SCIENTIFIC ABSTRACT VOLNINA, N.V. - VOLNOV, N.N.

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• Collection: Scientific Abstracts
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• Document Creation Date: November 2, 2016
• Document Release Date: August 9, 2001
• Sequence Number: 17
• Publication Date: December 31, 1967
• Content Type: SCIENTIFIC ABSTRACT

VOLNINA, 11-V-, kand.fiziko-matematicheakikh nm*
One problem on embedding for a field vith the extended group of
an lcc)eahendron. Uch. zap. Ialin gos. ped. inst. no.5:11-33 '58.
(MIRA13110)
(Galois theory)

4
,WA IROV I.I.', AMMOT, F.G. Prinimali uchastiye: PSGUSHOT, M.Ye.:
CIRIGORI MA, 0.1.; POPOTA, L.P.; GONCHAROT, M.Ya.; TCLNISTOYA,.
L.T.; SORCKINA, G.Ye., tekhn.red.
[General machinery industry time norms for establishing norms
for milling machine operations; small-lot and piece production]
ObBhohemnshinostroitellnye normntivy vremoni dlis tekhnicheskogo
normirovanlia rabot na frazernykh otankakh; malkoserlinoo i edi-
nichnoe proizvodstvo. Koskva. Gos.nauchno-tekhn.izd-vo mashino-
stroit.lit-ry, 1960. 142 p. (MIRA 14:4)
1. Moscow. TSentrallnoye byuro promynhlennykh normtivov po
trudu. 2. Zaveduyushchi3r otdolom mashinostroyeniya Tsentrall-
ncgo byuro promyshlennykh normativov po truduo3ri Nauchno-
iealedovatel'skom institute truda (for Shapir
(Metalwork--Production standards)

CHEPINSIM', - A.M.; GESS, B. A.; KANAVETS, P,. L.; MELENT IYEV, P.N.;
K!i0DAKq L.ap SOKOLOV, G.A.; BORISOVS Yu.I.; CMUTM, V.I.;
Prinimall uphlistiyeo VAVILCV,, N.S.; MAKARCHENKO, Y.G,;
KISgLrf, G
opo; L, Ro.A.;, MOREYEVA, G. ft.
Testik.g gr&CnuIes made by the method Wchemical catalysis
ill a laborat6ry -shaft fumace. Tr~dy IGI 2200-78 163o
(MIRA 16'-.11)

IXOGOP
VOLIXOGORSKIII P.
VOLIXOGORSKII, P. Velikil. put'. S kartoi, sibirskoi zhe3.ieznoe dorogi 1 79 risunkami v
~tekstie. Moskvap 19C4. 240 p. "Iztochnikd" e..: p.
I
DLdFCDK7550V
JZ c
S
0: W. Soviet Geography, Part 1. 1951# Uncl,

VOLINOGORSKI/S P.
Velikii put. S kxrtoi si.Mr-5koi zhelieznoi dorcgi 1 79 risunkami v tekstie.
Llfhe Great route, with a map of the Trans-Siberian rallwag. Mcs~-va, K. I.
Tilchomirov, 1904. W p. Ulus., fold. maps (Po blelu svietu. Illuatrirovannaia
geograficheskaia bibliotekR.. vvp. 2e)
"Istochnikill: p.,g DLCi DK755-V
SO: Soviet Trar.9portation and Copwiunications) A Biblioaapbyj Library of Congressp
Reference Itepartment, W`KFhIr_.g_ro_n, 1~52, Unclassified.

VOLKOEWSKr, R., mic
Te,chnic of sawing'tandons. Acts. chir. orthop. trous. cecb. ?-4
nct-3:259-264 May 57.
(TI=NS, surg.
technic with radioopaque sutures (Cz))
(SUTURES
mdloopaque sutures in tendon surg.. technic (Cz))

VOLNOV, A. M., GUIENKO,, G. B., ISJLyEV, B. M. and MARGULIS, U. Ya.
ItDistribution of Deep Doses in Water Phantom from Tele-Curie Units Charged
with Radioactive Cobalti" Medgiz, 1955

VOL11:011 D A - SOROKOV, D.S.
Geology of Bennett Island. Trudy VIIGA 123:5-18 161.
(MIRA 14-10)
(Bennetta Inland--Geology)
I

VOLIBOV, D.A.; YASIUN, 11S.
Interrelation between the S~rues-Salinskaya and Laparakaya
aarias In the Cambrian of the nortbeastern part of the Olenek
Uphouval and ti,is of their formation. Trudy INGA 114:62-64
16o. (MIRA 13:11)
(Yakutia--Qeology, Stratigraphic)

VOLINOT, 1
Machine vith an electric motor drive for bending pipes with a
diameter of from I/Z to 11. Rate. i izobr.predl.v stroi. ne.124:
7-9 '55- (Pipe banding) (RLRA 9:7)

of Tin Chlorija Solutions In Sonis bitiji b
Solvents. O- '" and 0. N. Vol'nor (zhur. n,, Whim.,
SIN
Imu. m of Goln.
-ofSnCI ini%lcoholm carboxylic micls,and astars. using graphite
in the virinity of the anode and evolution ofCl. Deposittonof
'l,
nC + I;nwu).In the eamofgnClsoln. in MeOff,&Mitlan
S
of Sa mk the callode bkm 1)13m. A Wativa ochome of
diemiat~iun ofl3nCl, cmaL&jjn with sloohols, carboxylic wide,
''anti esters is mlvrd,--,45 1% L.

VOO/61/
USSR/Chemiatry - Electrolysis
Card 1/1 Pub. 110 14/27'
Authors 3 Kuzl!mina, B.G., and Vollnov, G.N.
..........
~Title I Eleotrolysis of SnCl solutions in certain organic solvents
4
'periodical : Zhix.-. fiz. "im. 28/2, 282-286, Feb 1954
Abstract Exp~rimsnts were conducted to determine the electrolysis (with graphite
ele,itrodes) of the following solutions : SnCl 4_'Methyl alcohol, SnCl4 -
ethyl alcohol, SnC14 - isoamyl alcohol, SnCl 4 - acetic acid, SnCl -
amyl-acetate) SnCl - butyric acids SnCl 4 - ethyl formiate and SI - ethyl
acetate. The electrolysis of SnCl - acetic acid solution was carrked out
wita an Ag-anode. An increase in 61 ion concentration and decrease in Sn
ion concentration was observed in the anode space and vice versa in the
cat1iode space. CI wac the product of electrolysis over an anode and an
SnCI 2+ Sn deposition was the electrolysis product over a cathode. Six re-
ferences: 4-USSR; 1-USA and 1-German (1916-1948). Tables.
Institution *
Submitted April 23, 1953

ElectrnIrjI* of sttfqnfi,~ rhInrlife soltitkial In come afgLmle
golvent i;,' sandG.IUM'"My Zhar.rig.-
h, '2L8 9,54 .-
Khim. 2 of such In
MeOH, EIGH, Iso-AmIDII, ALOIL AMOAe, PrCOH, HCOr
Et, or EtOAc were electrolyzed between graphtle electrodes
for 10-70 bro. with a current of 2-30 ma. - The anolyte after
"I clontaintd applox. 10% less Sit and 100/0, more CI -
orilluil soln., and the cathol:rte showeil the up-
M. ite changes. The anolyte cantaffind free Cl (whkh
p-Aually reacted with the solvent), it ,td on - the cmthodr
there w2s a deposit of Sn and SnCle. When a Ag Qnode.
wo uted, the-Mrt. of A&CI agreed with ParadAy's low.
Thmi the complexes of SnCL with act. COMOS., R, hive
the structure (SnCli-nRj03 (SnCl:xRl +4' + 2C1-.
Bikermait

00
Go
God
0
00,
so:
powgfffg 4w V~9-1 I
Me I I
min& AV
Sm"im a# Ms.' N
aubm dm ad mw
ON
&bow
so
U-NIPPON6, d on, typ
wjdwp w
+16
RAW9+44460= me, pr. ft.
a WAM Complex
ple",
A-A A X-A.-S
00
'00
wee
.001
INGO
lose
mso
600
Woo
%o
%o
goo
%9
woo
Mso
186400 mat ART
o I T a I it 0 9 a 4 1
U a all 191 W.
10009 0 1 0 ***Soo a 0 0 0 6 0 0 0 0 0 0 0

YQLMV. I.F.
on
Beat alarm used for checking cooling conditions. Mashinostroitall
no.3:33 Mr 157. (KLRA 10:5)
(Thermos tat)

atw Nib i "107is.s. No. 23.
Itpal. qq'Aws P'Oloy AW I'so moiw fiquaf
()bsb(k$ f swc. Khi-.. c;~~ in and pl. in
(d ASN' in. Iloah
""Kh
lufm*

Z)1-4.-7U tensary systeas vm studW by the &hrrint-
withers "arot rvaWw" melbod at 66* and 76". and by ukina
the data of theft the Hytivermal diagmat was drul. for the
runavol-lou'. AIM bg *Wid Own and Lbe points on the
only. cw" limiting tbitir stability. gives w parventw ot
P of CaCls. C&Ch.-
-0 ptom W
211.0: 0 ,0*67,271o4l.74 39-00; CA(Cl,%)j: 41.N.W.ft
to 51,7M. 21.114; CA(CIO&LINA): AIJIL 21A4 to 71.78,
00. The ca-spivadiij dots at 761 afts CaCle-2110.
0:0. 69.A3 to 41.94. 34.03; Cs(Cl(h~.- ~ 41,94. 34.03 to
77.83.0.0. The coxoplete polytbertnal diwass slimn Sdil-
lemat retimas wbere the wAid pbaws wv, Marti" with
the" fljkw at the lg",e*9 tempo.; Otch-611100 ar-cach
Ca".2HIO. -d "66.),-
Ariki Millet
4~

