SCIENTIFIC ABSTRACT URBANSKI, T. - URBANSKI, T.

• Document Type: CREST
• Collection: Scientific Abstracts
• Document Number (FOIA) /ESDN (CREST): CIA-RDP86-00513R001858020013-3
• Release Decision: RIF
• Original Classification: S
• Document Page Count: 100
• Document Creation Date: November 2, 2016
• Document Release Date: April 3, 2001
• Sequence Number: 13
• Publication Date: December 31, 1967
• Content Type: SCIENTIFIC ABSTRACT

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00 Nuration protlucu so stardt. 1. m Of suma nitrates from potato starch.
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An Increase of the odd cancia. cuumis an lixmism III the N content and of the viactwty of
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the mitratims. Stabilliting boiling of the olustirs it" a detrimental rffcct Issilticiall de.
00 s nitmUmandanlncftomolibekgy.laStOll. The N "tent inctivismis with hicrrasi
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amb.oill.SOandliO. Such mixts.shaiwings snai. pastial Invsawcut IIN(hvslmxs Soo
extillill, a tons. nitrifying poutt. and behave here in the same manner as in the nitratkm
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01CCUU10ft. M&M Pow is H.SO. differ Its tbek.GKt on ptuch frogn that an tension Vo 0
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insdam, as nitrated is prolms ad. In them. 1. WINATIL.AK 2Soo
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00 it d.^C. A- 27, 49W-I'lie detonation -00
j,,,m of #&k " mid afawadvat was studied by "ad the cenier am formed. 7% am. of on flimp
60 S pertnittlog the dissection increases steadily until the " is
"mm of a Mgk-opted cammem btlimect the enter wA On ffq b by
iles of Pletwel Meting
'A a deum" fimmiss Into a me With num radifint points. Andy* of da pism, Gim
go j Oman raefs otbar by a &a- of '/,&- of a me. 7 pt-JI2 the COOdUAM that the fisidleass of tk pl~ ggy
picrk sed ow PlImm, a- m-ts the main One! qrcooll- Products do not g In the tobsk
go #I partly tim avandw jonction jand mns6ts of a center
immoundell by furrilmoom bundles. JU progress of the Pago
Woomdary reaction depends an the rate of cooling Of the ffum, but are ffrolin up Into secondary centers kond"
plem'. nnes around the place of the 4vtommation. T%e Ammar zoo
reaction products t1lected by reduction of the I
inig of free C mind Is Induced akmi the charge axis &bow oil cbminseterbries of &a
The lumiremneam is due to *w 0 Goo
by varjam Mneikm In the efrploolon The hot xplosAmn fleme. After eittioctifift of tba primmy bow, .1
00 a 1:1 graphic teas permitif the establish-t of the = a woondary, am appeass I , by Oddstim Of the 660
49 ;;j mbeene of th, isplasion pOV : The ch"p. b g the reaction =Ucts: C. CO, C114. 14, MCN, fit. The
din contains all A d an I IPK"~* too
Maier of the PsimW Sense. Is the place of the deoxq-. P"Oury
of the expiamire. The &vumpn. Products Internet Ifin- in the sectiodwy one. blue is eibmved feefily, fed 1000
intra-red Intensely. 71w loweat tmV. Wask of ton
ofdiately, formaimig bdAter reaction 10"" upon 6 darker :goo
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fm. 7-bb matt is expedally well perceived in PbOt- prionsfy f1sune is caW. to XXXIi-M11. Ninocdhdm
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IcAvt is confined Only behaves similarly, except that the form of the rbp amused coo
cWhing b1- -U. in the
I =five."xVittsplacedinagifass the center is afore mirdar, and their dkm. is manager thm's
with other ---Lng with picric add. The lowest temp. ad 600
tube, the diffamt zoOm ran Into each Par.
01 the Whok Wd, upon whicii, darlia bantis i having 132% N. is cLkd. to I9W2"'. zoo
wmpn. peaducts dirti.
T%e Interseft a
:1a sod ram ka , ban& around the center. Tbe &-be we 0
MW" whb theme tom- the inner pan beveby Ilion -60
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16-00. tube wbieb in tun is ~' , In a S&UM. tube 94.7'; -1.2,4-eblocutlinitrubmu-ne. 3. 49': -Sym. -00
cvftq.OycvvW,1*bv&Wdtob-10'sbvv kon.p. Daring trifthrobentmor. AVPMX. 30, 101.1"; --trinitrowlirne.
04
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00 Z Taurp.-empa. cufv" we glvm =y1diphearivrom. 32.5, 102.7"; -difthVidipbrityl- i o0
aft. r"P.. the P"=1w of iiw lot The urem. approx. 12, W% mannital nitrate vrytbriW nitrate Ge
04 13 'lift, 12.6. 14.5, VV; ptntamthritrA nitrate-munita nitrate.m.
euk,ctk M&Mkd ,a- ___ 1
101 j': PEDUerythrit0i Ritratt-Crytho'ttni nitrate.
6, OPP"
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itraimmmosm. 16.6. 39.7"; -'a-aftwo- 5, 50.5 . Mannitol nitrate was the only eornpd "nc
so 14, 52.5': -ow-fliekralomanw, 32.3. 65.61. dome to mol. addn. comptis. Probable compnq. (~'tgd'. by S zoo
00 Mmbm*. 55. 77.64; -1.2.4-c~itro- extrupoistim) am, in nwh. per mol. o( mannital nitrate.
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slow whiftv wo*
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c;;;;eme eta" are alved. The okownimnylam Agurn
& ", lbe pm=e of the Ant latirtillent arA the
U 101 Mitfalt-w-Ultrotol 11*1114
t4lat, U
m"..um . (in ratio of 1:2) whkb fornis a eulwtk-
th mannital aftrate, X, 14.4% mannitol nitrate-
mpbar, 4A. BAI. Krythrital nitrate- 1.2,4-dieflenoMi -
r 61 40 10,
P6~;hjj~'37 ii.2% "Mtol pentanitmie-philtal.
P. 20 66 9 ; -k - arytbrit.4
I Phasylearbarnate, A. 411 it I
+ 2) and yM& 2 auteelki: cow with the nitfusnimme
d the otW twit trythritol nitrate M. at AP-11, owl A2,
In to m1w 76%. "f rrv.11H114 nitrate,
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LOWMM and Tadcuss 1'rbGhski, po..iki is. .0.6
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go
rtetylkeital letemitrate (ID cdkdow nitrate (13.24%
) was evaluated im terms
W tdwt
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Tbeffterat ure 6 reviewed; 24refen-m Amodl-
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firsition of the awthods of Una (Atli I I zcn,:,r
2M) Is edoWcd. AV".
MMAIM srA Kdst (C. A - J.
Mrill tw1w"n "Sultscas" 1W Iojr4o'r., lf the J~Jltaalo# 111f,
Mut art shouki
Ions obacived: The P1111111tr of the aPP-
be subjected e than 10 or 2) strokes before nis"
1097
tbe detba. in . to arrive at such a condition that the
rad of the pluntier will not be further defortned by the
blow. The harder the steel the fewer the blows needed
to stabillse the plunw. 1'. shows cIeArlY the effect Of s
such stabillution. The rebound 14 varioux w1s. famns
Plungers
from various heights shouhl he detd. for each Wt of
similarly Prgpd. from The "me material, FMM this the
work done by the wt. is oRW. and expressed in ka./sq.
can, A, leas, two 11pp. abould be used aft"nately. 7U
qmstity ON subs'. used "Wit I.. should be stand,
stdised at 001 to 0.02 S. The substance should be put-
virised too pain Aso cc about 0.1 rout. diam. Theapp.
sbould be cleaved after every stroke, oW all defornto'borts V
~ away. In order sufficimily to describe the be-
havior of the material under shock at least 2 btights
sbmMbcdttd.witbanaccurjwyofl.Ocm.,. tbernin.at
which 10% explosions are obtained and tbe was. for 30%
of atplosloos. Fitch of the above should be detd. on the
bad$ of at least 10 r"Ainas. In view of theworied br-
'Ima4rcag CL,1SwsC.,T1"__
1, 1 a
"A,_ _., I
.0 0
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haviotso
4 diffettut tiploslv~s undti shuck at least 2 *1 and
srd substances should be used. t. q., kx*C! for the mom
sensitive Substances MW Pictic SCM for t less senlitivC
NutntabcC4. When the rtwt a the explosion is Qum.
titmoble, then the appea"MV of amt or the Prew"c* a
-- tmn -
xkr of It= shijuhl wrvr as addal, r0terift of ex-
I'" An sevIMACY of 101, to obtained, It. S"W-
Pk, M.
It of sisixtum, 1"d. 171141r.-Hy the Method
'"'Tib.
des. d above, inixts. of ftelArim and Union with
various ultra comptis., an 0 ciarrier. and a neutral salt
were studied. Mists. of 2 explestivir substances of differ- s
ent sensibilities %bow a sensibility witich varies with
Con"Ma Wt the transition of Mists, fnxn tbow rich in t1sr
sensitive componrnt to those rich in the olb" shows a
pronounced dI2CvGtJntd1V- It a NOR wry stmaitive sub-
WISUCt. c- kkiFYI, I Vol,, or PWrk SM. Is added to the
extent at I to a se tive subg!4we such " bows of
St"*
tiV*WM Is also Increased by tht adds. of asat 0 everwr
such as KNOS up tG60%or of& wMatra wit (KCI). The S
addo. of a anall quantity (8%) of & ,UMUV, subataw*
SUCII IS b*XONM at Penthryl to sucb substaw" as Cem
-pda. 11ACT06"s the amgtlvvnm awkeMy. The &bow
observation am interpreted to point to am
the Increase In sensitiveness is produced by Mach. arm.
of crystals of the farrign mubst"or. Wh" ScP13. "WAlts
in gremer interior friction of an MM, A. C. Z.
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00 '~e I"'
Tive-peatittaity (I vuk-jnfri~j "11.1wr ftith
00 11-fifl.11,1rhyde resin% hdiicu%*"1on thtl"aijtif the wrork III
ladjf~h. V. Iflift-t. Cismiren. Fimirl. K.*13. and Van firr
Ff kilk C""Irt
00 - 00
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alut it% Ime cant. V'(jqC,,t A fly fit, e'llialt'lls lasiolur".
fullAII.,111 U-1011-MU f- LO.S. wliffe IS, iwrt o( the
00 j rrAction. f lug. of I liberated. anti I tinw its mill.
00
For Owdriwilin. sit uilrlwcltuh~ XI the value of
00 I'll t-It I, dO lrllmill~ coll.t. wit b tittle. ilrs'lliell,
00
III r1jul'tur to ullf.1vu-1vt light, chmisr,t &".14'r frmu *hill- 09
00 it, yrilim, hill 11.1 V.JjIJr III thbILI-111I.AblP Of tl%i,IIAIISJ KI Z:
-.ur ittroduerd. Nitwl.lycrtin exj*p~ril It? UltritVitilri filght .00
vmtiuu,~ to dreoulp. dirr the flight mmurcr Io rritinvi-4.
*Oil MIS%, a ~ttupk- of niffuglyvi-tin oil irradiation low III initt. 0
00 1 W"A %hUkCU With 113001 Ibli JAPU SO KJVC All VILI. IFf 111[ 0

