SCIENTIFIC ABSTRACT SPIVAK, G.V. - SPIVAK, G.V.

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CIA-RDP86-00513R001652720011-6
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December 31, 1967
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SCIENTIFIC ABSTRACT
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66702 sov/log-4-8-22/35 Report on the Second All-Union Conference on Gas Electronics L.A. Sena and Yu.M. Kagan deal with "Elementary Processes of Determining the Motion of Ions in Gas". A paper by Ye. Bedereu (Rumania) dealt with "The Role of Resonance--!-recharging in the Kinetics of Ions". I.S. Stekollnikov considered the initial stages of the development of sparks (corona-leader, main channel and the final channel). B.N. Klyarfelld gave a survey of the ignition processes of the discharges in highly rarified gases. The mechanism of the breakdown of a high-vacuum gap was elucidated in a paper by V.L. Granovskiy. L. Tonks (USA) expounded a theory of the motion of electrons in a magnetic trap (see P 1316 of this journal) Academician R. Rompe (Eastern Germany) dascribed a number* of experiments on non-stationary plasma conducted by himself. M. Stenbeck (Eastern Germany) gave a generallsed theory of Dlasma. The conference was divided into six sections. ihe first section was presided over by L.A. Sena and was Card 2/15- 66702 sov/109-4-8-22i35 Report on the Second All-Union Conference on Gas Electronics concerned with the elementary processes in gas discharges. The following papers were read in this section: Ya.M. Fogel- "Transformation (if Positive Ions Into Negative Ones in Rarified Gases". Ta. M. Fogel' with V.A. Ankudlziov and D.V. Pilipenko "Capture and Loss of Electrons During the Collision of Fast Atoms of Carbon and Hydrogen with the Molecules of Gases". N.V. Fedorenko et al. - "Dissociation of Molecular Ions of Hydrogen During Collisions in Gas". I.P. Flaks and Ye.S. Solov1yev - "Capture Cross-sections of Electrons in Multicharge Ions in Inert Gases". R.M. Kushnir et al. - "Experimental Investigation of the Resonance Recharging in Certain Single-atom Gases and Metal Vapoursst. O.B. Firsov - "Qualitative Investigation of Inelastic Coillsidna of Atoms"* L.M.2Volkova - "Effective Excitation Cross-sections of the Spectral Lines of Potassium and Argon". Card3/15. i.p. Zapesoahnyy and S.M. K:Lshko "Some Results of the 66702 sov/loq-4-8jf2/35 Report on the Second All-Union Conference on Gas ectronics Investigation of the Optical Functions of the Excitation Bands of a Negative System". A.A. Voroblyev and A.G. Vlasov - "Investigation of the Scattering of the Electrons in a Betatron Chamber". The second section was presided over by B.N. Klyarfelld and was devoted to the problems of the electrical break- down in rarified gases and in high vacuum. The following papers-were read in this section: G.Ye. Makar-Limanov and Yu.A. Metl-itskly - "Electrostatic Control of the Ignition of Glow-discharge Tubes"(see p 1274 of the journal). S.V. Ptitsyn at al. were concerned with the breakdown in a high-voltage mercury rectifier (see p 1278 of the journal). L.G. Guseva "Ignition of the Discharge in Non-uniform Fields at low Gas Pressuresn (see p 1260 of the journal). A.S. Soboleva and B.N. Xlyarfelld - "The Discharge Phenomena Between a Point and a Plane at Gas Pressures of 10-3 - 1 mm Hg11. Card 4/1.5 66702 sov/iog-4-8-22/35 Report on the Second All-Union Conference on Gas Electronics Card5/15 T.B. Fosellson - "Methods of Reducing the Energy Lost in the Formation of a Breakdoicn". L.I. Pivovar and V.I. Gordiyenko - "Microdischarges and pre-breakdown Currents Botwoon Metal Electrodes in High Vacuum". V.A. Simonov and G.P. Katukov - "Investigation of the Processes of Initiation and Developmeut of a High-voltage Discharge in Vacuum". E.M. Reyk-hrudel and G.V. Smiraitskaya - "The Character- istics of'Ignition in High-vacuum in Magnet;c Fields". L.V. Tarasow et al. dealt with the transfer of the electrode material dur�ng the pre-breakdoim stage in vacuum. N.B. Rozanov et al. - "The Motion of Mi-cro-part1cles of Substances During Electric Breakdoim in Vacuum*. The third section dealt m1th the problems of electric sparks, corona and thetrpractical applications. It was presided over by I.S. Stekollnikov. The following papers were read: V.I. Levitov et al. - "Probe Investigation of the a.c. Corona Fields". P~ 66702 sov/log-4-8-22/35 Report on the Second All-Union Conference on Gas Electronics G.N. Aleksandrov - "Elementary Processes in the Ionisation Zone of Corona-type Conductors at Atmospheric Pressures*. V.A. Burmakin - "Appearance of a Corona Discharge in Hydrogen and Nitrogen" P.N. Chistyakov et al. - "Some Properties of the Corona Discharge in Hydrogen ifl/Coaxial, Cylindrical System". A.S. Soboleva and B.N. Klyarfelld - "Appearance of Discharge 11honomona Dotwoen a Point and a Plane at Gas Pressures of 10-3 _ 1.0 mm. Hg". Ya.Yu. Reynet et al. - "Nethods of Unipolar Ionisation of Air By Means of Acro-:3*Lonisers (see p 1335 of the journal). M.P~ Vanyukov at al. - "Timo Spoctra of the Radiation of a Spark Discharge in Inert Gas~s" (see p 1284 of the journal). M.P. Vanyukov and A.A. Mak - "Production of High Temperatures by Means of Spark Discharges". V.A. Peretyagln - "Influence of the Magnetic Field c:C -the Electric Discharge on the Dividing Surface of Two Median. Card 6/15 66702 soViog-4-8-22-/35 Report on the Second All-Union Conference on Gas Electronics I.S. Stekollnikov - "New Data From the Study of Long Sparks". M.I. Sysoyev - "Properties of the Breakdown of Compressed Air in a Comparatively Uniform Field in the Presence of Localised Non-uniformities". A.A. Voroblyev et al. - "Pulse and Oscillographic Techniques for the Measurement of the Discharge Lags in Dielectrics" (see p 1257 of the journal). A paper by B.N. Zolotykh dealt with the problem of the basic theory of the electric erosion (see P 1330 of the journal). The fourth section was presided over by S.Yu. Luklyanov and was concerned with the non-stationary and low- frequency discharges. The following papers were read: I.G. Nelcrashevich and A.A. Labud - "The Nature of the Current Interruption During the Electric.Explosion of a Metal Wire". V.A. Simonov - "Propagation of Plasma From Local Pulse Sources". Card 7/1 G.G. Timofeyev et al. - "Observation of an Electro- 5dynamically Compressed Arc By Means of an Electron-optical 66702 SOV/109-4-8-22/35 Report on the Second A,11-Union Conference on Gas Electronics Converter". M.S. Ioffe and Ye.Ye. Yushmanov - "Investigation of the Radial Electric Field in Ian Ion Magnetron". V.A. Belyayev and DI.K. Romanovskiy - "Experiments with an Electron Model of a SYste", With Magnetic samples". A.M. Andrianov et al."'Distribution of Magnatiq and Clectric Fields in Powerful Pulse Discharges". G.N. Harding (England) - "Spectroscopic Determination of the Plasma Temperature in the "Zeta" Equipment" (see p 1326 of the journal). The papw by Harding aroused a lot of interest and Academician L.A. Arts!movich expressed the opinion that the electrons and ion temperatures in the "Zeta" should be of the same order; instead, according to Harding, the electron temperature is lower by an order than that of the lons. A paper by S.Yu. Lultlyanova and V.I. Sinitsyn 'was devoted to the problem of spectroscopic investigation of heated Card8/i .15plasma. 66702 so)r/iog-4-8-22/35 Report on the Second All-Union Conference on Gas Electronics I.M. Podgornyy and N G. Kovallskiy - "New Data on X-ray Radiation During Pul;e Discharges" V.A. Klivabrov and M.M. Sulkovskaya dealt with the investi- gation of the neutron radiation in powerful gas discharges in chambers with conducting walls. N.A. Borzunov et al. - "Investigation of the Gas Discharge in a Conical Chamberel. S.M. Osovets et al. - "A Turn of Plasma in Transverse Magnetic Field". I.G. Kesayev "Data on the Division of a Cathode Spot on Mercury in a Low-pressure Arc" (see p 1289 of the journal). A.E. Robson (England) - "A New Theory of the Cathode Spot" (see P 1295 of the journal). L.N. Breusova - "Positive Column in a Hydrogen Discharge With Stationary and Pulse Loads". I.G. Nekrashevich and A.A. Labud - "Current Distribution on the Surface of Electrodes in Electric Pulse Discharges". L.S. Eyg - "Some Properties of Gas Discharges in Low-voltage Cardq/15 in Halogen Countersil. k 66702 5011/109-4-8-22/35 Report on the Second All-Union Conferonco on Electronics G.I. Glotova and V.L. Granovskly - "Ca=paxiaon of the Initial De-ionisation in the Isoto-pes of Hydrogen (H ;And D)11. L.A. Akollzina communicatod rostilt-n on the pre-breakdown current pulses at low pressures. M.Ya. Vasillyeva and A.A. Zaytsev - "Charge-density oscillation Waves in Cylindrical Plasma". L. Pekdrek of Czechoslovakia communicated some information on the wave-like phenomena in gas-discharge plasma. B.G. Brezhnev dealt with the problem of the deteradnation. of the energy of fast ions in pulse discharges. B.B. Kadomtsev - "Convection Instability of a Plasma String 5.1. Braginskly and V.D. Shafranov - "Theory of a High- temperature Plasma String". The fifth section was presided over by N.A. Kaptsov and dealt with hIgh-frequency currents in gases. The following papers were read: V.Ye. Golant - "Formation of Ultra-high Frequency Pulse Cardlo/15 Discharges in Inert Gases". 66702 SOV/109-4-8-22/3 Report on the Second All-Union Conference on Gas ilectronics G.I. Pateyuk - "Influence of the Boundary Conditlons.on the Formation and Maintenance of High-frequency Discharges". P.S. Bulkin et al. - "Investigation of a Self-maintalned Ultra-high Frequency Pulse Discharge and the Process of its Development". G.N. Zastenker and G.S. Solntsev - "Some Results of the Investigation of the Formation of Low-pressure High- frequency Discharges". G. Margenau (USA) - "Conductivity of Weakly Ionised Plasma". A.A. Kuzovnikov - "The Conditions of Transition From High-frequency Corona Discharge at Atmospheric Pressures". V.Ye. Golant - "The relationship Betwee-,-,L the Character- istics of -the Ultra-high Frequency Current and the Direct Current in Gas Discharges". B.B. LagovIyer analysed the conductivity of the disin- togrntiiiF p1n.-imn lit tho window of." ti rovottntic* dincliargo tube. S.M. Levitskiy and I.P. Shashurin dealt with the Ca.rdll/15 applicability of the probe method to high-frequency A- 66702 SOV/109-4-8-22/35 Report on the Second All-Union Conference on Gas Electronics discharges (see p 1238 of the journal). The paper by V. Ye. Mitsuk et al. was devoted to the investigation of the ultra-high frequency plasma by means of the Stark effect. G.S. Solntsev et al. dealt with the problem of electric fields in a high-frequency discharge at low pressures. Ye. Bodereu of'Rumania read a paper entitled "High- frequency Discharges in Nethane". The work of the sixth section was devoted to the problems of plasma and its radiation; the section was presided over by V.A. Fabrikantr The following papers were read: Yu.M. Kagan "Ne;k7iYin+Ue~robe Methods of Plasma InvestigationV V.I. Drozdov - "Oscillographic Measurements in Plasma". V.A. Simonov and A.G. Mileshkin - "Investigation of the Movement of Plasma by Means of a Mass Spectrometer of the Transit Time". A.V. Rubchinskiy - "Application of the Oscillations on a Small Anode to the Measurements of the Vapour or Gas Cardl2/15 DonsitY" (Soo P 1311 o-C -the journal). 