SCIENTIFIC ABSTRACT TRESVYATSKIY, S. G. - TRESVYATSKIY, S. G.

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• Collection: Scientific Abstracts
• Document Number (FOIA) /ESDN (CREST): CIA-RDP86-00513R001756520020-3
• Release Decision: RIF
• Original Classification: S
• Document Page Count: 100
• Document Creation Date: November 2, 2016
• Document Release Date: March 20, 2001
• Sequence Number: 20
• Publication Date: December 31, 1967
• Content Type: SCIENTIFIC ABSTRACT

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TREMATSKIY, S. G.
Cand. Tech. Sci;
Dissertation: "Yethod for Determination of Electrical Conductivity and its
application for invecti-gating Refactories at High Temperatures."
Yoscow Order of Lenin Chemicotechnological Inst.
imeni D. I. Mendeleyev
3 Oct. 49
80 Vechery-j~,,.-,,, (Ic V
71

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kmko --S.,
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W"t+
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,r ml op".

-11-~F-SV~ATSKIY,
BMINDY, P. P. ;
Fusibility diagram for the system YgO - Ca7p. Ukr.khlm.zhur.
19 no-5:552-555 153. (MM 8:2)
1. Moskovskiy khimiko-takhnologichaskiy institnt.
(S~rstems (Chemistry)) (Magnesium oxide) (Flnorite) (Fusion)

-.,, - - ,
I -~
-~ ~: -. - --l. - . --r. ~,
, '. 1- '. ~ -

BUDNIKOV, P.P.; TnSVYATSIKIY, S.G.
DiaUam of the composition of 0-TiO2
no-5:371-376 154.
1. Diyaniy chlew.AN URSR (for Budnikov).
(Sodium oxide) '(Titanium oxides)
.An
a7stems. Dap. AN URSR
MaA 8:7)

USSR/Chemistry - Physical chendstry
:Card 1/1 Pub. 22 25/56
Authors Budnikov, P. P,, Memb. Corres. of Ac. of So. USSR,; and Tresvyatskiyp S. G.
Title I Study of the structural diagram of GoOZ - Li
20
Periodical : Dok. AN SSSR 99/5.. 761-763, Dec 110 1954
Abstract I The presence in a GeO ?I - Li Osystem of Li 2GeO and Li GeO compounds with
meltin,~ points of 1237 and ?295,+30, respecti4ely, ua4 established by study-
ing the structural diagram of the above mentioned system. The two eutectics
I Ition and
discovered in the GeO9 - Li 0 system their percentage composL
orientations are desaribe2 A113olymorphous corversion of GeO in compounds
1 2
containing from 85 - 95 mol. "." of Ge02 and 15 - 5 mol. !4 of Li 0. was observed
at a 1035 t3o temperature. One German reference (1929-1931). 2~able; graph;
illustrations.
jnsti-~,,4~.ion The D. I. I-Iondeleyev Chemical-Technological Institute, Moscow
Subm.tted June 22, 1954

v~
BUDNIKOVSP.P.; TRWYYATSINIT,S.G.
Electric conductivity of typical refractory clays subjected to high
temperatures. Dop. AN URSR no.2:165-167 '55. (KLHA 8:11)
1. Diysniy chlen Akademil nauk URSR (for Budnikov) 2. Moskovelkiy
khimiko-tekhnologichnly institut imeni D.I.Mendeleyeva
(Refractory materials--Electric properties)

In t'

plact6 at 5- 10 ngtv to Oic tilectradts sc, h- E hc
gas,ts formed we-ep upV~Ird. prormfing the fused globult.
Gic,bules, sufficit-lit frA ptta-c analyses, were thus pjrcpd-
from Fe-O,. Cc~O, C -Cr.0%, MgCr-O., etc- Tlii-i
n-'eth"'d ri'W'j :-r 1 "! C" Oki& of low elec. '-ond -'t
70 P W)O' (, A;~,~',, M "OIL,

T-S
VMectrical conductiit, at high tempm-
f
U
7
!
~
~
-n�
v
Vls
turm P. 1. BudnikOv
b~
(Fireproof
Y-,1
K
Afes,10tu. 19-05, 20, M). This type of refractory often comes into
t
contact with electric heating-elements. & &raph relates the
logarith ru of the specific electTical Tesistance of corundum rofmctories
to ihe temp and the content of bnnd clay. rh~ highest tesirtance
is shown by conindinn ffomens mado without a bund (2-35 x 109
ohmicin ~t 700'). Those made with an addition of 2-S' clay
have a rrsiqtance tpprox. onf~-tenth of this, 1,4 the clad content
increases from 2-5',', to 20%, the resvitance de, -7-5 tinim
With 20-50"0 clay, the resistance is latgely indeperuient Of the

r
composition. its value approaching that of sp--cimens d f---
the aame !irodav. RUIT Can-,n. Rps. Ass. An R
....,.

F-SVI ATS Klyl
Meth of
R. oll'-Jlllly b;-s0
0 CqUiplutnE Dd PrGCMUrC fOr big
tilemal:1111lysb (m.p., up to '1200'. Tmp. i5 lneans-:
w,ith a W-Mo thermocouple. A Mo dish ifl 5URges"di
=
for M-Jting and an ckcUcmic gloteniommer for mcotding
tUmnoirrams. B, Z. KaiTAC-4

A~R -,mi

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137--1958-1-177
Translation from: Referativnyy zhurnal, Metallurgiy,,t, 1958, Nr 1, p 28 (USSR)
AUTHORS- Budnikov, P. P., Tresvyatskiy, S. G., Cherepancv, A. W
---------------
TITLE: Highly Refractive Oxides and Their Products (Vysokoogneupornyye
okisly i izdeliya iz nikh)
PERIODICAL: V sbornik Fiziko-khimicheskiye osnovy kera.miki, Moscow,
Promstroyizdat, 1956, pp 301-3Z4
ABSTRACT- Current views on the processing of raw materials, chirges,
molding, and sintering, and the properties and areas of application
of products made of highly refractive oxides melting at over 20000
A1203, BeO, MgO, CaO, ZrO2, ThO2, and CeO;,. In
accordance with the data of Hume-Rothery (Hurne-Rothery, W.,
Metallurgical Equilibrium Diagrams, London, 1952), practical
recommendations are adduced on the choice of material for
crucibles and the atmospheres and fluxes to be used in the fusion
of 45 different pure metals (from light ones such as Li, Na, K
and others to heavy ones like W, U, and others). Bibliography:
12.4 references.
Card I /I S~ G.
1. Refractory oxidav--t~pplicationa

V Y,~2 7--Zkt 'k
Translation from: Referati-rvy zhurnal, Metallurgiya, 1958, Nr 1, p ~~5 (USSR)
AUTHORS: Budnil-cv, P. P., Tresvyatskiy, S. G.
TITLE: A Method for Determiring the Temperature of the Liquidus and
the Solidus itl StAidies of Fusibility Diagrams and Phase Diagrams
of Highly Refractory Oxides (Metodika opredeleniya temperatur
likvidusa i solidusa pri izuch~erii diagramm plavkosti i diagrarnm
sostoyaniya vy5olcoogrieupornvkh ok*~slov)
PERIODICAL: V sb, -, Fiz.-khim. osnovy keramiki. Moscow, Proms troyizdat,
1956, pp 5ZO-536
ABSTRACT: Literature data are employed to set forth methods of determin-
ing the temperatures of the liquidus in systems where smelting is
done in air, in an inert gas atmosphere or in a vacuum, a method
of annealing and hardening, and a method of thermal analysis at
high temperatures with employment of high- temperature W-Mo
thermocouples. The latter method, developed by the Authors,
is described in greatest detail. Fusion and crystallization curves
of A1203, 3 Al? CaAl? and CaF~,
,q3, 2S'tO? , M9?- Si04, _ 04
obtained by the W-Mo thermocouple method, are adduced,
Card 1/1 Bibliography: 32 references. S. G.
1, 'A*efractory oxides-Temperature--Datermination 2. Ores--fto-
cess:Lnp_---'-Vquj=ent

p.p.; VOIDDIS, P.L.; TRESVYkTSKIY
BUDNIKOV, - ukr.khim.zhuroZ2
Roview Of data on the 878tem: Cael 2 -- Bac 12' (HjU 9:9)
no-3-292-294 156 ichlorides)

Tf j F_ :5 V yj# -F5 t< i~5' g-
PHASE I BOOK EXPLOITATION
83
AUTHORS: Tresvyatskiy, S. G., and Cherepanov, A. M.
TITLE: High-refractory Materials and Oxide Products
(Vysokoogneupornyye materialy i izdeliya iz okislov)
PUB. DATA.- Gosudarstvennoye nauchno-takhnicheskoye izdatel'stvo
literatury po chernoy i tsvetnoy metallurgii, Moscow,
1957, 246 PP-o 3,000 copies
ORIG. AGENCY: None given
EDITORS: Matveyev, M. A.; Ed. in chief: Badnikov, P.P.,
Academician; Ed. of the Publ. House: Rozentsveyg, Ya.D.;
Tech. Ed.: Vaynshteyn, Ye. B.
PURPOSE:. This book is for engineers and technicians working
with,refractory materials in the fields of metallurgy
and industries using high temperatures.
COVERAGE: The book provides data on the manufacture and uses of
high-refractory materials made from pure oxides and
presents'a method of classifying products made
Card 1/5