t It 24: r%14. USA& After 1. 4, 44. ASK! 7,J11M 11411 Jill VAII~ o0
k of 5.INS. 5.32'. atul 1. r-p. IL It. SIMAIII r
see
zoo
BOO
t:00
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'
it

-
l
11
1
100

it: , I .
0 .
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1941
`
~0
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30
9 IN
10 OF
1
go 00 94 0 06 006 0 Is 0 0 0 0 0
t
elil
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CArms. 36. 1&3-N(1947)-A rerkw-W-The-phys. anti
phys.-ebem. properties of C111, and of its use u rlw FrLa.
terial for the production of r4riaw mterials.
.00
Ave
Zoo
roo,
so
also
COO
"0 0
zoo
As& ILA &IIALLLArical. 1.1711talLAr CLAtSWKAIICIO
U U A .0 le W, it a,
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ao 0

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004
000
00 A
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00
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00
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00
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Is IF Id its
I 1 11 1 1 -_ P__ f I X. "-_ !~
1 1 -- .. . . _.__ .-- ___ . .-L- - __ I
plectmo #10 par.V00111)
Cb*Md*r, of "MRII1014
rd" on the dwmdsuy of pyri4oxiae desa-sibed. Jip-
mucst workers have btated-hezows with N11. wits in an
autodaventI50-1W. Fmw the productsof Ilse rrwtloo
wem derived the following 3 (omub3
A
100
*00
goo
=00
4%*
goo
goo
goo
moo
800
we 0
200
MOO
480
Thcve 3 forwAdam aft derivs. of 3-pyrklol. H cootairts a
CHAM Vm* dwairwink of yridemine. This wAwk
indicates the m mp
a,6. WNll#mkstocx~npds.
minallar to Vitande as No muesto a Similar re"Imn in
fivial; orpolomma. U. rdww" a oussmium friAtive to
the biftratbroll Go pyridoxim trout kw*A&km "Id S
compds. This mamotiogs Is based on the wwkal)"ww
workers on the formation of 3-pyrldol dorivs. indicated
aNmemodupom U's warkon Owcoadeautione(3-pyridol
with laromm"ple, to &(hydroxymarthyl)-3-pyridol. The
pooductim of #.Pyd"m at PYWWQUIILhw in a living
twemsdam is discoxod. fliwej:!!:!~V4ays a rok,la
Fe holim, its use In the Anonia Is a to
U 0 11, *0 UI;
0 0 0 0 0 0 to 0 0 0 0 Ole :10 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0
OT418 -000000*000000000-d 0*00000060000000000

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son
set
so=
00.
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of x is It cr of cr It
Int'll
ILI .1. f!L
JwD 1. &Not),*
PAVIRMLS "0011
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1~- rr"

v
-p.1MajA3J 3jVP0j PQtqtjqf)%jjn%-1J 3q) POT
an vmn-uNto lrquum 01 "n qual!" M)nad J. too
so
p.Cm
10 kh-w-qo

r
00
of
'If-m-sa T- r-11
it It R. r i
-T1
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f0 1
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0
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eel is 11118j"Itid ov "Vol :1 D a jo is A ?f 36 v a 0 At m u a a
I-IL-L #A 04 (A up M
it .. ... ..a
!17 ......
Re"ot dovoticipmruts in th* field of expiosives. 40
~Mleuas Urwdshi. prieOryd C". 4,
-00
in tbe productitin of With And per.
Im"ill1c Fiji'
0: k%1M. LWINW4111, Mid IkkkEt jUtlS air fr-
viewed. 3J mfetriwes, FrAnk (Imet .00
.00
:0
00 SO*
0 coo
Joe
see
9 top a
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9 1"
I v L a 1( TALLL~rKal
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00*00*000000000000:00ooo* sees** ~00

T-U
ad t4borC1110 C.A i 42'
cbemack"Airy 57-4W 1949 re-
.ya Cjw,,, S(28). 4 ht~vAhrrfy a I" of lAffe ""' of
*" the c
C,nt advAnct.*% I and PbY-- OOS*"F,..k C--'t
viewed ajul t1te 4tructure Ifcmnccs-
-b-d 39 'T
."mt, .. dren .

