ".. 7, NO,. lito-A , cor;jIlgr rjjhvT %lable. 421) (C.0, lisc lognink x1ml I') 11.1111,1114ml 11.4il dl".v Is, inailar fie fin larrin vIlletio. it, U111"ll . 11,4 Inol. 110. NjC,,(XI0,j( He(%) ;111,4 1. ~infllaf Re, ily. 141 tc,cl.- A L., 11"I sees fir ~h Ill; I -c-1-141, ..nd P, 'Ilegie. 4 if 411,1). dlva,enp. in mis,. 11,0, A, r%elfrin-v that the ll~o I i, sells Nmnd;t"~ 1kat 11 Is 1we. . wMiumni Jf, I C'I 1. 1 I'Sh! ~ 11?;, 1 '711,41 %:4.: I-Fel.1 : it .~17114 e lin-Irl ta6lom It li-to events ill qnq~rlltv .4, 1110- wle'.11 Iffli4d %villsAWL'I. it _z. ~ilh 1crol NIL sr(:Ii! (rntii, 1:0: 110,0411,ShNIC(of Nils QCL-1114Y! i. '11,1 sigh M. N64 i0mnmL : Few- in'Ithal lot the 111~ ighikwia of all tht, tlisilliird Anll,ff,-r A 44W class of AMOW". TbW numme thlocyammes, Q,t4qx~u Aski F- -;4)wu (Uttivt 11twhar"t, Rumania). Aojzd, .4i ". s"p-ropuldrr kaw4m, 30q. Alai.. lkx. A. 2. Mitmile twis Ckfim.. Afem. 12. 30 pp.(1969) (Flcllch ojnnLmy).-Uy enwintl aq. mahts, 0 their Wts with phtluktalise (111stli) anil then with NH6WN. Fre: cu. 01, Zn. and Ni kirtu MlPb1:,#~4SV%h Ph larm PbPbd:- (.ScN6, Un fotm-. Muphs Rj0Il)9CN.MsftUASCN),.-. and co 'Thc Mn and Xi saks have 3 of 11A, dat eibns at ittit: hydcou4- The Fe compicz is sol. in sciatic arg. sAtent's id,mity Imtoii, kntO; all 11w uthers we either In". d,yomjk~ its vic ~Ilvvms. MI diNvulp, In atiwtial vieW, uml lmw~. Aji mmijpk- of the ast-ahml of P#vPn. It: tivul 0.7 g. ZnSA)..7114.) itt 10 itti. 11,0 witho.7 g. phlbAUsime in 3 itil. 10) an,l 0 1 s. NII.SC,%', In 10 1111. jfj(), MA&hLt be abitt, I)Pt. with A on" itsilt. 1110. MW dry pla e he vww at Tom tmp. ()mhavil Mftvirkt~~ j Clt L& A. Fit Cum PAPPS"ro, Room". J 00 v 2. Now. 22. 20 pp.( 940)( 94ructum of the e h OH)sIll 11101 HC1) P117'"! icu.-2ii.o 1. J()jj ,T,Ad.(IICI 0 -WOll "0 (.V"d,- msm Oil, 0 IM u U'Al,k) 41,01), weiv pgpd, by tirating 4-0K ummat,r with the chimideb and "WAtts Of lwfilllne ~A" Ai.jine (1-V) and by tzpmdnd m 84- 90im- the K am 10 tht action of morne metsianumboa (VI-TM). Tbry dimmolve in dil. IIC1 with deconsPe. ejxvlA M MA V. 16"ved only to 1119 p"Onmt of tartmic mm. tins the ben&by*"Y- hydrolysee In 111#0 -6t- I II :1*11mmic, achl. which 6=7 LVOI-4*01 W60 416d. ~ Wb-" armemd to the dehydratirg action of Cach - Hs" all con*ds. um 1.5-3 mols. H.O. G. Audqw ;"iv, ROMAtn'. MJ~ 'Thiffilo, pit, CU." Sm %trill 24, lit pll.(l%iIXFltudI -ul(at,s of Itcuchtine and tolidine and ccuopl~% met.d.11W minc-4 are added to K stannsite to v"pi ,,new Sn(Oll" broL, 31 (WS11,6111k). Tile? arc all ctjmt. COMIXIS.. MA. ill icalli till. Itcl. U1141AISIC its hot 11,0. 