66702 sovioq-4 8;22/35 Report on the Second All-Union Conference on &a Electronics A.A. Timofeyev - "Measurement of the Gas Density During the Dynamic Operation of a Discharge" (see P 1306 of the Journal).A.V. Nedospasov - The Nature of a Striated Positive Column". V.1. Perell and Yu.M. Kagan - "The Theory of Probes for Arbitrary Pressures". Yu.M. Kagan et al. - "The Positive Column of a Discharge in a Diffusion Regime". M.Y. Konyukov - "Influence of the Processes of the Annihilation of the Negative Ions on Their Concentration in the Column". M.D. Gabovich and L.L. Pasechnik - "Anomalous Scattering, Excitation of Plasma Oscillations and Plasma Resonance" Yu.L. K11mantovich - "Energy Lost by Charged Particles for the Excitation of the Oscillations in Plasma (the Langmuir paradox)" and "The Theonjof Non-linear Plasma Oscillationsu. Ye.G. Martinkov and I.G. Nekrashevich - "Dependence of the Temperature in the Near-electrode Region of a Pulse Discharge on the Material of the Electrodes". Cardl3/15 k 66702 sov/iog-4-8-22/35 Report on the Second All-Union Conforonce ori Gas Electronics N.A. Neretina and B.N. Klyarfelld - "Formation of Light Spots on the Anode of a Gas Discharge (see p 1301 of the journal). N.A. Matveyeva -"Distribution of Binary Mixtures of Inert Gases in a d.c. Discharge". V.G. Stepanov and V.F. Zakharchenko - "Some Phenomena in Rarified Plasma". V.G. Stepanov and V.S. Bezel' - "The Possibility of Obtaining Highly Concentrated Plasmas". G.V. Smirnitskaya and E.M. Reykhrudelk - "Some Character- istics of the Discharge in an Ion Pump and in a Magnetic Ion:Lsat:Lon Vacuum Gauge". Ye.T. Kucherenko, and O.K. Nazarenko, - "Properties of a Discharge with Electron Oscillations in a Magnetic Field" (see p 1253 of the journal). The paper by L.M. Biberman and B.A. Veklenko, considered. the approximate methods for determining the concentration of atoms at the radiation levels. Card 14/15 66702 sov/log-4-8-22/35 Report on the Second All-Union Conference on Gas Electronics I.I. SobellmAn and L.A. Vaywohteyn road a paper on "A Non-stationary Theory of the Stark Broadening of the Spectral Lines in Plasma". M.A. Mazing and S.L. Mandellshtam - "The Broadening and the Shift of Spectral Lines in a Gas-discharge Plasma*. R. Lunt (England) - "The Kinetics of Electron Collinions Leading to the Excitatlon of the Molecular Hydrogen in a Hydrogen Discharge". V.N. Kolesnikov et al. - "Some Properties of the Are Discharge in an Atmosphere of Inert Gases". A.A. Mak and M.P. Vanyukov - "Productlon of High Temperatures By Means of Spark Discharges". Card 15/15 SOV/126-7-6-14/24 AUTHORS: Sj~,:Lvak1i-.Q1.V.7 Yurasova, V.Ye.j Klenova, A.I. and Vlasova,T.A. TITLE: On the Exposure of the Structure of Metals by Gas Ion Bombardment PERIODICAL: Fizika metallov i metallovedeniye, 1959, Vol 7, Nr 6, pp 893-898 (USSR) ABSTRACT: In order to show the possibilities of revealing the metal structure of a heated material by a cathode sputtering method, the authors investigated several characteristic alloy.~o. Atomizing of the specimens at a definite t eftl 13erature ti~as eiirvlod Out in the apparatus for the ionic etching of metals UIT-1. U,*.od tiy Sptva.k et al.(Ref 3), in which there is a special device for 114~?Acitqg tho specimen (from 100 to 7000C) and for measuring its temperature, Sheet specimens of an Al-Mg alloy (6% Mg) were submitted to ion botubardment at 5000C. Cathode sputtering (together ifith selective evaporation which takes place at such a temperature) reveals the grain boundaries of an Al-Mg alloy (6.5% Mg) heated to 500*C. In Fig lb the surface of this alloy, etched with neon ions Card 1/5 at 2800C and in Fig la the structure of the same alloy . revealed bv cathode sputtering at 500*C are shown. From a -oil the Exposure of the Structure of Metals by Gas Ion Bombard-mt?~-~-, comparison of these photographs it can be seen that 5000C the grain size of the alloy is considerably coar4er and the grain boundaries are finer. Apart from this alloy,etching of specimens of steel YalT was studied with the apparatus UIT-1. In this case, chromium carbides precipitate(] along the grain boundaries at 5000C. The presence of chromium carbides after chet-,Acal etching is only apparent from the holes where the carbides were attacked. By means of ionic etching at 6000C the chromium carbide precipitates along the grain boundaries could be seen in the form of small dark spheres of approximately 1 to 2~L diameter. A photograph of the surface of steel YalT specimens etched at 6000C and fey-rite ,iiibsequently cooled is shoim in Fig 2. In Fig 3 and atistenito grains revealed as a result of cathode of HIC Steel YaIT are shown. In Fig 4 the structure or ptiro. miuminium sheet is shown (.I - after chemical etching: b - after etchitig by ion bombardment). The extent to -.i-hich the metal structure is rovoaled can be best judged by the depth of etching of the intergranular Card 2/5 boundary. Therefore, in order to select the correct SOV/126-7-6-14/24 On the Exposure of the Structure of,Metals by Gas Ion Bombardment sputtering treatment, the dependence of the depth of metal grain boundary etching on the parameters of the gas discharge during simultaneous sputtering was studied. The depth of the boundaries was measured by a stexwscopic method. A quartz print was taken from the atomized surface of the specimen and a precise portion of this print was photographed in the electron microscope UEM-100 under an angle of +6 and -60 relative to the optical axis. The stereo-couples obtained (Figs 5a and b) were studied with the precision stereometer SM-3, which gives the volume effect. In order to obtain more reliable results, the atomizing of the grain boundary was studied in neon and in air for several types of technical copper with two different instruments. Ionic etching of the specimens was carried out initially in a glass tube. The investi- gated specimen was used as the cathode in the tube. During atomizing, the specimen temperature was kept constant by cooling it with water. The dependence of the depth of etching of the grain boundary on the potential difference between the cathode and anode during atomizing in neon Card 3/5 was determined. The density of the discharging current SOV/126-7-6-111/24 On-the Exposure of the Structure of Metals by Gas Ion Bombardment was kept constant (j = 10 mA/cm 2). The results of the measurements carried out are shown bv the curve 3 in Fig 6. The dependence of the depth of etching of the grain boundaries on the density of the dischargingr current was studied on two types of specimens which were cut out from technical copper of somewhat different compositions. The density ~f the discharging current varied between 5 and 15 mA/cm ; the potential difference between the electrodes was kept constant at 5 W. The specimen was atomized for 5 mins. The dependence of the depth of etching of the grain boundaries on the density of the discharging current was found to be linear (Fig 7). From an analysis of the curves obtained for the dependence of the depth of etching of the intergranular metal boundaries on the density of the discharging current and on the potential difference between the electrodes it is possible to arrive at the following conclusions: there is no advantage in raising the potential difference between the cathode and the anode above 8-9 kW to accelerate revealing the metal structure. It is better for the density of the discharging current to Carcl 4/5 be increased. The greatest permissible density of the SOV/126-7-6-14/24 On the Exposure of the Structure of Metals by Gas Ion Bombardment discharging current in cathode sputtering of metals is determined by the intensity of the cooling rate of the specimen. In the case under consideration, in which the atomized specimens were cooled in a mixture of dr~ ice and alcohol, a current density exceeding 15 mA/cm should not be used. However, at a more intensive cooling rate, greater discharging currents can be used. The best operating conditions for atomizing technical coper aret j = 10 mAlcm2, u = 9 kW, t = 5 min, P = 5 X 10- mm H9 col. There are 7 figures and 7 references, 5 of which are Soviet, I Engljsh and 1 German. ASSOCIATION: Moskovskiy gosudarstvennyy universitet imen� M. V. Lomonosova (Moscow State University imeni M.V.Lomonosovj SUBMITTED: January 25, 1957 (Initially) November 12, 1957 (After revision) Card 5/5 AUTHORS: Spivak, G. V.,, Lyubehenko, V. I. SOV/413-23-6-8/28 TITLE: On the Resolving Power of Immersion Objectives in the Presence of Electric and Magnetic Microfields (0 razreshayushchey sposob- nosti immersionnogo ob"yektiva pri nalichii elektricheskikh i magnitnykh mikropoley na katode) PERIODICAL: Izvestiya Akademii nauk SSSR~ Seriya fizicheskaya, 1959, Vol 23, Nr 6, pp 697 - 705 (USSR) ABSTRACT: In the introduction, short reference is made to papers in which the domains of ferromagnetics and ferroelectrics are inves- tigated, and the structure of electric and maanetic microfields is investigated. The fields behave like microlenses, nodulate the electrons passing through, and make it possible to investi- gate the microstructure. When emission systems are used for the investigation of emission center distribution on the cathode surface, the microlenses of the cathode produce a "pseudocontrast" in the image of the emission. In the second part of the present paper the influence exercised by the macrolenses upon the contrast range of the microlenses is investigated. The equations of motion of the electrons in the magnetic and electric fields Card 1/3 serve as a basis and solutions are found for the position On the Resolving Power of Immersion Objectives in the SOV/48-23-6-a/2a Presence of Electric and Magnetic Microfields coordinates of the electrons. The results obtained are quali- tatively given in a table for various combinations of macro- lenses. When dealing with the resolving power of immersion objectives without microlenses on the cathode, the paper by Artsimovich (Ref 7) is mentioned among others. In these papers the resolving power of emission systems with larger aperture had been investigated. Moreover, resolving power was investi- gated in the case of the use of mechanical diaphragms. Much space is given to the treatment of the enlargement of photo- optical immersioL objectives and to the irising of the electron beam by magnetic fields acting on the cathode. Formula (18) is developed for the resolving power. In the last part of the paper, calculation of the resolving power of immersion objectives according to the method of the "sightingihit" is dealt with. Again, the equations of motion serve as a basis, and if E = H = 0, a formula for the resolving power is obtained. x z Q Next, the influence exercised by the electric microfields is Card 2/3 investigated, and for the deterioration of resolving power, formula (24) is given. In conclusion, the enlargement of photo- On the Resolving Power of Immersion Objectives in the SOV/48-23-6-8/28 Presence of Electric and 11agnetic Microfields optical objectives and irising by magnetic fields is investi- gated in the same manner. There are I table and 22 references, 11 of which are Soviet. ASSOCIATION: Fizicheskiy fakulltet Moskovskogo gos. universiteta im. M. V. Lomonosova ( Physics Department of the Moscow State University imeni M. V. Locionosov) Card 3/3 AUTHORS- Spivak, G. V. , -Pryr:smko,;ra, 1. A., igras, E. SOV/48-23-6-15/28 TITLE: On the Investigation c-f t-he Domains of Forromagnetins and Perroelentrics by Means of an Electron Mirror (0 nablyudenii domenov ferromagnet-ikov -- se6qietoelektrikov pri pomoshchi elektranncgo zerkala) PERIODICAL: Izvest--'L,-a Akademii nauk SSSR. Ser.ya f~z-:.cheskaya, 1959, Vol 239 Nr 6, PP 729--733 (USSR) ABSTRACT: In the introdue-tion the advantages offered by the electron mirror, as e.g. the fact that here the object is not bombarded with electrons and a considerable resolving power existsq are enumerated.The working methods with electron mirrors have already been dealt with by the authox-s in papers published at, an eaxlier date (Refs 1, 2), whil,~, others investigated the resolving power. The infiuence exercised by the strong macro- field upon the weak minrofields of the surfaoe is dealt with, and rafaven-:* i,3 made to the aforementioned papers. Further, the mechardsm. of o3ntrast formation is dealt with in the intro- duction. The se~:ond part deals w-ith the investigation of the structure of demaj,n-s of monocTystalp- of" ferromagnetics in the Card 1/2 elerjtror, mirror. In this c!onnactl-,)n~ the investigations carried On the Investigation of the Doma-_ns of FerrGmagne tic. a SOV/48-23-6-15/28 .and Perroelectrios by Means of an Electron Xirrcr out by the authors in 1955 (Ref 1) are mentioned, in which the possibility of ob-ta.