Schi W Ndlare
j&,&;6 I'Ma 9), 0
pd~- 22. LM(HW) sm. 68
(910* 176-S' (quick brating). w-As converted to
Its -U ttestment with NmllCOj. The
NA wit Was 9W. in H% mW a 0.1 N soln. pvt pit 7.7.
The bacterimstatic come. of the Na Salt was 1.0 Mg. per
100 Mi., the sam as sodkm t-anthwaslicylate. in n1re
us Younwas nwdmm against MycobadWriams Imbacalarts
MAP strain). The , . sweet tested im fim by MAW$
white mice imerukW (intravenously) with 0.1 mg. of M.
fulmm,cat"is. The cmpd.. no. of animals. dady dome -
(Mg. per UNOW). nsortality, ay. tuberculous I , and
av. survival ti= (4mys), rup.. were; sodium t-amino-
saficylate, Mi, 10. 60,311, awl 23.1; sodimus s&Hcylhydrox-
arnate, 60, 3, 62, till, and 22. 1; control. 60. -. 1W. 100.
vW20.1. The win. What ion of sodksm "licy1hydrom-
amte on orlike mk-e was about 12 times time curadvi am.
Wasky It. Hartung

URRANSKI, T. o
Salicylhydroxamic acid as a possible antibuberculous agent. Gruzlic%,
Warszawa 18 no.2:206-208 Apr-June 1950. (CUM 20:7)
1. National Institute of Tuberculosis, Lodz.

looon" 4111' -mitt*-
and"s,
z
shomnki awl 51*.!ba
T* %2'tpt9WV"1*W CWT Z.;
IN= ctr
Ij
1766. 44.4WAW.-Tho rimelims twtw"a MeNch. "Clio.
Ire 411, Am. md 0' load to Wynwril at bsok-
-
16100). by fit tit. ew 1lihjmh"%T
awshyl d"itivilvir. car %,1f. by WICNIls 111".4 the sonal re.
Aultil. I'millord tion."Wilu r oll'i
Iftwiltm. fmll a 6u
rempillLbsynthesized;
+
oll
11
HCHo
Col, CKJ -t If,
I I
Ilk N" R R %, "N R
Col.
WIN" R "IcHr. *"it
4W*' or, 87% -A If X --- , - -
il Of 17F -ma -W' "'. Sol, di.
M'). 0-0 m an tram
Wb" ja ilm-er. I
fic di-
R is YI,
A - vitro krdm thyl
. 71W twit Irk-
M. IrA , is
ymakylinitra"Wilssne 11) ro- th)wrr than the-
billfbirdmrnwithyl) dmites, (11). 1
irmian cif (Ci Itolf 4CXo, (111) t.
are esttrili
W1 alai hv,lnqvsnl (dif 11019101f) Ill
atili with 14011 t-lealn-hath. Itere I'l Cnrf. 110J.) tit g1tv
its, 124 W,
a
Ind i4 torritkil to tho amlat,, tit mV. Allti botia4mag. to,
16-17", tit with afthyd. MP10 ill the prieftmicir 44 slithyd. -
CuS0,. at town imp. pmlucr4
sit. Amfols. w. 64':
limmuste.in.117-18". PbCIIA:110 and Ill (stmus blob.
tram et c"", 11.400 -form (2-phenyloltyl b 1-y-
an remisiont to aft. hy*Wys4 (boilmir with 16% KOH a,
X&OH) whik seW hydrolyM 0% HCI at 60') k ouvirte
its 5 win.; they are neitimer "w1hylated by Mes,90q, wir
. atildhod by alk. KlfuO, or 1(,(N; on hosting with MeO.N.1
- WHO 14 relm-tird. Alw no stmialt atir f.*mrd train 11
cyche tnwfmr (IV; i4 lgg-ted rjW &k
R.- Clio, . Cill-L)",
R. Clio
q I
(IV)

1"'WIP in it- f-f-ifil~ f-All IM SMiMA1431, giving 2-4"h-
-11w
Amwinwhyl. M. 1214, (1 I'Ll salt en W &.101w1hyl.
Pit A", A-Mfthjkrniftr~
nwtbvi. in. K"* Olcl "It, m ISA A*' nil MA- rwr.. "I.
(mity-A slrrlv~, M. 111-12')l X-olifnelbylAntinamtkyl,
-M. 97 Wr (nilrtma dociv.. m.
(do" ow fom a ssitip4a amy t, Ahn 2-phrorl
_dkou"t
"a. IM").. "i'lMsIng of the
110 WN brr*U Ow. Mmom ring to foorns (smiomw4hyli-
an-I to librtAtr an at-
mdw. its-
174-d" (IM tell. 0. 1914, t' Is "Mailml rz;. lw.l
.-of the wnthowA and %My, qlato of All mnp&. we ji"m.
V. BASSOM$ of "W somd"Y sapopwaillow Wilk
ko"Go god wif*.=P* WA diridc TAdmes UrtmodAl
And Wolft'Ll, Our kit. 213-2L--Pr'NN (I
ry6.kx. 1
its the povwnm of ankyti. N#OAr with
SIT" a volatile bhw [Weghoort (111) and MrCIl(X;()X1Ai,
ne kr(MCOMOAr. funnrd by dirml amlyLitlint. 'rlw
t"Irir" PMIU-rt (Allfr diAl". #4 u"mrtml 1. orthot utin..
urotmfirathm 4 thr rit .. 1 (.0 vmobn. unif dion.) I, a oiliw.
k~ oil. h, 12.1" b. 1114'. mV 1.4-VU fyirlif. 12% ba*41 on V~
?41r,Cilx#N I M ims the A unhya. Vi()Ac with It
At 7fo-ml, civet fit amI0k'"-rtjWf Nlr.C: -
N( -; O)OAr (Y) Which. puri;1;4 A4 olmyr. 11 131'.
h- 1 _2*. mi? 1.41M. am[ siv" floAr m hydriAv-1, aith

I s"i
I! W

Tadeusz
(D
Pentor- and hexanitrates of 99z
Q(an
ft.. &2S',1'3'l2-14(1951)(EngILsh sum
The nitration of sorbitol gives a mixt. of penta- and hexani-
trates; however, a nitmPon temp. of -10' favors the for-
mation of the pent& deriv., while the hex& detiv. Is formed at
3-6*. To 15 bit I in 75 t. HNO, K 1.62). 150 g.
Chemical Abst. H:SO4 (or 20 g ~Ifiew,,U)Owas added drepwise at 0-3* for 1.5
hrs.; from k-e crY3t. 29.7 jr. product, to. 38450, was
Vol- 48 No. 9 obtained 8 g. sorbitol hemitrate, m. 64.5-65%
May 109 1954 by fraLflonal crystn. from 50% eq. ale.; from the fractiou
easily sol. in 50% &q. ale., was pptd. 2 g. pentanitrate by
Organic ChemistrY adding H30 to make an approx. 85% sic. soln. Sorbitol
(b g.) added dropwise to 50 g. coned. HgSO4 at -10 te
-70* gave 7.5 g. of a mixt., mostly pentanitrate. . Tht
hexanitrate Is emlly denitrate4 by warmin" 'it In sic.
pyridine. Geqe A. Wy