High-refractory Materials and Oxide Products (Cont.) 83
from alumina, zirconia, spinellides, oxides of bivalent metals,
actinides, lanthanides, and mixed oxides. The principal stages
of the manufacturing process are reviewed.
TABLE OF CONTENTS:
Introduction 5
Ch. I. General Information on High-refractory Oxide Products
1. Classification of high-refractory oxide products 7
2. Principal stages of the technological process of
manufacturing high-refractory oxide products 9
3. General survey of the properties of high-refractory
oxide products 42
4. Use of high-refraotory oxide products 61
Bibliography to Ch. 1. 66
There are Ill references of which 55 are Soviet, 50 English,
4 German, 2 Japanese.
Card 2/5

High-refractory Materials and Oxide Products (Cont.) 83
Ch. II. High-refractory Materials from Alumina
1. Manufacture and properties of alumina 70
2. Techniques of manufacturing products from alumina. 86
3. Use of products from alumina 99
Bibliography to Ch. 11. 102
There 64 references of which 47 are Soviet, 13 English,
4 German.
Ch. III. High-refractory Products from Oxides of Bivalent Metals
1. Products from beryllium oxide 105
2. Products from magnesium oxide 123
3. Products from calcium oxide 139
Bibliography to Ch. 111. 151
There are 106 references, of which 42 are Soviet, 49 English,
13 German, 3 unidentified.
Card 3/5 '

High-refractory Materials and Oxide Products (Cont.) 83
Ch. IV. High-refractory Products from Zirconia
1. Products from zirconia
2. Products from zirconium
Bibliography to Ch. IV.
155
182
188
There are 67 references of which 26 are Soviet, 33 English,
6 German, 2 French.
Ch# V. High-refractory Products from Oxides of Actinides
and Lanthanides
1. Products from oxides of actinides 191
2. Products from oxides of lanthanides 215
Bibliography to Ch. V.
218
There are 45 refereneps, of which 11 are Soviet, 30 English,
4 German.
Card 4/5

High-refractory Materials and Oxide Products (Cont.) 83
Ch. VI. High-refractory Compounds From Spinellides and
From Mixtures of Oxides
1. General characteristics of high-refractory
spinellides 220
2. Products from magnesia spinel 225
3. Products from mixtures of oxides 227
RLbliography to Ch. VI. 233
There are 27 references, of which 6 are Soviet, 20 English,
1 German
I
P43pendix I. Some properties of high-refractory oxides and
oxide products 237
Appendix II. Thermodynamic and physical properties of
oxides 240
AVAILABLE: Library of Congress (TN677.T67)
Card 5/5

TRESVTATSKIY. S.G. [Treaviatalkyt, S.H.]
Study of Ge02-'- Ha.0 state diagram [with summarv in Zngllshl.
Dop. AN URSR no.3:295-298 158. (MIRA 11:5)
l.Moskovelkiy khlmlko-tekhnologichniy institut. Predstavleno aka-
demikom AN USSR P.P. Budnikovym [P.P. Budnykovy-ml.
(Germanium oxide) (Sopium oxide)

AUTHOR. Tresvyatskiy, S. G. 131-2 3-5-9/16
TITLE: On the Influence of Vibrogrinding on the SinterinE_: of Active
Mhgnesium Oxide (0 vliyanii vibropomola na spekaniye aktivnoy
okisi magniya)
PERIODICAL; Ogneupory, 1958, Vol. 23, Nr 5. pp. 229-233 (USSR)
ABSTRACTu L. I. Trenin took part in the experiments. In previous
experiments it became evident that active magnesium oxide can
well be sintered, but is difficult to press in dry condition
and also by means of plasticizers. The poor compressibility is
explained by the particularities of the_wwder structure, in
figure 1 the photomicrography of a preparation is mentioned
which was produced from magnesium oxide, The latter was obtain-
ed by means of burning basic magnesium-hydrocarbonate at a
temperature of 12ooO to 13000, The material was burnt in pow-
der-form and was not ground afterwards. In photomicrography it
can clearly be recognized that the fine periclase crystals have
a longish shape of 10-15&1 A powder from such longish
crystals poorly deposits in charging and pressing, which ex-
plains its low bulk weight and its poor compressibility. A dry
Card 1/3 grinding in ball mills proved impossible here as the material

On the Influence of Tibrogrinding on the Sintering of Active 131-23-5-9/16
Magnesium Oxide
sticks to the walls. But it became evident that this does not
occur in vibromills. Furthermore the experiment for the purpose
of explaining the influence of vibrogrinding on the sintering
of active magnedum oxide as well as the processes occurring on
this occasion are described. Basic magnesium-hydrocarbonate
of the "Chistyy" type, corresponding to GOST 6419-52 was used
as initial material. From figure 2 it can be seen that by vibre-
grinding the bulk weight increases and the sintering improves~
In figures 3 and 4 the micro-structure of magnesium oxide pow-
der is shown after 30 or 6o minutes of vibrogrinding respective-
ly. It can be ascertained that the longish form of the crystals
disappeared and that they assumed a roundish shape. Then the
sintering of samples of ground and unground powder was invest-
igated. The samples were pressed dry under a pressure of 500
kg/cm2 and burnt in a vaccuum kiln. The results are illustrat-
ed in the table and figure 5. As can be seen from them the
sintering of vibroground samples begins at a temperature of
135o0 and is finished at 16ooO. For ungrorad samples the sint-
ering begins at 1450 0 and is not finished even 1t 18ooO. It
seems to be practical, to ascertain the microstructure and the
bulk weight of the powders before the processing, and also the
Card 2/3 volumetric weight of the unburnt samples, whioh-ghould

On the Influence of Vibrogrinding on the Sintering of Active 131-23-5-9/16
Magnesium Oxide
not be less than 0,5 - o,6 of the specific weight of the
material. There are 5 figures, I table, and 7 references,
all of which are Soviet.
AVAILABLE: Library of Congress
1. Yagnesium oxide - Sintering 2. Vibration mi33A - Applications
Grinding - Effectiveness
Card

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5(2)
AUTHORS: Budnikov, F. P., Corresponding MemberAS USSF4SOV/20-128-1-22/58
TresyZg,~~~ Yushakovskiy, V. I.
TITLE: Investigation of Phase Transformation of Uranium Oxides in Air
PERIODICAL: Doklady Akadamii nauk SSSR, 1959, Vol 128, Nr 1, PP 85-88
(USSR)
ABSTRACT: In the present paper the decomposition of uranoso-uranic
oxide occurring with heating was investigated, as there are
only contradictory data on this problem (Refs 1-6). The decay
temperature was determined by means of continuous weighing
of uranoso-uranic oxide in tabloid form or pulverized during
heating within the temperature range of room temporaturo up
to 16oo-i9OOO. The curves of change in weight of uranoso-
uranic oxide on heating and cooling in air are given in
figures 1 and 2. For the determination of phase composition
at different temperatures hardened samples were used~ The
results of investigation are given in table 1. The results
of two series of investigation indicated that uranoso-uranic
oxide loses oxygen to a large extent already at 9000. Howeverp
UP to 14500 the quantity of oxygen still corresponds to the
Card 1/2 formula UO 2.63- The radiogram taken of the oxide of this

Investigation of Phase Transformation of Uranium SOV/20-128-1-22/58
Oxidea in Air
composition differs from the radiogram of U 308' At still
higher temperatures, up to the boiling point, U 409 at
atmospheric pressure is in equilibrium with o4ygeh. The oxygen
content within this oxide decreases with temoerature increase,
This causes a lengthening of the lattice spacing (Fig 3). The
results found made it possible to complement the high-tempera-
ture range for the phase diagram of the U-0 system (Fig 4),
plotted by Akkermann(Ref 2). The samples UO 2,093' U02~14' and
UO 2.08 calcined within the vacuum (10-1 torr) at 1050, 1100,
and 16000 proved to be two-phase and consisted of U02 and U 4 09'
However, it is possible that the two phase,, found by the authm
during the decomposition of the solid solution have been formed
due to too slow cooling. There are 4 figures, 1 table, and
6 references.
SUBMITTED: June 2, 1959
Card 2/2

84699
vl' .214 2e
AUTEEORt Tresvyatskiy, S. G~
S/13 60/000/010/002/002
B021XBO58
TITLE: The Influence of the Structural Type of the
of Highly Refractory Oxides on the Relative
Temperature
PERIODICAL: Ogneupory, 1960, No. 10, pp~ 467 - 470
Crys-ta-l-Lattice
Sintering
TEXT: The results of experiments on chemically pure aluminum~lq
beryllium-0 an6biagnesium oxides are mentioned in the preseni paper. The
relative sintering temperature was assumed to be equal to the firing
temperature in 0K The dependence of the relative porosity on the rela-
0
tive firing temperature in K is shown in Table I and on the relative
sintering temperature, in Fig. 1. The values of the microhardness f th
oxides investigated were determined by'means of the JTMT-3 (PMT-3 )A
instrument. The dependence of the relative sintering temperature - d the
microhardness of highly refractory oxides on the type and energy of the
crystal lattice is shown in Table 2. The dependence of the relative
sintering temperature'on the energy of the lattice of highly refractory
Card 1/2