111suns)IM of 111clul: O."A 0. K,~41(01114 and t.2m licitridi"CAICI am, Submit 114:11 oil a to,prw " Iii1r. :6'5 4-t-, I #to is Added %trilwi.... filterni afte" I0 Illisk willinut na-Idnic. dri,,I gin ligynmi% little, at rtillft tellip.. Allafrild mit er. V-1 111.4, (.Sn by the Ijklientlid .14-1114i.1 liCuAtlint-N kY KjadAhl). (5) to 19, K StAlln4tr th,s,oltit'i in 6 cc. water + 4 cc. colml. Nif.011 1.5g. Cu(,Nii,),.*) 'i~ ad'itil, vvsixv~l. mull vwAvif tilt ilmr. , Aftrv W min. the bill., rtystalt stv filtered. titut wwArtf twim:witlt Ftoll %.,61 -illi X16.16q.1 mvrwlitl .144011 its ad-i-aror ill N118'stin [,-r lhcli 61,11.11)FICII. TJIV (InI311114 14W K 31AIIIIAW i (011)6), lilla L 'llown 1-1 Iw KsIsn fintLil by flehavi und I'ani- Vtno C-erbard Aullects,";I ftzl DOWSOM of cart" from Csibuism And Cot and 'Runtania), starips Crilitem Aedd. Rep. Polmlose Romiiilm, Ya:.. Yij.,j, Milt. 2. 487-MI00:(Preach sussimary)."Trtal thc';jij~ --ohi. contg Ca wW Cd with a %light mrss of R.S0. and X11.80C.N. 'Tbe Am grftuish plit. of CfsSC%, turn, ~hkr. Filter thraticb a filtercriacible A.. H10111, mW fiaWly withi shm, HttO. ilry AwIll min, in nUmd, :101weilb. RWI the dltrole until OCA iq rentavell Atilt th't -01n. is only Illotly Amic. Cant the 1)(HIP Mi. (JI'miln, contg. only Cd and tseat with 0.5-1 g. SH.SCS and 11-1 W YrWi & dropwise until a ppt~ formit. fleat until the pin. 'i.a= and adc! one timme nil. of pyiWine. Stir, miil. k ;s I filter tbnmigb a filter enicitile At atilt WTLA the Ppt.with a Wn. Ca"t4.3 g. N1164C.*4 + 6 MI. Pyrkline In 1(0) fill. 1110. then 4-h thimes with I MI, of 2'%)1. (entax, '25 1111.451;', PtOll.73sul twice with I'ml. of a 10% ~mlst. of pWaline In All. Mill, ithe plit., CclPyr MN)t is slightlY -0. in xhq~ Moll? ilml timilly with a -4n. rosilm. 2 slrup-s of 1wrioline 1;1 10 Fill. alk. rthm Dly Illul welith. 6erhard An"viger Z: Rapid m*dWd fm god daigamilaing CoWl and _glt and t.l'jliv .4cod. Rep. Pepulare Momolor, 111.1, Seri: Mat., Fig.. CkimN'2'.T13 marylI. -*tmt the all. -%Ali. "mag. Cumd Cil witha %1~~hl eu-ims o( 111.40t and SIUSCS" adding the Wirt 1froll"I.-C under 4-mulnuall, slilring., Fill" off he while lips I sit Cto.'K:N, wtA with UP. F101f,and finally with all%. FiAl, few I0 mirs. in a vacutsm, ti-kcalor milit wrists. 1 6nil filmotir ontil all S(h 1% removeil, owfl, and ltrat Isith 11.5 1 a. NII.SCN and these with ron"Ifth livriditir tit iirnliil- ire it an't leave I Int. in exce". The 171111WASION ~!; (hr I-pt. is fincly tv"i. Filter Aft" IS inin.~ tiA,h with o "it rmta. :I g. NH.WS + 5 nil. pyridiote in [ION) iisl.~ thvil Kith it *Aft. Coma. 13 tsil. 0,57C P.W11 + PCP.5 nil. 1114 1! -f 1.5 lilt. pyridiur + 10.1 g~ N11.1'kN, theft with 1 2 lilt. .41e, q I-MIll I'milt. 1f)% plifidline lulul filially." A. lim" i. ills k-16.1; z 2 llssit~ of joytidini: in 01 n1l. Div Ow, l'i'l. fill 1.1 111111. In it VAC1111211 414-si'x~lot at 1,N,Ill and 4i A new, rapid and Opmadma at QPPW =i-b= 111216 *Ad tim. G. S d r~viina. Pirtea (irniv. litteliamt, kurniulijL)-R5v,R, Paptlurf Rttmdmr,- ,tittimary).