deAr""'b"O" ~FVnbA, of I
ivedin. T. ~.. t, S. T~vk,*.' Venuirt
(Inst. Tecbnor7l armaw, PoUnd). Nature 4. 2D(JUM).
-T28 was prrpd. by action of SallSOO on &nitrrmi~&
hydroityquitmline to *kf the rimohydritte of N-oulfo-N-
1.'-quinWY141-hydroxylbydmxytamine. In vitro ex to. on
rat beart obowed T28 has no effect em the heart wEen 0.1
sill. of 5% soln. is lidministered. Intravenous doors of 14)
n,g.jkg. body wt. to rabbit showed little effect. Ouinex i"
in-wislated with Myrobsciteriam W-frishms stful IKIF-c-
41101311Y SICSIO vilsh r214 Showed a bulb% .4 fV4.
A~ v,m.t%&ml vvith stirpt,mitm-in A.. Odics dritv-. tv.t.1
.rce mil.
We. 5-mmino- and 5.7~11oitimquintilsor. Thr Law Own,
wtir prro. by reduction with SaHS(h of S~nitru*),- and 5.7.
T. 1. Ainnick

ViJrba&*i T. I&Ih.15k, 13. Preparation on Labomtory Scale of Ergo-
:;j
URBANSKI~ T. I
-Wr-oi fWm- Mycellu'tn AiVergillm; Niger.
110"Y)vule ergost-6rolu % gmbnl Aapcrv!.'!u& Niger w tkill IA4)-
ratMJaej'~.'(Prace GL but. Przem. Rol-i. I Sp-at. ?la, 3) Wamtwwj,
1152. PWT. 4 vD., I tab,
'the cesitent of ergosterol In A-p-~~rgillus Nlg:~r takt;n frcTn a citric
zrcid factory -wi3 determined. Two p.-Imc~pal methods of extraction of
ergosterol were wed: 1) extraction of Eats and stc.-oLs anti the hydrt~-
Polish Technical. Abst. lysis of fats, followed by the isolation of ergc,~te.-ol from the nenhy-
No. l' 1954 drolized portion, 2) hydrolysis of the whole material with potassium
Chemistry and Chemical Technology hydroxide in hydrat2d alcohal and the cxLr3cicn of the unhyd:oli!Cd
po-tlon with a suitable solvent. The eviparati-n of the scIven., left the
residue of ergcsterol. In order to Und the most convenient parameters.
a narnWr of experiments, in modification of both methols w2re c=rled
out: the quantity of potas-flurn. hydroxide the time of hydrolysi-s and
'
ivent. The most suitable me-
extraction, the kind and th
e quality of 6.
ftd was found to be, hydroUsIng the fungus with KOH in hydrated
alcohol, using 3011# of KOH -calculatel on the bisis; of the dry-fungaus
- mixing with water, filtering the precipitate and extracting the solu-
tion three times,'wIlth benzene. Then the fungus was extracted three
times with alcohor Lnd the solution was filtered hot. The predpitite,
from benzene and alcoholic extract was recrystallized several t!nvn'
from the mUttire of alcohol and bewene (4 : 1) or dichlor-oothane. 1)4:1-

-am g crol. _
ferent kinds.-oUltihe yielded various quant: r osrt
It 6 1
idble Ilia' '*-i yield depmWs on the condRions of fermcatation (medium.
airatlon) aad~of'the age of fungl. The content of the crude ergosterol
was. 6.12-- 0110/s. After ;.triltcatlon, It dccreased to 0.08-0.12Nt. As
the tests-were, -mcuLed an laboratory scale Le. with small quantItteg
of faneW the 30S&ft Were fel&dVely great.

7A
V) a
Phenolic rcittif(MCGO-h dr
-
1
&1
R
,
r
1
Dalilig and Tadcust
chrm. 1952, NO. 1,

(1), V mtotrm c( yit-m-
n.c Nff, -fAt -f I trAi rhtafrxf in 75,47,r yir~LJ
d rt)pIv1sc.1 pinki pyridhw (1), 114 If' ') to:1, :-Y ev . il , ', mi
fit lircience of 6.5 g. jig; the r(actor. eqi1il'I'Vil IT411a ,
dens". %vas cooled with water. and tlictl Mowly ht - tight to
2801, and kept at thi-4 tentp. for 8 firs. The rv-,, i mixt.
tfissolved in water, neutralized, and coned. gave g. ~s7114
salt of 1, crytaufs from water, I,,%. 23S-42'. The Nil, alt
0 mole) fuwd with 9 motes KOII for 3 hr3. at IR)' gave, after
neutralization and extn. with hte~CO. SOIL,,, off. In. 124.5-i
5.0". 1 was characterized by its saltv hWr&,h1e?-jde, b,,:
'
.5* (froin I
2N--rj-, bto 2(rUY-110"; picraht, In. 200-l

l Ab
t picritlotwle, in, 211,r-3.10' (froni
s
.
Chemica CNON-14C6, 111. 162.0-2.6" Mom wattr);
Vol- 48 No. 3 Cu(OA6, in. (ffom ivater). Carboxylatiou o( [I

0
Feb
1954
picolinic acids. Dry -Na salt of I antj Co"
gavc.hydroxy
'
"
1
11
3
9
6
.
, -
-
.
at atin. pmzure Itave
heated
rapidly to 1
0
%
'
OrFanic Chemistry hydroxypiccUm4: acid (11). WitJ2 slow heating lt~sq~ or Ito 11
l
"
and 45 ntm. the yield nf Il
was obtained. At 215-20
22%. Same condition-i with Ksalt of I gave 2-1c;,,, 5-hwl~avv-
4, ic acU (111) and 31~'/O nf 11. 1 tuixed with atillyd.
wated with CO, at 215' and 45 atia. fm- 8-1) lim
gave III III yfeleA which depen'ted all th, ratict of ~:,W. to
3-hvdr"N-epyridine, ratio t.5 gave jt-*.-Ijc~q yi0d, ILS-71!1;
a
ratio 1.0 ,ave 70',,,. 1190! wit of 11, crystah, fru,n water,
'
picril? in. 1M.5-62.0"
in. above 220* (decoiapm). It
~from ivattr?- Afe 3-hydroupfcolinafe. in. 7.1-4*. F-1 .1-
,
wolroxyp~c4mak (IV), ba 124", 1j,,-! INI-1*, lin 1432%
/ircif !t.1 *!, in. 147-7.6" (frtint water), in. ! 18-0.5"
lv,tts)~ 111CII sill of 111, 2f~;--I, Mom Watit),
I~t~.ero!c fit. 2415-tJ."j, (fr(Hil W(In-0,
ate III. 71.5-r,-W (ftfan CHO,); t,61, tit.
"froill %vater). vqftrs And c(lierg of 1 imp ft-I
characteill.m. I and AcO rave 9.5%
92', 14, 1:37% pi7, rple., III. 155.15y-70~ (fretin Me");
ale, in. 111111.5-7.5' (front n1c.), %-'I, in. Ill;-O' (ft(lit
Water). I am] 117.('l R,Iv~ Wl, In, -~O-
`
om Cfic!3),, 11r.0i
W.61 (frim, n1c.): f(rrit,, in. yr