8h699
The Influence of the Structural Type of the 5/131/60/000/010/002/002
Crystal Lattice of Highly Refractory Oxides on B021/BO58
the Relative Sintering Temperature
oxides, related to the unit volume (U~, kcal/cm3) is shown in Fig. 2, and
the dependence of the microhardness on the same quantity, in Fig. 3. The
foregoing refers to the sintering of pure, highly refractory oxides of
the solid phase 1Lnd cannot entirely be extended to sintering processes in
the presence of liquid phases, nor to the sintering of oxides of non-
stoichiometric composition (such as Cr203; CeO 2)9 or to the sintering of
oxides with polyntorphous transformations (ZrO 2) . There are 3 figures,
2 tables, and 7 referencess' 5 Soviet and 2 German.
Card 2/2

5.'41*10, 21-1330 77219

AUTHORS: Tren~~~ Ku s ", a 1,-. ov sk i yI
_
TITLE: Melting Point Determninations in Air af,
of Uranium Oxides With Some Ot'.ner Oxides. Let-_=r
the Editor
PERIODICAL: Atormiaya energiya, !960, Vol 8, Nr 1, PP 56-58 (USSR)
ABSTRACT: An increased interest in interactions of u-_ranium cxide
with other oxides in air prompted this investigat-ion.
The authors used UO BeO, MgO, CaCO-.,, BaCO Al 0
2-1 3 " 2 3
La201.31 Sio 2 T'02' Zr02 Th02' Ce02 H3F02"' V~:p 5j Ta 2011
Bi O"~j cr 0 (mtl H WOL~, Fe and 11inco-
02MOO4 2 203J
2 2
3
or., tiiem classified as pure, analytically pureand
chemically pure. The degree of purity of Ta 0- and
2 ~)
v 205 was not certain. Equimolar ratio was taken, ex-
cept in case of oxides of Mg, Ca, Sr, and Ba ;,rhere
additional 1:2 and 2:1 molar ratio mixtures were pre-
Card 1/5 pared~. The mixtures were first heated in porcela4l,
U .1. ~11

Melting Point Determinations 1- 41_r Q
Binary Mixtures of U_"an_-*'~~,-, OxIde-s
Some Other Oxides. Letter to zrie Ed-'z;cr
containers at '3000 C, and formed into bricauets 2~,
in diameter, and then roasted at 800-900o C. 7'ne
briquets were afterwards pulverized and the proce(:t-re
repeated at 1,000-1,1000 C and_1,200-1,3000 C in
platinum containers. At 1,300- C the procedure ,,,-as
reneated until the briouets looked stable, sho-wed
no cracks, and did not shrink. Dell-erm-'Inatil-,r
melting temperature of mixtures. Except for r-_fxtures
which melted during prelim-inary roasting, the melt-ng
temperature was determined by method of cone deflorma-
tion. The cone vertex was heated in electrl_,~al arc
maintained between carbon elect-rodes. Temperature
measurements were taken a. microoptical pyrlor,-Ie-~Ier
with an accuracy of +30-500 C for specimens forming a
droplet, and +50-1007 C for those melting along the
surface with a hard to obtain droolet. Results are
listed in Table A. There is 1 table, and 1 Soviet
reference.
SUBMITTED: August 3, 1959 Card 2/5

Melling Point Determinations iri Air of 772-19
Binary Mixtures of Uranium Oxides With SOV/89-8-1-13/29
Some Other Oxides. Letter ~o the Editor
Melting temperstures 17.:, air of binary mixtures of
uranium oxides with other oxides
50
67
50
33
70
50
30
67
50
33
Card 3/5
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30 CaO
50 cao
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33SrO
50 SrO
67 SrO
I It
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111112
1/1.53
1/0,404
1/1
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1/0,4
1/0,93
1/2,37
See note Card 515
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Mcnj -th d,upicr

Melting Point Determinations in Air of 77219
Binary Mixtures of Uranium Oxides With SOV/89-8-1-13/29
Some Other Oxides. Letter to the Editor
67
50
33
50
50
00
50
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67 BOO 111,9 1 Gs)� 50
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50sio, 1/1 1770 -t- '3()
i4,,A).j- ~w
50 ZrO2 50
.50 Th02 lie 11:1"1111ITC11
50 CcO2 2700-L- 150
50 11207,
120(j.,:1350
Me IT. 7" 0 q-
SO-- t~
Deopit. ri ,ro- Po,mcd b.r nor ci-~
ftoAoly o-Asn th-L Prw,#V~ "Ixtuoc-
MtArs uijrh deiptcr Po,"a.-na,
w^ d,~Psz..(
M.Itt t&cj*jy
M-14 w.Th AO JtQi"'ti
- 1
i9i.,"r ace4 nD7- k"e.1tj L.4tjLf To T-4,
r , a , r,,,.,]
Card 4/5 See note Card 515

Melting Point Determinat ions in Air of
TlJnary Mixture-3 of Uran-u:~, 0- -IdCs W10h
Some Other OxIdes. Lotter Lo the EdItor,
a
C .-p.4 a T,on
...... - MIT.n )"odt-
U02 C-
A ~l ys,c
o& d r-
~A) X,2(15 84 1 Sli
!AX) - 10M
50
I I x 12(-X)
W H.
.-A 1 :10 Bi.0:1 A) M~Irs hlTle.) evcLoc.,rci
11.~
64&r1,%3
.5o
5(1
5t)
.14)
Ilk)
Card 5/5
I
185l) ~~A)
5()Silt). oc.,, r kh c j j, ),, rnf a,, 4 r r A
5u (:r-.(I:i -2115(1 J-. fix) 0;-Opi~t-; Prm WJA
W FA-10, 1370� ~31) M-Kc emstly
-A) .11110: : I I 6o W
HeT 1 !,700-27-~O:~- NO! VlFP*, LV t.,
In coses where chomical anDlysis wbs not perforr-ed,
changes in cherr.icq1 constItution were oractically
ne-ligible, with the exc~3ption of mixtures with
oxidos of bismuth, lood ond tin.

As-
AUTHORS:
TITLE:
PERIODICAL:
82285
S/08 60/00QV01/09/011
B014YB070
Treavy :akLy,,.~t G.. Kushakovskiy, V. I.-, Belevantsev,
V. S.
Investigation of the Systems BeO Sm9OA and BeO - Gj-223
Atomnaya energiyaq 1960, Vol. 9, No. 19 PP. 54-55
TEXT: The starting materials for the preparation of the sample had a
purity of 99.5 to 99.c The temperatures of still liquid and already
solidified melts contained in a molybdenum crucible were measured by
means of a tungsten-molybdenum thermocouple. By a chemical analysis of
the slowly crystall iZ4 ng alloy, the composition of the eutectic was
determined. The analySiS shows that the composition of the alloys is not
different from that of the layers. Microstructural analyses of molten
samples indicate that in the hypoeutectic alloys beryllium oxide
crystallizes first while in the hypereutectic alloys samarium and
gadolinium.'oxides do so first. If the lattice constants of beryllium
in thermally treated alloys containing oxides of rare earths are measured,
Card 1/2

82285
Investigation of the Systems BeO - Sm203 S/08 60/009/01/09/011
and BeO - Gd203 B014YI3070
no solid solutions are found in beryllium oxide. The eutectics contain
35 mole % of samarium or gadolinium oxide and 65 mole % of beryllium
oxide. The phase composition of the samples that contained much Sm203 and
Gd203 could not be determined roentgenographically. Samples that contained
0.5 or more mole % of be-7yllium oxide and were annealed between 13000C
and 15000C showed two distinct phases in reflected light. This supports
the theory that in the systems BeO - Sm903 and BeO - Gd203 in the
temperature range 1300-1'500'C solid solutions do not occur in the oxides
of rare earths. The phase diagrams of the above systems are reproduced
in Pigs. 1-3. The melting points of the eutectics of these systems are
lower than those of the ;aystem BeO - La.203. There are 3 figures and 3
references; 2 Soviet and 1 German.
SUBMITTED: January 7, 1960
Card 2/2

S1069~105~ 009/003/009/014
B006/BO63
AUTHORS: TresvyatskiLL_�_~ G., Kushakovskiy, V. I., Belevantsev
S
TITLE: Investigation of the Al.0 -'Sm OVIand Al 0 3-1
Systems 2.3
PERIODICAL: Atomnaya ertergiya, 1960, Vol. 9, No. 3, pp. 219-220
TEXT: In the introduction to the-present "Letter to the Editor"i the
wr-'itprs discuss the re3ttlt.a of other authors who have studied the systems
mentioned in the title. The main part deals with experimental determina.-
tions of the solidus and liquidus temperatures of these systems between
`700 and 23500C. For thii3 purpose, the authors used the high-temperature
thermal analysis accordin,3 to the method described in Refs- 4 and 5.
Sm203 and Od20 3 with not more t~.an 0.5% imPuritieH (other oxiden cf rare
earths), and Al20 5 of the type qAA(ChDA) served as starting materia.19.
The thermal analysis indiDated the following: The eutectic (Al 0,-.Sm 0
2 2 3
Card 1/3