-ning a magnetic contrast was pointed out. An instrument of this construction with axial symmetry is shown by figure i.To the-!'act that the elections move very slowly in the range of Tetiecting eleotrodes, the high degree of sensitiv- ity of this method is ascribed~ because the electric and magnetic miorofields are very weak. Figures 2-5 show examples of micropictures, v-*Lz,, first ordinary structural pictures compared with elsettron-optio-al Images of the domains, and further, p-_1,1-;ti,_re8 taken in warlovs magnetic fields are compared. The investigation of the structure of the domain in ferro- magnetics is fi-nall.y dealt wlth and Is supplemented. with examplee. F4na7ly, further development was investigated and found to be promising. There are 9 figures and 7 references, 3 of which are Soviet. ASSOCIATION: Fizicheskiy fakulitet MDskovBkogo gos, universiteta im. M. V. Lomono8O-Ta (Physical Department of the Moscow State University Card 2/2 imeni M. V. Lomortosov) SOV/48-23-6-16/28 AUTHORS: Sbitnikova, I. S., Spivak, G. V., Sarayeva, I. Y. TITLEi Electron Microscopy of the Temperature Variations of the Magnetic Microstructure of Ferromagneties (Elektronnaya mikro- 0 skopiya teaperaturnykh izmeneniy.magnitnoy mikrostruktury ferro- magnetikov) PERIODICAL: Izvestiya Akademii nauk SSSR. Seriya fizicheskaya, 1959, Vol 23, Nr 6, pp 734 - 737 (USSR) ABSTRACT: In the introductiontolder works (Refs 1,2) by the authors and others are mentioned, in which an electron-optical method is described, by means of which an image of the magnetic micro- fields is obtained by secondary electrons. Although the micro- fields have a field strength of about 1o4 oa, the images are of poor quality. In the present paper experiments, which were carried out for the purpose of developing methods of investi- gating magnetic microstructure, are described. Particular account is taken of the use of secondary emission microscopes for the investigation of the dynamics of thermal processes. On the basis of results obtained by other investigations (Refs 4,5), the damaging of the object surface by electron steel and the Card 1 decrease of this damage is discussed. The secondary emission Electron Microscopy of the Temperature Variations of the SOV/48-23-6-16/26 Magnetic Microstructure of Ferromagnetics microscooe used in the investigations dealt with has already been described in detail by another of the authors' paper (Aef 2); it has an anode voltage of not more than 10 kv. Three pictures (Figs 1,2) are given as examples. The structure re- corded by means of a metal microscope is compared with its magnetic contrast, and information is obtained concerning the formation of the magnetic contrast. The whole-metal construction of a secondary emission microscope, which was worked out for the purpose of avoiding the occurring aberration, is then described. By iaeans of this instrument the authors investigated the influence exercised by temperature upon the magnetic micro- structure. Exoerlments carried out with cobalt monocrystals show a sudden change of the domains with temperature. The additional device constructed for the purpose of heating the object is briefly described, and, finally three pictures (Fig 4) are shown as examples of structural domain changes at various temperatures. There are 4 figures and 8 references, 5 of which are Soviet. Card 2/~_ LUTHORS: Krokhina, A. I., Spivak, G. V. 3OV/48-23-6-18/28 TITLE: Investigation of the Structural Changes of Dielectrics Which Ire Under the Influence of Temperature, Chemical Attack, and Ian Ionic Bombardment (Izucheniye strakturnykh izmeneniy di- elektrikov, podvergnutykh vozdeystviyu temperatury, khimiches- kogo travleniya i ionnoy bombardirovki) PERIODICAL: Izvestiya Akademii nauk SSSR. Seriya fizicheskaya, 1959, Vol 23, Nr 6, PP 741 - 743 (USSR) ABSTRACT: The authoisfirst refer to previous papers by themselves (Refs 1,2), in which they showed that by the bombardment of dielectrics with ions attack figures are produced. These figures show the ionic structure of the crystal. The structure of these figures is similar to that after a chemical attack. In the present investigation, the crystals of a number of di- electrics with different orientation of the crystal axis were prepared. The investigated crystal planes of the various crystals are then given, and the structures obtained in this way (Figs 1-6) a:.- sho,,m- !)y i3--1x figa-es. S'1_ !Tte method described ha- certain diradve-n-bages because the foca3ing of the microlenses de- Card 1/4 pends upoa the discharge current and the air pressurre in the tubei- Investigation of the Structural Changes of Dielectrics SOV/48-23-6-18/28 Which Are Under the Influence of Temperature, Chemical Attack, and an Ionic Bombardment and further because the discharge cur:nnt in die3i-actrics can be accomDlished by the use of netal cont-actu nets. In order to inhibit the influence of temperature and the variation of ion-current density on the dielectric, tubes with intense water cooling were used. In order to elimi- nate the disadvantage of the metallic nets, a new method was developed, by means of which the dielectric is heated to such temperatures at which it is in a semiconductor state. By means of the instrument UIT-1 rock salt was treated for 3 hours at a temperature of 4000C, an accelerating voltage of 3 kv, a current of 3 ma, after which it was investigeted by means of an electronic microscope. Figure 3 shows the result obtained. By means of this method, the influence exercised by the evapora- tion of the dielectric and the critical temperature for the intense evaporation of the dielectric were investigated. The result obtained shows that the structure formed by evaporation of the dielectric is identical with those obtained by applying Card 0 the two other methods. There are 6 figures and 5 Soviet refer- ences. AUTHORS: TITLE: Yurasova, V. Ye.,_S-pivak, G. V., SOV/48-23-6-19/28 Kushnir, F. P. Methods for the Development of the Structure of Metals and Alloys by Ion-bombardment (Metodika Yyyavleniya struktury metalloy i splavov ionnoy bombardirovkoy) PERIODICAL: Izvestiya Akademii nauk SSSR. Seriya fizicheskaya, 1959, Vol 23, Nr 6, pp 744 - 749 (USSR) ABSTRACT. In the first part of the present paper ion-etching of the granular boundaries and of the structural composition of the alloys are investigated within a large temperature interval. First, the advantages of cathodic spraying as against chemical etching and thermal evaDoration in a vacuum are pointed out. One of the most important advantages is the possibility of carrying out structural investigations within a large temperature inter- val. For visual investigation and for photographing a special attachment was constructed (Fig 1). Seven pictures are then shown of aluminum bronze (Pigs 2,3), which were taken after various forms of thermal treatment by ion-spraying and cathodic Card 1/2 spraying and 350-fold enlargement. The first series of picturea Methods for the Development of the Structure of Yletala and SOY/40-23-6-19/28 Alloys by Ion-bombardment distinctly shown the formation of the martensite structure in the three range6 of temperature , whereas the second series shows the structural grains at various temperatures. In the 3e- cond part of the paper the destruction of the surface of the structural grains of polyorystals or of monocrystals by ion- bombardment is investigated. Pirst, the fact is pointed out that by the investigation of the symmetric indentations,our knowledge of the mechanism of.cathode-spraying has been extended, and that new possibilities of applying ion bombardment may now be found. It follows from the pictures (Fig 5) that the symmetry of orientated indentations agrees with the orientation of the sur- face of a monocrystal. In the following, the influence exercised by the increase of ion energy is investigated and explained on the basis of figure 5. The results obtained make it possible to assume that the orientated indentations may form in the course of ion-etching. There are 6 figures and 7 references, 5 of which are Soviet. ASSOCIATION; Fizicheskiy fakulltet Moskovskogo gos. iuniversitet im. M. V. Lpmonosova (Physics Department of Moscow State University imeni Card 2/2 M. V. Lomonosov) M AUTHORS: Dubinina, Ye. M., $pivak, G. V~, SCV/AS-23-6-23/28 Pryamkova, I. A. TITLE: The Obtaining of Images in the Pu,1se Principle in the Emission Microscope With High Resolving Power(O poluchenii izobrazheniy v impul'snom rezhime v emissionnom. mikroskope vysokogo razresheniya) PERIODICAL: Izvestiya Akademli nauk SSSR. Seriya fizicheskaya, 1959, Vol 23, Nr 6, PP 762-7641 (USSR) ABSTRACT: In the introduction to this paper it is shown that by investigating pulsed emission in an emission microscope, it ia possible to investigate the conditions on active cathodes in pulsed operation. Images of the emitting cathode in normal operation are compared with those in pulsed operation. The impulse increase exercises considerable influence upon resolving power. The work described was carried out by means of the industrial electrostatic microscope ESM-50, which has an immersion object with 150--fold enlargement. The block scheme of the current oupply of the instrument is shown (Fig 1) and discussed. 1.s examples, two pictures (Fig 2) of the cathode Card 1/2 in steady and in pulsed operation are shown; the pictures were The Obtaining of Images in the Pulse Prin,::iple sov,142-23-6-23/28 in the Emission Microscope With High Resolving Power not found to differ. A further investigation carried out on an L-cathode also showed no essential differences. Finally, the possibility of using pulsed operation when investigating the domain structure in ferromagnetics and ferroelectrics is shown and a stroboscopic arrangement is described by means of which images of the domain structure with higher resolving power were attained. There are 3 figures and 3 Soviet references. ASSOCIATION: Fizicheakiy fakul'tet Moskovskogo gos. universitet im. M- V. Lomonosova (Physics Department of 'Moscow State University imehi M. V. Lomonosov) Card 2/2 PHASE I BOOK EXPWTZATION SOV/4337 Spetsialtnyy fizicheskiy praktikum, tom. 1: Radiofizika i elektronika (Special Practicum on Physics,, Vol. 1: Radio Physics and Electronics) (Moscow] izd-vo moskovskogo univ.,, 196o. 600 p. Errata sl-ip inserted. 10J,000 copies printed. Compiler and Ed.: G.V* Spivak, Member of the Faculty of the Physics Division of Moscow Universiti, -Ed..* (Inside book): I.A. Nosyreva; Tech. Ed.: G.I. Georgiyeva. PURPOSE: This book is intended for university students in physics. COVZRA=.s This is the first volwAe of a miltivolumed work in physics approved by the Ministry of Specialized Higher and Secondary Education as a textbook at the uzdvers-Ity level. Volume I presents a description of laboratory tests in radiophysics and electronics. The volume is divided Into 2 parts. Part I reviews oscillatory systems., rexUo waw propagation and acoustics; the second part contains problems relating to h-f electronics and pbysics. The authors of the work are faculty members of the Radio Physics Section of the Physics Department of Ybscov University. Chapter I of Part I was written by C FH[,SE I BOOK EXPLOITATION SOV/4705 FaAiofizicheskaya elektronika (RiLdiophysical Electronics)(Moscow]Izd-vo Mosk. univ.., 1960. 561 p. Errata slip inserted. 15,000 copies printed. Ed.: N. A. Kaptsov, Professor; Tech. Ed.: N. S. Yermskov. PURPOSE: This book has been approved by the Ministry of Higher and Secondary Special Education,, USSR, as a textbook for sch661s of higher education. It can be also used by tcientific personnel working in the fields of radio engineering and electronics. COVERAGE: The book presents problems of vacuum, cathode, semicanductorp and glLs electronics., on which is based the operation of vacuum-tube and gas-filled devices, including microwave devices and also apparatus and instruments used in electron optics. It is assumed that the readers of this book bavea pre- liminary preparation in the fundamentals of nuclear physics, quantum mechanics., statistical physics and electrodynamics. The book was written by a group of lecturers of the Physics Division of Moscow State University. Card lj~a, Wiophysical Electronics sov/4705 Chapters I. II, and III were written by Professor N. A. Kaptsov; Ch. IV. by Professor S. D. Gvozdcver,- and Docent V. M. Lopukbin; Ch. V. by Professor G. V.-gPivak and Assistant Ye. M. Dabinina; Ch. VII. by Docent A. A. 7Aytsev -Eid-Profesg-or N. A. Kaptsov,*, Ch. VIII. by Professor N. A. Naptsov and Assist- ant G. S. Solntsev. The authors thank Professor S. Yu. Luklyanov and Docent M.D. Karasev , who reviewed the book. There are 76 references: 68 Soviet (in- cluding 14 translations), 6 English, and 2 German. TABLE OF CONTENTS: Foreword Ch. 1. Subject of Physical Electronics. High-Vacuum Electronics 9 1. Introduction 9 2. Transmission of electric cux-rent through a high vacuum 13 3. Space charges in gaseous, liquid and solid media 21 4. Physics of electron tubes 21 Ch. II. Semiconductor Electronics 29 5. Electron energy levels in crystals 29 6. Impurity semiconductors 32 7. lAw of electron distribution along the separate energy levels in semiconductor energy bands 36 8. Density of energy states in any energy band of a crystal 39 Card 27-1-~r- Padiophysical Electronics SOV/4705 50- 1~_--flex klystron 194 51. Trawling-wave (W) tube 205 52. Back-ward-va-ve oscillator (BWO) PP9 53. Magnetron 234 54. Space-charge effect. Concept of space-charge longitudinal wa,4r-, s 249 55. Electron-wave tube (EnN) 264 Ch. V. Electron Optics 271 56. Subject and prcbljems of electron optics 276 57- Optical properties c.' alectric and magnetic fields with axial symnetry 276 58- Lense,3 of electron optics 281 59- Magnetic lenses 282 60. Electrostatic lenses 286 61. Ricrolenses 303 62. Electronic mirror 305 63. Geometrical aberration 307 64. Chromatic aberration 314 65- Fesolution of electron-optics instrments. Space-charge effect and certain methods of correcting lenses 318 F42.Uophysictal Ej.r~ctronics SOV/4705 66. Electron guns 321 67. Cathode-ray oscillographs 329 68. Blectron-optics devices realizing transformation operations 330 69. Electron microscope 341 70. Double focusing in a mass spectrograph 353 Ch. VI. Electric-Discharge Formation in Gases 356 71. Nature and special features of the movement of free electrons in a gaseous medium 356 72. Diffusion and mobility of charged particles in a discharge 359 73. Theory of mobility 364 74. Dependence of effective atomic or molecular cross section on tbe speed of tne interacting electron 367 75. Independent and dependent electric discharges in gases 371 76. Avalanche theory of discharge 373 ',77. D:,-pendence of factor 0( on electric field intensity6 376 78- W. Rogowskils theory 381 79. D--pendence of avalanche-discharge igniting voltage on product ,pd and other conditions 384 Card S/058/61/000/012/060/06,3 A058/AlOl AUTHORS: Sbitnikova, I,C., Spivak, GV, Sarayeva, I.M, T=- Temperature variations of the magnetic microstructure of ferromag- netics detected by means of secondary electron emission PERI06ICAL: Referativnyy zhurnal. Fizika, no. 12, 1961, 384, abstract 12E694 (V sb. "Magnitn. struktura ferromagnetikov", Novosibirsk, Sib. otd, AN SSSR, ig6o, 41 - 46) TEXT: Using the technique worked out earlier (PZhFiz, 1954, no. 9, l0419~ 1956, no. 10, 2916_3; 1957, no. 12, 30558), magnetic microfields set up by marten- sitic needles in a steel specimen were observed in a secondary-emission electron microscope. Weakening of these fields wiih increasing temperature was observed. A change in and weakening of domain-scattering fields on the hexagonal surface of a Co single crystal incident to heating to 2400c was also observed, N. Serov [Abstracter's note.- Complete translation] Card 1/1 S/O 58/6 1/000/0 12/055/0 83 A058/A101 AUTHORS: Spivak, G.V., Pryamkova, I.A. TITLE- Development of an electron-mirror method for visualizing domain structure is ferromagnetics PERIODICAL: Referativnyy zhurnal. Fizika, no. 12, 1961, 383, abstract 12E685 (V sb. "Magnitn. struktura ferromagnetikov", Novosibirsk, Sib. otd. AN SSSR, ig6o, 185 - 189) TEXT- There is described a glass model of a direct electron mirror in which in contrast to earlier models (RZhFiz, 1956, no. 9, 25867) - the reflected and the primary electron beams are not,specially separated. The primary beam passes through an aperture in the screen, approaches the investigated object, is reflect- ed and, after being focused, hits the screeri. This makes it possible to increase the magnification and sensitivity of the instrument. With the aid of the describ- ed,electron mirror there were observed domain structures in different ferromag- netics, A metallic model of the direct electron mirror with electron-optical mag- nification,-,-,250-is also described. Problems are discussed concerning formation of images of domain microfields in the mirror. [Abstracter's note- Complete translation] N. Sedov Card 1/1 S/058/6 1/000/0 12/054/083 A058/A 10 1 AUTHORS: Spivak, G.V., Shishkina, Ye.I., Yurasova, V.Ye. TITLEi Concerning a method for detecting magnetic inhomogeneities PERIODICAL% Referativnyy zhurnal. Fiiika, no. 12, 1961, 383, abstract 12E684 (V sb. "Magnitn. struktura ferromagnetikov", Novosibirsk, Sib. otd. AN SSSRJI 196o, 191 - 194) TEXT: The feasibility was demonstrated of detecting magnetic inhomogenei- ties on the surfaces of ferromagnetics by means of chemical etching. The indi- cated method is based on the fact that ions in solution that have a magnetic moment are drawn into the region with the highest magnetic-field gradient. The most effective etchants and etching conditions were found by the trial-and-error method. 'Using the described method, an electron-microscope image was obtained of magnetic inhomogeneities in an artificial specimen built up of alternate Permen- dure and Mo bands, as well as an image of natural magnetic inhomogeneities in martensitic needles in steel. N. Sedov [Abstracter's note: Complete translation] Card 1/1 AUTHORSt I'll V1kh11^,~1a, R.P. Zhd... A.G. T H.N., !..k. 6.V.. A.E* and To... P!o! A. A TITLLt Report on the Ninth All-Union Conference on-Cathod* EJet tr..i.. 1960. Vol 3. 4~ 5, pP8 6-879 ( USS A) AUSTRACTt This conference took place In Moscownf"m 2!-211h October 1959 with the participation f I .1.ntj.tm end Cr.- 11-4.ry, E.:!-%G.Tmany~ the Chi.*.* nd .. I people.. R.Pblt. Ch ~ k. . Th. that- of Ih d-ition V*k.ht..k&y. p rt consist. ""'I 7:bk" r 2!.j. Per. Th:.r., of brl I r:tt,,, r e ted I t Plenary he !. Me of 5 Re 'is were P,:d the conference. I p .. t.d in the section on surface properties oor ..lid. dealt.& .1 1h city. surface P!t* C t% h (1,1-1a: on Card 1/2 -faces .... d,.c.u..l.d. 6 F.p.t. . nth - ----- physics of cathode. are gi- I. the it.. on th.r.i I. mission. 17 1,, a ,:r pr ... nt.d I. the ::cti.n an photo. '*'- Many papers discussed industrtal t.1hoTog, -.fhol...11. p is nda~~It ipli*r.. 16 pr:.:. d..t.th. action ..I on t . -d-y;-1-tron - - Th field ii paper. di ...... Put.. high or ... t urf... phd Id on --de" or memtconductorm)~and the -r- And bri D. cathode. More r covc~unlcatio t he ...trs t 0 :are presented !ha--5U p pion 0. prop r I .. ... type; 'd technology of cathode., relating to the tachn0l.. thod:,,r!h.,.ir b aviour in :h p-t="1'd!w !n. h - of *f YP::. ~h individual cat 19 Pap,rotw,r, zM".1:t the tho".. section on interaction of -Lid b.di.. with tr.... of charged partl' I.:.and residual Samoa. Notes of di u Job Indicated that sever.1 sharp end Card 2/2 critical *xcaeftx.. or view. took place. s/log/60/005/008/023/024 7- 0 (lo X31 // ?;71 // ~/a) E192/E382 AUTHORS: Sirotenkog I.G., ~.pivakG.V_ and Groman, A. TIT-LE, Field Emission from Filamentary Semiconductor Monocrystals or Whiskers PERIODICAL, Radiotekhnika i elektronika, 1960, Vol. 5, No, 8, pp~ 1348 - 1350 TEXT,. The work reported deals with the manufacture of semiconductor whiskers and measurement of their field emission, It appears that the data relating to the field emission of such monocrystals are lacking (Refs. 7, 8), The whiskers of tungsten and molybdenum oxides obtained by the authors are larger than the usual micro-whiskers, The whiskers are produced by the following technique, A small quantity of tungsten or molybdenum oxide was placed in a quartz tube having a length of 15 cm and a diameter.of 6 mm, the tube being closed at one end, The oxides were obtained by burning fine wires in an oxygen atmosphere. By heating the lower end of the tube in air a sublimation of the oxides was achieved and the vapours condensed on the comparatively cold portions Card lj~. 1;a/ S/109/60/005/008/023/024 E192/E382 Field Emission from Filamentary Semiconductor Monocrystals or Whi8kers of,the tube (see Fig. 1), A growth of whiskers occurred at various areas of the tube, depending on the concentration of the vapours and the temperature gradients, At very high vapour concentrations the whiskers were in the form of dendrites. In order to obtain the whiskers in a suitable form, a metal.loop was introduced into the quartz tube and the whiskers were grown on it (Fig. 1), After that the Wire loop was suitably mounted in a gun and investigated, In the case of molybdenum oxide, the whiskers were also obtained by the following method: a spiral having a diameter of 5 mm and a length of 5 cin was made of molybdenum wire and one of its ends was bent in the shape of a loop; this was then placed inside the spiral so that the end of the loop was roughJ-y in the zentre of the spiral; when the end of the spiral was heated by an oxygen flame the molybdenum was oxidised and the resulting oxide vapours were condensed on the loop in the form of whiskers. The whIskers -were investigated Card 2/4, S/048MOFC24/06/03/017 B019/BO67 AUTHORS: Spivak, G. V Pryamkova, I. A., Sedov, N. N? TITLE: On the Formation of the Electron Optical Contrast in the, Observation of "Hollow Spots" in Emitters PERIODICAL: Izvestiya Akademii nauk SSSR. Seriya fizicheakaya, ig6o, Vol. 24, No. 6, pp. 640-646 TEXT: This is the reproduction of a lecture delivered at the 9-th All- Union Conference on Cathode Electronics from October 21 to 26, 1959 in Moscow. Contrast problems of emission*nd of quasi-emission (mirror-type) electron optical systems were investigated. In the first chapter, the authors describe the influence exercised by the normal and the tangential component of the electric field on electron kineticst and in the second chapter they deal with the mechanism of formation of the contrast. The formation of "hollow spotsl*ue to local potential differences of the re- flecting electrode is ;xpla-lned, and the faot'that the microfields of these electrodes can be investigated at any temperature is shown to be the' most important property of this type of electrodes. The influence Card 1/3 82158 On the Formation of the Electron Optical 3/048/60/024/06/03/017 Contrast in the Observation of "Hollow Spots" BO1q/BO67 in Emitters exercised by "hollow spots" on the resolving,power of an immersion ob- jective is briefly dealt with, and in the following the local micro- fields on emitting surfaces are discussed in detail. Here, "hollow spots" observed by the authors on polished, well activated diodes consisting of copper-aluminum-magnesium alloys and on rather smooth L-cathodes (Ref. 1) are described.By comparing the secondary electron emission images and the thermionic emission images the authors observed that the former are caused by the roughness, and the latter by the inhomogeneities of the work func- tion, i.e., by the "hollow spots". The formation of the contrast in oxide cathodes was investigated in detail where the formation of the mirror image,the thermal image, and the photoemission image were studied. For this purpose, the combined electron microscope shown in Fig- 4 was used. It was found that the geometrical relief of the cathode surface, the "hollow spots" and the electric microfields play an important part in the formation of contrast. In the final chapter, some typical cases of the formation and the inversion of the contrast by superposition of micro- fields are discussed. There are 5 figures and 10 Soviet references. Card 2/,3 S,/048/60~024/06/09/01T Boig/Bo67 AUTHORS: Sirotenko, I. G., Spivak, G. V. TITLE: Pickling Demolition of Semiconductors by Ion Bombardment), PERIODICAL: Izvestiya Akademii nauk SSSR. Seriya fizicheskaya, 1960, Vol- 24, No. 6v pp. 679-684 TEXT: This is the reproduction of a lecture delivered at the 9th All- Union Conference on Cathode Electronics from October 21 to 28, 1959 in Moscow. Cathode sputtering of semiconductor crystals and monocrystals1s investigated (germanium, silicong lerritea). The aim of the present paper 'Was to extend the pickling by ion bombardment to a larger number of semi- conductors, to get to know the type of eputtering for semiconductors, and to develop the pickling demolition of the acmiconductor surface as they occur in electronic devices and disturb operation. The initial cathode sput- tering of semiconductor for the ion-pickling by the glow discharges in two-electrode tubes filled with rare gasesshowed poor results. Better re- sults were obtained by treating the targets in plasmas with high current density and low pressure. The pickled germanium crystal surfaces shown Card 1/2 82167 S/048/60/024/06/12/017 B019/BO67 AUTHORS: Krokhina, A. I,., Spivak, G. V. TITLE: On the Prob,lem of Anisotropy of Cathode Sputtering of Dielectrics -;-k PERIODICAL: Izvestiya Akademii nauk SSSR. Seriya fizicheskaya, ig6o, Vol. 24, No. 6, pp. 694-697 TEXT: This is the reproduction of a lecture delivered at the 9th All- Union Conference on Cathode Electronics from October 21 to 28, 1959 in Moscow. In the introduction, some papers on the destruction of metal surfaces, dielectrics, and semiconductors by incident ions are discussed, and V. Ye. Yurasov (Refs. 1, 7) is mentioned. In the present paper, ex- perimental results are given which show that an anisotropy of cathode sputtering in the bombardment of dielectrics with ions occurs, which is caused by the structure of the ion beam. First the authors describe the test tube shown in Fig. 1, and the target holder shown in Fig. 2. Figs. 3 and 4 show distributions of deposits on NaCl and KBr crystals which are due to the inhomogeneities of the incident ion beam. The authors are of the Card 1/2 SIROTENEO, I.G.; SPIVAK, G.V. Exposure of boundary dislocations in germanium by ionic Lombard- ment. Kristallografila. 6 no.2:2?4-277 Mr-Ap 161. (1.1IRA 14:9) 1. Moskovskiy gosudarstvennyy universitet im. M.V.Lomonosova. (Germanium) (Dislocations in crystals) (Ions) SPIVAK G V - VERTSNER V.N.; LUKIYANOVICII.. V.M.; IBVIN, Ye.Ye.; ..I.. -I __~. " P 1. 1 1 SKAKOV2 Yu,A* Third All-Union Conference on Electron Microscopy. Radiotekh. i elektron. 6 no.5:852-862 MY 161. (MIRA 1424 ',' (Electron microscopy---Congresses) 25791 s /0 _,18 / 6 10 J F 104 'B2 01 AUTHORS: Spiva"," 111. V.. Sirotenkc. I. G., and IvanDv. R. D. TITLE: Domain s~_-uc~ure of ferromagnetic films produced by cathode ?ERIODICAL: Akademiya nauk 38SR, Izvesti.va, Seri-ya fizicheskaya. v. 25, no~ 51. 1,96,, 581-.583 TEXT: The vresent in,,-esti,,ation was the sub'iect of a lecture delivered 7 at a symposium on thin ferrorna_netic films ~Krasnoyarzsk, ju'y 4 I to 7, ig6o). Cathode ~--putfoving w!is nerklormed in a pla.-zma under an intense 10-) m.'11 Ht-; 'I .The free-rath discharge and at a low Oress~:re '_?-O' len-th of sputtered aroms wa-s some 77:1at Ion,--er 'han the distance between tar,~etl and base layer-, The appiLimen intended for sputtering was con- nected as the third electrode wish a ne.-at-i-ve potential of I kv- A hot cathode served fcr augmenting di:_-,clnari The ge current and ion density, dischar-e current vi-as of the order of ', ampere. while that directed or"o 'ne soecimen to be 3put*ered ,vas of *~e order cf 1 milliampe-re, The base layers were made cf glass and arranged a~. a di'Otance .~f -2 --m, fr_-M the Card 1/4' slo-48,1`6 C _;' '55/0 0 5 // G 0 5 // 0 2 4 Domain structure of ferromasne-lic 0 target. The specimens tI- be sputtered Y:ere disk-shaped and had an area of, The f ilm tinickness of permallcy s-.,2c im; a n s( 7 91/0 Ni, 17"' Fe , about 1 cm2 4/_'O Mc) changed lin-early soutterin`-- time (30-3~ minutes ,i, when the specimen potential xa_o 800 T. the discharge current ?, a S r, 7 1~ a. the xre was ,current dL-nsity to the specimen was 1.6 ma~sm and he pressu '_ 3 9. 10 'mm Hg, At ~~Ie same ~iffile. the temperature of the specimens ranged from 100 to 1?5LC Tne films "'crmed in a oersted magnetic field r~ara.1~11 to the film, clane, tT- nn ali - es a .vh'c,h was oritinted i o a e ng p-oc 8 S i:oolk p-lace in a maL~,ne-i~~ ana1yses 5howed Thai +,here was no difference bet-.-.;ePn -%e ~om,,)osition cl~' SL)uttered films and That of the init'ial material ., Vre au-hors ,,;are able ~o obServe magnetic powder patterns or. SOO hi!:k c~obait -I'llms. Tile direction oil easiest mag- netizing co-incided wit,`, the mrag-reric field direction during the process Of film sputtering. The sputtering of iron silicide -,ook place under the iollowirg condit-~ons. the specimen potptial, -relative to the cathode was 700 v, the current density was 6 ma,cm the discharge current was I a, the pressure was 6.10-3 mm Ha. The sputtering timeZ were 10, 20.. and 410 minutes. The wedge-shaped powder patterns observed on iron silicide Card 2, 4 J, 21;_;C~,:! :-,5/024 S ~-,4 /61 :R, 1 Domain structure of ferromacrnettic films with '~7i were orien,~ed in the field direc-con,_ -1 n f i I of the abovementioned )erTa',lc,,,- oorzriponition.. produced under "linear" ccnditions, i.d1sc,:arge cur---.- the sputterinig rate aad tc be irncreaz-ed sharply -, ri, f .1 a potential of specimen ',.2 k1r, current density tc 72,6 ma.,,rm-, pressure 6-10-. mm H-) to obtaln distinct powder patterns, Differently thick films of this type 9~iowed the domains to di-vide into equal intervals Lrom the 17hickneps of onwards. In addition, !-~,e domain stru,~3ture is somewhat increased ;;Al larger t-ickneE~ses.. anO tne -,-,,-3dges extend in the fiel-d on a fur'.~,.e- increas_~~ -e we-,'EQ~_ are -rans'_~?~,mad ir~-: Lianes -T~l PL-trallel -ides wl-'ch ar,~ cr`an'ed in "rL- Cie-fd di-E~~--ion. T n-~! cox, f i -ura I- Lon c. f t il d oma in ~~_z be Orro~ 5 G I _~ C r i t, r-,~a C. '. C, J_ eri me nt results are -as Foll1c,,-,- 21,; :,~-: n '-e oa:! i I v pr7 Z:I%re~_' rom any naterial by nathode m 3 C f ,-! 0. n. j can be obtained und~~r we-11 ~-tcrtrt,"ed production corditlons,: (3) a gcrd uniforr,--~ty oi- an-JI a Suff,,._~_iant of film p_-ep_~-raricn are ensured: (d) 'i',ms thus pi-odu,7ed do nct differ ess.~ntial',y fr~:,m -,e lni-.ial mat,zirial_ to ~i,eir 2-omz)c.-i -~icn . 111'n,~re ar~ 1~ fi-2-ure:~ anj 7 -3 bloca referencez Clard, 3/4 25791. ii ~'S L) C 1 S't T 101.1 ?4- 1 2 i-~ i v fa kule ~`-c ske-) v s', oar 6c. suniversiteta im, V ~ Lomc no sc~7a v si en. o" -'-:~Iys i c s~,.Os3c'w Sta-~e -meni Card 4/4 SPIVAK, G.V.; PRYMEOVA, I.A.; FETISOV, D.V.; KABANOV, A.N.; LAZAREVA, L.V.; A. 1. I-1irror-type electron microscope for studying surface structures. Izv.AN SSSR.Ser.fiz. 25 no.6:683-690 je 161. (MIRA 14:6) 1. Fizicheskiy fakulftet Moskovskogo gosudargtvennogo universiteta im. M.V.Lomonosova. (Electron microscope) -2,12-300 AUTFURS: Spivak, TITLE: YWT-3 (LTIT-2) ductors 24803 S/'U48/tl/025/006/005/010 B117/B212 G. V., Kushnir, F. F., ard Yurasova, V. Ye. installation for etchIn& metals, serricon- and dieluctrics through ion bombardment F --,R ID I Ct, L: Akademiya nauk SSSR. Izvestiya. Seriya fizicheskaya, v. 25 no. 6, 1961, 707 - 712 T:.~AT: The present paper has been presented at the Ir d A1.1-Union Conference or.. Electron Microscopy, held in Leningrad from October 24 to 29, 1?60. It describes a new model of ,q. technical installation of type YvT-3 (UIT-3) for etching metals, semicoi,dul-;tors, and dielectrics through ion bombardment. The models UIT-1 and UIT-2 hELve been described in Refs. 1 and 2 (Spivak G. V., Yurasova V. Ye., Kushnir F. F., Prilezhayeva I. N., Pribory i ts?~-.hr,ika eksperim., 119 2, 10~, 0`157); Yurasova V. Ye., Spivak G. V., "UShnir F. izv. All SSSR, -er. Piz., 21, 744 (1959)). The UIT-3 installation is designed for the following investigations of the surface structure of materials under different conditions: 1) heatirg of a sputtered suecimen not above 12000 C; 2) cooling of the specimen during Card 1/6 24803 ,/04 b/(; I /0?15/006/~;O.~//U 10 YHT-3 (UIT-3) installation ... B117/B212 ctching with running water; 5) observation of the object surface during sruttering or evaporation by using an ortical syotem with P- long focal length; d) expansion or :ownro:~siori of the specimen duvin,7 icnic etching cr evaporati-)r, 5) arplicu'lioll Of quartz or met,~,l foils, (reccs~iary for Url--- sol-.sequent eAe,!!.ron-oi.,tj.,,tl ztudy of the powdeT'ud surf~j(-e) rij~JA after iuftic etching o!' the specimens. The UIT-3 installation COLSLSts Of the 1'0110-~-ing rnain com-ronents: system for generating and measuring the vacuum, feeding device, control console, device far expansion and compression of the snecimens, me!:allo-ranlic microscone and a device to sioutter and heat the suecimer.s. The vacuum system of' UT-3 is analoeous to tbat of UIT-1. 'N e electric system consists of tI,e following main comnorients: hiph-tersiun rectifier for 10 Vv and 50 ma; beHting current transformer ( '( v, 250 a) with a device to transfer the potential either to het or evaporate the snecimen; pla'L.4ir~um-platinum-ri.odiiiir, or chromel-alumel thermo couples with a millivoltmeter for measuring the temperature of the specia,.en; Gevice for measui-in.-~r the vacuum af-.d turring on the pumps; interlocks which switch off t~.e high tension whQn the doors of the installation are opened. Fig. 2 shows a dia~-,ram of the UIT-3 installation. The shaz)e of the specimens to be sDuttered may be arbitra,,iy if no load is applied. The :aaximum size of a Card 216 24803 IS/048J61/025/006/00/01.0 YOT-3 (UIT-3) installation... B117/B212 specimen bombar,,d with ions should not exceed 30 X 30'~ 6 mm, When the 0 specimen is hea ed up to 1200 C it should not be larger than 20 x 20 x 2 mm., 2 During sputte-ring a specimen having a maximum cross section of 20 mm and a length of 60 mm can be expanded o7r compresse"d under a load of 400 kg., Right' after the ionic etching a quartz, metal, or carbon foil can beput on thq V specimen. The ionic etching may create impressions at the edges of the monocrystals which have the symmetry of these edge*S:.' The oriented figures, which are'obtained by cathode sputtering and corresponds to the symmetry 6f the surface where they are located, may be used to determine roughly the It. indices of simplest crystal edges. The application of ionic etching seems' very promising to visualize dislocations, especially for heaied specimefid i chemical etching cannot be used. There are 4 figures and 4 references, 3 Soviet-bloc and 1 non-Soviet-bloc. ASSOCIATION: Fizicheskiy fakulltet Moskovskogo gos. universiteta im. M. V. Lomonosova (Division of Physics of Moscow State University imeni M. V. Lomonosov) Card 3/6 30- 24804 S/048/61/025/006/004/010 J) B117/B212 fla=1 AUTAORS: Sedov, N. N., Spivak, G. V. and Isayeva, N. F. TITLE: Electroa-optical measurement of electric and magnetic micro- fields on surfaces PERIODICAL: Akademiya nauk SSSR. Izvestiya. Seriya fizicheskaya, v. 25, no. 6, 1961, 725-729 TEXT: The present paper has been presented at the 3rd All-Union Confer- ence on Electron Microscopy, held in Leningrad from October 24 to 299 1960. The author8 invesLigated expF--imentally the quantitative ratio between the strength of the local microfield on the surface of an electron emitter and the image contrast in the image plane. If such a correlation exists, it is possible with an electron-optical emission system not only to observe the electric and magnetic surface microfields but also tk measure their strength. Using an additional secondary emission device with an 3)M-75 (EFIVI-75) emission microscope, the structure and distribution of the ther- mionic emission of effective cathodes has been investigated. Due to such studies it is possible to establish a correlation between the structure Card 1/5 21,8o4 S/048/6~,/025/006/004/010 Electron-optical measurement of B117/B212 and emission of such a heat emitter (Ref. 6: Sbitnikova I. S., Dubinina Ye. M Spivak G. V., Fetisov D. V., Pribory i tekhnika. ekspexim., NQ 5, 76 (1959i,; Radiotekhnika i elektronika '. 5-,1077 (1958)). A com- bination of photo- and thermionic emission leads to the same conclusions in the same emission microscope (Ref,, 3: Spivak G,)V., Pryamkova 1. A., Sedov N. N., Izv. AN SSSR. Ser. fiz., 24, 640 (196 ). The microscope used by the authors was similar to that described in Ref. 3, It in a com- bined glass-metal device. The vacuum was measured to be (3-5)-lo-7 mm Hg with an external glass casing and good degasification. The magnification of the microscope varied from 50 to 500. A beam catcher not used in the microscope described in Ref-a 3 was mounted in the center of the lumi- nescent screen. The microscope was built in several variations with photo- and secondary emission from the surface of the object. In the latter case, the microscope had a socket with an electron gun instead of the lighting device, which was used to bombard the object with about 100-ev electrons. A heater allowed to observe the hot cathodes also during thermionic emission. The possibility of measuring local magnetic fields was checked by using a number of artificial specimens consisting of alternating mag- netic and non-magnetic stripes (e.g. iron and copper). The front side of Card 2/5 24804 S/046/61/025/006/004/01C Electron-optical measurement of ... B117/B212 the specimen was polished. Magnetizing was done by an external magnetic field. The distribution of the magnetic field across the specimen and the current density on the screen were compared during focusing onto the area of magnetic inhomogeneitLes. The image was shifted by means of Helmholtz coils to measure the uurrent density across the individual sections of the specimen. In some cases, the brightness of the luminescent screen was also measured by employing an 034-19 (FEU-19) photomultiplier in a housing impervious to light. The test results of the brightness of the screen and the direct measurement of the current density on the screen agreed. The magnetic field across the specimen was determined from the change of the resistance of a thin bismuth wire (50 and 100tLdiameter). From the typical curves obtained for the magnetic field across the surface of the specimen, it was found that points with maximum values of the ma6netic field corre- spond to a minimum current density on the screen and vice versa. The . measurements showed that the relation j 11j2 = H2 /H1 (2) is actually ful- filled with an accuracy of 5-101o. (The subscripts I and 2 denote the fields and the current density of electrons across the individual sections of the object). The accuracy depends on the exact performance of the exper iment and especially on the even lighting of the specimen, With the given Card 3/5 Electron-optical measurement of -I,-14804 S/048/6,1/025/006/004/010 B11,0212 ae-uracy it is possible to measure small magnetic fields which are difficult to measure by other methods. Measurements of magnetic fields were done with artificial inhomogeneities of-wO.1 mm. At present, this method is applied to measure natural magnetic microfields which can be found in a number of ob- jects. Active heat emitters were also investigated. The current density of individual sections of pressed cathodes was measured in the temperature range from 6000 - 8001C. The lower temperature limit was determined by the thermionic emission. The upper limit was determined by the bluiring of the image caused by the space charge. Richardson lines were drawn by using the temperature dependence of the current density. The work function deter- mined from the inclination of the straight lines ranged from 1.9-3.1 ev. Most of the emission spots had a work function close to the lower value. If the spacing of the spots and the difference of the contact potentials determined from the difference of the work function are known;then it is possible to estimate the field potential of the spots for the object in question. It is in the order of several kv/cm. Electron-optical emission systems make it possible to determine inIagnetic and electric microfields on the surface not only qualitatively but also quantitatively. The authors thank the student E. Sh. Gasparyan for cooperation and A. I. Shallnikov for Card 4/5 -24806 - /,,4,/,-1/C2;/OO6/oO6/010 0 a,,ji Osadlko~ G V. f, sp- Ar, .0 f e SL J. L1 r ~5 V - PERIODICAL,, 5,-d A -M The TEXT! T am )w 2.4 2,; n oy!.des Ej-:w'tOn go Thi5 e'-*,in;ka eksperim. 7 11 -d Tflodell g un d~! Jut ry, on It IL 0- the ?hj;;; j: C:7 s-,.zrfaOO Of F r -or, M, ele-tr~~,r 1, ~he, form of ud ed ,ry s t a! s nr 5 0,.:','T. L bike r I ad -, 1 i k ',a!. pcill'- A 2,CIC M t ri 7 Ti - ~ t ,q h n b;~ 7was-i by - e 9 h c a- i de , , a a..d -a" e C-M rj Ta- 7 A_rld 5 ~, T he i-- r tz- P _ a W-Ire 10CP w e r r 0 grown a fore- b y Tr. e Var~;,j7., %7a- created ,-,e zube and fr-?ezi-rg a, t r ,, :7 anc. w a a g there t h e m J6 A : -C h ~ - -:o:-, - w I , , a appea,, C av d 24806 6/048' /61/025/0006/0006/010 study ... B117/3212 corresi-ond to the emission of the various thread-like crystals. The image might change when the potential is raised: The images of single thread- like crystals ~"of smaller diameter) disappear, while the images of others appear, Tile crystals resist a lasting heating to red heat of the wire. Due to the heating of the ci-ystals, the same emissicn, current aill be ob- served with a potential increase. Some emission images disappear and the screen luminescEs evenly. It is assumed that the ends arWrounded off during heating and the images of some crystals overlap. Quite often one car see images on the screen, which consist of four individual luminous spots, Sometimes it can be observed how. the image is rotating by 900 around ~ts axis, This might take place under -the effect of ion bombardment of residuai gases, Very seldom it was cbserved that a sudder. rotation took olace when increasing the potential, with a subsequent disappearance of the image.Iti.-3 possible that these phenomena are relaied to the occurrence of a screw crystal emission and to a stripping of these crystals by tn'z! field. Investigations of the thread-like crystals after the tes-. showed that their ends become pointed due to ion bombardment. The ion bombardment is the main cause for til'i instability of cold cathodes (Ref-5: Elinson M.I., Vasillyev G,V.., Avtoelpktrornaya emissiya. Fizmatg--'z, M., 1958). A fairly stable Card 3/4 2006 6/04A/61/025/006//006/010 _'lectron-microscopic study B1 17/012 current can be expected ICrom crystals having the form of straight needies of a small diameter. Studies of the efiect of ion bombardment on the.-.. emissicn i~roperties of thread-like crystals showed that the emission curzent increases by a multiple and reaches up to 3001Aa. The stability of the emission current also increases. At.the same,time,more,four-leaf images can be ob8erved on the screen. For a certain "point brush", the conditions furnishing constant emission currents a_-u.chosen experimentally. Ther are 7 fiEures and 7 references: 5 Soviet-bloc and,2 non-Soviet-bloc. ASSOCIATION: Fizicheskiy fakulltet Moskovskogo gos. universiteta im. M.V. Lomonosava (Division of Physics of Moscow State University imeni M.V. Lomonosov) Card 4/4 21L807 S/046/0 1/025/006/007/010 -N B117/B212 o 0 (lo S~r, //,~ 31 AUTHO' RS - Lazareva, L.V. and Spivak, G.V. TITLE: E.~,-tron-microscop,, observations of magnet-r; m-;c-o47j.e'ds by -.mpressions PERiODICAL: Akadeniiya nauk 33S,d., izvestija. Seriya ilzicheskaya, v. 215t M). 6, 1 '41 , -14 2 -714 7 TEXT: Tnr-~ ~reserit -p-,per has been presented at the 3:-1 Conference "n El~c~rcri Yicroscopy, 'Qe..d in Leningrad from October 24 to 2'11. 19Q(-)~ TMe va uti eAlectrun-micruscupic irettiod which make;, it J.'Js,jible -,o --,~-!~,te tile surface geometry of a ferr-cmagneti:! matur."al wiLh its mj-c-rcmz18t.et.ic s;vucturze. The method is based or. an impression taken of the itself but riot of the feFrom-agnetic. powder dusted or, the ob-;e-~~. Thiq inelhod haz; "he following ad-~antages: The impre3slori taKen dire,-.-~Iy f1rom th-~~ spe-cimen dependq neithei, on the magrietic nor oil the geometri:, lata of tl-~e powder. Therefore, high magnifications -arid alst-.1 M,-:~:-e ~-f tile ma~--ietI*c-,r,,eoaetr--'c characteristics are possible. Llagneti- :).-rid s'ructural zrGperties (micro-eome'ry) of the m-ler4al can Card 114 24P~07 S/048/61/025/006/007/010 Electron-m_icrcLcopic observations 3117/B212 be studied simultaneously. The microgeometry of the specimens was .rv~~_ltigated lby means of carbon or quartz impressions and a transmiGsion. plp~ ...-7tron microscorie. At the same time, the magnetic structure correspond- in.6 to thq 3tate of the specimens (annealed, mechanically or electrolyt- ically polished, stretched ,) was investigated by the powdar method. Textured ";,rrosilicon. (" Si) was cliosen for the tosts. Aboul, 10 different specimens were stGdied. The results are characteristic and viell reproduc- i ble ~It was f~)und that the crystallites are oriented nearly parallel to the (1 10) plarie in 16-he rolling direction, and alorg the direction of roLLine they are oriented -in the (,',OOJ direction, For ferrosillicon this is "he direction of easiest magnetizat-on. Monocrystals were etched out from single large crystallites by using nitric acid. The crystallo- ,.raphic orientation of the specimens was determined by X-ray photographs. The syecimens -were chosen such that the surface investigated was located in a rolling plane inclined at an angle of 2 - 3o to the crystallographic plane (110). Tile specimens used were of various geometrical shapes (disks, rectangies and polyjguns) with suriaces ranging from 0.5 cm2 to several centimeters, and thicknesses from 0.3 - 1.5 mm. The monocrystal was Card 2/4 24807 S/048/6.1/025/006/007/010 E-'ec tron-ml~:rcscopic ob Eerjations B117/B212 polLshed mechanically. The pcwder patterns in the optical microscope are typ.--~;al of' su~.,h F,~pecimen3 for the (110) plane if stre5ses are present. The St-ucture depsnds on the grinding direction and does not seem repr,~.-,ent !,;ie structure of' the internal domains. It iz3 known that tile K,urdaries of the mosaic zigzag, A value of' 1060 was obtained for stable -.~gzag anglec z,f ferrosilicon (Ref.11: Chikazumi S., Suzuki K., J. Phys. Soc. dapan, 1.2. 523 (19~5); "Magnitnaya struktura ferromagnet-ikov" str. 204. Pad red. S..V. Vors,-vskog~,., IL. 1959), This angle will 'cr- smaller than 1060 it str-nj~ StT~~-.Stz- are p.oe2ent in the crystal. oil specimens wLth vary-.-n~ strt,53-vs showed values 'cetween 8()'-' v~ad 11,1U, w,-,-;ch-a-grei with the For studies wit-hout str-~ss,ls the specimens were polished electrolyt'cally;afte~r ,hat they were annealed ir vacuo at 10000C for 3 hr and -hen. c-d-Aed slowly. The powder patterns which represent the ma6netic stz-u-~tu-e of an annealed specimen, are para--Iel ctraight lines. I They co~~e- the wh-,~.~e s~irfane and. are ,-,~,.aracteriistic r-f the (110 ) plane of . fery-c'silicor., It carl be assumed that the I.ine relief is caused by cold ro,'1J,.ng uf the uititerl.all, and that .1 the character of the linear magnetic domains -)f annea~d 6pec'imens is closely connected with 'the character of tHe micro6tri.;?~.ti,re. investigations have shown that stror.6 internal streises C 314 2W907 0/048/61/Q25/OU6/007/010 El r-c tron-m i~; obstirv at i ons caused by thermal treatment will chan6e thte magnetic structure of the spec imens. In ~,he pr,,~sent paper, it hao been found that there Is a certain relation betwe~~i. the microgeomptry at ti-Le surface of fer-rosilicon specimens. ana the characto.r of their magnetic otru.-.~tuve. The stre*ses cau6ed by me(.hanica.' cr th,~?rmul treatment seeir. to cause a change of the microgeometry -it the surface -,f the specimen, This can b~. explained by the anisotropy of the stricA2.~)n prop~-,rtjes. The totu~ity of a."I.chariges, appr~a,--_rifg in the specimer. due t,.:~ aniootropy of -the mechanicai and magnetic proper..Jeo wiil bring abQut the xagnetic structure cliaracterizing the staTe of the mat.?rrial. Ya..S. Shur, VA. Abel's, L.V., Kirensk-i'j, If..V- Veter are ment-loned. There are 8 figures arid 15 references-. 9 Soviet-bloc and 6 non-Soviet-bloc. ASSOCIATIONt F.fz-.cheskiy fakulltet Moskovskcgo gos.universiteta im. I.V. Lomonosova (Divisior. o--:' PIK,,sics of Moscow State University imeni ."'L.V. Lomonosriv) Card 4/4 S/04 61/025/012/007/022 B116X138 AUTHORS: Spivak, G. V., Kirenskiy, L. V., Ivanov, R. D., and Sedov, TITLE: Development of mirror-type electron microscopy of magnetic microfields PERIODICAL: Akademiya nauk SSSR. Izvestiya- Seriya fizicheskaya, v. 25, no. 12, 1961, 1465 - 1469 TEXT: The authors present electron-optical photomicrographs of domain structures of various ferromagnetic materials and compare them with powder patterns. The distribution of the local magnetic fields scattered by the specimen is obtained from the contrast. G. V. Spivak, I. N. Prilezhayeva, and V. K. Azovtsev (Dokl. AN SSSR, 105, 965 (1955)) were the first to re- commend the el&ctron mirror for photographing magnetic microfields. They carried out their experiments at the laboratoriya elektronnoy optiki MGU (Electron Optics Laboratory of MGU). The electron mirror has the following advantages over the methods of secondary electron emission or photoeffect: high field sensitivity (the illuminating electron beam is stop-ped by an Card S/04 61/025/012/007/022 Development of mirror-type ... B116YB138 electric field in front of the specimen, i. e. "probing" of the spatial field structure; high contrast, due to the forwards and backwards motion of the electron; and the possibility of examining the magnetic structure at different distances from the source of the microfield. The optical system can be traversed by both slow and fast electrons% A 50-kv voltage focuses the reflected electrons and enhances the resolving power of the instrument. 1)omqin structure electron-mirror pictures of a PbO(Fe2O 3)6 crystal magnifi- cation: 400, 800. and 1500), cobalt (400 and 800), and a cobalt film (-1000 a, 400 times), were in good agreement with ones produced by the powder method (400). The local magnetic fields were determined from the contrast. Calculations have shown that the contrast depends on the product Hz (z = extent of the H-field), The magnetic field decreases almost ex- ponentially. Results are shown in Fig.. 6,. Knally it is noted that magne- tic fields can be examined under an electron mirror microscoDe and that their thE!ir strength can be measured at different distances from the specimen, The magnification here achieved (about 2000) can be further increased. There are 6 figures and 7 Soviet refere.-~ces. Card 214- 8/04,3/61/025/012/007/022. Development of mirror-typed.a. B116/B138 ASSOCIATION: Fizichnskiy fakulltet Moskovskogo gou. universiteta im. M. V., Lomonotiova (Division of Physics of Moscow State University imeni M. Vi Lomonoeov), Institut fiziki Sibirakogo otdeleniya' Alcademii nauk 3SSR (Institute of Physics of the Siberian Department of the Academy of Bdiences USSR) Fig. 6. (a) Field above the artificial specimeng measured with a bismuth Z/zo micrometer at different magnetic biasing currents H - H e W mirrorl~ 0 calibration curvel (c) scattering field above the hexagonal plane of the i PbO(Fe 0 crystals z - 0.02 mm; (d) scattering field'above the hexagonal 2 3)6 0 axis which is nearly parallel to the cobalt face, zo = 0-05 mm. Legendt 7, 15 a con5tantf B I ahd B2 are the various degrees of brightness on the acreen& Card 3/~ 31608 S/048J61/025/012/022/022 Ile B125/B112 AUTHORS: Ivanov, R. D., Spivak, G. V., and Kislova, G. K. TITLE; The properties of ferromagnetic films produced by cathode sputtering PERIODICAL: Akademiya nauk SSSR. Izvestiya. Seriya fizicheakaya, v. 25, no. 12, 1961 , 1524-1525 TEXT: A method worked out by G. V. Spivak, I. G. Sirotenko, and R. D. Ivanov (Izv. AN SSSR. Ser. fiz., 31, 581 (1961) for the production of one-component and multicomponent ferromagnetic films of high quality by cathode sputtering was improved. The magnetization curves and the hysteresis loops of such films were studied and the most important loop parameters were determined by a magneto-optic method, suggested by 0. S. Krinchik (Fizika tverdogo tela, 2, no. 6 (1j60)) which uses the equatorial Kerr effect. Polarized light i~_cident on the surface of the film through two windows in the discharge tube, was transmitted-to a photoelectric cell by reflexion. In case of static operation, the hysteresis loop was recorded by means of a bridge circuit with two selenium photoelectric Card 1/2 316G8 S/048/61/025/012/022/022 The properties of ferromagnetic ... B125/B112 cells of the type C_1-10 (SF-10) and with a galvanometer M21/2 (X21/2) without exposing the film to the atmosphere. During the formation of the ferromagnetic films their properties were checked constantly. All the films were sputteredtD hot surfaces under approximately equal conditions (amperage of the discharge current 0-5-1 a, potential of the specimen with respect to the cathode 1.8-2.2 kv, krypton pressure in the tube (4-2)-io-3 mm Hg, current density in the specimen 1-3 ma cm-2, generating field -44.2 ce, period of sputtering 4 2-5 minutes) and their magnetiza- tion was reversed in direction of weak magnetization. The film was then exposed to air and the change in the coercive force was studied. The coercive force which is rather small prior to oxidation increased notably at the beginning and more reluctantly in the further course of time. An analogous behavior of He can be observed also in other ferromagnetic films. Adequate measures should be taken to protect the film exposed to the atmosphere and the essential parts of the receiver should be made so as to permit recording of the whole magnetization process by oscilloscopes. There are 3 figures and 2 Soviet references. ASSOCIATION: Fizicheskiy fakulltet Moskovskogo gos. universiteta im. M. V. Lomonosova (Physics Department of the Moscow State Card 2/2 University imeni M. V. Lomonosov) 23734 S/0~,7/61/031/006/016/019 9~ 4:3 ro 0 7 11 C4;~ /.3 q Ins-, B 1 /B' 2 Ol - -ak G. V., Sirotenko, I. G.~ a-rid I-ranov, R. D. AUTH; .3~ -Sp-L TITLE-, M, c r -- ma6r, e. t, c- atruc.tura of films obtain-ed by cathode spui.tel-ing PERIODICAL: Zb.-.jLrnal tekhn-i.cheskoy fiziki, V. 311, no. 6, 1961, 754 - 756 TEXT~ A des,-ripticn J-s gi;rea of the. applicatiori of intense cathode spu-,tering f*o7 the ptjrpcls-l~ obtaining different ferromagnetic films. Compared with existj.ng me-thods, this one is shown to display a number of ad-rantages. The doma-,.r, s-~r-uortvr-e and its ohanges have been observed on ferromagne~!.~ -,tc~balt f1*Jms,, molybdenum-permalloy fillms (119M, 17Fe 4mo),., and sili~,-~n- iron f-i-ims (3-~3',/o S-0 wi-~h the aid :if pcwder pattarns. The characteriel-l'as of the change of the domain structure with a change of thickness have been es,tablishad on molybdenum-permalloy films. Ferromagne- tic film3 are usually ---.t'ained 1,y vacuum evapoxation or by electrodeposition. Such meth--,ds ` h,:we-ar~ display a number of essential drawbacks- 1) The chemical compo',sitio n of tbe fi.1m differs from that of the initial material; 2) difficalf'.1es arise Ln the preparation of homogeneous films of a desired Card 1/4 SIO 57/6-!/031/006/018/019 Mi.(,, r.,)magne t i.c s truc ture cf films . . . B 1 6/1320 thi cknps~7.. Air ar*~emp-r has been made by G. S.idda.'.'-' (Ref. !; Proc. Inst. fq"~B.' and Q. Wehr)pr (Ref. 2., Adv, in Electronics a. Electron Phyq.~ '9-5) Lo obta.tn films of different. metals by CELtbode sputlering. A paper by L. Reimer (Ref, 3~ "Os. f'. Phys..~ 149, 425, 1957.). descr-0-jes at,~ewptrj t,,- prepare nick#~I. films by cathode sputtering. These expe:.imej1t=_,. were condncted with relative~'y weak discharge currents and in a glow d.ischarge; in addition relaturely high gas pre:3s... ures (of 0.1 mm Hg and more ) ware applied. In such a case,, a long -time is needed to obtaln films of a desired thickness. which, however, causes the film to be polluted and oxidized.. The authors of the present paper have carri.ed out an intense cathode sputtering in the plasma of a low-pressure I d-ischaTge (-',-'0 _) 10 -3 mm Hg). The mean free path was in this case lar ger than the dist4rice between the bombarded target and the base on which the film was foimed,, The sputtered specimens were introduced into the plasma as the third electrode with a negative potential of the order of I kv with respect to the caT;node.- A ho" cathode was used to raise the density of the discharge current. The discharge current was of the order of some amperes, and the currea:-. appl-;ed to the sputsered specimen was of the order of some Card 2/4 23734 S/057/61/031/006/018/019 Micromagnetic structure of films... B116/B201 milliamperes. The glass bases onto which the films were sputtered, were placed at a distance of 2 - 3 cm from the target. The setup used was so constructed as to allow several films to be submitted to sputtering simul- taneously, without having to interrupt the sputtering process. The disk- shaped sputtered specimens had an area of I cm , which ensured a sufficient deposition of the sputtered material onto the base. The film thickness varied linearly with time. Therefore, the thickness could be easily regu- lated by changing the sputtering time; thus, films of any desired thick- ness were obtained. The film thickness was measured with an WA- ~(MII - 5) microinterferometer. The glass bases were heated up to 100 - 125 C. The films formed in a magnetic film of the order of 175 - 200 oersteds, which was parallel to the plane of the base. Quantitative chemical and spectro- scopic analyses of films obtained by cathode sputtering and with different modes of operation showed that -their composition did not differ from the initial components in the sputtered materiils. The domain structure was observed on the films with the aid of powder patterns. When submitting molybdenum-permalloy films to sputtering, the specimen potential amounted to 800 v, the discharge current was 0.75 a, the density of the current to the specimen was 1.6 ma/cm, and -the pressure was 9.10 mm Hg. The domain walls Card 3/4 23734 S/057/61/031/006/018/019 Micromagnetic structure of films ... B116/B201 changed in appearance with an increase of the film thickness. The * silic-on- iron films, on which wedge-shaped powder patterns were established, were submitted to sputtering at a specimen potential of 700 v. a current density of 6 ma/cm 2~ a disoharge current of 1 a. and a pressure of 8-10-3 mm. Hg. The method described here for obtaining ferromagnetic films by intense cathode sputtering is characterized by the following circumstances: 1) It is possible to obtain high-quality films of different thicknesses under easily controllable conditions; 2) cathode sputtering may be applied with materials of any melting temperatures; 3) uniform sputtering and pure films are ensured; 4) most important, the films obtained display only small deviations from the composiltion of the sputtered ferromagnetic substances. [Abstracter's note: Essentially complete translationq There are 2 figures and 3 non- Soviet-bloc references. ASSOCIATION: Moskovskiy gosudarstvennyy universitet im. M. V. Lomonosova Fizicheskiy fakulltet (Moscow State University imeni M. V. Lomonosov, Division of Physics) SUBMITTED: September 16, 1960 Card 4/4 SPIVAX, G,V.; KROKHINA, A.I.; TEREMETSKAYA, A.G.; TEWIOVSKAYA, M.V. Studying the microstructure of ore minerals by ion bombardment. Zap.Vses.min.ob-va 0,0 no.6:695-697 '61. (IIIIIA 15:2) 1. Fizicheskiy fakul'tet Moskovskogo gosudarstvennogo universiteta. (MineraloQr) S/048/62/026/011/003/021 B125/B102 AWHORS: Sedov, N. N., Spivak, G. V., and Ivanov, H. D. TITLE: Electron-optical study of a p-n junction in germanium and silicon PERIODICAL: Akademiya nauk SSSR.' Izvestiya. Seriya fizicheakaya, v. 26, no. 11, 1962, 1332-1334- TEXT: The authors describe an electron-microscopic method of examining a p-n junction with the help of ion-induced electron emission. This method offers the following advantages: (1) The surface of the specimen and the junction can be examined simultaneously; (2) the overall length of the junction is visible; (3) the image is not darkened by any auxiliary grid; (4) the method is likely to be suitable also for greater enlargements; (5) quantitative measurement of the potential distribution in the p-n 'junction is very simple. The secondary electrons are knocked out of the specimen by positive ions of 3-4 kev and then are accelerated and focused with the immersion objective of a high-quality emission microscope with improved metal mirror. Such secondary emission microscopes are Card 1/3 S/048/62/026/01-1/003. /021 Electron-optical study of a B125/B102 particularly suitable for examining semiconductors with surface junctions that are not heated. The photographs are taken inside the vacuum chamber. The disturbances of the accelerating field that arise over the p-n junction bend the electron trajectories. The electrons deflected by these disturbances are kept away from the screen of the microscope by an aperture stop. When a voltage of 5-10 v is applied in the back direction, the image of the p-n junction assumes the shape of a dark band which need not be straight and which broadens as voltage increases. The range of the potential in the p-n junction can be determined from a comparison between the secondary emission image and the electron mirror. The construction of a mirror electron microscope was described by G. V. Spivak et al. (Izv. AN SSSR, Ser. fiz., 25, 6a3 (1961)). The shape of the Dotential barrier on the p-n junction was determined by using the sharp contrast between the reflected image of the surface and the boundary of the "snot" of secondary emission. The method described here permits measurements at sufficiently small intervals. Its accuracy is dependent: upon the properties of the electron mirror which is more sensitive to inhomogeneities, such as p-n junctions, than is an electron microscope with ion-induced electfon emission because the impurities change the work Vard 2/3 S/04 62/026/011/003/021 Electron-optical atudy of a Bl 25YB1 02 function. There are 10 figures. ASSOCIATION: Fizicheskiy fakulltet Moskovskogo gos. universiteta im. 14. V. Lomonosova (Physics Division of the Moscow State University imeni M. V. Lomonosov) Card 3/3 S/04 62/026/011/004/021 B125 102 AUTHORS: Spivak, G. V.1-Saparin, G. V., and Pereverzevs N. A. TITLE. The potential distribution found in a p-n junction by means of an electron-optical raster system PERIODICAL: Akademiya nauk SSSR. Izvestiya. Seriya fizicheskaya, v. 26, no. 11, 1962, 1339-1342 TEXT: The authors discuss the possibility of visualizing the junction and of quantitatively measuring the range of the potential in p-n junctionsof germanium and silicon single crystals directlyand quickly, using an elec- tron beam that scans over the surface. The method is based on the, following assumptions: (1) The radius of the 'scanning beam ha's to be smaller than the width of the p-n junction; (2) the potential drop iir the junction must be greater than the mean energy of the secondary electrons. .The accuracy of the method in weak fields can be improved by reducing the electron energy and when the radius of the electron probe is reduced, the method can be applied to measuring potentials of thin junctions. The width of the junction can also be determined by varying the blocking Card 1/5 S/048/62/026/011/004/021 The potential distribution ... B125/BI02 voltage. The potential distribution of a p-n junction is determined with t..qe integrating circuit (12) and the oscilloscope (13) (Fig. 1). If the blocking voltage is given, the width of the junction determined by the electron-optical method is 25-305/o greater than that measured with a micro- manipulator. The method described here furnishes data on the dependence of the electrical structure of a p-n junction on various factors. The device displays'600 scanning lines and supplies 50 frames per sec. There are 7 figures. ASSOCIATION: Fizicheskiy fakulltet Moskovskogo gos. universiteta im. M. V. Lomonosova (Physics Division of the Moscow State University imeni M. V. Lomonosov) Fig. 1. Block diagram of the electron-optical raster system. Legend: (1) electron gun; (2) anode cylinder; (3)-(4) magnetic lenses; (5) deflecting coils; (6) object; (7) collector; (8) amplifier; (9) the deflecting coils in the circuit of the electron probe are connected in serie to the kin,~scope; (11) kinescope. Card 5/18IJ63/005/002/P241051- B1041BI02 AUTHORS: Predvodit'419- A vi A4, Ab Ak.-'Go V.i Kof -Ye,,'# and Kushnir# F&I, Yurasovaj. V. TITLE: Study o*f non-idecoreA 'dislocations In sin Ingle arysf,~Ll br ion boAardme'nt': PERIODICAL: Fizika tver 'ielap-,vi- 5t 0 a d og*d' n 2 1963 9` ~542-545 TEXT: This ap 'is 'a.imed ,to,,'pro ve -po'sei-bility, of' i9vi p er detecting, 4in dislocations',.by.ion.bombardeent::df.single-orystal- f d-66~ Cilindkidal.".. zinc single.'arystal 5 mai"In diaim"etert'50 Mig high.),'"ie split:'along - the (Odol) plane'at:~ihitrbgen-l'tefii~'ar'aturo, and the faoes were,, boubarde with ions in flowing neon gas.' Thin pieces of specimens that - had,'bein'~ n'.both (0061)'~lane6 a a ed-the-_a~aae ich iitierns. bombarded with ions P, -4 w 8 ni: Of -;any-, .one surfa*o* isso icin pro udie", - t on both sides.--Ropqated.etchi d, no new etch patterns.-but"iiiteniifiiis,:thd6e existing'. The' 1tej :resu on bombardment'are cons ht i ";'Th~ chemical-etching and f rom, I iste a .oat. favorable experimental conditionc are: neon* presauro -between 107.2,and ~Card 1/2 -T IVAK, G.V.; YURASOVA, V.Ye.; KUSIMIR, F.F. UIT-r apparatus for fast etching of metals, semiconductors, and dielectrics by ionic bombardment. Izv. AN SSSR. Ser. fiz. 27 no.9:1188-1192 S 163. (MIRA 16:9) 1. Fizicheskiy fakulltet Moskovskogo gosudarstvennogo universiteta. im. Lomonosova. (Electronic apparatus and appliances) (Ion beams) SPIVAK, G.V.; IVANOV, R.D.; PAVLYUCHENKO, O.P.; SEDOV, N.N. Formation of contrast in mirror-type, emission, and scanning electron-optical systems. Izv. AN SSSR. Ser. fiz. 27 no.9: 1139-1146 S 163. (MIRA 16:9) 1. Fizicheskiy fakulltet Moskovskogo gosudarstvennogo universiteta im. Lomonosova. (Electron microscope) SEDOV, N.N.; SPIVAK, G.V.,; DYUKOV, V.G. Use of an emission electron microscope in studying semiconductors and dielectrics. Izv. AN SSSR. Ser. fiz. 27 no.9:1173-1178 S 163. (AURA 16:9) 1. Fizicheskiy fakulltet Moskovskogo gosudarstvennogo universiteta. im. M.V.Lomonosova. (Electron microscopy) SEDOV, N.N.; SPIVAK, G.V.; DYUKOV, V.G. Use of an emission electron microscope in measuring the potential distribution in a p-n junction. Izv. AN SSSR. Ser. fiz. 27 no.9: 1179-1183 S 163. (MIRA 16:9) 1. Fizicheskiy- fakulltet Moskovskogo gosudarwtvennogo universiteta im. Lomonosova. (Electron microscopy) (Junction transistors) SPIVAK, G.V.; LUKIYANCV, A.Ye.; TOSHEV, S.D.; KOPTSIK, V.A. Observation of the domain structure of triglyalne sulfate by means of an electron mirror. Izv. AN SSSR. Ser. fiz. 27 no.9:1199-1202 S 163. (NIRA 16:9) 1. Fizicheskiy fakulltet Moskovskogo, gosudarstvennogo universiteta im.M.V.Lomonosova. (Glycine) (Domain structure) (Electronic apparatus and appliances) q.-),:6- 6, iTJP(C)__F~-'r,4 - ~AT/JD .47FT (.!','ASD/ ESD ACCESSION IM: A?3007823 S/0048/63/027/009/1203/1206 AUT11OR: Spivak, G.V.; Ivanov, R.D. TITLE: A mirror I tr microscope and its use$ for quantitative investigation of semiconductor Report 113~urt_i_ATi-Uuion Conference on Electron Microscopy haZ hc17Cin -Simiy* 12-1_~ March 1963/ SOURCE: AN SSSR, Izv.Ser.f.izicheskaya, v.27, no.9, 1963, 1203-1206 TOPIC TAGS: p-n junction , semiconductor , electron microscopy ABSTILACT: The paper is a general report on investigations of the width of p-n junctions and the potential distribution across them by means of a mirror elec- tron microscope. These investigations are part of comprehensive studies of p-n junctions on semiconductors by different techniques. The mirror microscope has been described elsewhere (G.V.Spivak and others, Izv,AN SSSR,Ser,fiz.,25, GS3, 1931). For -111v Dresent work therc was bult a special specimen holder with pro- ir~sion for applying a blocking voltage to the p-n junction, heating the specimen and ireasuring t:ie temperature by means of a thermocouple (see Enclosure) for khH .=rpasas one c'_ ic our-noses was to investigate the effect of temperature. The Card i, igg,56--63 ACCESSION NR: AP3007825 junction in mirror microscopes is visualized by displacement of the boundary of secondary emission across the junction incident to variation of the potential ap- plied to the semiconductor specimen. Actually the electric field emergingto the surfacc of the junction usually combines with the field due to a poorly conducting~ film that forms on the surface, so that the observed pattern is a superposition of; the two fields, which are characterized by different dependences on the teihpera~ ture of -the specimen (hence the interest in heating thespecimon). Six micrographs of germaniun surfaces are reproduced, as well as a family of curves-charactdrizing the variation of the junction width with applied voltage at 30, 60 and 1200C'% Some of the microph9tographs illustrate the results of heating. Orig.art.has: 6 figure& ASSOCIATION: Fizicheskiy fakultet Moskovskogo gos.universiteta im.M.V.Lomonosova (Physics Department, Moscow State University) SUBMITTED- 00 DATE hCP: 070ct63 ENCL: 01 SUB CODE: P11, SD NO Mr SOV: 006 OMR- 000 Card 2/6 SPIVAK, G.V.; IVANOV, R.D.; FAVLYUGHSNKO, O.P.; SEDOV, N.N.; SHVETS, V.F. Visualization of a magnetic sound-recording field by means of an electron mirror. Jzv. AN SSSR. Ser. fiz. 27 no.9:1210-1218 S 163. (MIRA 16:9) 1. Fizicheskiy fakulltet Moskovskogo 4osudarstvennogo universiteta im. M.V.Lomonosova. (Electron optics) (Magnetic fields) KROKHINA, A.I.; SPIVAK, G.V.; RESIETNIKOV, A.M.; ZHELNINSKAYA, R.I. Electron-microscopic study of the structure of ceramic materials revealed by ionic etching. Izv. AN SSSR. Ser. fiz. 27 no.9-. 1224-1-227 S 163. (KRA 16i9) (Electron microscopy) (Ceramic materials-Testing) 1 1 1 "Di(--, Struktur des 1, -retfe-des irmei+,alb der Doman-enwand, mit Hi-Ife des Spiegelek,tronenuii-k-fos--r~c,as sicii-.tbar gerzmc~t." report submitted to 3rd European Regional Conf, Electron Microscopy, Prague, 26 Al,'E'-3 Sei) 614. S F --i- -~,; G. V. ; G. V. 3 - Y~.KOV 1. V~. -". "Der Kontrast des R-ildes dies P-n -Cberganges in derr Rastelektronerimikrosk-oD." report submitted to 3rd European Regional CoInf, Electron ILIcroscopy, Prague, 26 A4-3 6h. DYIJK(N. V. ~;PIV4~~, (,. V.1; `S"~,J,CIV7 H. N.; YEVI.,tc)KIIA)V~ V. "I". "Ubur die Beobac lit Ling der dynwrdschen Vorgange in ier p-n TYberganger, m," Hii-fe vor. ftem ETni-ss4-.onelel~~'uror~erLaikrosko-T)." port submitted for '-rd European Regional- Conf, Electron kicroscGpy., re - - Frague, 2b Aug-3 Sep 6D 4. E i IVAKI) V. LIJIK7ii'diC)V~ It. "lYber das quantitative Studium der Emitter mittels eines Ho-ch-vak-Lium- Emissionsmikroskopes." report sWomitted for 3rd European Regional Conf, F~Iectron Microscopy, Prague, 26 Aug-3 Se-n 64. PYTIYEVA, M.B.; SPIVAK, G.V.; DUBIIJINA, Ye.M. Hig~-Vacuum ion ScUrce. Zhur. tekh. fiz. 39 no.1:142-145 Ja '64. (MIRA 17: 1) 1. Moskovskiy gosudar3tvennyy universitat imeni Lomenosovat fiziches- kiy fakulltet.