UM/Chemistry - Oxidauts Jul/Aug 51
"Interaction of Potassium Peroxides With Carbon
Dioxide," S. Z. Makarov, 1. 1. Vollnov, Lab of
Peroxidic Compds, Acad Sci USSR.
"Iz Ak Nauk SSSR, Ot&el Xhim Nauie, zio 4
PP 370-376
Established that, at 00 and 100 C, X02 and X204
react with C02 to form 02 and K2CO4 (stable over
vide temp range; not previously described in
lit), which reacts with C02 to form K2C206; lat-
ter decomps into 1!~C205 and 02. At 2.50 w-ad 500 C;
3.92=8
UMR/Chemistry Oxidants (Contd) Jiul/Aug'51
112C206 and X2C205 do no"- fom; K2C04 -in C02 atm
dtcomps into 02 and. FL~CO 3* Higher temp &ccele-
rates formaLtion of 'K2C04 from X02 and subsequent
decompn of former.
K
19M8
#4

U S s
SYAOF113 Containing concentrated hYdrogen pamilde. V. Thermal
charicterlstics of the solid phases of the systeru Ca I OW, 11,0. 11,0.
S. Z. Milia-, and N. 1%. VI. Ttruary System 116 Mll,-
11.0. at 0' and 20'. S, Z. Mahamv an, It. 1, v"In"v (Iroioia
Nauk 'O;Sle- 01M. Nhim. A'auk. 193T.-STYK-403. 763-
7611).- V- 11w h%clrac~ C~O 814 0 and Ci(3,. fl,O trAdily 1-c
lip, 14ili.IV C~O, t 111C P-I.VkIrAC CA'J,. 21i,t),
iA UlWal-Tv. clinlif-ating 0. at 48-70% t., give CLO, 211,0.
TIW ~Ihd pha- Iuf"I aw sig0l, "ad
I I'a R. Tttc~c,)r

USSR
and 201. AW.
Nogli 3.3 il. C-4.1
49, 700e. "e givrn sit 0* jidA +!N)*i
19, ~ in
or IIA ;n
Roginskil. Dicklady Aked, Naxk S.S.S.R. 94, 7a 1054);;
~.rf. 4r.A. 44. M27d.-The. cffect w4a defd M aMlair 1,80,

KAMOT, S. Z.; VOL!EUVA-4"t
coneentrated, hydr
Stud,r of systems contaWn ogen peroxides Report
no*6,, Isotherms O'D and 20 of the ternary system: Yg(OH)2- H202-
H290 Isv*AF SSSR Otdokhim,, nauk no-5:765-769 3-0 154.
(MLVA 8:3)
1, lustitut obahchey neorganicheekor khtall in. N.O.lurnakova
Akedouli nauk SM.
(YAcnesi-um peroxide) (Hydrogen peroxide)

VOLIMOV, I.11
Thermal characterlstio of dibydrate calcium cUorate. Izv.SeL-t.fiz.-
khin.anal. 24:160-161 154. (XIaA 8:4)
1. laboratortya parekisnykh soyedineniy Akademil nauk SSSR;
(Calcium ohlorate)

PIZ^,
Distr
'i The IS- alubUll Ltathe.-- hor the z3vom ca(cla
CX,lOH - H10.
hug;- s
sa!r. ivscc,~f- , %
the frd'matkn 'J ."h, 'A C., C ~rl.
This omurA li Inge

f solubility of s7.06
~Oth;ms 0
4
(~,'e7 M M a Fis-
I if. 1~ IM
Matt- Mauk,
Ma2S
49
-75*
r S. 25, 32G Isotherm ly, for 0
1 rM t. depending on conen. and temp., only 2,
rj~
hydroxychtorides, CaC[jJCe(OH)j.l2ffjO and CaCl,.Ca-
(OH 3*.H%O, are formed by reactIm of CaCla solm. with
oil for which field-9 of sepa. and limits of stability are
eitAhllsked CaCIOC0011 1.131110 IS ItAbIC In CqUil,
with sottis. contS. up to 32N. CaCil, up to 38.9'. C*C1
11),.11.0 Is stable In tquill. with volus. cmtg.
C&T 324N
Sep . of CaCls frot
CA it, from 5 to 75'. Conditions to a
r 0
sot"s. as hyawlychlarides can be dttd. n the basis of th
-U.' of Polytherms. Eurilla f4reffe
,"'Cu.
'40
F,

VOLINOV, I.I.
Thermography of proxide compounds. Dokl.AN SSSR 94 no-3:477--479
ja 154. (91-RA 7:1)
1. Institut obahchey i neorganicheakoy khimii im. H.S.1urimkova.
Predetavlano akademikom I.I.Chornyayevym.
(Thermochemistry) ~Psroxides)

VOLINOV, I.I.
SObLbility isotherm 00 for the system: Be(OH)2-H202--920. Izv.Sekt.
fiz.-khim.anal. 26:211-214 155. ()aaA 819)
1. Institat obahchey i neorganicheskoy khtnit im. U.S. lurnakova AN
SS.71. (Solubility) (Beryllium hydroxide) 01ydrogen peroxide)
a

VOLIMOV, X.I.
OXydrogen paroxicle.9 V.Schumb, C.I.Satterfield. R.L.Wentworth.
Reviewed by I.I.Vol'nov. Zhur.noorg.khlm. I no-8:1932-1934 Ag
'56. Mak 9:11)
1. Laboratoriya pereklanykh ooyedinenly, Institut obahchey i
noorganicheakoy khtnit, imeni, N.S.Iurnmkova, Akademil, uaqk SM.
(Hydrogen peroxide) (Schumb, W.) (Betterfield,C.N.)
(Wenthworth, R.L.)

,TJSSR/Inorganic Chemistry. complex c"on.1pounds. C
Abs Jour : Ref Zhur - K~himiYa) No. 81 195?, 2A4.
Author : _V~ollnov, I.I., Chamova, MI.,
Sergeyeva-1--T~-P., Latyshevaj Ye.I.
Inst
Title Ifesearch ill Region of Synthesis of Silper-
peroxides of Alkali Earth Metals. henoet, I
Interaction of CaO2.81120 with Perhydr.ol.
at about 1000.
Orig Pub Zh, neorgan, khJmii, 1956, 11 No. 91
1937 - 1942~
Abstract The bibliographic data (Traube W., Schulze W.,
Ber., 1921, 54 11 1626; Erlich P., Z. anorgan.
Chem.1 194u1 2~21 370) referring to the for-
mation of dark-cream colored paramagnetic pro-
ducts containing up to If.% of Ca(02)2 at t1le
Card 1/2

VOL MDV, 1. 1.
Thersal stability of calcium hydrox7chlorides. Isy.Sakt.fis.-khim.anal.
27:251,-254 156. (MA 9: 9)
1.1natitut obahchey I noorgasichoskey khIsIi Imeni N.S.Kurnakeve AN
SSSR. (Calcium chlorldo)

USSR/Inorganic Chemistry. Complex Compounds. C
Abs Jour : Ref Zhur - Khimiya, No. 8, 19579 261441.
Author : Vollnov I.I.- Shatunina A N.
_iFl
Inst ca ~;;~ 'oi-;iences of USAR.'
Title Possibility of Preparing Ba(02)2'
Orig Pub Dokl. AN SSSR, m67 1109 110. 17 87 - 88.
Abstract Assuming that the structure of Ba(02) was
similar to the structure of superperoiides
of alkali metals, the authors estimated the
value of the equilibrium constant of the
reaction Ba02 (solid) 02 (gas) Ba(02)2
(solid) (1). Using the approximately de-
termined values of LH298- -11+.2 keal and
of L S998 = -45.1+ entr. units, the equili-
brium pressures of 0 were computed for the
reaction (1) at 25, NI 2007 210 220 2309
250 and 3020, which were 32, 759 1300913150,
Card 1/2
------------ 1- ------ -

TOMNOT, r.r.
I
OA now treatise on inorganic chemistry" (in French], val. 1. by
Paul Pascal. Reviewed b7 I.I. Volinov. Zhur. neorg. kh1m. 2 no.ls
229 JS '57. (IM 10:4)
(Chemistry, Inorganic) (Pascal, Paul)

AUTHJR: Vollnov, I I and Latyshevaj E.I. 558
TITLE: Research in the Field of the Synthesis of Alkali-Earth Metal
0
Superoxides. 11. Foxmation of-Sr(02)2 from SrO .21 0
i:
N
ek
(Folski v Oblasti Sinteza Superoksidov Shcheloc
oz
e
nykTa
'
Metallov. Il. Obrazovanie SiPr2)2 iz SrO2
,2H202,
PERIODICAL: -lib'mmal Neorganicheska-Khimili" (Journal of Inorganic Chemistry)
V-07.11y 140 21 Pp.25!J-2b2. kU.b.b.A.) 11 -
3
ABSTRACT: 5~OC, that is at a
By the vacuum-drying of Sr%'.2H202 at
temperature lower than the ecomposition temperature of crysta-
111isational hydrogen peroxidep.and at a residual pressure of 10
mm. mercuryp a perbxide preparation of strontium has been pre-
pared for the first time which contains Sr(02)2 in concentration
of the order of 17.5 wt. %. The mechanism proposed by Kazarnovs
ki3,*for the formation of superoxide from peroxide perhydratess
ba.sed on the formation of the intermediate radicals OH and B02
haS apparently been confirmed by the results obtained.
Thore are seven Teferencesv three of them Russian.
Ref .4, quoted in the textv is:
I' A.Kazarnovskii and A',B.Neidingp DAN SSSR,Vol.86jNo.4,p.7l7Pl95
There are 2 figures and 3 tables.
The work was-carried out at the.Institute of Inorganic Chemistry
imeni Xurnakova of the Academy of Sciences of the USSIL
Received 4 August, 1956.