82957
Investigation of the A! 2 05 - SM20 3 and 3/089/60/009/003/009/014
Al20 3 - Gd 2 03Systems B006/BO63
melts.from the ride of Al,,O at 1770 + 20, C (F'-,g. 1), while that of the
A 1 10, - Cd 0 syst5,m star'~s melting at 1760 + 200C (Fig. 2). From the
2 3
side of the rare-earth oxides, the eutectics reach their melting points
at 1860 + 20 0C and 1930 ~- 20 0 C, respectively. The compounds SmAIO and
30
GdAIO melt practically at the same temperature, namely, 2060 + 20 C. A
3
microstructural anal,,yrsis aft'er thz7- thermal s~,nalysin (in reflected light)
showed that in aj.joys having 0 '20 mole of rare-earth oxides A190
Crystallized fir~it; a It2S GfiAIO-; at '15 100
:~O
1 )n 2
3j,
e(itectic.)-'and bnt%eer: (0-and mole's of rstre-earth oxidQs
(high-melting eutectic),-. Samples containi'tig mor-0. than I cr less than
j9 mole% of such oxides.',were found to be two-phoise substances. The
LrjQ'ariant points of the two syst~~ms inv~?sti-gated (.above 17000C) are
li2~ed in a table and compared with the data published in Ref, 3. The
Ca-rd 213

82957
Invest.igation of the Al20.2 - Sm20, and S//089/60/009/003/009/014
Al,~O - Od 0 System.4 B006/BO63
e 3 2 3
numbering of the.poi*nts co:.Iresp.onds to that of Figs. I and 2. The results
obtained by the authors pal~tly agree with those of Ref. 3. There are
., figures, I table, and 5 references: 2 Soviet, 2 9S, and 1 British.
SUBMITTED: March 24, 1!)60
Card 3/3

BUDITIKOV,P.P.,; VOL40IIIN,I,.k.; TRESffATSKIY, S.G.
Ivestigating the clinkering and recrystallizatIon of pure wguesium
oxide. Ogueupory 25 no.2:70-73 160. (KERA 13: 10)
(Magnesium oxide) (Crystallization) (Clinker brick)

15(
AUTHOR-,
TITLE:
1'2R10DICAL-
ABS'.22ACT:
Card 1/2
S11 3116010001031GOV01 3
Tresvyatskiy, :3. G. B015/13005
On tile Role of Glo (j(' d Po 1,o -9 in the Sintcrinj-, of Purc,
Highly Refract6ry Oxitios
-17
Ogneu-iory, 1960?, ur 3, vp 130-132 (USSR)
A
To investiE;ato the rca.;oa.,; for the anoi:ialouc bchavior of
hiagnesiun oXide in sintc_-,i;,v,, tile author der;criboc the sinter-
ing conditions of active Maq;nosium-, beryllium-, and aluminun
oxide under similar condi'G."Loy,.q. The inveuti'~-,Jtion resul t 3 are
graphically reprc~;cnt-c.C. in fi,liires 1,2, and 3 which show th 0
dependence of real, o--)en V.-O, closed porosity on the wci('-,ht
by volume of the Tl.:.~ fine -tructure of the na(,nesium-
oyide sartiple is jAiown in fili~rc 0, In concluz.-ion, the author
states that the sinterin.- (if -tar-.iploo up to a hiCh density can
only take place in the absence of closed pores. If the closed
pores are mairtly situated along the crystal boundaries, this
process occurs at a sufficiently high rate, which is not the
case with tile formation of pores inside the crystals as can be
observed in the sintering of active magnesium oxide. There

0
On the Role of Closed Porosity in the Sintering, of
Pure, Highly Refractory Oxide.,,,
are 4 figures and 3 Soviet references.
Card 2/2
8/131/60/000/03/008/013-
B015/]JO05
117~11
01//

TRESVYATSKIT, S-G-, KUSHIKOVSKIY, V.I., BWAYARTSEV, V-S.
High-temperature thgrmal analysis using tungstic zolybde
thermocouples. Ognempory 25 no.4:180-181 160. (MIRA 13:8)
(Thermcouples)

TRESVUTSKIY2 S.G.
Determining sintering temperatures of highly refractory masses.
Ogneupory 25 no.f;:232-233 .160. (Mia 14:5)
(Sintering)

TRESVYATSKIT, S.G.; GRIMOV, V.V.; VOLODIN, P.L.; SEROV, K.M.
High-temperature vacuum kilns for calcinating high-strength
refractories. Ogneupory 25 no-7:313-316 160. (HIRA 13:8)
(Refractowy materials) (Kilns)

TMVYATSKIY, S.G.
11~- *,,.e
Nfect of the Otracture of the Qr78*Ll lattice of highly refractory
oxides on tho rolative temporatura of olinkoring. Opeupory 23 no.10i
4,67-470 16o. (Refractory materials) (MIRA 13:10)

so D029/DlOg
AUTHORS: Budnikov, P.P., and Tresvyatskir, S.(;.
TITLE: Methods of high-temperature thermo-analysis of oxide syste~.-:s
PERIODICAL: Silikattechnik, no. 9, 1961, 396-398.
TEXT: Static procedures such as the quenchin- method accordin- to Belyani-in,
D.S., Lapin, V.V., and Toropov, N.A. (Ref. 1:" The physical-chemical systc:;is
Of silicate technology, 2nd ravised edition, 1iloscow, Promstroiisdat. 195,14)
or the cone fall point method have found wide application for ti,e investigra-
tion of phase diagrams of highly fire-resistant oxides. The fall Point
method is easily applicable although the diagrams obtained must be considered
fusibility diagrams under given t,~-st conditions rather than Phase diagrams olf
the systems examined, according- to Balyankin, D.S., Lapin, V.V., and Toropov,
N.A. (Refl. 1.). The quenching method allows reliable results only if test
material forms glass on rapid cooling. If, however, the material has a high
crystallization velocity and does not form -lass on quenching, resul-,z; accord-
ing to the quenching method are not always reliable. The authors describe a
Card 1/5

2 r'. 2
!!~N 4
Liethods of high-temperature D029~DlOQ~
high-tommerature thermo-analysis which is largely free of the mentionc~d
shortcomings. The method is simple, reliable and permits the determination
of solidus and liquidus temperatures of -nell crystallizin:r melts oC "-';L~hly
fire-Droof oxides in the teal-Derature range of 15000 - 24000C with ~n exaci-
+
ness of - 100. The method is suitable fo- -naterial which does not reaC 4~-
with molybeenlam under purified helium, argon or nitrogen. Such sul-stances
are: BeO, -0, CaO, SrO A12031 2 3
La 0 , and oxides of the rare earths. S'021
Zr02, Th02, UG2. The method cannot be reco:.-.mended for systems cont-ain'ing
oxides which are reduced at high temperatures or which,in molten stage,
react with molybdenum, such as oxides of cobalt, iron, nickel, etc. The ar-
rangement of the thermoelements in the furnace, the consturuction of the 'ur-
nace, and the device for the mountinn- of the thermoolement are shown in
Fig 2. The upper part of the furnace was closed durinff the test ;,rith a
special hood according to Budnikov, P.P., Tregvyatski, S.G., Fushakovoki,
V.I., (Ref. 5: Lecture -", 12193 at the 2nd International Conference of the U110)
on Peaceful Application of Atomic Ener~7y, Geneve, 19;8) for the feeding and
distribution of the shielding Car. The hood was not used -at th-e be,-innin-
'I
Card 2/5

2,'1250
G/00 61/000/009/001//003
Methods of high-temperature ... D029YD109
in accordance with Tresv atski, S.G., Kushakovski, v.j., Belevantsev, V.S.
(Ref 4;, Ogneupory (19M no. 4, P 180-181). Satisfying results withou-:
1100d Wovlo, howtivor, obtained only if the solidus and liquidus temperatures
were at 2,OOOOC or below. &n aloctrouto oofiiponnatinn recorder P.PP-09 with
., cu r%, L
scale up to 10 mV was used for recording the heating, and coolitir -,.%,
Such curves are usually recorded with a palper feeding opeed of 6 mm/min.
The tests were conducted with a cooling and heating velocity of 20 - 80
degr/min. It seems important to stress the following facts: On recording
by an electronpotentiometer the thermoelement is grounded throuch the cir-
cuits of the apparatus. It is therefore necessary to isolate the furnace
and secondary coils of the transformer against the ground potential. If
thio in omittod, parasite electromotive forces appear in the thermoelement
circuit, produced by the thermo-ion and thormo-eloctron emission at high
temperatures. This parasitic EMF distorts the resulto of th(., rocordor. The
switching-on and the breaking of the heating circuit must have no influence
on the comDensation recorder. The whole arrangement thermoelement - potent-
iometer was calibrated according to the melting points of pure fire-proof
Card 3/5