$,A, n;. 108-70'- 1 ane, messc,4 pvcr-% J-Pyrid)i He
ether. b. 178-9'; I/C02 Sall, ill. 110-11 . K salt of I *nd,
I'linr In presence of I anti CuCOJ gave J-Pyridyl Ph ether
.(V). Best y1eldq of V were obtained with I-PhUr
nialarratio of I:L5, 211% excess of lover Its K salt. 2.8g.
C11CO, per mille of K r-alt, anti ficating rencticni *ulxt. for &
lirs. at 150 4nd 15 hrq. at 190'. V lmdritrAferhk tit ' 05-7**
tr.CrOe, in. 13fl-2* (fr(rn ale.), p'crafortate. in. 102-4'
jfmai atc.); HoC1, (als, in. 76-7.5* (train atc.). I ccupkii
with P-01W.M.N.'Cl alt'l the ago WittA. feduceii with
StiCli pvc 2-amina-3-hyd,azypyriditte. tn. 163-7.6'
(fr,,tn C.11,-ale.): piefoler. m. 257'. lodinat'an of I In mild
nlk-. s,,In. gave 90% 2-iodo-Y-hydroxypyeidipce, in. 195-6'
(from McOll). I failed to undergo n1trosation, rcaction
uith CII.CIC0,11 to give (3-ps-ridoxy)aettle a61, or the
W.'rimr-Tiemann teaction, CsIIsN.IJg(NOj)i did not give
hydrux)nittopyridine with HKOO, Janina R. n)ejim

UBBANSKI T;SNRAPINDWA, B;KALINOWSKI, S;SLOPEK, S; KAMINNSKA, I; VSNULIT, J;
K.
Research on new drugs for the treatment of tuberculosis. Gruzlica,
Wares. 20 no.2:157-170;conti. Mar-Apr 1952. (CLNL 220)
1. Of the Department of Chemotherapy of the Institute of Tubercu-
losis (Director-Prof. J. Misiewics, M. D.).

lv'o 4...
auft.Z"BIWINOWA, B.;M&LINOWSKI, S.;SIA)PEK, S., UMxMKL, I.;VENULET, J.;
JAKIMOWSKA, K. I . . .
Research on now drugs in the treatment of tuberculosis; thiossmicarba-
zones. Gruslica. Wares. 20 no,3:292-302; conrl. X&Y-Juns 1952.
(GIAL 23:2)
1. Of the Chemical laboratory of the Inctitute, of Tuberculosis (Director
-Prof. J. Hisiewicx, M.D. ). Warsaw,

UEBANSKI, T.; HALINOWSKI, S.
------- -11-,V-110~-
Synthesis of antitub*rculou drdgs at the Institute of ftberculamls.
Gruslica. 20--6 Gvffl. 2:81-91 1952. (=L 24.02)
1. Of the laboratory of the Syntheses of Therapeutics of the Institute
of Taborculosis. Varsaw.

A ci
of PrUJI11 - U1. On ttic carboxylittion of 3-
90,Z11141 LA1173, ~40. 1LMN-'U4t4VJ~rj tISHRIP,11 WT1111TAty);
d. VA. 41, 51,Ml; 40, lW-1-.-NJI,
(I mole) wl~ ful"1 with KOU (P fool") at 10" (or .1 lirs.,
&.c melt dissolved in watt-r, ndjusted to a till of about 10
%vith ror.M. HCI and thEn to afw;ut .1.5 with 11OAc, arid the
re'ailting Pilt. LStd. with MC,Co to giic 86% "i-hy-
droxypyridine (1). m. (froin watvr); HO sail,
bj%'.~M-5' i;,sid Lui =-O'; pimj4, in. fjcr,,jo_
nate, in. 241.:~3.0*; 119C4 eo"'Plex, m. 162% Cti(O.-Ic)t
.i5ni. IM-9* OtTompit.). After I as the Na salt
emiP(~,~x
g.) was Iteatcd to 220", dry CO, (at atm. pres-
s re) W" intrWiief.4 while the temp. was raised to TS61
durb!g 30 min., kept there 6-9 brs., the mint. dissotved in
2f, ml. wattr, acidified with coiicd. HCI, filtere,j, ticutralind
with Nallco" the unteacted I filtered off, the filtrati-- acidi-
11A Ivith HOAc. -and 3-hydroxypicoliIiie acid (Ill) PPtd. Lis
the C" salt (!V) froin the briffing filtratc oil ~atn. witil
NIOAC. IV Was tlfT',mI?d. with HIS and two purifications
were (-frr,-P:d thrmigh IV tip yiela -O.f;r) g. Ill, in.
-4*; Picrafe, m. 1,59 62': 1[,C1, crimplur, tit. 2_1W
f(citillyn.). fit (2.6 g.) as lbe 'jg Gilt w,:.i rcfltic,l 3.5
i
ir.;. with 1.2,5r, Pil hi2l mj.flryC.ff,, filitredoff,
suld the 1A.11zCaL. -Io. evapil. to ~ ield
pirolinale,l), IfIV.-and It,-, 121'; piemir,iii. 118 1~)'; JJ~Cj$
cami#lrx, tit. It'i", Ory CCJ.~ mii ititti,duced to t.9 1'. 1.
astlic .wesstire of I(J-45
a(m.. Ow Minle ficsic.1 d1o;!Ij! 1 1!1. 1 12 1 29)" ki-pt :it thi-4
tvinji. for 1.) firi., arld t!?.- rx:'ulti1'j' ini-it. wmki-d 1.1) a5
%IKr1FCyk:ILI1;dQ.fr-9.U1. 1(1.qS.)astft,^ K wttw~atrtzzv ~d
.2-j2i COi, und"r prc~~aar. Ific mixt. kc-ited #Ls-.I:4Yc 8 :7.vv.,
the produtct di-,=~Ivcd I" 2U ml. vnt". the it-In. -jet;d, fraci
rathfiaLol qubdaricri by filtration, ticuttalixf."I with"Car"M.
f[Cl,grid acHiritcl with HOAc to give czystals; of 54y4rtix~
pirxhaic acid (V). The filtrate was ncutratizO %vii i
~!,diCo,, any scpd. I filtered off. ttud after ucidifyiug %vtuli
11OAc, the Cu salts of the 0-hydroxypitolinic ficid-i wa,
pptd. witi, Cu(OAc)2 from hot solit. Tit-- Ctt)tWtq w,!re
decuaijid. with l1zS and twe fractious with difftrent
solubilities were obtained. The Ic,3 sol. fractkin co:v:i~tr#i
of V (0.75 g.); the total yield of V ~vas Z1%, m, M7-8';
picrate, in. 265.0-4i.6'; 11gCj comp!ew, in. 25-3-4'; Aft
csttr, tit. 72-3*; 11gC11 consplex of Afe es!er. w. 194'. The
more bol. fraction was UI (3%). 1 (O.rf2 mole) was mixed
with KICO, (0-03 mole) and the inixt. treated in an auto.
clave with dry CO, ( 10 at tit.) at 2 1 ~* fo; 8.5 hrs. Frou, the
reactiou product. worked tip in the usual way, %vas (.1ttained
2.73 g. V. When I and K~CO, were mixed in muLir arriti-
and truteil aq above 70-1 V pad 1% W %vere oNtained.
I=lc%, cxcc:~Srs of K-CO, di'd 11tit iiiiljruv,: the yitJ-d of V.
T. T. Galk',)%Kj~~