TLE:
ODICAL:
Inov I I Latyshevv E -I..1 and Chamo-----V--N.
Vol 3va., -
Research in the Field of the Synthesis of.Alkaline-Earth-Metal
Superoxides. III. Formation of Ca(02)2 from CaO ,2%011 .-
(Poiski v Oblasti Sinteza Superoksidov 5hche1ocLoz'emb11nYkh
Metallov. III'. Obrazovanie Ca(02)2 iz Ca02'
.2H2O2
"ill:i~nal Ne (Journal of Inorganic Chemistry,
organicheska-Ebimii
Vol. 1, No.2#
Contrary to some theoretical expectations it has been found that
Ca(02)2 can exist in preparations containing relatively large
quantities of CaO2. Ca(02)2 in concentrations of the order of
16.5. wt % could be obtained reirilarly by vacuum-dryin2.
Ca02,H202 at 500C at 10 mm Bg. The presence of Ca(02~2 in such
preparations has been established by chemical analysis, from
heat~mg curves and from magnetization measurements. On prolonged
storage the Ca(02)2 content decreases.
3 Fi)presp 3 Tables,
The work was carried out at the Institute,of Inorganic Chemistry
imeni Kuxnakova of the Academy of Sciences of the U.S.S.R.
Received 1 September, 1956.

VOLINOV I
Vfall--
w5upplement to .22or's comprehensive trestlSib-of-1wrommic
azd theoretical cbevietry" Lin IselishI4 Revie"d I.I.
Vallnov. ZhunneergAhim". 2 20.4:10 Ap 157- ("u 10, 8)
(Ghemistry, Organic)
(Chemistry, Physical and theoretical)

A/V -r
SHATUNINI, A.N.
VOLINOV, I.
Reactivity of superoxides of alkaline earth metals with H 0 and
C02- Zhur.neorg.khIm. 2 no.7:1474-1478 JI 157. (Mig 10: 11)
1. Inatitut obahchey i neorganicheakoy khimii im. U.S.Xurnnkova
AN MR.
(Alkaline earths) (Water). (Carbon dioxide)

0
VOLINOV, 1,1.; IATYSHEVA, Ye.l.
Restarch in the field of synthesis of superoxides of earth alkali
metale, Zhureneorg.khim. 2 no-7:1696-1698 J1 157. (MIRA 10:11)
1. Institut obahchey i neorganicheakoy khimli im. N.S.Kurnnkova
AN SSSR.
(Barium peroxide)

,.,,VOLINOV, I.I.
"A. new treatise on inorganic chemistry, volume If): 111trogen, phoFfpho-
Me" [in French] by P. Pascal. Reviewed by I.I. Tollnov. Zhur. neorg.
kbim. 2 no,12:2838 D 157. (MIRA 11:2)
(Nitrogen) (Phosphorus)
(Pascal. P. )

--41,
SHATUNIM, A.N.
. 1,
Irbriation of LIO from L12O2-2R2O2. 1xv. AN SSSR Otd. khts. nauk
no.6t762-76) .19 ;5?. (KIRA 10:11)
1. Ingtitut obahchey I noorganicheekoy khimil im. N.6. Xurnakova AN
sssa.
(Lithium oxide@)

,ad
~f
h
h
t
W
(011V
.
em
erm
At
t
e syff
I
11:0 wm dad. 'Me solid phAses tee,' CitCliZCm(0U)v,-
q '12HsO (1). and CaChAH,0 witre present. Promtbmitno~
earlier avallable dat% the Polyttiam w%3 owsix Kiect; Ati~ ~
triple point lomted at -01' by lntrrPolAtIon"CImt?jAt#)CA-"

l
"
I-Ca(011)s with cmly 6% CACIt. - SYtIthctic 10W. t
"
'

F 10, 1 _"c`4 CaCls vrere studled, ne forruet were
If
e
t
11

compartd.with solrLs-.'. appfcochlag the Cocipts. of SIXmt -
ODD
CaW
NaCI 4
99
Ca (011)
C
Ct
03
t
10
11
,
.
,
a
1
4
or wi
g.
s
,
,
q
U. 10, and KILOH 0.001 vrt. %, d. 1.112 (A% .. Scitam. omitt.
22% Cacig WeTe Iritetol. by tilt addil. VF CaQS to milk 0t
11ine at U)-CO* (B) and compared with voluts. &P oaddriC
the Com )f of -s'v-nt 14uor whidi had tial 11
Coutg. ELI, 21.1s, mici 61" Cast). OA I.QH 0.

0
-
1
C
M
S
A
). Coohns ILlowly to 1
d, t.2$ (11
K
act 05 7 from
WI and U,1501 frcnri A mid A' and 51 A
'M
of I exilibit 11 CnZt eiguic
ve
d 2P
B
h
ti
.
ei
ng cur
s
,
an
e
cflects: it W"Asta-ble Lip tD50" at 110' Ill0tvapd.,skridat
iornpd. to CaO and Hj0. DV'V"'FV of
6401 Ca(011), dee

.
I at 506 em. 1470 140 (b;tsfd an wt. ol I
i
.
con(g. 241,~o ;tCly- I n
~A;r'
7

V'() C,
AUTHOR; 78-2-41/43
-
TITLZ: On the Thermographic Curves of the Peroxyhydrates of the
Metals of the Second Group (0 krivykh nagrevaniya gidratov
perskioey metallov vtoroy gruppy)
PERIODICAL: Zhurnal Nearganicheskoy Xhimii, 1953, Vol- 3, P1)- 538-540
(USSR)
ABSTRACT: The thermographic curves of the proxyhydrates of the metals
of the second group of the periodic system were
investigated with the aid of the recording pyrometer of
Kurnakov. In a comparison of the thermographic curves of
the octahydrate-peroxides of calcium, strontium and barium
with the curves of the hydrated peroxides of maCnesium, and
cadmium the great difference between these two thermo-
graphic curves is distinctly to be recognized. The thermo-
graphic curves of the octohydrate-peroxides of calcium,
strontium and barium are characterized by throe successive
endothermio effects which represent the melting, dehydratiin
and decomposition of the peroxide to oxide and oxygen. It
Card 1/3 was found that the thermal stability of the peroxides in-

On- the Thermog:raphio Curves of the Feroxyhydratea of the 78-2-41/43
Metale of the Second Group
creases with increasing atomic weight of the elem nt Thus
* 6C,
e. g. the thermal decomposition f8r Ca02 lies at 38o for
SrO2 at 48ooC and for BaO 2 at 790 C-
The thermographic curves of the hydrated peroxides of
magnesium, zinc and cadmium are characterized by only one
endothermie effect in the temperature range of from loo to
1150C which corresponds to the dehydration of the peroxides
and an exothermic effect which corresponds to the de-
composition of the peroxides to the oxide form and oxygen.
With an increase in the atomic weight of the elements
the decomposition temperature of the peroxide compounds of
magnesium, zinc and cadmium decreases, thus S. g. the de-
composition temperature for MgO lies at 375 C, for ZnO
at 2250C and for CdO 2 at 1950C.2The h1drated form of thl
peroxides of magnesium, zinc and cadmium does not occur as
hydrate form of the peroxide of the type y2+0 2-
, but as
OH.Me(O.OH).xH 0. There are I figure and 3 references, all
of which are Havic.
Card 2/3

On the Thermo,graphic
Metals of the
ASSOCIATION:
SUBMITTED:
AVAILABLZ:
Card 313
Curves of the Piroxyhydrates of the 78-2-41/43
Second Group
Inatitute for General and Anorganic 17hemistry imeni 11. S.
Kurnakov AS USSR (Institut obshchey i neorganicheakoy
khimii imeni N. S. Kurnakova Akademii nauk SSSR)
may 9, 1957
Library of Congress

'Alt? T
AUT1101112 i Vol I nov. 1. 1. , Chamova, V. N. 7,5 -3-5-06/39
Shatunina, A. N.
TITLE3 VaThe Formation of Ca(009 bv Irradiatica of Ca02*2H2O2
With Ultra-Violet Rays (V. Obrazovan'-ye Ca(02)2
oblucheniyeri Ca02.211202 ult'ruf'oletovym' luchami)
PERIODICAL: Zhurnal Noorganiche3koy Khimii, 1950, Vol 3, fir 5,
Pp 1095-1097 (USSR)
ABSTRACTi By irradiation of CaO 2H202withultra-violet light.,
Ca'(02)2 is Obtained, i~e presence of which can only be
verified by chemical analysis.
The obtained preparation is lemon-coloured, similar to
11a02- The final product is not uniform.
The manufacturing proceas is difficult to reproduce.
In some cases the final product contains from 7-*'
Ca(O ) and in others it has a higher content of from
J/2)
10-1 %.
Ca(02)2 was also obtained by irradiation of Ca02-211202
in a Pischer pistol consisting of quartz-glass3at a
Card 1/2 temperature of 25-450C.

The Formation of Ca(02), by Irradiation of Cao 2' 211202 713-5-5-"-/39
With Ultra-Violet Bay#
Ca(02)2 is very unstable.
There are 1 table and 0 references, 5 of which are
Soviet.
ASSOCIA~?ION: Institut obshchey i noorganichoskoy khimii im. N. S.
Kurnakova Akademii nauk 03311 (Institute of General
and Inorganic Chemistry imeni 11. S. Kurnakov,AS US3R)
SUBMITTED: May 10, 1957
AVAILABLE: Library of ConCress
I. O*Icium oxide s-Produation 2. CALlcium exidem-Froperties
Ultraviolet r&ys-:11,pplicationa
Card 2/2

NO V
AUTHORS: Vol nov I. I, Chanova, V. 1". N-3-5-7/709
TITLEt Vi. Surfaco Effects on the Formation Proccou of Ca(02)2
From Ca02.211202, (VI. Vliyaniye poverkhnosti no, protsess
obrazovaniya Ca(02)2 iz Ca02.2H.02)
PERIODICAL: Zhurnal Neorganicbeskoy Khimi-4, 1958, Vol 3, 11r 5,
pp 1098-1099 (USSR)
ABSTILkC'!: The dependence of the yield of Ca(02)2 from the surface on
which CaO ?' 2HJ02 is dietributed,was determined.
The experimen s have been performed on different
surfaces from 70-910 CM2. By the increase of the surface)
the yield of Ca(O )2 in the final product is also in-
creased. On a curiace of 910 CM2 the yield reaches
40%. In cn of further increase of the 3urface.Ifrom
f
910-3630 cm the yield of Ca(02)2 is from 40-45`.~,
The obtainee final products contain also calcim/oxide,
calcium hydroxide,and calcium carbonate.besides"Ca(02)"
E.g., the preparation produced on a surface of 36630 cm~
exhibits the following compoaltion: Ca(02)2 - 44:99';J,
Card 1/2 Ca02 - 12,67%, Ca(OH)2 - 31,17~6, CaC03 - 12,07~,4,-

VI. Surface Effects on the Formation Pracesu of Ca(02)2 78-3-5-7/39
From Ca02-2H202
The obtained results indicate that the production process
of Ca(02)2 from Ca02.2H 202 proceeds according to the following
equation:
CaO 2- 2H202 1/2 Ca(O 2)2 + 1/2 Ca (OH)2 + 0" + if202*
There are 1 figure, 1 table, and 3 references, 3 of which
are Soviet.
ASSOCIATION: Institut obzhchey i neorganicheokoy khimii in. N. S.
Kurnakova Akademii nauk SSSR (Institute of General
and Inorganic Chemistry imeni 11. S. Kurnakov, A:3 USSR)
SUBMITTEM: April 17, 1957
AVAILABLE; Library of Congreso
1, 041cium c)xideP---'r(dv,-r.U t:,---s7u:j tee efff3cts
Card 2/2

VOL' MV.,.:E.I. ~-*TYSWA, Te.I.
Preparation of magnesium peroxide. Zhur. prikle khim. 31 no,10;
1597-1599 0 '58. (MIRA 12:1)
(Magnesium oxtasp)

5(2) SOV/76-4-2-2/40
AUTHORS: Vollnov 1 1. Chamova, V. N., Sergeyava, V. P.
TITLE: New Data on the Formation of Superperoxides of Calcium and
Strontium (Novyye dannyye po obrazovaniyu nadporekisey
kalftsiya i strontsiya)
PERIODICAL: Zhurnal neorganicheskoy khimii, 1959, Vol 4, Nr 2,
pp 253 -256 (USSR)
ABSTRACT: The Ioptimum.conditions for the production of Ca(02)2 and
Sr(O 2)2 from Ca02*2H202 and SrO 2- 2H .02 were &termined. , Mh~t
percentage of the Ca(02)2 and,Sr(02)2 content in the de-
composition products of Ca02.2H202 and SrO 2.2H 202 depends on
the temperatur4jii.time and surfaoe area. A temperature of r,-OOC,
a duration of 160 minutes, a surface area of 1800 cm2, and a
pressure of 10 mm Eg are recommended for the production of
Wo and Sr(O On6 gram initial sample of MeO 2H 0
2)2 .,,2)2' 1 2 2@ 2 2
is distributed ~; the surface of 1800 cm . On the decompositicn
Card 1/3 of Ca02*2H2O2 the analyses of the solid phases formed show

SOV/78-4-2-2/40
New Data on the Formation of Superperoxides of Calcium and Strontium
that with an increase of the percentage of Ca(O 2)2 content
the Ca (0H)2 dontent.rises and the CaO 2 content drops. This
dependence is caused by the occurrence of a secondary re-
action between Ca(0 2)2 and steam, or by the participation of
hydroxyl radicals in the reaction. The transformation of
CaO 2' 2H202into Ca(0 2)2 mixed with solid siccatives (silica-
gel, P2 05, anhydrous Ca02' alkali hydroxides) or liquid
rectifiers (absolute ethyl alcohol, Col 49 dioxane, diethyl
phthalate) was investigated. The Ca(O 2)2 content of the solid
-products is 40 weight %. On drying in a vacuum KO and NaO -
2 2
containing products are formed from a mixture of CaO 2' 2H2 02
and KOH or NaOH. Samples with 40 weight % Ca(O 2)2 can be
stored in hermetically cx~sed vessels. With an extension of the
surface area, on which the preparations are distributed, the
Card 2/3 Ca(O 2)2 and Sr(0 2)2 content of the reaction products in-

SOV/78-4-2-2/40
New Data on the Formation of Superperoxides of Calcium and Strontium
creases. There are 3 figures, 3 tables,.and 4 Soviet
references.
ASSOCIATION; Institut obahchey i neorganicheskoy khimii im. He S. Kur-
nakova Akademii hauk SSSR (Institute of General and In-
organic Chemi-stry imeni N. S. Xurnakov of the Academy of
Sciences USSR)
SUBMITTED: November 3, 1957
Card 3/3
_00

5(2) SOV/78-4-2-3/40
AUTHORS: Vol'nqX__1__Z,~ Shatunina, A. N.
TITLE:, The Formation of Lithium Superperoxide From Ll 20 20 2H 202
.(Obrazovaniye nadperekisi litiya iz Li P2 .2H 202)
PERIODICAL: Zhurnal neorganicheskoy khimii~ 19599 Vol 4, Nr 2,
Pp 257-259 (USSR)
ABSTRACT: Lithium.peroxide is formed on drying Li2 020 2H 202in vacuo
at , =~-1200 and 10 Hg , A thin -layer -of the Li 202' 2H2 02
sample was laid on the cryst.allizer surface and was dried.
Th e change of the-percentage of the LiO 2- content of the
preparation-in dependence on temperatures of 100o, 1200, and
700C and time, was investigated. The results are shown in
figure I There-is 1 figure, 1 table, and 12 references,
8 of;which are Soviet.
ASSOCIATION: Institut obshchey i neorganicheskoy khimii im. N. S. Kur-
nakova Akademii nauk SSSR (Institute of General and In-
organic Chemistry imeni N. S. Kurnakov of the Academy of
Card 1/2 Sciences, USSR)

5(2) SOV/76-4-7-5/44
AUTHORS: Vollnov, 1. 1., Shatunina, A. N.
TITLE: The Forming of NaO 2From Na202* 2H 202 (Obrazovaniye Na02 'z
Na202* 2H 202)
PERIODICAL: Zhurnal neorganicheskoy khimii, 1959, Vol 4, Nr 7,
PP 1491-1493 (USSR)
ABSTRACT: The compound Na 20 2' 2H202was produced according to the slightly
altered method by F. D'Ane (Ref 3) by the action of 98-99%
hydrogen peroxide upon solid CH 3Na-0-5-CH 3* After the decay
temperature of the crystalline compound had been determined as
amounting to 1520 by plotting a heating curve of this compound
(Fig 1), the compound was dried in a vacuum at 70, 100 and 1200j
i.e. below decay temperature The peroxide-oxygen was determined
gasometrically according to ;. Seyb (Ref 4). The experimental
results are given by table 1 and figure 2. Preparations with a
content of about 30 weight % N&02 were obtained, which is con-
siderably more than has hitherto been known in publications.
There are 2 figures, I table, and 4 references.

5(2) SOV/75-14-2-18/27
AUTHORS: Vollnov, 1. 1., Lalysheva, Ye. 1.
TITLE: On the Separate Determination of Peroxide- and Superoxide
Oxygen in Superoxides (0 razdellnom opredelenii perekisnogo
I nadperekionogo kisloroda v nadperekisyakh)
PERIODICAL: Zhurnal analiticheakoy Ichimii, 19591 Vol 14, ?Tr 2, pp 242-243
(USSR)
LBSTRACT: The differences in the character of linkage between the bridg-
ing oxygens in peroxides and ouperoxides become manifest in
the hydrolysis of the compounds. Peroxides hydrolize accord-
ing to the equation ?As202 + 2 It20 - 2 MeOH + H202- Superoxides,
on the other hand, hydrolize according to the equation
2 MeO 2 + 2 H20 - 2 UeOff + a202 + 0.4 In this case only 2/3
of the active oxygen ("superoxido-oxygen") are transformed
into 02 , and only 1/3 of the active oxygen ("peroxide-oxygen")
forms hydrogen peroxide.' Seyb and Kleinberg (Ref 4) devised
a gasometric method of determining separately peroxide- and
auperoxide oxygen in NaO 2 and KO 24 By thin method diethyl-
phthalate as buffer and then a mixture of glacial acetic acid
Card 1/3 and diethylphthalate are added to the weighed portion. Super-

SOV/75-14-2-18/27
On the Separate Determination of Peroxide- and Superoxide Oxygen in Super-
oxides
oxide oxygen is then separated and gasometrically determined.
For the determination of peroxide oxygen the hydrogen per-
oxide formed in the acetic acid solution is then decomposed
by a solution of ferric chloride in hydrochloric acid; the
volume of the oxygen formed in this connection is measured.
Thin method gives reproducible results in the analysis of
alkali metal superoxidea; for the analysis of preparations
containing only small amounts Of 3UPOroxides it is not suited
because the weighed portions should be very high for the de-
termination of peroxide oxygen. On the basis of the investi-
gations on the separate determination of peroxide- and super-
oxide oxygen from a weighed portion the authors suggest the
following method: the superoxide oxygen is gasometrically de-
termined according to Seyb and Kleinberg. The gas formed in
the preparation of the weighed portion with acetic acid mustf
however, also be analyzed with respect to CO since a con-
tamination of the superoxides by carbonates in unavoidable.
Peroxide oxygen is,however,not ganometrically but only per-
manganometrically determined. An aliquot portion of the
acetic acid solution still containing diethylphthalato in
acidified with phosphoric acid (1:4) and titrated with a,O.1 n
Card 2/3 potassium permanganate solution. The results of the determina-

5(2)
AUTHORSs Vollnovq I*I.l Kolotovat Ye.I* SOY/78-4-9-34/44
-----------------------
TITLEs The Solubility Isotherm -200 of the System Na2 so 4 - H 202- H 20
PERIODICALt Zhurnal neorganicheskoy khimii, 1959, Vol 4, Nr 9, pp 2143-2145
(USSR)
ABSTRACT: It was the objective of the investigation to determine to what
extent crystal water can be replaced by H 202- Reference is made
to previous publications dealing with this subject (Refs 1-10),
inter alia to the paper by M.I. Ozerova (Ref 8). The results are
given in table 1 and in the phase triangle given in figure 1.
The isotherm for -200 could be found in the H202 concentration
range of 12 - 82 % by weight only, since aqueoue.H 202solutions
with values below and above the values forementioned freeze at
-200. Beside the known hydrates Na 2 so 4# 10H20 and Na2so 404H 0 two
2
chemical compounds with crystalline H 2 02were found: The already
known compound- Na 2SO 4*O-5H202*H20 and the compound Na 2soV 3H202t
which was prepared for the first time and whose thermogram is
Card 1/2 given in figure 2. A comparison of the data found in the

The Solubility Isotherm -200 of the System SOV'/78-4-9-34/44
Na2so 4 -H20 - H20
relevant publications and those found by tho authore suggests
that the abovementioned system has to be investigated over a
wide range of temperatures in order to clarify the laws
governing the replacement of crystal water by H 202 and to find
the range in which these compounds can be formed. There are
2 figures, I tablep and 12 references, I of which is Soviet.
ASSOCIATIONt Institut obabohey i neorganichookoy khimii im.11. S. Kurnakova
Akademii nauk SSSR (Institute of General and Inorganic
Chemistry iment N.S..Kurnakov of the Academy of Sciences, USSR)
SUBMITTEDs June 12, 1958
Card 2/2

SOV/75-14-2-18/27
On the Separate Determination of Peroxide- and Superoxide Oxygen in Su;er-
oxides
tion of peroxide- and of suporoxide oxygen according to this
method in technical NaO 2 and KO2 and in peroxide preparations
of calcium, strontium, and barium containing impurities of
Ca(0 2)2' Sr(O 2)2 and Ba(O 2)2 are listed in a table. The re-
liability of the determinations of peroxide oxygen was check-
ed by control analyses with separate weiahed portions. The
differences in the results of the two determinations are in
the order of magnitude of 0-03',t. There are I table and 3
references, 6 of which are 3oviet.
ASSOCIATION; Institut obshchey i noorganiclieskoy khimii im. 'IT. S. Kurnakova
All SSSR, Moskva
(Institute of General and Inoreanic Chemistry imeni 11. S.
Kurnakov of the AS USSR, Moscow)
SUBMITTED: December 4, 1956
Card 3/3

VOL NOV, I. I. j CIW40VA, V. N.
Mechanism of the transformation of Ca02v2H202 into Ca(02)2.
Zhur. neorg. khim. 5 no.3:522-523 Mr 160. (MIRA 14:6)
I# Institut, obshchey i neorganicheBkoy khimii im. No So Kurnakova
Akademii nauk SSSR, Laboratoriya perekisnTkh soyedineniy.
(Calcium superoxide)
(Calcium peroxide)
-11~nV Me- R&MKIII

209WI
S/062/61/000/003/01i/o~t3
//1 1190 B117/B206
AUTHORS: 7ollnov, I. I., Tsentsiper, A. B., and Chamova, V, N~
TITLEs Synthesis of tagged hydrogen peroxide from vapors of heavy
oxygen water in a glow discharge
PERIODICALs Izvestiya Akademii nauk SSSR. Otdeleniye khimicheskikh nauk,
no. 3, 1961t 531
TEXTs The authors of the present "Letter to the Editor" report the
realization of the H 201 synthesis from H20*- vapors containing
1.75 1 0-01 atom% 0'8 in a glow discharge. They were extracted from the
discharge gap and frozen out in a trap cooled by liquid nitrogen. The
device used has been previously described (Ref. Is A. I. Gorbanev,
A. B. Tsentsiper, Izv. CO AN SSSR 195B, no- 5, 45). The glassy substance
frozen out in the trap contained 28-4 wt% H 0* after melting. The
18 2 2
0 content of this peroxide was 1.82 1 0.01 atom% (mean value obtained
from 35 mass-spectroscopio determinations of five samples). The concentra-
tion coefficient is 1.04. The method applied by the authors for preparing
Card 1/2

209 U-
S/062/61/000/003/011/0!,;
Synthesis of tagged hydrogen... B117/B208
H 0* is, according to their opinion, more convenient than that described in
2 2
publications, 3ince in this way a sufficiently concentrated and pure H 0*
2 2
may be obtainel directly. LAbstracter's notet This is a full translation
from the originall. There is 1 Soviet-bloc reference.
ASSOCIATION: Institut obshchey i neorganicheskoy khimii im. N. S. Kurnakova
kkademii nauk SSSR (Institute of General and inorganic
Chemistry imeni N. S. Kurnakov, Academy of Sciences USSR)
SUBMITTED: January 11, 1961
Card 2/2

,161100610081011.1 18
25.512 S/078 10
B127/B220
-------------
AUTHORSs Vallnov, I. I., Molodkina, A. N.
TITLE: Symthesis of hydrogen peroxide from elements by silent
discharge
PERIODICALt Zhurnal neorganicheskoy khimiip v. 6, no. 8, 1961, 1952-1954
TEXTs A new convenient synthesis of H 202 was developed based on methods
described in the literature by N. I. Kobosev, I. A. Semiokhin,
V. L. Sindyukov (Zh. fiz. khimii, _3A, 771 (1960))q S. Z. Makarov,
I. I. Vollnov, A. N. Atavina, T. V. Shatova (Otchet laboratorii perekisnykh
soyedineniy AV SSSR, Moskvat 1950). The apparatus used is shown in
Fig. 1. A tin foil on the inner wall of the external tube and a silver
film on the outer wall of the internal tube served as electrodes. Reac-
tions were effected on different parts of the electrode and with varying
2 2 2
surfacest 115-300 Mm , 94-176 mm , and 24,000-62,500 mm , The inner tube
of the discharge tube was treated with hot concentrated nitric acid,
washed with distilled water, then treated with concentrated phosphoric
acid, and again washed with distilled water. Without this treatment the
Card VA

8/078/61/006/008/011/018
Synthesis of hydrogen... 25532 B127/B220
yield did not exceed 5W.. The apparatus was fed with line current,
regulated and varied by an nkTPL1.(LATR-1) and an electrolytic circuit
breaker connected to the first winding of the coil PYMKOP~ K~ - 150
(Rumkorf M-150). The experiments were made at a voltage of 20kv and a
frequency of*lCOcps. The amperage on the first winding of the inductor
was 4.6~44aj on the Pbe, howevery 5-7mae The current density varied
between 2 and 2-5a/mm.olo-7. The highest yield in H202 was observed at a
content of 3-5-3.7vol% of 02 in the initial mixture. The initial mixture
was dried by using a Tishchenko phial filled with concentrated sulfuric
acid. Then, it passed a copper coil cooled by liquid nitrogen* The pres-
sure was maintained at 50 mm H in all reactions. The reaction time was
6 1/2 hr at a flow rate of 1 1~hr. The optimum working temperature was
-170C, since the concentrated solution had to be maintained in liquid
state. The reaction yield varied between 67.2 and 82.8% by weight Of H202-
There are 2 figures, 1 table, and 6 references, 3 Soviet-bloc and 3 non-
Soviet-bloc, The reference to the English-language publication reads as
follows: Ref. 6; T. Bellinger, Ind. Eng. Chem., 38p 627 (1946).
ASSOCIATION: Institut obahchey i neorganicheekoy khimii im.
N., S. Kurnakovs. Akademii nauk SSSR (Institute of General and
Card 2 Inorganic Chemistry imeni N. S. Kurnaklov AS USSR)

VOLINOV., I.I.; SOKOVNIN, Ye.I.; MATVEYEV, V.V.
Synthesis of alkali metal ozonides b,,f the interaction of Super-
oxides with ozonized oxygen. Izv.AN SSSR.Otd.khim.nauk no.6:
3-IZ7 162. (MIRA 15:8)
1. Institut obshchey I neorganicheakoy khimii im. N.S.Kurnakova
AN SSSR.
(Ozonides) (oxygen) (Superoxides)

CHMIYAYM', I.I., akadenik, red.; RAZUVAYKV, G.A., red.; VOLIVCV,
I.I.j kand. khim. nauk, red.; DOBRYRINA, T A., kand. 6.,
nIXIX,- rediDRAGUIRIV, E.S.) red.izd-va; KUM, Te.V., tekhn.
red.
(Chemistry of peroxide compounds] Khimiia perekisnykh soedi-
nenii. Moskva, Izd-vo A14 SSSR, 1963. 313 p. (MIRA 16:12)
1. Akademiya nauk SSSR. Institut obehohei i neorganichaskoy
khimii. 2. Chlen-korrespondent AN SSSR (for Razuvayev).
(Peroxides)

;1144"1 '" v'l','v'
Hydrates of sodiu.,a metalillionte.,. /Ble6 vv #1 v"
with 4 - 20 % by weight 11 0 and Hr. Sio 3H 0 4.
2 21 2 5' 2 2' N 20 With 20 - 34 -~ bx
weight 11 0 For' Lite it-tvastigaViorl Lit 150C, R, 3iO,;.3u 0 U 0 was taken
2 2- 2 1 2 2. 2
as initial oub3tanoo. Equilibrium waa obtained arter 4 - 5 bru, The phaso
diagrata ohowe 2 solid phdee6i Nu 23 io 3* 9R20 2. It20 With 0 by weight
H 0 and Na Sio 311 00 with 5 42 ",~ by weight I!
2 2 ' 2 34 42 - 20 2- The he;iti-ng carve
plotted for Na 2Sio 3* 31!R02.P, uIrg a Xkurnakcor differential pyrometer
0
showed an oxathurmaio off cot et .~60 C Indloakilig the CICOORIPOfiltiou of the
cr3rBtallized 11 and an P-ndotherutic rtfpct d-ji to dehydretion al rjI2000%
1 2'J2 1
The Snneral Tormuln antablished for theac oonpounda io Na 2310 3' XH202'YH201
where x - 2.11 3i and y ;* 0 - i, Thare are fir -ree and 2 tublea.
ASSOUATIO17t In3titut obnhohey i u,,oi-j3xLnIchr;fjkor khimii im. R. S. Kurmkovu
Akndemli nouk--SSSH (InutItlite of Gvno,FzI and Inorganic
Chamiatry iment N. I. ?.ui,n;jkf),; or I.h~i Ao,-,(jemy of $Ciencej WHO
SUBMITTM)i 18, !962
2.0,?
Card 2/2

as -J881-63 I/EwF
ACCESSION VR:: AP3002299 S/0062/63/ooo/oo6/1136/1139
AUMOR: Vol 'nov, 1. 1
a-1 ~. -0; !!j~ygev, V. Ve
9
TITLE: Synthesis of cesium ozonide, from cesium superoxide
'SSR, Izv. -1139
SOURCE: AN 1) Claeleniye himicheskikh nauk, no. 6, 1963., 1136
TOPIC TAOS:;~synthesis, cesium ozonide., cesium superoxide, ozonized oxygen,
ammonia exIxaction, pure cesium ozonide, thermal stability of CsO sub 3,
melting of C110 sub 2
ABSTMCIT: HA-Puri4 CBO sub 3 has been synthesized for the first time from
CsO sub 2'M zonized oxygen. The starting mterials were cesium superoxide
containing 9E~.6% cso sub 2 and 1% Cs sub 2 0 sub 2.1 and oxygen -containing
about, 8% ozone. The synthesis was conducted in a special molybdenum glass
reactor at 4-CIC for 1.5 hr in a fluidized bed created by a stream of the
ozonized oxyf, Ozonized CsO sub 2 was extracted with liquid ammonia by
en.
means of a special apparatus. The average CsO sub 3 concentration in the
products., as~indicated by a determi-ration of active oxygen and CsO sub 2)
Card 1/2

L 9881-63
ACCESSION FR::' AP3002299
vas 924- CHO sub, 3 is unstable to moisture and CO sub 2. Differential
thermal w-aly3is showed that its deconposition into CsO si,.'j 2 and oxygen
starts at 70C;and attains a maximum at 100C. CsO sub 2 z7!--.Lts'at 408C wA
then deconposes Into Cs sub 2.0 and orjgen. orig. art. has: 4 figures and
2 formilas,
kSSOCIATIM#. -Institut obshchey i neorganicheskoy khimii im. N. S. Kurnakova
Akademii nauk,:SSSR (Institute of General and Inorg nic Chemistry, Acaderay
---of Sciences SIM)
SUBMITrM: 2:jJan63 DATE ACQ; 16jui6l ENCL: 00
60 CODE: 00 NO REF SOV: 005 Onw: 008
Card 2 2

ACCESSION NE: AP4039620 S/0076/64/038/005/1182/1187
AUTHORS: ham
(Moscow); Tsentsiper, A.B. (Moscow); C oval
V ft. (Moscow); Laty*sheva, Ye.I. (Moscow); Kuznetsoval Z~I*
(ioscow)
TITLE: Synthesis of oxygen-labeled hydrogen peroxide from dissociated
heavy oxygen water in the glow,discharge
SOURCE: Zhurnal fizicheskoy khimii., v. 38, no.'5, 1964, 1182-1187
i,' TOPIC TAGS: oxygen labeled hydrogen peroxide, hydrogen peroxide
Synthesis, heavy oxygen water, glow'discharge, heavy oxygen water
'ki vapor, labeled peroxide synthesis parameter, oxygen isotope, dvuter-
labeled. oxygen peroxide, oxygen isotope content
11 ABSTRACT: The equipmeht-for this-efficient laboratory synthesis is
figured. The discharge tube was fed with a U50-1800 volt,'0.1-
0 5 amp. current. The oxygen-labeled water vapor was fed at the rate
oi 0.03-1 114 mol/hour, thavapor pressure was 0.43-0-53 mm H The
dissociat;d water vapor was removed from.the discharge arealg;ooled,,,,-,
etc. an
d the yield determined i by titration. This was a function of
rate.
the rame';er,Up,,ty, where U,is*the,d~acharge force (kwa), v the
CqrSj 113

7
ACCESSION NR: AP4039620
of adding the water vapor and p the pressure. of the vapor entering
the discharge tube. The isotope content of oxygen in the'starter
water and the peroxide was determined by maos spectrometry. Both
the water remaining in the4gporizer and that formed upon decomposi-il
tion of the synthesized 1i were found to differ little from the i1
starter water. The gases collected during the process were found
'to consist of' hydrogen, thus confirming the reaction
21120 2H 2OH; 2H 112; 2()11 -.9. ljtoi.
The au4Rrs also synthesized D 0128 by subjecting a mixture of' D20
and H O-LO to the discharge* ifie so obtained peroxide container 26%
activ3 oxygen, somewhat enriched from the starter material. The
advantages of this method are a high degree of purity of the peroxide;
the entire heavy oxygen contained in the initial water passes into
the peroxide-; the latter is somewhat enriched in GLP; solutions of
the oxygen labeled peroxide ranging from 1-50% may be obtained,
depending upon the energy supply for the discharge and the rate or
supply of tho water vapor. Yields for 5-7% solutions wore 1-g/hour
on a 100% H2018 basis.* Using the same equipment, -the peroxide may I
11be.concentrated to 90%'weights Orige-arto hasi 2 figures and I table,
2/1
Card 4

ACCESSION NIL. AP4039620
ASSOCIATION: Akademiya nauk SSSR (Acaderny of Sciences, SSSR);' Institut
obahchey i neorganicheskoy khimii im. N. S. Kurnakov6(Inatitute of General and
Inorganic Chemistry).
SUBMITTED: SOMay63 ENCL: 00
SUB CODE: ~(10 NO REV SOV: 006 OTHER., 001
3/3
- - - - - - - - - -AA.

1P. L tIN t '-Z r.
--L- -"'V 11 ya jv&nQj;Lgb; VIKH. -FEW , V.I., prof., otv. red.;
D11GOG11.9 red.
(Peroxides, superoxides and ozonides of alkali and alkallre
earth metals] PerekiBl, nadper(Ai-I i ozonidy Achelocb-
nyi:h 'I im)tallov. MoAvn) Nnitknj 19('4.
120 p. (1,11RA 17-13.)

J_A571
&ZIL I
ACC NRt Ap6u.,jw SOURCE COM UR/0062/66/000/007/1267/1269
AUTHOR& Vollrxrv. 1. 1.; Tokarovar S. A.; Mmanovp V., Io; Pillpenkov G. P.-
ORGI Institutt, of General and Inorganic Choodstry in, Ny_ Sq Kurnakov, Aoad~!Z of
Sciences, SSR (Inatitut obahahey I noorganichookoy khirdl AkadT nauk 553R)
TITLES Synthesis of potassiuM otonide via potassium superoxide sustpended in
3OUFC31 AN SSSR. Izv. Ser khim, no. 7v 19660 1267-1269
TOPIC TAGS1 ozonidep superoxidep potassium compound
ABSTRACTS This reaction of XCIt with ozone was carried out in Froon-12, a liquid Inert 1
toward ozone. Potassium superoxide had the following compositions X02p 90.22%; K?02p
).8.5%; KOH9 2.7.5%; X2CC5# 1-83%; HzOr 1-33% (by difference). Its particle size was
0.05 mm or less. The ozone content of the ozono-oxygen mixture was 9 wt. %. 7he stop
of extraction w:Lth liquid ammonia was omitted. Analysis of the ozonized product gave
K
v 77.2; K02o 6.4; KOH, Jo 6; KzC( The increase in the amount of KOH
and ~q 5.6 wto %.
0' K2CO~ Impurlties in the nd product aa compared to their content in the original
potaaBium superoxide Is due to the reaction of KO~ with atmospheric moisture and COz
during tht withdrawal of the samples foravialysis# despite all. the precautions taken.
Orig. art. hass I figure and 2 tables.
SUB COM W SUM DAT91 i8Dsc65/ ORIG REF1 003/ am Rat oo3
Card UDCs 542.91+542.943.54621--3-8415�546t3-Z-

L 47554-66 EW(m)/-NP(t)/bT1
ACC NR, AP6032907
JD1JG1RO
SOURCE CODE:
uR/oo62/66/ooo/009/1665/1665
AUTHOR: Vollnoir, I. I.; Dobrolyubova, M. S.; Tsentsiper, A. B.
ORG: Institute of General and Inorganic Chemistry im. N
Sciences.SSSR nstitut obshchey neorganicheskoy khimii Akademii nauk SSSR)
TITLE: Synthesis of rubidium ozonide f 0m rubidium superoxide
-'~j lp
SOURCE: AN SSSR. Izvestiya. Seriya kh'7micheskaya, no. 9, 1966, 1665
TOPIC TAGS: inorganic synthesis, rubidium ozonide, rubidium superoxide, rubidium
compound
ABSTRACT: Rubidium ozonide containing 96.6% Rb03 and 3 ''4% Rb20 was obtained by
I
using for the first time a new reaction which was earlier successfully applied for
the preparation of high U *tyk 20311- 1. Vollnov and V. V. Matveyev. Izv. PIT SSSR.
-p r1 C
Ser. Khim., 19639 I-1-36T. -The reaction between rubidium superoxide RbO. and ozonized
oxygen was carri,-d out at OC in a fluidiLed bed. Rubidium ozonide was extracted by
liquid ammonia.,V'jThe RbO. starting material was prepared by--Matveyev by spraying
Rb metal in gen and argon in a special apparatus which was previously described.
The purest rubidium ozonide which was obtained by an older method from rubidium
hydroxide contained only 66.6% Rbo3- . IJKI
IJP(c)
SUB ODE: OV GUBM DATE,. 19Feb66/ oRIG REF: 004/ ATD PRESS: 5094
Card 1/1 uDe: 942.9i+542.Q4i.9+946.-35

ACC NR, SOURCE CODE: UR/0062/66/rjro/fOll/2032/2033 1
AP7000813 !
AUTHORs :V611nov, I. I-;.~4atuninap A. N.
ORGt InstitutD of General and Inorganic Chemistry im. N. S. Kurnakov, Acaderrj of
Sciences, SSSR (Institut obshchey i noorganicheskoy'k.himii Akademii, rwjk. SSSR)
TITLES Now data on the formation of Ca(02)2 via Ca.02,,2H202 -
SOURCE: AN SS'3R. Izvostiya. Soriya khimichoskayag no..119 1966, 2032-2033
TOPIC TAGS: calcium compoundp superoxide
ABSTRACT: The reaction
2CaO2-2H2O2 - Ca(0202 + Ca(OH)2 + 3H20 + 1-502
was carried out a:t reduced pressures, a constant temperature of 400C0 a constant time
of 60 min, and i4ith a distribution of Ca02-2H2Ct Of I g over 100 cm2 -of surface. It
was found that the maximum content of Ca(O~)2 in the end prqducty equal to 55.4 wt.
%, is reached tit a pressure of 6 x 10-3 mm. The dependence of the C&(O2)2 content on
the surface ovor which 1 g of CaG2-2H20~ was spread at a residual pressure of
6 x 10-3 mm was determined. The value obtainedv 55.4 wt. % Ca(G2),z at 100 cmZ of Sur
face, is close~to the limiting value, since according to the reaction given above, I
mole of Ca(02)Z and I mole Of Ca(OH)2 are formed, which corresponds to 58.4,wto" %
UDCt

NR, AP7000813
'Ca N
2)2- Crig,'art. has; 2 figuros and 1 for=la.
SUB. CODEt '071 SUM DATEI OgApr66/ ORIG REFt 007/ OTH REFS 002
2/2
Co rel
ntg Bull
ME -0
1~1, V-- M, MRS

----- -- -----
SOURCE
ACC NR-. AP700"305: CODES uR/oo62/661000/01212,235/2237 1
AUTHORS Sokol, V1. N.; Matvayav, V. V.; 'Iol*novj
ORO: Instituto Gonoral and Inorganic Chemistry in. N. S. Kurnakov, AcadeV of,
Scidneesp SSSR (Istitut obshchoy i neorganicheskoy khimii Akademii nauk SSSR)
TITIES Datermination,of the-density-and refractive-indices-of cesi= ozonide
SOURCES AN SSSR.' Izvestiya. SerVa khimichaskayap.no. 12p 19660 2235-2237
TOPIC TAGSt cesiiam.compound, ozonide, refractive index
ABSTRACTS The refractive indices of cesium ozonido crystals were measured by an im-
mersion method (described previously) in a stream of dry nitrogen at 0 to -100Gp using,,,
a goniozater in zonochromatio light. The density was measured in the same tomperaturo'
range by hydrostatic weighing. A special dosing apparatus was constructed for hand-
ling the microsamples of cesium ozonide, which is very sensitive to the action of,
moisture and carbon dioxide and is thermally unstable. Like sodium and potassiu=
ozonides, cesium ozonids has the lowest density as compared to the peroxide and super-1
oxides G% 0 j Cs 0, rA o.
d245 4.47 3.80 3.19
and has the highest density in the series of alkali metal ozonidos2
UDC1 531.'75+51

ACC NR& AP7003305
jNaOx KOj CsOl
dWj 1.6 1.00 3.10
Orig, at, has: I figure.
SUB CODES 07/ simm Dam '25V.&766/ ORIG REFS 007

ACC NRs AP7000012
'SOUPCE CODS:
AUTHORI Vcl':jovj 1. 1.; Dzyatkevich~ B. S.
ORGI laboratory of Poroxy Compoundal Inatitute of General and Inorganic Chemistry
im. N. S. Kurnakovq Academy of Sciences) SSSR (laboratoriya porekisn7kh zwjodir4oniy,,
Institut obshahey i noorganichoskoy khimii kkadorgii nauk SSSR)
TITISt Itrdrogon peroxide solutions and metallic gallium and indium
SOURCE: Zhurnal fizichoskoy khimiij, v. 40s no, 11# 1966, 2907-2909
TOPIC VM: hydrogen peroxidop gallium indiun
ABSTRACT: Tho influence of metallic gallium and indium on the decomposition of hydro
-ron peroxide solutions (33-96 mass %) was studied at 200C at a constant ratio of the
area of the metallic mirror of Ga or In (deposited on the inner surface of reactor
vessels) to the volume of H202 solution. The decomposition rate was dctermined gaso-
metrically arxl pormanganetometrically, and found to be virtually the same on the in-
dium mirror, gallium mirrors and glas3 No. 23. Ga2O~ (in various modifications) was
formed on the gallium morror. T'he decomposition of the 93.5% H20~ solution on '
gallium is characterized by the presence of an induction period; the numerical value
of the docomposition rate is 8 x Jo-5 mi 02/mins, g9 i. o., one.- orejer of magnitude lest
than the valua for the 33-5% concentration, 7 x 10'~4 ml Q2/min, g. The decomposition
of the 95.8% 112C2 solution is also characterimed by the presence of an induction
1/2 1 UDC: 541.128

ACC NRt AP7000012
period,, and the decomposition rate is equal to 3.5 x 10-5 M1 C2/zin' Z, which is one
order of magnitude less than the value for the 33.8% solution, 2 x 10-4 MI. C)2/aing g.
Orig. artt has;I 8 figures..
SUB CODSt 07/, SUBM DATEI WOW/ ORIG RM 001/ OTH R&FI 001
C d 2/2

_YOLI~qVj, "V MINETSOVA,
J,j.; TSENTSIPER, A.B.; GRAMM, V.N.; LATYSIJE A, Ye.l.; K I
#I*
Synthesis of oxygen-labeled hydrogen peroxide from dissociated
heavy oxygen water in a glow discharge. Zhur. fiz. khIm. 38
no.581182-1187 My 164s (MIRA M12)
1. Institut, obshchey I neorganicheskoy khImli Imeni Kurnakove
AN SSSR. Submitted May 30, 1963.

L529 1-65 EWG(,)/!--WT(m)/EPF(c)/EPR/EuJP(t)/FVP~b) Pr-4/ps-4 UP(c)
ACCESSICU RR AM50 U010 BM ElIPWITATICH
Ivinovich
Peroxides* ouperocide and ozoniden 'of alkali and allcali earth m
2"~Perekiaip
3- nadper kisi t :,zonidy shcT-Gl-0-C-R--0-7kh i shchelochuozemellnykh metallov , Moscow,
Izd-voe"Hauka", 1964, 120 p. illus., biblio. (At head of title: ikademiya
nauk SSSR. Inititut obshch87 i neorganich~eskoy khimil im. N. S. Kurnakova),
I Errata printed on inside of back cover. 1000 copies printed.
TOPIC TAGSi alkalt metalp alkaline earth metal, peroxidep tsuperoxide,, ozonide
TAKE OF CONMTS(abridged)t
Foreword -- 3
Introduction
Ch. I. 'Classifiattion and nomenclaturo of inorganic peroxide compounds - 13
Ch. II. Paroxidet of metals of the first group of the periodic table - 24
Ch, III. Peroxid9s of elements of the second group of the periodic table - 52
Ch. TV. Superoxifes of alkali and alkali earth metals 80
Ch. V. Ozenides of s3lw-li metals 108
Conclusion 122
Cardl/2

ACCFMION HR AM502101C
SUMUTTEDI 03saP64
wt REP sov 187
Card

L 43204-65 EPF'c)/ZPR/&-,JG(J)/,4TdJi-(m)/aIP(b)/Z~.?(t)
JD
ACCESSION NR: kP5006695
Pr-VFs-h1Peb DIAAP/IJP-(C)
S/0076/65/039/002/0452/0453
AUTHOR: Vollnov, 1. 1. : Chamova, V. N. ; 4tyqheva. Ye. 1.
P
on
TITLE., Induced iAchange of oxygen between KO sub 2 and water , taining qxyg!qn-18
SOURCE: Zhurn;l fizicheskoy khimii, v. 39, no. 2, 1905, 452-453
TOPIC TAGS: Navy oxygen, hydrogen peroxide, potassium hydroxide, molecular oxygen,
potassium superperoxIde, superparo)dde rattical, oxygen exchange
ABSTReICT- Wh.lo conducting the hydrolysis of K02 in H2018 with 1. 76 at. % 018, it was
discovered that tfte K011 produced contained less 018 (1. 37 at. %) than the initial water.
To explain this LLCt, the authors investigated the mechanism of the intermediate reactions
in the hydrolysis of K02'-
2KO2 + 2H20 -v 2KOH + 2HO2 (1)
2H% 11202 + 02 (2)
2XO2 + 2H20 - -->2KOH + H,202 + 02 (3)
Card 1/2

L 43204-0'
ACCESSION NX AP5006695,
In ey suggested Umt'the heavy oxygen was distributed between the KOH, H202 Mad 0?,.
This was confirned by direct measurement of the isotope composition of both the molecu-
lar oxygen and ihe 11202 produced in the 2nd reaction. The reaultinv isotcpe balance in-
dicated that there is a very slow exclLinge, in alkaline medium, between the oxygen of tho
v ater and the ai itive oxygen of tho superporoxide radical. Orig . art. has: I table and 3
formulas.
ASSOCIATION: Institut obahchey i neorganloheakoy kblmii im. N. S. Kurnakova,
Akademlya naul. SSSR Unstitute of General and Inorpnio Chemistry, Academy of Sciences,
SSSR)
SUBMTTED: 30Jun64 ENCL: 00 SUB CODE: IC
No REP SOV: 00 OTHER: 006
2/2
I I-Card.

DOBRYNINA, Tatlyann Aleknandrovna; VOLINCIV, I.I., kand. khIm.
nauk, otv.red.; E.O., rVi.
(Lithium peroxide] Ferekis' litha. Moskva, lzd-vo Illauka,"
N
1964. 49 p- WIRA 17:7)

SIOOOO163100010001000510010
ACCESSION NR: ILT4028327
AUTHOR; Vol'nov 1. 1.
TITLE: On the Ittate and prospects of research in the field of the chemistry of
inorganic peroxfda compounds
SOURCE: SovesbchanLye po kbimil parokinny*kh soyedinenly. Second# Moscow, 1%1.
Xhimiya perekisny*k1h. soyedineniy (chemistry of peroxide compounds); Doklady*
sqveshchaniya. Moscow, Izd-vo AN SSSR, 1963, 5-10
TOPIC TAGS: peroxide compound, superoxide, ozonide, inorganic compounds, peroxide
groups
ABSTRACT: The ituth'or traces the history of peroxide compounds from the beginning of
the 19th Century and Humboldt's discovery of barium peroxide to the present day, in-
cluding the development and changes in peroxide concepts. In post-war years,-con-
siderable successes in science and application have been attained in the Soviet
Union. The works of I..A. Kazarnovskiy is mentioned in a synthesis and the study of
P.Foperties and reaction capability of sodium superoxide and a new class of peroxide
compounds, inorijanic ozonides,, along with the research by A. I. Brodskiy who first
used the heavy J'sotope of oxygen for explaining the formation mechanism and decay
Card 1/2

'ACCESSION NR: AT4028327
of peroxide compounds. Also mentioned are M. 1. Gurevich who systematically inves-
tigated the nature of uranium peroxide compounds; N. 1. Kobozev who investigated the
synthesis of hydrogen peroxide in.an electrodischarge; G. A. Bogdanov who investigat-
ed the mechanism of catalytic dissociation of hydrogen peroxide; and S. Z. Makarov
who it~stewaticzilly investigated-the interaction of hydrogen peroxide with the
hydraies of oxides and salts enabling the development of igational methods for syn-
-thesizing' a nuriber of peroxide compounds. Work in the United States, England and
Wesi Germany its also mentioned. The Coordinating Committee for Scientific Research
Work by the Couhsel of Ministers of the Soviet Union and the Presidium of the Soviet
-Academy of Sciences have defined a most important mission for modern science and
'technology and decided to set up scientific counsels which will coordinate this pro-,
gram and evaluate the obtained results.
"ASSOCIATION: Institut obahchey i neorganicheskoy khimii im. N.S. Kurnakova'AN SSSV
(Institute of -.3eneral and Inorganic Chemistry'Aff SM)
'SUBMITTED: 13Dar.63 D&Z Aft 06Aor64 ENCL: 00
SUB CODE: CH -NO RJKF SOV: 000 ann, o0i
-,Car~d.2/2

VOLINOV.-T.N,j XOSOLAPOVI T.T.p PERYT)Ij S.C.
Stewn Pipes
Self-sealing p:.ug for hydraulic testing of high-pressure pipes. Rab. energ. 2 no. 4,
1952
9. Monthl List of Russian Accessions, Library of Congress, IMly 1952 -IYM, Uncl.

1.11., VC.'3CLATCV, I.I., T-11KIN, S.G.
Steam Pipes
Self-scaling plup for hydraulic testinF, o.11 high-pressure p1pes. Fuib. f-ncrg.
2 no- 4, 1952
1952
9. Monthl List of Russian Accessionsp Library of Congress, July -I*n, Uncl.
50
k

- ----- ---- ---- - -, - --- - -- -
KUZIMINA. T-D.G.; VOLINOV,,G.B.
-- ----I
Alectrolysis of solutions of stannic chloride In certain organic
solvents. Zhur.fit.khim. 28 no.2:282-286 Y 154. (KLRA 7:5)
(AlectrolymiB) (Stannic chloride)

YAKOVLEV, N.N.; VOLINOVO..-N.I.1,LESHKEVICH, L.G.
Effect of pangamic acid, imethionine, and a mixture of gluconate and
glycin on the metabolism in a heart muscle and the electrocardiography
cf muscular activity. Ukr.biokhim.zhur. 37 no.5-818-835 165.
(MIRA 18:10)
1. Nauchno-lasledovateliskiy institut fizicheakoy kulltury, Leningrad.

USSR/Humin and Animal Physiol.Dgy - (Normal and Pathological). T
Blood Circulation. General Problems.
Abs Jour Ref Zhur Biol., No 4, 1959, 17413
Author Vol
Dist
Title On the Level of Arterial Pressure in Athleter
Orig Put Terapevt. arkhiv, 1958, 30, No 6, 65-71
Abstract. No abstract.
Card 1/1
- 17 -

Sec. 6 Vol 11!12 Intprwil r-td. 1)C'C r0
7098. ARTERIAL PRESSURE LEVEL IN SPORTSMEN (Russian text) - Volnov
N. 1. - TERAP.AHKH. 1058, 30/6 (65-71) Graphs I Tables 6 -
The MR-pressure was studied in 5.975 athletes (4.107 men and 1,868 women).
As anorrral value for blood pressure 100-129/60-89 mm.Hg was taken. The dias-
tblic pressure was on the lower limit of normal In 5076 of athletes in the age group
up to 20 yr. The percentage of athletes with a low blood pressure is equal to that
of the rest of the population. Higher blood pressure is more often observed in
athletes ( 12.379) than in other persons. The majority of athletes have a low blood
pressure, on the lower limit of normal. The lowering of the blood pressure after
training in the majority of cases does not exceed the lower limit of normal and so
the term hypotonia cannot be used. The term athletes' hypotonia does not charact-
erize this sort of lowering of blood pressure. The fact that there are among athlet-
es persons with a blood pressure under the lower limit of normal has to be explain-
ed. The higher blood pressure found among athletes can be explained by overstrain-
Ing. which can in this manner reveal persons with higher reactibility of blood pres-
sure- regulati ng centres. There is no homogeneity in the group of athletes with a
higher blood pressure. This group includes hyper-reactive subjects. potential
hypertonics and even patients in the neurogenic stage of hypertension. For these
reasons every subject with higher blood pressure needs an Individual clinical
examination. The problem of allowing persons to practise sports and of deciding
the kind df training can be solved only on this basis. Hence it is clear that the
differential diagnosis of higher blood pressure has great importance in sports
medicine. in prophylaxis an well as In revealing the neurogenic stage of hyper-
tensive disease in its early stages. Mestan - Prague(XVIII, 6)
J

BUTCHENKO, L.Aj VOLINOV, N.I.
Statistieal methods used in working out norms for the
evaluation of the electric heart systole. Prim. mat. metod,
Y biol. no.2sl96-201 163. (NIRA 16:11)

VOL T0,11) 11. 1.: mster Mod Sci (diss) -- "Arterial pressure jrjong r-portmim".
L-jnln(~ead, 15,59. 18 pp (Min xToalth RSFcN,, Leningrad Sanltai-,,-Hyglow Med Inst),
200 copies (11, I~o 18) 1959, 128)

VOLIIOV. N.I.
Bl3od pressure level in Athletes. Ternp. nrkh. 30 no.6s65-71 Je '58
(MIRA 11:7)
1e Iz eektorn sportivno;r meditsiny (-xav. - prof. A.G. Dembo)
Loningradekogo nauchno-isaledovetellnkogo instituta fideheskoy
kulltury.
(ATHISTICS,
blood pressure in athletes (Run))
(BWCD PFMBSURF,,
in Rthletes Oun))

ACCESSION NRv AT4001248 6/2776/63/000/032/0164/0174'
AUTHORSs ovayannikov, Do. M.; Melekhin, At X*; Lebedev, Do V.;
Vollnov, K. 11.
TITLE: Stre;ss rupture testing of refractory metals and alloys at
temperatures up to 1800*C
SOURCE: Moscow. Tsentrallny*y nauchnol-isaledovatid'skiy institut
chernoy metallurgii. Sbornik trudove no. 32, 1963, 164-174
TQPXC TAGS.- refractory metal, refractory alloy, ultrahigh tempera-
ture stress rupture test, refractory mate-eial strona rupture test
ABSTRACT; In view of the shortage of suitable equipment for me-
chanical tests of high-melting-point metals and alloys at tempera-
tures above 12006C, the authors describe some of the main equipment
which they constructed for long-run tests in air (up to 1SOO--1600*C)
and in vacutn. The system constitutes.two typox'of small vacuum
Coid

7
ACCESSION NR-i AT4001248
furnaceswith seals to ensure bermeticity of the system at relatively''
large displacements of the clam's of the testing machine, heating
elements for the furnace, and control circuitry. Some operating
features of the furnaces are!discussed. Orig. art. has: 15 xigures. i'
Toentraliny*y nauchno-ionledovatellikiy institut
cbernoy metalurgii. (Central Scientific Research Institute of Ferrous,,`
Metallurgy)'
ENCLt 02
SUBMITTED:-. - (30 DATEACOi l0Dec63-".1.
SUB CODEt &P, 14A NO REP SOVv 006 OTHER: 000.;;
Card 2/4

OVSYAIRIIKOV, B.M.; ~MEKHIN, A.K.; LEBEDEV, D.V.; VOLINOV, N.N.
Testing of high-maltinp, merals and alloys for stress-rupture strength
at temperatures ult to IP!f~o 4y C. Sbor. trud. TSIIIICHM no.32:164-174
163. .(KRA 16:12)

ACCESSTW WR: AP40133-14
S/0032/64/030/002/0229/000,
APTHOR: Ovsynnrxi)c,)v, B. M.; Lebedevy D. V.; Velekhin, A. K.; V
!.11.nov
TITLM An Irst-illstion for testing long range durability under vpcuum at tempera-
turns up to Irooc
SMIRCE: ZAvodskaya laboratoriyal v. 30,, no. 2, 1964p 228-229
i
T61-IG TAGS: durphility, durability test, long,:rp-nge durnbilityt vacuum effect,
effect, vacuum oven, heated vacuum oven
OSTRACT: The installAtion consisted of a two-section steel vacuum oven of cylin-
drical shape, 2-9 cm in diameter and 30 cm long, provided with E, weter iecket and two
centrelly loanted rp~iation heaters. By these means it was possible to bring the
teuperature up to 1300C within 2D minutes and to ISWC within 65 vftutes. Fowever,
It was found thpt a too rrpid rise of terpersture caused an accelerated evolution of
gases from the test samples placed.in the oven, which affected the vacuum. A
gradual step-by-etep rise in temperature was found to be the proper procedure. An
additional source of error in a vacuum of fluctuating magnitude was due to the
presence of eouB:Izo-tion loads of the leverage system of the testing mEchine.
Pigure I on the Emalomires gives the structural details of the vacuum ovens WWNIML
Card "A