27 250) G/005/61/00--/009/001/003
I'Viethods of high-temperatura ... D029/D109
compounds, For this purpose the following values were established:
MgAl204 2135�250C; A120 3 ~ 2050+-100c; 3A1203 - 2SiO2 = 1900tlOOC;
TA92S'04 1860�200n,; CaA'204 = 1600t5oc; MgSiO3 ~ 1563-~-20C; CaF2 = 141C.
10OC; MgO , CaO - 2SiO2 = 1391-+30C. Chemically pure initial ovides were
used for the proauction of binary and ternary compounds. The described
method can be used successfully for the investi-ation of phase diagrams of
metals, mixtures of metals and oxides, carbide, boride and similar systems.
In such cases, however, the molybdenum plz--te -.-.ust be coated with a metal
oxid-e, a high-temporature enamel or a similar substance in order to avoid
its melting and fi,,sing with the substances tested. There are four figures
and 5 Soviet-bloc references.
ASSOCIATION: Chemical-technological Institute ".D.I. Mendeleyev", Yoscow
Card 4/5

s/oF,1/62/000/003/047/090
B156/3101
AUTHORS: Budnikov, P. P., TresvvatskjZ._Z,.G.
TITLE: Procedure for high-temperature thermal analysis of oxide
systems
PERIODICAL: 'Referativnyy zhurnal. Khimiya, no. 3, 1962, 370-371,
abstract 3X182 (Poroshk. metallurgiya no. 1, 1961, 75-81)
T=.L- A. pro-cedure is described for the high-temperature thermal analysis
of oxide systems. A tungsten-molybdenum thermocouple, with a small
molybdenum plate relded to the junction to serve as a crucible for the
substances being investigated, is recommended for determining the solidus
and liquidus points between 1500 and 2400 00. The furnace used for heating
0
to 2400 C has a heating tube made of electrographite, the tube is fitted
with(a special system of baffles to develop a circulating flow of inert
gas argon, helium, or pure nitroeen) which is fed into the furnace from
above. This baffle arranCement prevents carbonization of the thermocouple
and the contents of the crucible from the gaseous phase. The procedure
Card 1/2

s/081/62/000/00'-"/047/090
Procedure for high-temperature ... B156/B101
provides good results -,hen determinin.- the solidus and liquidus points for
systems in substances which do not react with molybdenum up to 24000C.
LAbstraoter's note: Complete trunslation.]
Card 2/2

-50
-2.1
31610
S106 3/61/006/006/00 2/0 016
A057/AI26
AUMORS: Tresvyatskiy, S.-G.,_, Doctor of Technical Sciences, cherepanov. A. M.,
Candidate of Technical Sciences,
TITLEi Highly refractory systems with oxides of lanthanides and actinides
PERIODICAL,. Zhurnal vsesoyuznogo khimicheskogo obshchestva imeni D. I. Mendele-
yeva, V. 6, no, 6, 1961, 612 - 618
TEXTt A review of literature on oxides of lanthanides and actinides with
other highly refractory oxides is presented and discussed. This discussion of
phase diagrams is of practical and theoretical importance,.since oxides of' rare
earth elements became valuable not only in atomic industry, but-also in the-manu-
facture of various highly refractory materials with special properties. Since
tha-phase diagrams are still insufficiently developed, some of themare.only ten-
tativej International papers,containing phase equilibrium.diagrams of systems
with U02,.Th02, Sm2031 Gd~03, Ce02_ZrO2I-ZrO2-La9O3-and Zr%-Nd~03 are mentioned.
Based on the presented review and discussions the following tentative general con-
clusions were drawn by the authors- Apparently all 3ystems of four-valent actinide
oxides with beryllium-oxide are simple eutectic systems in the temperature range
Card 1/4

31610
S/063/61/006/006/002/006
Highly refractory systems with... A057/A126
of the Bolidus and liquidus. Formation of solid solutions, or at high temperature
stable compounds could not be observed. Systems with magnesium oxide are probably
also simple eutectic systems, but here the formation of solid solutions with a
limited solubility at the side of the actinide oxide is possible. Systems Wit-b-
calcium oxide contain a liquidus of an eutectic type and a region of solid sahi-
tions at the side of actinide oxide. In these systems formation of melting (w,_tk!
decomposition) compounds Is possible, but this question needs some further in-
vestigations. Systems with aluminum oxide are analogous to systems with beryllil=
oxide. Systems with zirconium dioxide are characterized by wide regions of solid
solutions of two types,iA, based on actinide oxide and on zirconium oxide., w1th a
two-phase region of these two solid solutions at intermediate concentration-Q.
Characteristic for actinide oxide systems is the formation of solid solutionz w_-n
an almost infinite solubility in the solid state. Systems with actinide oxid--s'
and S102 are characterized by an eutecticum close to S102 and by the formation. oft"
orthosilicates of the type AcS104, melting with decomposition below the -tempera-
ture of the liquidus. In systems of actinide oxides with oxides of trlvalen~ T-6T'e
earths a region of solid solutions is formed on the side of actinide oxide having
a two-phase region of the solid solution and Re~~03 (Re = rare earth) at- the side
of the rare earth oxide. In relation to systems with oxides of trivalent rare
card 2/4

31610
S/063/61/006/006/C)02/Tj6
Highly refractory systems with... A057/A126
earths,the following conclusions were presented: Systems with beryllium oxide are
eutectic and analogous to systems with actinide oxides but they have a very low
melting temperature of the liquidus (about 1,450 - 1,5000C). No investigations
were made yet on systems with oxides,of magnesium, calcium, and strontium. Cna-rac-
teristic for systems with aluminum oxide is the formation of compounds of the type
ReA1031 melting without decomposition above 2,OOOOC, and the presenc.e of two eutec-
tica, one between Re203rReAlO 3 and the other between ReA103 -A1293- Apparently no
solid solutions were formed between the components in these systems. Systems with
zirconium dioxide are characterized by wide-regions of solid solutions,- anddiffer
from other systems by complexity. They.are not yet suffIciently investigated.
Systems of rare earth oxides between themselves are not investigated, but the
authors assume the possibility of the formation of regions of solid solutions,
soluble in the solid state almost to infinity in these systems. Systems with S102
are characterized by the formation of three silicates* and the presence of a wide
regioR,of immiscibility in the liquid state at the side of S102, The authors
point out that the conclusions presented are only tentative because of the Insuf-
ficiency in investigating the whole discussed matter. There are 17 figures, an
30 references: 11 Soviet-bloc and 19 non-Soviet-bloc. The references to the 4
most.receni EnglishTlanguage publications read as followsi P. E, Evans, J. Am.
Card 3/4

Highly refractory systems with.-.
Ceram.j Soc-, 43, no. 9, 44&-(1960); E.
for Ceramists. Part. 2, USA, Ohio,,1959,
Soo.,, 40, no. 1, 15 (1957); F, Alfred,
no. 4, 199 (1959).
31610
S/063/61/006/006/002/GC5
A057/AI26
K. Levin, - H. - F- Mcfftidic, , Phase Diagrams
C. Curtis, J. Johnson, J. Am. Ceram,
A. White, Trans, Brit. Ceram. Soo., 58.
card 4/4

s/o8o/61/034/003/001/017
k5_7/A129
AUTHORS: Budnikov, P. P., Marakuyeva, N. A., Tresvyatskiy, S. 0.
TITLE: Effect of the composition of the binder on properties of mixes in
hot-casting of ceramic products
PERIODICAL: Zhurnal prikladnoy khimii, V. 34, no. 3, 1961, 492-497
TEXT: The effect of the composition and amount of the binder on rheologic
properties of alumina-containing ceramic mixes on paraffin-wax-stearin base
binders with oleic acid admixtures was investigated. The quality of hot-cast
ceramic products used in electro- and radio-ceramics and refractory materials
depends on the cast mixes, which represent thermoplastic suspensions of a ceramic
material in the binder. For the latter various thermoplastic organic materials
with low melting point were used (paraffin, paraffin mixtures with wax or stearin,
and oleic acid admixtures etc ). Studying the structural viscosity for rate
gradients until 80 - 100 sec-1 and the casting ability of mixes furnished on fine-
grade skeletons (mean grain diameter 1-5~0 and paraffin-wax-stearin binders with
oleic acid admixture, abnormal viscosity, i.e., thixotropy in stearin and paraffin-
stearin mixes and dilatation in wax and paraffin-wax mixes was observed. In
Card 1/7

s/080/61/034/03/ow/07
Effect of the composition of the binder ... A057/A129
casting under pressure of 2-8 atm. mixes with a binder containing 8% paraffin,
12% stearin and 3% oleic aoid had, due to thixotr6py, a more than 1.5 times
higher fluidity than the other mixes investigated. The last-mentioned composition-'
of the binder is also recommended for casts with greater height (400 - 500 mm).
The strength of casts containing 15% stearin in the binder is 20% lower in
comparison to casts with a binder containing 15% wax. The present study on the
important effect of composition of the binder on properties of mixes was made
since few data are published in the literature related to this question, and no
information at all is published on properties of fine-grade mixes (1 - 1.5/A).
In some investigations, as published by P. 0. Gribovskiy (Ref. 1: Goryacheye
litlye keramicheskikh Izdeliy [Hot casting of ceramic products], Gosenergoizdat,
M. [19561), tiscosity was determined with an Engler viscosimeter and thus abnormal.
changes in viscosity of highly concentrated suspension effected by changes in
pressure were not observed. As structure-forming agent in the present investi-
gations "koraks" N = 320 ground with water for 6 hours in a vibration mill was
used. The grain size of the powder was determined turbidimetrically and was
found to be: 50 - 40p, 5%, 40 - 301.4, 4%, 30 - 20/,t, 11%, 20-10 21%, - 10 - 5/,w
25%, below 5/4, 34%. Specific surface of the powder was 1.05 49, i.e,, the
mean grain diameter was about 1.5/k determined by the method of diluted air
Card 2/ 7