-To the miln. amig. Cu and Sh sonsadd 0.7~*, P. virtaric acid firw each 0.1-40.3 g. W- Dil. to 7111-19) nil., asiol nil. pytiolineand 0.5 g. m)lid MI.SC.N gr~jdmillv whilemirring. metfiately. When the ppt. hat, filtef thrmigh a filter crucible As. Wails the plit. with a ~oln. of 11.75 g. J + 0.75 C. tartaric acid + 2,5 nil. pyridigie ~- :t`tll nd. HrO anti then 7-8 tinics with 2 -3 till. -f J Will- M11K. 1). 13 g. Nff.SC.*4 + 2 mJ. pyridine + 48 ml. 11,0 in '-0) till. 'Al%E1011. Finally wash with abs. HtOff and Etiormax, A %moll atilt. of ftymille and dry filr'-N) min. in vacito at "~m temp. If Di, Sb, and Sn are livesent In the Cu -tlN#y,w Mineral, treat with bot,coned. IICI, introduce a few nil, IIA dropwisc, heat until all metals are ditisolved anti the e~- cessiWirenwited. Add 0.75 X. tartaric acid, dilute to 75.r fill., anti nil() r? mi. pyridine anti f).5g. x)I,SCx withstirritiR. W.-l-h a* dt~cnljcd above. Gerhard Aullegrr i~~ , O~w , . I I ; 1 , i :,!I ~- -: f 7 :; , '! ~ I : , I : :., L : *, L %I A, ? : . . : . ; " ; ;i I . ~ i. 1; ; , I t- , 77 a H f 7 ~T 177- i!, I. .- - A 6jld and convenient procedure F 4 4 C6 r add lq#A, ari!d-m px~clse .0 S- , -1-C f of (mila w H I se Ovo -enients!.,~ ~.C 1u I n IL it. M PAR. mm Arad "Ware P 71, "T t,, I 4. a. a (.qj ti A n h N! ~Jid in the co*d with NHjCNS and fl-so.;; - Alux ofri tlie~ washr with mater, ale., and abs. ~thEx,~ -)w ~6j all CuCINS. Evap. em IC~ L -mil N weigh as C CES.. If SOOrt ';7 tie ~t filtrate, neutralize with: -r* -ocit o P~ ittitte; and 4";MM crystals (;f Nipy,(~3CNI). Filter -thrpugfi`~ ~rucjhloi Fit -Cft 'r[; 4: t he, pp t,~' -im-111C idW jyiflia I; 6f:jaieric~~j~;A-)~,:t and,6 g; pyridin-c; -was i isitli I( I )o all ;Wiifer It 'ale., 1.5 sfil.-pyrWiue; axid 0.1 g. NIWNSI-ilitiii ~th~11 rA. abs. el.her mutj ; 10 drops of pyriditie; dry nit rtfota tem -T. i F-I ~z D6 vI Ti! u T! t RVI MI, -7 law microm. and- raft roch US SRI e C:Md bll'utw -d-eterffininatt n, G Z A-wd.-74~. Popular, -, Rait-Ij -Chuys,4; 425-31(1', )9~)-~nimdh -J-13 based*d# the f H 0 , P-:; new cf tioti J f implex7j* Nl~, tbafl-thi:Bi; ;! -I!- -,,, : v. Wts -Ni: ~mo prp-viaugy~u,& 'BI fif, 6,1:361 0 :,-The salt -,st dlss6lved in a s o 0l N,- ..-,j6rra KBllj,;- troittneat: 6f -this %,with- (Cr,(O%eQ 4 a -A llow~ ppt;. IVCS a ye The ppti; is rbis#,d*Itk-*a#ili find isn then 060" ale-and. Wier; anti &k(1 i thlgii~ T Ov heov, P 0 A b accuimNiAnd rTe~41reSiV., v; f _t;"Tj6 acp AoIh -1-di 777r7777 MIM 1 j~- "At IF? R,~ ,j I J- M-- t ........ . .. "Mill! it ILI' n We" rm Or f 11 ltd Rep, pa~ C! AMU% am: (C. vv;tw ~py yridiiiie mo 7 1' tt, ~11' t l&; 1k h Win sal C 'a Cu fro"ITO~ tif*,rk~ idd AS;79M).!qTbd I I I A, en 1drox tilt Wi fgtrl~ te~ 4, Rh ki lh 0014. fmq FM 41 !i". i~J ol ji ol~ j j Coater from 4 method. for thi Soparation d: "1611b Coint R U denum and their determimition 411ta '13 d Re h (U i " 11c . n v- p.' m Oco Populare - Romint, Sludfil Cemrs1ri :Ckiw.111. 