T - I- I ~ A. T~F i . c -
I , If-j F. I e I . L .1 L
11 t

t
yll.---]~'ejctiona of u(trG-.
rnrth.Ln with acculd h d d .1olneg. zugamn-1- =70,51:11
1.1L1 , I .0i lilt - a t,
41 'tit ~Oltl I MIVIINZ I Wur
ZUT44i J--:0
d. C 1 40, 7"li:Ic All lif A,A I In 1,1,,,:0, ga.c
g.j ia ~Ii ;Ill.
ou ill, rc,lctiml -twdilions. 11i'll (SQ.,
W:Iter ;Wd'A Willi C-ling tit Ui Mt,N43- awl 0. 1 I_ K.-CO.
?, lJjorg' K2CO$ dillo., r~actiws U) L, 'j, tlw pit
lit 7.,--S.(I) ajO tlw~ inkt. It-it, 3 6 Ill- It :"), ga%c 7.1-.
1: , "(11. sNiGl 3, 1. lit,() ;IIA I'litill"t tLtuititi, I,,! Na
- t, - ,.it, I.. *l) 1*10.2- 1.,- 1 A If'-'. ~ ltlqi i-
11:11io,j , vt At of I gaNe 72~ T tudc M-CIAPIOCH-
ONO,t1W. tit,. N,, -U (I~i-,
aii.i 76..', lilt. Ilr it% 21XI ml tt i'1 1~-I-
~11,lc Alet IV ~ ; _~ )
IV C;,k blirm~ 11*11~., A. I I I mt '
to 2 44 , Nlc'~( i~ t ilh
Gi ml. w~tl~
ei,tiling to mid flic lutt. ~atri,d U-:, f, A t
J-,~om unip. 4A fir-- ill a tivilik 1-10,111 1 1" 1 (I'll - 1 -'-'7- )
ill e Iill ,f fliv reacti,m). ttvale,l With Ci I- :lwl 6 -*.' L Ft4U, and
t ried Etf) layer distif ~Cff. I - n)-ITi fig' prCssurt, 7xv_C_ sa~
(bawd wt MeNO:) Crude 11, lti`)t cryst(I., yj
AeCl (2:)
K~) aull 1.1 K. H ill 'M Jill. CIICI; rtillilril until
evi'luri'm ,I IICI cm&rd guvc. niteril6ta., a rv,uitie (j ~,ttjjj.
cry,t. 1)r(-Ik!,-t tdiiai, filtemi. yicIjI,,j S6 ;.
Ltic-) 1.11 -i~d A. H
61.31 , 0,YCO(CHA,
'eolf), (v), 11. ll~-
du~td. Act( ( I.S lilt.) ill IS lilt. %,al,l all:1 :~G.S 9. IV il-ltl~l-
ized (litillus'l Nvilli ;ill. Koff, the i;".\t. 1~1 (-"I w ~
Salted 'Jill With \.icl, extil. .1itla tl), m"I 111C 1---, E
crym(i. rrim, cci, ;,,,(I ciici, ( I: I ~:,% v , Iiiii:
Ill. M .):J,. Cvill, ii'viah (v:
ov;!IICJ) of (tic fyj~v tjti,li."f,..(,R;~;Vf),,;.Clilfe.['.('Jt'i~t
L____ - - - --- _-)
,vrv frwn 11 lly ; i I I I . 1 11 ... 1, ,
1 11.4 1.5 111,4~ ~ lh!, Iq'Ir %- l't d 1 2 , 1- .--d
St P,, t:,, m 1, ~-vral Ill - ~, . " -, -, I : t
i-latc,l I jd,lii J Ell() ur alt.; , i
.1111 1.:; F.I.Av, ill C-11.
al'.. IWI, alid It's(),. th, ""al "i- A~
tlmni~I:mtt tfi~ c."M"e --f lilt- TIACtiLITI, ~!J~j t1j,
.I ht fi'll-%ing
(VA, k, - It, .. . ....
ViAl gi\ 'It) k, l I " 1.1t I'd. by Im I I'l,,I ( I I - 11, %J~ c
(111, tyll) 161 11" :!.6'; P1, COO). 1;',, l"",

ks i7 Z,
,~Xlt. =~I% 15.7; t~AWCJI. (XI), 132.~-
14. XU), 1!4-"*, 3.7; p Oil
Ul --3- CS114
'(dX6yd),'e1'r'A'srein'o'v")' lnti,cptci)ll.ofxl.-Xllitinre-,tttedal-
ed withaq, NallSosbefolre ij,,latiouat the
uct. The VA "ere crystd. frolit ale. (VII, LX, .K11,
11). front 11q. wl
ex:2) of Cj I. and - . 1:3) ale. (Vi, XI), of from a mixt.
cc ale, (X). They -cidi. They give pseudo-
nitrolPets VwUit)h, bul NthYdrolYze In dil, 2"re rc~li!;tant to dil - alkali
, . 0; while 11 with 11N0, splits off Acil to
Live the nitrofic acid. The following VA (RI - R3 - 11;
It', in.p., and 70 yield given) were p-cpd, by method (2):
:P-CIGH4, 107--o", 30.4; 0-110CY-4 (XIV), 144-0', 21.2;
AcNHC41I.. 20C-7.5', 13.2. Fit-Dioxaxes (VA. R' - 11;
V, R3, rn.p.. and clo yield given).- ":NC4114, Br, 142-4%
32.5; p-AWC.11,, Br, 124-0', 9.2; Ph, Br. 36.5,
P-OWC.H., 0, 124'~71, 551.6; Pis. Q, 01-2.6% 36.5. All
i the VA derived from 4,"imethyl-m-dioxanc are white cryst.
' compds. except XW, which 6 yellow. XIV mquircil W firs.
4or its prcpn. and could be n=ifc b;- tnc~hod (2) only.
" JR1 - RI - Me, R1 - H (XV), and R1 - Me, R1 - Pr,
R1 - 11 (XVI)j were prepd. Crude H (150 g.), 6W nil. dry
MeiCO, 200 g. anhyd. CuSO4, and I ud. ale. JICL (3070) re-
fluxed 24 hrs,., the sulfate filtered off, and the Ue,CO distd,
gave an oily residue which, washed with water and distd. till
:to 79*/5 inni,j yielded a cryst. residue of 40 g. XV,
needles with camphotle odor, tit. 73,6-6,h' (horn ale.).
U (30 g.). 80 g. PrAc, 100 g. anhyd. CaSO4, and I drop ale.
") XV!, needles with
,HCI 16 firs. at WO* gave 15 g. (28%
camphocic odor tit. 68-70* (frwu 1: 1 2q. ale.). Attimpts to
synthesize tetrahydroOxazine or hexahydropytimiditic derivs.
frorn 11 arid primary amines were umuccessful since H de-
compd., splitting off Acil and focruing resiaous polymers.
Cyclohexylattline and III gave AcH and fL cryst. unstable
product, tn. 62-4% ptesuniably the &-%It of cyclobtxylamine,
and the hydroxamic acid ICIC(O)NIIUIII
R.

toll-

Vt

it! 1'J, 1.1, ('U'A H
V/1 C(.VU:
IIF. 11 ;~ro 4 P
:'VI/ Ifv,~,
%Vjj, 1",
IfI-_,.~,,wt,1,.,1 t"Wh%
.
no- if
fV~ j!, jr-tl, $77'; R'M I P .0-A
COtiji
fl~,
1. VII

-~.
"On the Structure of Some Aliphatic Nitro Corgounds." In Eaglieb. F. 239,
(GEODEWA I KARTOGRAFIA, Vol. 1, No. 6. 1953, Warszawa, PolaiLd.)
(Polska Akademia Nauk.)
SO: Monthly List of East Ruropean Accensiona, (ZEAL), LU, Vol- 3,
No. 12, Dec. 1954, Uncl.

~,
I _',t
11-11'1~i"-

44iim TTT ALsi0ap :f
a~ TICA mr-I T139 0,01
Af, 'T%5~. m I le 10' 6- 11, "7 i 196 2 5 - V~
14
TIR~, 1-97 T-j(Xj- TIIJ, nd rii'l
Wm amthesUed IrM NfftOH btik~KOH IK
the Bre esttfs of the ccm-t5v=di--jr M.11 &M%.
cbky(on F. Hol'awmv,

M~y

(1) iz if, tti! prer jf Ft C~:,,rx
yj 'TY, tn~ h,
Cl I-V !7
0" lit FTC*

2_4-11 ~hvdr=,,itroji,uwz,)IInc froru -1 . iiin .,i, ~~i lira nilic
ua n 1111110
il;t', Ent. qj-fti~~A
CA11.1-27, 167- 111
C.J. 4b, 1;m17.1. Aktit't
t I wit i IWI, 4-timt~;mOmmilic ;icitf antl t ; anogni,knitfin'!
(1). tatilomeric xNill,
I li~o Iwvii prep'l.
..o,,ih,r way by Ifuntrt.-.;mid Gla.1,fitig(C.A. 37,6.-.40).
f,

ij
ion ol hydiroxxtruic acfj;. it. 5-ilrotno-
OXY111.1tarn.1c a0r- 177-. Ai joul
1*wznite4n (Patytech., M'"" *
I& I . - ' 1,11. 01
dat HOAe was vAled slowlY to -.5-3 C, of salicvIlty-J(D-'i-
&ink atid lit 140 ivil. of glicl-Al 11OAc at 00% Arve%s 11r'
was removM with Nallgot ini, after conling, the lir"Wrt
wA-,q distd., washed with cold w4ter, and dried to ilt'l(I 351 9-
crude 6-brommlicythydroxamle acid, white crymals, (front
ate.), M. 232" (dewmpn.), pooriv srA. 1u wate and sol-
vents such at ether, actione. CU,, bvizene, and xylene
at boiling temps., mdily iol. lit boiling a1c. rind JlOAc; It
hq a bitter ta%te. C. P. 11010%jAy-
AV

S*4e derivat!"S *f .414*41b drogEwill Multont.
Karl-ai-i OL~ft .1 JV,4~-, " -
27. 34'~~6301111 (37.1 C., L.
txddt-l o~cr ~P) min. tq 1~A X. HiSO. ,~ M~4,)'. the m;..:,
heateLl ~!awly to t1kV for S h".. dit! ;,, z.isurc r",!tt%:-t
X-0 u) P- mm. 'I.-Ijile the t,~Mp. i4% rai'~~,l JU 1,V,$* C~ef .." ) h~s.
The If,() fwint,l in the r%tacticrt ii removed tiir, diltai. `t'h-
,temp. i:i then 1,),%t:Mj to 116'. 2N.NaOR a44,-1 t,~ ,If P.
filtered. in,l t! filtrate ~djus ed to Ill 13.4 voith I tCl. m-
sulting its !2.0 w!
g. of a mixt. of
dipAcd)l su;fotse (1) und its ia.
26~.,,V. The mi- i; disolved in bi~iiinz MtICO, its
vol. of %rnrra C,ill ii added. alut tile 111"t. 41 r1%1- A I Utr.
72- 1. ni. '_-i 1-1.5% .. a M117.110 ' m
220- 1'. Similarly. pyroc3tech,ll v 74-S)' whtbt a d1jci-tio~
temp. of :.'10' fz,r 2t 1!rs. Vivei of
diplot '~ sulf'one. lit. 247-4-~*. Jul.
[one (111) (.',1 g.) i~ added to !ZA]t ml. I f_.io. at VX~!Cd to
15',an-I 2.Y) ml. WN0. iiaddel, iiot jxr-Tuitting thritinp. to
rise above 35-40'. The miNt. i. tic-It"I at 6G-70'. kv, 30
mi,*t.. dild. with an equ3I vol. of 1120, ~-11211 Altcmt- Ki%'('AK tht
3,7'4~xi.lro ana!", of 1. Tn. 2;1-41' (Ir-Ofn ELMO. 31'g' of
which i,t dis,,olved i:i VO mi. of 25% aq. J., rw. 41
0 . S.
Na's,04 1, ad ded. the inivt. hra-,W on' a 14%0 b-~:!i for ftrs.
and cooled, to give 23.3 g. of the SX-diamiise) wsafor",,'M,
L", IX-Dr't juMw. uA, M-
,,.)0*, ii obtained 1 1:311, llj~,V!ic it-ij %,rjtb
I ryield bv treitillirLS4
11-Sko. (,t, ill tile prepti. of 1) at L~W.* , fir_%tin & M K, 11V tnd
2W) ml. Ac.-O with 0.1 g. NaOAc all IL HiC bifth'itw .4 hrs.
gives the di-Ac dermat 1, m. i7t)-1.5' , fr) g. ,I is dis.
solved in 100 mt. 2N SaOll twt 211 A. is added
stewly, pptr. 921~1 em'!a.f. nt. 1,r2_31
(front M011). M (25 g.) is in a i-ln, ot 17, g,
. .41 in 75 ml. 11.0 at 5G4,0% 19 r. CICII.C' AL t~ odded.
Na C
and'the mixt. lic:acd at 100' ftw I br. The is
dLA,olvt!,l in boiling 11!0, amt prp,.. I "J ""'Novy.
V 101'. ""1 W. McOfi-, the

U. ;"so
IV. Mt, ictic rLil ii Mcrr ari-I iA-!%1- Nii,f-Y), ppt-9
-and ILHU. m. 267- ~i*.
prri,j,: it f:,,r;sjz, jTj. ~2~4
V: ..JC., nni ~ittfT;;
In 01~ G,1111:t pl~mn r, ru.
l~! m rn,
Tv
'rill' -11A;~ Rr"""" th" ilnril
R, ~)y r; lit) di,jr, 2 4 1,. R'NIT!, wi!h I
C I mid '2; A C. J 7 C ) 1,0 h I f- :n 1. (n', I ty . ~71 (j 1w
iti J r1f. IT;(). '21 C. -
Z. U11,J) arc hu*cd on a IT,") f~T I hr., V pi,rew ni. 164-2, , III (1J &n4 I i~-;-dhLL'LA
141 , 21 pf< .i call-g-
t 120, also pr~pd. hr., the E'tOff 6 dlvtd., cmd tfir re-srdtie io Wndl
m. ;--'--,5% is by S!wAly R(I'ling, 2 4 for tvrnl mwltI14, Riviliq the un. 176--*
1.9g.J7-0 7.5'. By the ni~thAj dctaib~A, R'WICHOff (vV, M~
-7 R'N'U~Cllq (VII), rn. Zi64' 'a m
4(), for I ~..r, Vj hoi~!jr~e t 145,
a
f'r.-Atict pppg. aft."r tf,tli- 06-95 Orcr-r, pn~), VII m, 255-7', R-xF1c1fj-
, , . :1, Flf3~, ~r;! Vill J:ic,41~, n:
witf, ffm-~. "Ife,J10
add nioilt, :A VPT 01, a-im,
f. a!") ~'5 -0,
p,,,tJ. matc-

ThIri otmctmro of lesna
---ball RuIll
:c, Mo-
PIN ay~li
0-'l dO 00t ghOw the 270 fns chractcristiL., af t!le alflo
Am exNanatloa favaying ii t)aa&ng i3 wggetM
and crievy, -c-A. 33, 4A454; Shu, -C"4,45'
Can,.
IIS). Twoctam ks ft,,jutc
ani W94e Roo c1l, 1, tj
A.,

A A/',Sk'1) T* -
547-551.43 : 347.05.9
Tlrba!~Jkl--T., Skowrofiska-Seraflnowa B., Dibrowska H. Reactions of
Ts-anguarildi e WM Aromatic Anlifirm. FrcPar-&-tj-O-n--OT-h7C-W Derivatives
of Arrildine-Phenyl-Urea, MeIr Trot-7-)rmatlon inic, DlphenA Urea

,Rcakcje cyJanaguanidiny z aminami aromalycznymi. Otrzymywanie
nowych pochodnych am1dyno-fr.,YIo-tnncznlka I przeksz1ailcenle lch
w pochadne dwufenyIomoc7.n1ka". Roczniki Chemll IFA,N). No. 3, 1951,
pp. 423--437.
Continuing the work on the reactions of aromatic arnln" with
cyanguanidine In the presence of hydrochloric acid, n number of new
derivatives of amidine-phenyl-urea were obtained, corresponding to the
Seneral formula: X.CsTf4NIf-CO-NII-C(NII)-NIIj. It was found that
balling the amidine::urea derivatives In aniline led to the splitting of
these tompoundrdnd the forniation of various diphenyl-urea derivatives,
A hypothesis is advanced for a chain reaction mechanism.

V Reactions of -C Fat'.
motion of derivatives of 1 3,d cirreaction with
aniline. 'r. urt"kAM, ...... - At."II-IC I I
as~c IIT-11. 4~-i-, -I I
'T"110%viltz
Cf. 49 , 1; ... I it-,
%ICO.NIIC(.NI )NJ cte I)ICIA. M V. nfid ill.p.
Ci, if. 1 :1 -4 (V; flr. It, 172.3' (11); Nliv, If.
S0,11,11,2117-W(W); 1ANIft,
It. 212-13' (V); 11, (M. --- (,ulfatc, lit.:a-4) 'I lie
c4mlit'll.q. vvrre l"adc by I.Alisix the with
eyanoguaiddine in tile prectice of IICL V wati fryunird
from sulfanitainide-110 iii :l(l. niolium without addcd IWI
We rt-dCtioll lVith allilille k wu-l ified fly: p-xcjIJ4Nif-
CONJIC(:,NII)NII, + p-XC,I[.NIICONIIPti
, - k CO + p-
(VID -1 Nit; VII + I.: Nil, '11hNII ~
.XcilliNill. 1-V[ %trr imlix] ag.iiu~t Mycobatterio for
bacirtio talic adiolk %V1111 illhillililli, conells. from
1-125 ,~0. 11cpuldill? 111MI-1 tile &-liv, 11,4.1 1114 fit,-
Mpin of orrmimn. Nc,-T,:mlTJq_

ji.; nc,fj (I n"I iF,,~~
,~i4 ~t, i.t ,1 12-, ir; i,
i't'. ~ ~!,
S-11 il~fa(- W1 1, F~ -0% Ult k fill
i with l: 1:(:0!. 1 Itc- ct. is t-l- cl IfIl
idru,ic ;16,1 iVIA'], WiO Iff.'I ;,rid
"t itij :ttrr at. I t1r,

URBMSKI, Tadeuss; MALINOWSKI, Stanislaw; SKOWROVSKA-81R0rNOVA, Barbara;
UHNUHMLSKA, 11ozenna; DABROVSXA, Wina-, FAIACKI. Jerzy-, GUM.
Daniel&; HAT 1, Lessek; SLOPIK. Stefan; KARMSKA. Iron&;
VINU # Jan; JAKIMOVSKA, Krystynal URBANSKA, Alloja
Search for now &ntituberculous agents. Grazlica 22 no.10:681-690
Oct 54.
1. Z Oddsi&lu Syntezy Lokow Inetytutu Gruslicy; kierowulk prof, dr.
T.Urbanaki. dyrektor: prof. dr. JJUsiewics.
(CHNNOTHMLAPT, In various disease@
tuberc., progre)
(TUBERCULOSIS, therapy
&ntitubere. agents, research)

f al
rt"! -,-Fopir Ozq! r. 1~ f
tIrA
awl Fl. ajx"~!Tc--P
IsIl
"fal ;'I'd tr, !1:74 !,Elt
1.11CA, In. '-d;"ll T~,Icts wlt;~
'Wt
the. rn . I.,,` XI. A
elf Nvith fill
I.Lravlomint, Ta, lv w.x -6 i I;, I
cl-
h1s. at 0.5,; ;If~rr 11(: itli:i%) ,,It
taiwod 42';C
VIX4 Z I.ne (I.~, in 1 42-A To 7.!) j~. 4. N ~1,1--,
w:.07 -;:0, !:,j)
awi
A
20-127'. d 11
(A II(I

Gl!-,UoTp A.
if of Allprlat3 C
'jr~, r Z:
hy,IrrxazIr- AtIn A I , I a
-2c 17, r, I
(RCC~~IJKI ull"Hy Vcl . 2:', lo. 2, 2' 'T
LC: llot of
I.'an-h 1955, I"n 1'.

CRMCOO -M a 0yanormifte w Ith aroma So a m Insa
tics-of new derivatives 04 I-DhenTI-3-4-M )dtuea,
ozttl into MMA Gen"Oves.
r
arbam M===.
OW CUM.
2S, 4 WAIUAI 120d01 War"w).
1j)- d. C.A. 49, gWf.-'
V
Tht tdknviag P-RQ N ~(Nlr,): NY were ob-
talz ed: R - Cl (1), m. 143-4*; R - MR ~U). tn.
R -a Nfft (M). tn. > 300* (hydrochtaride . BoUlac of I
wltli PhNHs Cire!rlCffNRCONHwl" but 66 PCO-7
longed boding I yl ne CGC-.
Id In Olt" act
rMlonding uvAym. cubzngides fi-om n an
s2prophyLk mynbacterij. R. Dowbenko

-POL
1954 011gligh Silliltiltity).-TbloKmkvbcktorts of tile
(111owit g uldi were preIRL: -tunidobemy1formle, m.
100', 1~-hydroxybenzoylvropltuk, m. 102'- P-a"tAmkII,-:
benwy pyrttvk, m. 178-80'; and of the As tskri of the.
foltowitig jadrstitutLd ucetle acast -nitrobenzayt, in.,
108 *; ~.amiuobenz,wlj fn. 145'; niZvtIrloyl, m 217%
Lwakodu in. 162 :~ aud
acid, M. I Nomparativedeutiligiven. Thecognp&i
_p pit i gtested for tubercuinstatic activity. C.

17 - - - - -- -
ft*LVQWE
Marv-
VII-yr-NMI-V713. lom, 130 pp,
t, 4%A-A`~
.Lnfkk I T
t, r im
Tl~& thpnpv r-,f* nltralln~-

4 /V 5- /v
'3650
Cbclerska D. On Allithwile Nifromrnpoun4s. The 8(fucture
'~7 tt
--of adind Allithatto and Ifeerneyelle Nitrocorupcmadil an 1 a Basis of C"
SM(rum,
"o n1trozM1z"ch 011t4tycrnych, lludow:% n(ekthrych nitrotwitirk6w
Plifettycritych ! he4vrncykllcznych no pofttawle ba4A widma abiorbe)i
w ultratIoleviol. RotmikilChemil (IIAN)~ No, 1, 1935, pp. 11-21, 5 figN.,
I tab,
The autho:v T