S/080/61/034/003/001/017
Effect of the composition of the binder ... A057/AI29
filtration described by B. V. Deryagin et al. (Ref. 5: Opredeleniye vneshney
udeltnoy poverkhnosti poristykh tel po metodu filtratsii razrezhennogo vozdukha
(Determination of the external specific surface of poroiis materials by the method
of filtration of diluted air), Izd. AN 838R, M. (1958)). Homogenized paraffin
was used as binder (melting point 530), natural wax (softening point 48-520C),
and stearin (melting point 560C). The latter was of the commereial grade and
contained stearic, palmitic and oleic acid. Viscosity of the mixes was determined
by a rotating viscosimeter (with inner rotating cylindero of the Volarovich
system (Ref. 6: Tr. Poligraph. inst. OGIZ [19377), and the structural viscosity
shear stress V, and rate gradient D were caleulated from corresponding
7
0'rmulae. Fluidity for casting conditions under pressure ~2-10 atit), i.e., for
rate gradients thousand times higher than measurable on the Volarich viscosimeter,
was estimated by measuring the filling depth of a spiral-shaped cavity (4 x 4 mm)
with the mix at 2, 4, 6, 8, and 10 atm. The strength of the casts was determined
by torsion tests on rod-shaped test samples. Fluidity eurves (Fig. 1) of mixes
with 29 vol% binder show an abnormal character. The paraffin-base mix is similar
to a Bingham system and near to a Newtonts liquid, while the-.wax-base mix shows
dilatation, i. e.,an increase in the rate gradient effectB an increase in struc-
tural viscosity. The stearin-base mix shows thixotropy. The effect of shear
Card 3/7

S/08/061/034/003/001/017
Effect of the composition of the binder A057 A129
stress on structural viscosity of paraffin-, wax-, and stearin-base mixes is
shown in Table 1. Curves on the effect of pressure on structural viscosity fc
mixes containing 8.5% of a two-domponent binder demonstrate a similar character
of paraffin-wax-base and wax-base mixes, I.e., increase in structural viscosity
with pressure. Paraffin-base mixes, on the other hand,are like stearin-base
mixes showing thixotropy, i.e., decreased in structural viscosity with Increasing
pressure. This property is convenient for pressure casting. Curves on the effect
of the composition of the binder on structural viscosity (Fig. 4) show for
paraffin-wax base mixes a minimum at 25% wax content in the binder. Structural
viscosity of paraffin-stearin-base mixes increases withAhe stearin.content in
the binder. for a pressure range until 16,000 dyne/cm2 (F;lg. 4~. Structural
strength of casts decreases by adding stearin to paraffin-base binders. The
optimum composition for pressure casting was found to be 85% paraffin and 15%
stearIn binders. The greatest strength is observed in casts based on paraffin-
wax binders. Surface-active oleic acid decreases the structural strength.- but
has a positive effect on the fluidity of the mix. Optimumlamount of oleid acid
admixture is 3 weigbt % of the binder. Curves obtairied.for the casting'ability
of mixes under pressure (2-8 atm~, estimated by the cavity-filling test, are
linear and indicate that stearin-containing mixes have a much higher casting
Card 4/7

-S/080/61/034/003/001~Q;7
Effect of the composition of the binder ... A057/AI29 z_
ability than paraf f in- or paraf f in-wax-base mixes in spite of the higher viscosity
of stearin-base mixes measured on the viscosimeter. Thus it can be stated'that
structural viscosity data are insufficient for the selection of optimum oomposi-
tion if obtained only at small rate gradients. Also Engler's viscosimeter is not
convenient for estimations of the quality of cast mixes. There are 7 figures,
2 tables and 6 references: 4 Soviet-bloe'and 2 non-Soviet-bloc.
SUBMITTIED: September 30, 1960
Table 1: Value's for the structural Viscosity of mixes at 800c:
shear'
Viscosity
stress (In dyne/cm~2)
(poise) at
Type of binder in the mix 2,000 6,000 10,000 12,000
Paraffin 75 60 60 -
Wax 127 145 155 157
Stearin 3,000 1,080 520 320
Card 5/7

PENIKOVSKIY,'Ladimir Vladimirovichj SAMSONOVI G.V., otv. red.; TREgVYATSKIY,
_5,G._, prof., doktor tekhn. nauk, otv. red.; POKROVSYMA,'-Z-~~., --re-J-.,-
YEFIMOVA, M.I., tek:hn. red.
[Effect of radiation on metals and certain high-melting materials]
Deistvie oblucheniia na metally i nekotorye tugoplavkie materialy.
Kiev, 17,d-vo Akad.nauk USSR, 1962. 182 p. NIRA 15:7)
1. Chlen-korrespondent Akademii nauk USSR (for Samsonov).
(Metals, Effect of radiation on)
(Materialn, Effect of radiation on)

VT,SIffATSK.1-Y, _S.G.
113ome mathematical interrelationshios r)bs,.,rvrd in gintering high meltlmg C.-ides."
Paper presented at the Powder Metallurgy Conference
Smolenice, Czech. 17-20 Sep 1962

YERMENKOY V.N.,, otv. red.; FRANTSEVICH, I.N.p red,; SMISONOV,
G.V., red.; PISAMZKO,, G.S., red.; FEMCHEVKO, I.M.,
red.; TRESVYATSKIY, S.G., red.; IVASHCRENKO Yu.N.,, red.;
POKROVSKAYA,'-Z.~,'j red.; RAKHLINA, N.Pep tekhn. red.
[Surface phenomena in melts and in processes of powder
metallurgy] Poverkhnostnye iavleniia v rasplavakh i pro-
tsessakh poroshkovoi metallurgii. Kiev, Izd-vo AN Ukr.
SSP, 1963. 377 P. (MIRA 17;3)
1. Akademiya nauk URSR, Kiev. Instytut metalokeramiky i
spetsiallrjykh splaviv. 2. Institut metallokeramiki i
spetsiallrifth splavov ki Ukr.SSR (for Yeremenko).

YE,HMrP-,NKOP V.N., otv. red.; FRANTSEVICN, I.E., red.; Sk.=NOV,
G.V., red.; r(A.; FIEDOITIOIKO, 1,11.,
red.; TRESYIATSKI',,S.G., red.; PiASHUIENKO, Yu.116., red.;
POK-ROVSKAYA, Z.S.) red.
[Surface phenomena in melts and processes of powder R.-etal-
lurg-v] Pove-.-khnostnye iavleni-ia v rasplavakh i protsessakh
poroshkovoi metallurgii. Kiov, Iyd-vo AN USSR, 1963. 456 p.
(14IRA 18:1)
1. A&ademiya nauk URSH, Kipir. metal.3nLreramll- -'
spetniallyVkh splaviv. ", Institut metallokeramiki i spe-
taialln,ykh splavov AN Ukr.SSR (for Ivashchenko, Yeremenko)

M-m-'r-

M5~
777"-.
debermi7led, as Ix-is their electrical resistivity at 1400C. "Pie crystal-optical pr,)Pt-r--
'"EM
v-
OR :~Nl '-'55N~

X
4;50 WT, -RM-R!

Z-Mves aar.& ca rn ce- OT
~Rh i i , 0
N515

5-A

EN . . .....
ORION' MW`~

4
system
motaUc W, 1963. Voprosy*
teo-cli i primenoniyaredkozemej'ny*kh n-t.*-Wlov (Prowe.:.i3 in um U'-M;ui:y - 'i" ~.(
eart-1, maialil - mabnfalv* Mlogoow, lzd-va Nauka, 1964, 159-162
rL~ qr i np~ s Lne of eatigauons at me
S,, 6Le 11, i;-~ rii, -)r. ~;n--
rrardnrrnations, as weLl as tne iip-icius

-A !
TT ED -ul 6
L) E N m
OEM
81 IN

15261-65
ACCESSION INR: AT4048710
rt c
1400
4w
Card 3/3
a
gucLOSUR& 01
b
t SC
T
La III
40
WL 18~-
'joa. wt- rA2133
Figure 1. PhiLse tbagT,,Lrj of the 1
-aq(),Cr,,O, svstym.
..........
p- -- -A
NAZI.
MOM.

YAINAK 2 0. F. , S.G. ~Trujvlatsllqi, &PNIP [,6klm. naa-
'Ti PIMA= -~. -
Study of the arall-Itizat-2--cm pro-cesa in the -p,-)T:~ela5m ma-6:5.
-1-:7 Lr e , rit-I
proM. no.2g6C - I
I I ~ .3 04. , j

C~~ e S D 1 2 DD C I F U
ade-quately st,,--idled- Othe-. alithorg have es-t;ablished the, dependence
-n, ~- - , ~ , - :~r- ! .,- p - I at I v I tleF,

L 41217-65
17 7
~,qp
RPYIWWR--~
MOM- Prr -*lm-1111,
2 -E R, W
k

PARKHOIENKOp M.A, [ParkhomerAo m.p.j; YAREI/"PNKo Z.A. [ILremerik-o. Z.0,J;
TRESTfAMY-I-7. S.G, [Tj' yi. S. H. I
resviatslk- ,
Wev synthetic minerals of the mica group. Dop. AN 11FOR no.5:6.24-
627 '64. (MIRUI 17:6)
1- Irl3titut- metallokeramiki i spetsiallnykh splavov AN UkrSSR.
Predsta,krleno aleadamikom AN UkrSSR I*N*Frantoevichem [Frantsevych,
I.M.],

i085b_66 Err M W /['-'~'P` V ~/ T/Plo,"t/RP( k )/EWP( b )/L'W A\' c_'P c
'Irvifm
ACC NRi APS028715 SOURCE CODE: UR/0363/65/001/011/1878/1882
q il I ~- ~- V 7 1- C-- -
AUTHOR:
aj;s~4y emenko, Z. A.; Lc L~.M.; SokolovrA:i V.' A.;
I V_a~ G. Tar
Karpanko. V. Ya.
ORG: Institute of Materials Science Problems, Academy of~Sciences SSSR (Instittl
problem materialovedeniya Akademii nauk SSSR)
pe c ase stals
TITLE. Some physicochemical properties of synthetic ii 1 single cEZ
SOURCE: AN SSSR. Izvestiyao Neorganicheskiye materialy, v. 1, no. 11, 1965,
1878-1882
TOPIC TAGS: magnesium oxide,-~ingj,!~__pry~t~kl. ystal
2Rtic or
ABSTRACT: Th Ie-mi.crohardness, microbirttlenesgi, chemical stability, transmission spec
V trum, and working of synthetic magnesium oxide (periclase) single crystals were stu-
died. The crystals are characterized by microhardness isotropy which amounts to
926-946 kg/mm. They are more stable to attack by acids and molten alkali metals thpn
are polycrystals.or sintered MgO.- Single-crystals plates can te diffusion-welded/lit
1600720000C with a holding tJ'me of 30 to 60 min, and the weldirg seam obtained is op- -
tically transparent. Heat shock causes splitting of the single crystals along the
cleavage plane. HgO single (mystals are suitable materials for prepariqg optical win
dows, lenses, and prisms for the 0.3-7.0 v spectral range not only-at low but pro-
UDC: 546.46:548.55
Card 1/2
IL

ACC NNi APS028715
10
i
also at high temperatures as well. This must be verified by further studies.
'Objects made of MgO can be polished by combining mechanical and chealcat methods of
treatment. Orig. art. has: 5 figures, I table.
ORIG REF*. 002/ OTH REF-t 000
SUB CODE. 11,07/ SUBM DATE,. 24Apr65/
CID
tit

1:19257=46 EWr(l)/
ACC NRa kp6ool-303 SOURCE CODE: UR/0363/65/001/008/1368/137
S.
AUTHOR.- Lopato. L. M.; Yaremeriko. Z. A.; Iteavyatsk G.
gmy of Rej ~:es I rSSR (Institut problem 1
ORG: Inatituta of Afatgrials Science Problems,_&qo Pne
materialovedenlya Akademii nault UkrSSR)
TITLE: Study of the optical properties of compounds formed in the systems LnZO,3-SrO and
Ln203-BaO
SOURCE: AN SSSR. Izvestlya. Neorganicheskiye materialy, v. 1, no. 8, 1965, 1368-1371 1
TOPIC TAGS: crystal optic property, strontium compound, barium compound, samarium
compound, europlum compound, gadolinium compound, terbium compound, dysprosium
compound, yttriurn compound, erbium compound, thulium. compound, scandium compound,
lutetium compound
ABSTRACT: The optical properties: of crystals of type SrLn 0 and BaLn20 where Ln
Sm, Eu ~0- 4powders by tte
,, Gd. Th, Dy,, Y, Er, Tm-,Lu, and So, were studie n immersion
method and on polished sections. The refractive indices of SrLaq0A where Ln = Sm, Eu, Gd,
Tb, Dy, Sc were-Within the range ol'values exhibited by the orWal 2jides2,7whereas the
refractive indices where Ln =*Y, Ho, Er, Tm, Yb, Lu were higher by an average of O.Od
This indicates that the crystal lattices of these two sets of compounds differ In some res.",
1/2 UDQ 546.651431 + 546

L 12057-66
ACC NR1 AP6001303
even though the structural typa Is the same. ne crystal-optical characteristics show that
these compounds belong to the,calclum ferrite type. On the basis of the data, the existence of
a now type of substructures is postulated for compounds of this class. These substructures
belong to the rhombic class of eynunetry, but have a hexagonal-type unit cell. Orig. art. has-
j figure and 3 tables.
SUB COPE: 07, 11/ SUBM DATE: OlApr65 ORIG REF: 002 OTH REF.- 007
Rare' E'aAh ilements_.6.~5 jr7
Card 2/2

LOPATOp Lol4s; YANOM,~-Z&A,j TMSVrATSKnt Mo (Treaviatolkyi# Bails]
Interaotion of rare-earth-oxidet-irith strontius oxide#
Dops AWMA--nosIlt-2493-147 1656
I (MIRA ldtl2)
1# Institut problsm materialovedeniya AN WSM.

L L�2~-66 EWT(m)/T/EWP(t) IJP(c) JDIJG
ACC NRs AP6007250 (A) UR/0363/66/002/002/0269/0274
~3
)AUTHOR: TresvyatskIZ, S.G.; Pavlikov,_.V.N.; LoRato,_L.M.
ORG: Institute for Problems' of 14aterials,AN UkrSSR (Institut problem
material-ow-e-Uenlys. 11 UkrSSKJ I
~TITLE: Phase diagram of the system S0203-~~,r223
55 -11 _
SOURCE: AN SSSR. Izvestlya. Neorganicheskiye materialy, v.2, no.2, 1966
269-274 - -------
TOPIC TAGS: scandium compound, chromium compound, alloy phase diagram,
."J-os J,..+ 44A.6'4-,.~_ 4- k Al-t
ABSTRACT: IPha6.e'Jra1Jzf2rm1a&10n_0 In the scandium trioxide-chromium triox.
ide system were studied In samples subjected to heat treatment in a high
temperature furnace in an argon atmosphere. A phtographic investigation
was made by the conventional method with penetrating and reflected light
in the latter case with the use of etching in a melt of KHS94 at 20000 q
for 2 to 3 min. An X-ray Investigation10was made on URSma55aPand URS-70"
apparatus. Infrared spectra of the alloys were obtained on UR-10
spectroscope over an interval from 400-700 cm-1. The'change In the oxid(
content during heat treatment was controlled by conventional chemical
,analysis. The article gives a phase diagram based on the experimental
results, a table showing the X-ray results, and microphotos of the sam-
.1 Card 1/i~_ UJJ(;; Si4i .145.e

L 238o5-66
ACC NR. AP6007250
ples. There was observed the existence of a compound which melts at
2130t 3000. The probable (,,.omposition of this compound is: Cr203/Sc203
1:3 or 1:4. The initial oxides form solid solutions based on chromium
oxide with a specific solubility of chromium oxide in scandiUM Dxide is
10 mole %. With a decrease In temperature the specific solubility de-
creases to 17 mole % scandlum oxide and 5 ;Ole % chromium oxide. Orig.
art. has: 6 figures and 2 tables.
l
SUB OODE: 11/ SUBM DAT13: 05JU165/ ORIG REF: 005/ OTH REF: 008
Card 2/2
.

ON 11,
ON`
M-
i~_. N~ Ns,

L-36402-66 EWT (m)/T/EWP (t)/ET1 JJP (C) JD
A6CN_Rs A-P'-6018776 (A) SOURCE CODE: UR/0070/66/011/003/0459/0463
AUTHOR: Tresvyatskiy, S. Yaremenko, Z. A.; Lopato, L. M.
ORG: Institute for Problems in Materials (Institut problem materialovedeniya)
TITLE: Crystal optical properties of synthetic periclase single crystals
SOURCE: Kristallograflya, v. 11, no. 3, 1966, 459-463
ITOPIC TAGS: crystal optic property, single crystal, x ray diffraction analysis, ab-
~sorption spectrum
ABSTRACT: Large single crystals of periclase were grown by directional solidification
and their crystal optical properties were studied. The directional cooling resulted im
columnar crystals having the crystallographic growth axes 94, 93 and g2. Cubic shaped
crystals adopted 94 as the growth axis while 93 and 92 were typical of elongated crys-
tals. The crystal dimensions along the growth axis were 50 mm and 20-30 mm along the
cross section. Generally, the synthetic periclase crystals were transparent; only in
some cases did they appear cloudy as a result of micropores, (0.01 mm) or mic=cracks.
Photographs and micrographs of the crystals are shown. Negative crystals (gaseous in-
clusions having crystalline forins) were observed and micrographs taken in the center of
these showed a continuous mosaic structure. The crystals had a glassy shine and a Kohx
hardness of 6. Chemical analysis revealed an impurity concentration of 0.01. to*0.5%;
Card 1/2
UDC: 548.0 : 535/32

L 36402-66
ACC NRi AP6018776 (f7
further re
Al, Fe, Si and Cr were the residual impurities. Vacuum annealing to 220010C further re
duced the impurities. Refraction and birefraction were observed to occur in the crys-
tals. X-ray measurements gave '4.212t0.002 A as the lattice parameter of the primitive
cubic cell. Chemical and thermal etching was done in order to bring out the mosaic
structure (0.1 to 0.01 mm) and the screw dislocations emerging at the surface. Fur-
ther x-ray analysis showed the mosaic block dimensions to range from 0.01 to I M, the
angle of misorientation to be 50 and the dislocation density to be about 105-106 cm-2.
The absorption spectrum of the magnesium oxide crystals was measured for wavelengths
ranging from 2 to 25 p. From 2 to 6 u the absorption was absent, from 6 to 10 is it
dropped shuyly and ft 10 to 25 u it was very strong. orig. art. has: 6 figures.
SUB CODE., 20,11/ SUN DATE: MprW ORIG REF; 902/ OTH PEFt 002
rd 2/2///,.,~/:~'
'N.

EVITW/EwPMATI IJP(c) JD
Uk/66/66/002/007/1240/1243'.
ACC NRj ii~p6o23917 SOURCE CODE:
AUTHOR: Shevchenko, A. V.; Lopato, L. MT.; Tresvyatskiy, S. G.
ORG: Institute of Materials Science Problems, AN UkrSSR (Institut problem materialo-
veden3`y`a__X77Jk_rWR7
TITILE: Phase diagram of the GdZO~-Crpl~ system
SOURCE., AN SSSR. Izv. 'lleorg-laterikly, v. 2j no. 7, 1966, 1240-1243
TOPIC TAGSz gadolinium compoundv phase diagram, chromium compound, chromium oxide
ABSTRACT., X-ray, microstructurall and chemical analyses as well as iru'rared spectros-
copy were used to study the phase relationships in the Gd203-Cr20j system in the 1600-1
24000C range. The phase diagram obtained is shown in Fig. 1. It is shown that the
system contains only one congruently melting chemical compound, GdCrO~,, which has a
melting point of 235)�300C- The compound forms eutoctics; the eutect.'.c with Gd2c,-A is
.Cic 1
comoosed of 77 mole % Gd20~A and 23 mole % %0~ and melts at 206#2001.,; the eutect,
vrith Cr203 is COMPOsOd Of 15 mole ','0' Gd2~ and 95 mole % Cr203. and melts at M&300C.
Some physicochemical properties of gadol niwn chromite (density, coefficient of linear
thermal expansion, crystal optical proportios) woro determinod. Orig. art. has: 3 fig-~
ures,
UDC

L 46242-66
ACC NR, AP6023917
0
23D0 -
8*1 N
Fig. 1. Phase diagram of the 2100
Gd2O3-Cr2D3 system. GdZC~ A;
GdCrG3 B; Cr203 C /so#- ./S00,
to 30 so 70 so
GdjOj It. ve, CrOj
ISUB COME 07/ SUIIM DATE9 21Jun65/ ORIG MF: 004/ OTH RU s 002

SOURCE CODE: UR/0363/66/002/007[ii44/1247~
Ir
AUTHOR: Pavlikov, V. N.; Lopato, L. AM.;
ORG: institute of 11-Taterials Science Problems, Academy of Sciences, UkrSSR (Institut
problem materialovedeniya Akadomii nauk UkrSSR) LA
TITLE: Study of the phase diagram of the Y2(~-%03 system
SO(JRCE: k1 SSSR. izv. Neorg materialy, v. no, 79 1966, 1244-1247
TOPIC TAGS: phase diagram, yttrium compound, chromium oxide
ABSTRACT: The phase diagram of the Y?03-Cr20~ system was studied in the 1800-2500*C
rangeo apparentiy for the first time. The diagram (see Fig. 1) was plotted on the
basis of petrographic and x-ray structural studies of samples subjected to heat treat-
ment in argon. It was found that the system contains only one compound of composition
1:1, melting congruently at 23104-300C. The comDound undergoes a partial thermal dis-~
sociation in the solid phase, which causes the maximum on the fusibility curve to be
diffuse. The compound forms two eutectics: one with Y2C~, composed of 72 mole % Y2C~
and 28 mole % Cr2C' and melting at 2020300C, and one with Cr2
.3 -03, composed of 80 mole
% Cr2G3 and 20 mole % Y2(~, melting at 207Oi3OOC. No solid soltLtions were observed in
the system. Orig. art. hass 3 figures and I table.
Card 1/2 UDC:

L 46241-66
ACC NRt A 023918
e " c
YG
rO3
Frl I CrUA vrpn. 1.
Fig. 1. Phase diagram of the ZVOO - -,Zivvv
Y2C~-%03 system Cr, 03 t ycroj Y203 "YGP03
L I YZ Oj
V M.Wwsamw mpg
. -MO14L.%7
SUB CODE: 07/ SUBM DATES 110ot65/ ORIG REFs 00i/ OTH RM 005
hs
Card 2/2

_ L 46125-66 ETI IJP(r.)- JDjJG
ACC NR, AP6028203
SOURCE CODE: UR/0078/66/011/006/1442/14J~5_~
AUTHOR: Pavlikov, V. N.; Tre atskiy
sy
1ORG: none
TITLE: The Nd203-Cr2O3 system
0 77 -.,,1
SOURCE: Zhurnal neorganicheskoy khimii. v. 11, no. 6, 1966, 1442-1445
TOPIC TAGS: phase diagram, phase composition, niobium compound, chromium oxide
ABSTRACT: The phase diagram of the Nd203-Cr2O3 system was studied in argon atmosphert
in the 1800-25000C range. Samples varying in composition by 2-5 mol % were prepared
by threefold fusing of powdered mixtures of Nd203 and Cr203 for 2 hrs at 12000C. The
structures of various samples were examined on th 4,1ES-55 x-ray machine~oa~d the tem-
60
peratures were measured with an. optical pyrometer%PPIR-0 17.1t It was found that only
one compound, niobium chromite--NbCrO3, exists in the Nd203-Cr2O3 system in the 18007
-25001C range. The NbCr03 has a melting point of 23300 and a density of 8.06 ' 0.02.'
g/cM3. Niobium chromite was found to form one eutetic with Nd203 which is composed .
of 76 mol % Nd2O3 and 24 mol % CrZ03 with a melting point of 2060 ' 300C, and one eu-
tetic with Cr203, which is composed of 78 mol % Cr203, and 22 mol % Nb203 with a melt-
ing point of 2100 ' 300C. It was found that there are no phases in the Nb203-Cr2O3
system which contain divalent chromium. Orig. art. has: 2 figures, 1 table.
SUB CODE: 07 SUBM DATE: 20Nov64/ ORIG REF: 002/ OTH REF: 007
Card 1/1 TC! UDC: -54f).657-3lt546.763-31+541.123.2

L 02Y~;3-W Wt e) /194qTtm)/bwrk 3 )/T Larku Ivvrf/ [U-1/ VVn
ACC NRt AP6032957 SOURCE CODE: UR/0363/66/002/010/1897/1899
AUTHOR: Tresyyatskiy, S. .; Boychun, V. Yu.; Yaremenko, Z. A.; Klimenko,_V. S.
ORG: Institute of Problems of the Science of Materials, Acadeny ~f Sciences A UkrS
(Institut problem maEerlalovede-nrya AkaTemii nauk UkrSSR)
TITLE: Some properties of foamed quartz glassib
SOURCE: AN SSSR. Izvestiya. Neorganicheskiye materialy, v. 2, no. 1-0, 1966,
1897-1899
TOPIC TAGS: quartz, quartz glass, foamed glass,
thermal insulation, lilt 1 1 naW pd- i n1% heat insulation, 4-1 insulat-
ing material 9i-4S.S -W50LR-r10,J OX,9s.7 AevAPe7Y , PojeoS-Ilry
RCS'ismoor, al_ns-s 1 .1
ABSTRACT: Some of the physical properties of foamed quartz gi s have been studied
to determine its prospective use as aheat insulating materialkat high temperatures.
The material obtained had a'density of 0.3-0-35 s/cm-1 and an actual porosity of
80-85%, 20 to 30% of which were closed pores. Large pores with a diameter of .5
to 2 mm were seen; small closed pores with a 0.1 mm diameter were situated in the
wall of largerpores. The foamed quartz glass contained no crystalline phases. Its
refractive index was 1,455 ' 0.001. Compressive strength, determined on cubes of
10 x 10 x 10 to 20 x 20- x 20 mm, was the range 40-70 kg/cm 2 at 20C. Thermal con-
ductivity was in the range 0.1160 to 0.250 kcal/m.hr. centigrade,. The heat resistanc,
Card 1/2 UDC: 666.19+666.189.3