7713(1954 1 umary).-Two, mahods- art, desiiribiih IL (French - sur - 7 o1n. it 60", dropWlse with', treat the neutral or slightlj~ igid s it H.SOs and- NJ14SCN Flltir;the~ USCN;;. in excess of, through a filter- cruciblej~ wash. ~ vitl; ~ H&O. ~ HtOlffi~ ' ' ' ' weigh. vaima and dry for 10 min. in finally with abs. HtA WWI thc Bull the filtme 603-free, udd hot colird. IINO&' saim Is Colorless. and boll off thc~exccm idd., -The Tdo coW now be detd. volumaricalIv by mducklax with dectroMw Cd in the presence of Fas i snd subsequent KMnO4 thraiw; ravimetricall or t y, , g in I - 'c1 k:bW i I A 111 %o n. s nr e ) unt ( ! throurli kk i Was tile gret!n [CUPY46MA ih, 1 (0.15 Mkitill 0,11 IlAsrvi "all with 't Collig . taric addin 250 ml-1110, en:3 times with 2 M.-of i1 soln. eontg. EtOH (200,rni.)i 1120 (484ni.), 1 (0.13 : e 9 ith 5 MI I ll w h . onct! Ca t W c as and III (_ MI.);. flua y , Et O: : D~A o o d I h i i 0 o of Ill ne, ro . . cac c n T, tOff ant M g. 1 j its vacuo anti %veigh. Der. Mai in filtrate as~abovd~ J it A~ N M fN'.vi ~1~ -X N -A! _ 1 7 Z~ on Ise, s. , W% . _7 ..AllighUylhlic ~nrfz,.ij Ut -Addh a, K, Cq Ila, hr~ q. 7 -_A - t: 4. i fill i4iltz;;-, lu J; U ram 4 J IX- - - ea 4 As is .4 7 COMPIti'sak Of the'itio[d Cu SOW a1d 25730r~llil Of let thei6 tve-gre~sl Ip settle, _foil sl ith 20~' EEOH ~6**i a &V of and; finMl~V4106011 'tO; drylif: i~dciia": and !ig ai;y of abs; 1, ;V -teak: -do uOtimpfrep. and m 7'r' pz-- D". if tw F tip T XI i!J _j fill J i :j: obd I 4mn of -c;ob t 1,~#n G~, CU exid at -UT ~v RD, Acad-~ rep-~ P477FM ~v RD,-If no'. 7-73: W th! while-.At' sb1a,' p HSC W 1,11" isoln.1 k3U i .. 4 " - I ::. .1. i.- ;,':-, , -. .,. ;7 1144MJ1 'A ;Ildd" ex as; 'paudi wtcr- IM:0; 6t., O-rl 1-1m Cto Ill Ai: 19, It La to A and F -throul 44 dine! rA an(f. A jiter: A-4 6r Ail! fact lcrlkW~( L i (7 ml.VELXS~ml 1, tin 6i. Eitog lWill timep With C -nolrti: con. ca; contg,,Mfl: int.)j6:251 idWfEtqff-~ 6 8- times wit imall aw4it -T tioliontelut St Wt are sco, Atid dctd 4 si ~~il io r i "A t"N Ijii -W, i !j p ~Vt ~j -44i~ W q, ti, -J J_ 7,1N r e an a, gtr lot"? re fop sit M ltd 4$-MaOM~" .(French- Cloj,'a~ stnble st. cowpVr.i, -i) Ah~ acidjc' (HCI) i6 n~t 4d 10.3 41w`1N1LCi andl ail; C'f ah - t It (I) in dil. 11C1-(1:4)*. "Me, didAi'ailt. C- ~i y6log-Me = .. ; -f . . -. !I, '~ t Agitate'vit4j)uS1~1de rvn!dti.;~ 16c- We Or, c~` cced 75 Mi. so4r) filtm outl4l j! 'Wit (40'fii br in tvjlua to CIA15t, %-It,z 4411. PL614'-;- tate- ions do: fiat iliterilrTel 1410, ou 01~ ths~ )eti-lencei 4 nietAk J'~ :I":!: --~l from the 2n rTou 5, A :j jli f A f El: