SCIENTIFIC ABSTRACT YAGN, YU.I. - YAGODIN, I.YE.
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Collection:
Document Number (FOIA) /ESDN (CREST):
CIA-RDP86-00513R001961810019-5
Release Decision:
RIF
Original Classification:
S
Document Page Count:
100
Document Creation Date:
November 2, 2016
Document Release Date:
March 15, 2001
Sequence Number:
19
Case Number:
Publication Date:
December 31, 1967
Content Type:
SCIENTIFIC ABSTRACT
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S/f)32/61/027/011,1014/076
B100130
AUTHORS: Yagn, Yu. I, Myakinin, L. V., and Kovalov, K,, F.
TITLE: An instrument for measuring transverse strain by means of
wire-suspended mirrors
PERIODICAL: ~avodskaya laboratoriya, v. 27, no. Ili 1961, 1413 W4
TEXT: The authors point out the shortcomings of a device for determining
reduction of area in the plastic range in tensile-tested material. This
device had bpen developed by N. N. Aistov (Eksperimentalnoye opredeleniye
otnosheniya otnositel~nykh poperechnykh k otaositellnykh prodollnym
deformatsiyam v plasticheskoy zone (Experimental determination of the rela-
.tive transve,ise-to-longitudinal strain ratio in the plastic region)~
Nauchnyye Trudy Leningradakogo inzhonerno-stroitellnogo institutaq no. 13
(1952)). The authors of the present paper suggest the arrangement shown in
Fig. 2. In this, two mirrors (1) and (2) are attached to rods (3) and (4)
which are suspended on capron wires~i The levers (7) and (8) are supported
on hinge (0) andare depressed edge-on to the specimen (5) by means of rubber
band (6 The whole arrangement is suspended on cord (10). Any slight
Card. I
S/103 61/027/011/0-14/016
B104YB138
An instrument for measuring...
change in the diameter of the specimen is transmitted to the mirrors by the
lever system. The weights (9) attache(I to the mirrors are immersed in oil
in order to avoid rotation or oscillation of the mirrors~ This instrument,
which proved good in practice9 was found to have a 12,500 magnification
factor in indicating recording the change in diameter. Its great advant.age
is that its component parts cannot suffer deformation. Thereare 2 figures
and 4 Soviet references,
ASSOCIATION: Leningradskiy politekhnicheskiy institut im, b1, I. Kalinina
(Leningrad Polytechnic Institute imeni M, I, Kalinin.)
Fig. 2. Schematic representation of the suggested ~-evica.
Card 2/d-?
"MiV-Ila ;~Ilr~lil Z-M~1~ 95siN wPiv MAr~ *X~~5
ZAKHAROV
Kirill Vas--l'yevich; KUSHELEV, Nikita Yurlyevich;
SBIITSKIY, Anatoliy Konstantinovich; SEXENOV, V.P.,,
otv. prof., red.
(Laboratory manual on the strength of materials] Rukovod-
stvo k laboratornym rabotam po soprotivleniiu materialov.
Izd. 2., Leningrad, Leningr. politekhn. in-t, 1963. 126 p.
(MIRA 17:11)
25712 S/020/61/139/003/011/025
B104/B201
AUTBORS: Izotov, I. N.pand Yagn,,Yu. I.
TITLE: Study of the plastic deformation of a metal with a
deformation aniSOIrOPY produced by pre-stressing
PERIODICAL: Akademiya nauk SSSR. Doklady, v. 139, no. 3, 1961. 576-579
TEXTt A study has been made of the development of plastic deformations
in theinitial. stages of a second stressing of material relieved partly or
completely from.stress after a first plastic deformation. To determine
a deformation due tq tress it is necessary to examine the relationship
.,,s
between the vector 6-3 of the increment of plastic deformation and the
vector S of the increment of stress as depending upon the antecedents.
The geometric loci constructed according to the allowances of 615i
being the intensity of increase of plastic deformation) are examined, and
tile pos.;i'~ility.of their application for determining the directions of
vectors 0 are eatimated. At tile oame time, tho principles uridorlying, tile
modulus of pla8tic de-formability are studied, and a utilization of geometric'
loci of equal h values (h being the modulus of plast-ic deformability) is
Ca:rd 114
25712 S/020/61/139/003/011/025
Study of the plastic deformation-. B1041B201,
suggested for the first time to describe plastic deformation prcceascs.
Experiments have been conducted, in which thin-walled tubular.opecimens of
commercially pure nickel have been simultaneously strained and twisted.
The material concerned and the experimental setup had been described in
previous papers(Yu. I. Yagn ez al DAN, 11c), no. 1, 46 (1958); DAN, IL5.2.
no. 4 (1960)i Zav, Lab.,, no. 10, ~2tO, (1~958')). In they4experiments, (F5
and h were determined as a function of the direction of I 5-ix sample
sets were teuted (2 - 3 samples per set); each set was subjected to an
aqual firot streaelng, theri.relieved from stress, and, finally, subJected
to a second streas causing breakage, A-) the oxporimonta have own, it
is necessary j'or the practical application of formula h~7,S) to know
the Principles enabling one to determi e in every point of stress the
value of h and the direction of veo~tor as a function of kind and
direction of the first 8tress, those of the second stress, and the state
of stress attaLned. On spicimens subjected to an equal first stress,
the effect of the second type of stress was studied. The authors also
examined the effect of the -first stress (1inea-1 stretching , torsion,
Ptretching combined with torsion, pressing and stretching in two
different dir;Bctions, torsion in two different directions). 17he
following conclusions ire drawn from results! 1) the directions of
Card 2/4
.-
S/92 61/139/003/p11/025
,
Study of the plastic deformation- B1 04YB201
Vect r are de'-eim
-ined with sufficient accuracy
by the direction of ihe
0 s
,
Is on the locus of, equal 6F-,. Deviations therefrom rise with
notma
incrpasing distance from th8 strebs at which-the first experiment,was
Anterrupt'eA.. 2) The-- &"metric locus of all , equal. h is almost *i. circle,
whoge,'center is.displaced with respect.to the coordinate ori4in.' The
direction of this:' aisplaco,ment is determined by the bomponent 6*f the first
stress; the displacement value depends, upon h. 'The radius.R of this
circle is not,dependent upon the kind of the first stress; it is, determined-
b h. and the strain attained'-wit.h the first stress. 3) The direction of
deviates systematically.from the niormals to the circle of equal h. This
deviation (on avorage 6 - 70) is only little larger than the change of
~
direction of vectors'
-g , which is caused by the character of the second
4 alculate the ex
can be neglected in most case
stress, and To c pected
'plastic deformation with 'the aid of (1), it is sufficient to construct the
equal h -with the aid of equations
family of C;i-,Cle!3 of.
.
To
h et
h 1/58
o
10
(4) -
h ak R+B
D B
B
Card
3/4 ajo +
25712
s/b2o/61/139/003'/011/025"
Study plastic,deforbation... B104/B201
which:presuppose the knowledge of five constants and of the strai ped.
-ress
deformed'state of the material after the first st
Here, S)6- and
are:the iespective pi~ojections of vedtor of the
displacement of the
center,of circles of equal h; - a,, k are conslants~ found
from experiments-.
with.the first.strens, A, B, and"D are constants determined with the
second streset The results, ~f numerical integrationi of (1) have been.
compared,with results obtained by the-above formulas. A deviation of ab6ut~`
a - 12 ~c has been Iound. 'The present work was the sub4act-of a lecture
.delivered at the First All-Union Conference on- Theoretical and Applied
M6chanics in January,,1960. There are 3 figures and 4 ref6r6neest
and 1 non-Soviet-bloc.. The referqnce to Englieh-language'
publica-tions reads as follows: T. Prager, J. Appl. Phys., 20, no.. 3, .2,35
_0949)~-
PRESENTED.. April 10, 1961, by'Yu. N. Rabotnov,.Academician
SUBMITTED-_ Augunt 13, 1960
Card 4/4
5/032/62/028/006/016/025
B108/B104
C) 0
AUTHORS: Tagn, Yu. I., and Pavlov, P. A.
TITLE: Study of stress concentration on shafts of variable cross
section during twist
PERIODICAL: Zavodskaya laboratorlya, v. 28, no. 6) 19621 719 721
TEXT: A method of determining the local stresses in a shaft of varying
diameter during twist is presented. It consists in determining the angle
of displacement y s (in the plane tangential to thesurface) from the
measure(! trist angle (or: -Yscos(x - -2wr where a is the anglebetween
the radius vector and thenormal of the surface. There are 3 figures.
ASSOCIATION: Leningradskiy politekhnichesleiy institu* (Leningrad
Polytechnic Institute)
Card 1/1
FAVLVII
St"Idy of t-h(, comontration of SIxeqaes ir. tho torsion of
3b,'ft-5 of vill-lAble Ilaction~ Za,.r.lab. 28 rio.6~719-721
62.
1* Lening-r-adgkiy poll teIJ-mj.,,jjeLij,.jy -*,.n.9tjtut.
(Strength of zkiterlals) (StraJns and stresses)
YAGN , Yuliy TIVanovicb; 5&%!RIOV;i V,P., otv. red.
1
[Abst-ract of lecture, for a course in the machanicEi of a
solid -amd deformable body] Konspekt lek'vsii
kursit
rB-
po
khaniki tverdogo i deformiruemogo tela. Leningrad,
Leningr. politekhn. ir~-t im. I.I.I.Ka-linina. 1965 1.61 p.
- 'I,
(14 qA B.-12)
YAGNAKOV, A.F., inzh.; PAVLOV, A.I., inzh.; TARANUIUI, Inzh.
Pilot plant testing of the auger boring method fcT mining coal
at the No.1 "Begichevskayall Mine of the Tula-ugol.1 Combine.
Ugoll 39 no.10:25-30 0 164. (14IRA 17:12)
1. Podmoskovnyy nauchno-issledovatellskiy i proyektno-konstnik-
torskiy ugolInyy institut i Trest Kalininugoll.
riz-11~-~.:~,-~125-~--l~l_;":il"~~itqxo~r-~-1-1~;%- I~F,4 R MIR~- --ZE EX-M a F% AA jt;jM W-Z!
N
RESHETNIKCIV, ji.P.; PODUSOVSKAYA, M.V.; YAGNISHCHLK I V
Fraotlees in drilling wells 5000 m. deep in arainian
geological formations. Trudy UkrNIGRI no.?s7!;-85 163.
(MIRA 1991)
YANISHEVSKIY. Yuriy Dmitriyevich; KUZIMIII. P.P., otv.red.; YAGNO&ORODSKAYA,
X.M., red.; FIAUM, K-Ya., tekhn.red. .........
[Actinometric instruments and methods of observation] Aktinometri-
cheskie pribor7 i' metody nabliudenii. Leningrad, Gidrometeor.
izd-vo, 1957. 414 p. (MIRA 11:2)
(Actionometer) (Solar radiation)
NAZAPd,;IIKO, V.A.; SHUSTOVA) M.D.; SKTAREVA, G,,G., YAG11YATIVSKAI~, G.Ya.;
RAVITSMYA, R.Ir-
Zav..lab. 28 no.6:
Determination of impuritieS in tit-Inium,
Q,.5-(48 162. (MIIIA 15:5)
1, Institut obshchey i neorganichiaskoy khimii AN USSR.
(Titanium-Analysis)
~L-38116-66 - EWT(m)/EWP(t)/ETI IJP(a) JD/JG
ACC NRt ' AP6015723 SOURCE CODE: . UR/0032A6/O32/Oo5/05lo/05l3-,,
AUTHOR*. Yagnyatinskaya, G. Ya.; Wazarenko, V. A. Z'
ORG: Institute of General and Inorganic Chemistry AN UkrSSR Ynstitut
obsbebey i neo.rganicbeskoy kbimii AN Ulcrbbh)
TITLE: Photometric determination of microamounts of niobium in titanium
an.d titanium tetrachloride 10
SOURCE: ZeLvodskaya laboratoriya, v- 32, no. 5v 1966, 510-512
TOPIC TAGS: photometric analysis, niobium, titanium, titanium compound
ABSTRACT: The proposed method for determination of niobium in metallic
titanium and titanium tetrachloride is based on separs.tion by extraction
-witb a solution of tribenzylamine in CEC1 from 11 M HCl and final
deteirmi-nation photometrically using ortbohtropbenylflvorone. The
possible to determine down to 0.02 micrograms of niobium
method makes it *
in 1 ml. The determination of nibbium is not interfered with by the
following other Impurities (in micrograms/ml); Ta--O.k; Ti--4; Zr-'-8;
Sn--2; Mo--2; .W--l; Ga--k; Sb > kO; Fe ;>300. With the use of extraction
with an 8% solution of ~ribenzylamine in chloroform, a check using the
radioactive isotope NbW'~ showed that in a aingle extraction from 11 14
Card 1/2 UDC: 543.7
L 38116-66
ACC NR- AP6015723
hydrochloric acidl,, at 9. ratio of 100:25 between the aqueous and organic
.phases, 87% of the niobium went over into the organic phase. 0.1 M
hydrochloric acidl was a better extracting reagent, In a single
extraction, with a phase ratio of 50:50,, 94% of the niobium was
extracted. Titanium was not extracted end its presence in the solution
in the amount of more than 0.5 grams did not interfere with the
extraction.,.of niabium, Orig, art. has: 1 tables
SUB CODE: OV SIUBN DATE: none/ ORIG REF: 003/ OTH REF: 001
2/2
J Card
law%
Hill
ON;
W
dl
ge.
A
2
ig I --a I I `
pu
P! lit
\9 j
Vo M 1
fill
J11.1 -xv
Vo
vi
oil P-91 lit I
lit 91 Ull
ACCESSION NR: AR4040827 3/0058/64/000/005/EO09/EOIO
SOURCE: Ref. zh. Fizika, Abs. 5E61
AUTHOR: Voyutskiy, S. S.; Rayevs~ziy, V., G.; Yagnyatinskaya, S. M.
TITLE: Influence of the physical state of polymers on their adheidon
CITED SOURCE: S!-. Vy*sokomolekul. soyedineniya. Adgeziya polimerov, M.,
AN SSSR, 1963, 128-133
,TOPIC TAGS:, polymer, adhesion, polyethylene, elastomer, diffusion theory
TRANSLATION: There is investigated with dependence of resistance to stratification
-P of compounds of polyethylene with elastomers of different chemical nature on the
time of forming of a splice r at'room temperature aria., a temperature of fusing-
~of polyethylene of 120"G. During-preparation of the'uplice., elements of the
compound were placed in contact after achievement of the given temperature. It"..
that with an increase of rj adhesion is increased. Increase of tempera,-~
'Card 1/ 2
SM!! 0
ACCESSION. NR: AR4040827
ture of splice- foimdng to 120'C ificreaues the adhesion 40 70-fold. At 120uG
-curves P - T for aU elastomers have the fom P = kl-"(k and a - Paramcters).
With increase of number of polar groups in clastomers, adhesion decreases and
can attain practically zero values. The results arc explained from the point of6
view of the diffusion theory of adhesion on the basis of the idea of local
;diffusion, introduced by the authors, explaining the formation,of an adhesional)
bond between polar and nonpolar polymers.,
SUB CODE: OC, GC ENCL: 00
Card 2/2
VOYIITSKIY, S-,S-; JUYEVSKIY, V.G.; YAGNYATINSKAYA, S.M.
Adhosion between polymers as influenced by their physical state.
Dokl. A.N SSSR 150 no.6:.1296-1299 Je 163. (KRA 16:8)
1. Hoskovskiy institut tonkoy khimicheskoy tekhnologii Im. M.V.
Lomonosova i Problemnaya laboratoriya pererabotki i modifikatsii
po]J.merov Moskovskogo takhnologicheskogo instituta ;nyasnoy i
molochnoy promyshlennosti. Predstavlono akademikom S.S.Yedvedevym.
(Polyners) (Adhesion)
ACCESSION NR-* AP4042339 S/0138/64/0001007/00161/0020
AUTH0R*_Voyutskiy, S.. S.- Rayevskiy,.V. G.j'Yagnyatinskaya,,S. M.
TITLE: Role of adhesion in the' elastomer reinforcement phenomenon
SOURCE: Kauchuk i rezina, no. 7, 1964, 16-20
TOPIC TAGS: elastomer,rmbber, rubber.reinforcement, filler, active
filler, adhesion, adhesive oint, microscopic a*dhesive joint
ABSTRACT: It is hypothesized that mixtures of elastomers and active
fillers consist of a great number of microscopic particles of the
soiid filler bonded with rubber (adhesive joints). An attempt i's A
made to substantiate the hypothesis by the following considerations:_-, I
1) rubber can be reinforced only with fillers the strength'and hard-!
ness of which are higher than those of' the rubber; 2) carbon black
reinforces onl,
Velastomeric.(and not resinous) butadiene-styrene
rubbers; 3) flocculation or-adhesion of active fillcr~particlea re-
sulting in the
-formation of a "carbon-black gel" plays an important
role in the re,.Lnforcement of rubber; 4) phenomena of elastomer rein--,
forcement and phenomena.of.,adhesion or bonding follow1dentical laws,,,
11/2
Card
ACCESSION NR: AP4042339
"and factors such as.glue-lirfe thickness, contact time, temperature,
and vulcanization time which increase the strength of the microscopic
adhesive joints increai;e the,reinforcement of rubber and vide versa,~
The hypothesis on the adhesive nature of rubber reinforceqpt does
not contradict eithe'r the-chemi~al theory of reinforcement',-(because,
in many instances, adhesion is caused by chemical reactions) or the!
theory that reinforcement-is a result of the formation of filler
o individual filler particles b
particie chains (because tw can e
bonaed bysections of one and the same polymer macromolecule). The
electric-conductivity of rubber mixes and vulcanizates containing
certain blacks can be explained by the. formation of point eontapts
between neighboring filler'particles. Orig. art. has: 4 figures.
ASSOCIATIONS Hosk6vskiy institut tonkoy khimicheskoy tekhnologii ~i
ii im. M. V. Lomo-osova
n (Moscow Institute of Fino,Chewical Technology)
Ii SUBMITTPDs 00 ATD PRESS: 3054 ENCL: 00
SUB CODES ~MT NO.REF SOV: 013 OTHERS .616
e;1;jj,2'2
C
ACCESSION' NR: AP4021969 S/0063/64/009/001/114/115
Voyutskij, S. S.; Rayevskiy, G.; tiuskaya
TITLE: The role.of adhesion in the reinforcement phenomena of elastomerse
SOURCE: Vacaoyu2:noyo khimichaskoya obshchastva. Zhurnalp v. 9, no. 1, 1964,
114-115
TOPIC TAGS: elastomer, reinforcement, rubber, adhes io"n,*rAnfor'cement mechanism,
filled resin,' active filler, filler adhesion, resin.strength,. particle size
ABSTRACT: Experimental data and obs'ervations''from the literature.~re'offered to
substantiate the belief that the reinforcement of elastomers filled with active
fillers is directly associated with adhesion of the particles.. Measurements show
a linear function between the,coefficient of reinforcement of rubbers and their
resistance to lamination from glass of unmodified and modified (dimethyldichloro-
silana, vinyltrichlorosilane and allyltrichlorosilane) SKB and SKU-40. The
-thickness decrease*, to a
adhesive strength of polymeric adhesives increases as
limit, after which.the strength decre-asese The same relationship exists In
reinforcing roDiu with fillerv where the strfnSth of tba resin increases as filler
Card
1/3
ACCESSION XR: AP4021969
content increase6 (thickness of.resin layer between particles decreases), to a
limit, and with 6verloading the filled resin strength docreases, Decreasing
particle size, to a limit approaching molecular dimensions,also increases
reinforcement of the resin. Adhesion of polymers increases with prolonged contact
with the substrate and with increased temperatures The addition of filled resin
'ard preheati6g of the fillers are known to at .renStben the resin. The strength of
adhesion increases with vulcanization time and goes through a maximum. The same
relationship in the change of filled resia strength is observed by increasing the
extent of Vulcanization. It is concluded that the adhesive approach does not coa-
tradict present -theories on reinforcement, and in fact, partially explains the re-
inforcement phenomenon. The average distance between particles in filled rein-
forced recins is considered to be not more.than 200R, with the elastomer macromole-!
cule co=nectinZ the surfaces of several particles. Orig. art. has: 2 figures*
A.SSOC11%TION.: 14oskovskiy institut toakoy khimicheskoy teklmologit Me Ve
Lozonozova (a a s c G-4 Institute of Fine Chemical Tccbaol
2/3
Card
y9-_
*--2a V-S" ~--dq i" " . uwmmm~~
VOWrSKIYY S.S.; X-AkKkT1YSKAYA,-jqpM,; FRUNKIN, L.S.; 'MPTSFY.FVA, S.N.;
RAYEVSKIY, V.G,
Method for determining polymr adhesion + pc&*r--d, fillers. 7av.
la:b. 30 no.lOsl222-1223 164. (MIRA 1824)
1. Moskovskiy institut twonkoy khimicheskoy tekhnologii imeni
Lamonosova.
~O
~dvkaz'::,' Z-avo a aya-A aboratoriya :V. n 0.1 1 12214124
TAGSt adhesions polymerg filler, powder filler, sodium
-.ib-tstedLene rubber, nitrite rubbcr, chalk# chemical black'
n'e-w-n_eithi-O&__ has-, been develoged fcr determintag.the adhe-
-.-OSTIEAC
islou of polymers to any powder filler.l~ The method is bated an the
.1une of substrotes prepared from mixtures of various amounts of a
tipowder filler with a binder. The surface of the substrate must be
~-;!machaniaal 1y. -prepreared-.and zIeqne4.-.to_ ensure, C.Lose contact between the
t~iiier parttcles~-4n the poti:" - " e polymer to the
mer, The adhes Lo n ot th
pure filler was d,atertained by graphic extrapoldtion of experimental
curves of adhesion walues versus binder/filler ratio to a cero binder
,content. The results of experiments conducted with: 1) sodium buts-
.-,,.,Card,,- 1 /4
4.
chemical black (active filler) an the substrate
in Figs. I and 2 of the Enctosure. The dotted lines are
Ourve.. sections extrapolated to a zero bindstr co te t Their Lmtev-
~f On&-v th,-the-'4rdin-at-eF.Und c'atc,.t es on-*0 eopa ymer-to t a
it h
-,-Ri --,- Orig., act. has: 2 figures*
ler,
ki-y Ad "tonk" mith
Ah I
i0k6y,-tek
4-'~t amon, MW im i ca- Technology)
1 00-
CODE t Gic
HK TED;, 'oz:- SUB
OTHER-t-, T
00 A D PR SSi': 11124
k-W
M----
i
~-. 4-
rM W-1w/En_W_V(y VNI/W/JWD
twp(j) IJP(C)
ACC NRt AP6023431 SOURCE.CODE: UR/oigo/66/008/007/1247/1251
AUTHOR: Korenevskaya, N S lavrentlyevp V. V.;_Yagnyatinskayal, S. M.; Rayevskiyo
V. G ; I[MLtski2, S. S.
ORG: 2 Y
nd Moscow State 169dical Institute (2-y 14oskovskiy gosudarstvannyyyinstitut);
110scow Institute of TU777M71-c3l _T6cEo_1oPri im. N. V. Lomonosov (Noskovskiy institut
tonkoy khimicheskoy tekhnologiiy-
TITLES Effect of degree of oontaot on the strength of adhesive bonds between an
elastomerjand a solid substrate
SOURCE: Vysokomolekulyarnyye soyedineniya, v. 8, no. 7, 1966, i247-125J,
TOPIC TAGS: elastomar, adhesive bonding
ABSTRACT: An optical method was used to study the effect of the conditions/under
which elastomer - solid substrate and elastomer - elastomer adhesive bondslare formed
I-an G
on the strength of the/,bonds and the doe-rqe of the contact beEween aJFes ve d ub-
strate. The adho.,, 1190 N-Wri)utadione-acrylonitrilo copolymor, and the
,!iv(_ mployod was SK
substrate was a polished part of a paste prepared from a mixture of.channal-black pow-1-
der and polyvinyl alcohol binder.!,, The optical instrument used for determining 'the
area of actual contact is described. The effect of pressure and duration of the con-
tact on the OXtGnt of' the adhesive - substrate contact was determined. It is shown
that in both types 6f adhesive bonds studied, the increase of adhesive strongth with
CQd_ 1/2 UDC: 678,01 51
ACC NR: AP6023431
- 1
I
the observation time continues even after the equilibriiLm value of the degree of con-
tact has been established. It is Dostulated that the discrepancies observed between
the course of the kinetic relationships and the strength of the self-adhesive elasto-
mer - elastomer bond is due to volume diffusion.processes, and in the case of the ad-
hesive elastomer - solid substrate bond, to microrheological processes and surface
diffusion. Authors thank V. F. Isailtsev for carrying out a part of the work at the
colloid chemistry department of 'IMEhT im, M'. V. Iomonosov. Orig. art. has: 5 figo-
SUB COM: 11/ Sum DATE: 2-3jun65/ ORIG REi: 007/ OTH REF: 001
Card 2_/2/'~~v
I R,
AP6031155 SOURCE CODE: UR/0190/66/008/009/1493/15003
AUTHOR: R
Y Voyaskiyo S. S.
ORG: Mosc,ovi Instit 6 of M
ut ine Chemical Technology-im. M. V. Lomonosov
(Moskovskiy inotitut khimicheskoy tekhnologii); Moscow Tecilnoiggical Institute
of the Meat and Dairy Industry (MoSkovskiy tekhnologicheskiy institut myasnoy i
Molqchnoy promyshlennosti)
TIT LB: Affi'
h
2sionof e astomers to owder fillers and reinforcement of filled
systems. Third report from the series Reinforcement of Polymers
0
SOURCE: Vysokom lekulyarnyye soyedineniya, v. 8, no, 9, 1966, 1493-1500
TOPIC TAGS: ad
hesion, elastdmer, powder filler, polymer, polyisobutylene,
polymer reinforcement:
ABSTRACT: The Wect was studied of various additives, which change the
adhesion of SKN-40Wrubber to chalk, on the strength of chalk-filled vulcanization
of SXN-40. It, was. found that there is a linear correlation between adhesion and -
the reinforcement.'of vulcanized rubber according to rupture and tearing. The
1/2 UDC: 678. 01:53
lCard
21~+T~~.~~-w~,g~~kt-,;,,~,~~--iiq.~~r,~~-,z,,e4r-x!at_~ita~l-~~~smtt~--,!Mlrzrrllz~i~--~bTZ-71~1,44i2--*~-~.jLqK2.ql_~.,
~. . . . . . . . . .
YAMYATI NS ilYh
Yevj~,cni~_# Grigorlyevna.
Laboratory Diarnosis of scarletina kv tile method of precipitation.
Dissertation for candidate of a Iledicl.1 Science Degree
Chair of llurserj Infectious Disealcs (head Drof. 1.V. Rut-in) Saratov
Medical Institute) 1948.
C-; /V
YAGNYATINSKAYA, Ye.G.
lobarator7 diagnosis of dysentery. Pedistriia no-8:78-79 Ag 157.
(MIRA 10:12)
Iz 5-y detskoy infektsionnoy bollnitsy Saretove.
(DYSINTERY)
17(2012)~ soy/16~.59_9_5/47
AUTHOR:~ Yagnyatinskaya 'Ye. G
The Toxigenicity of Corynebaoterium Diphtheria Strains Isolated From
Patients and Carriers
Zhurnal mikrobiologii, epidemlologii i immunobiologii, 1959,ANr 9,
pp 23-25 (USSR)
ABSTRAC7f MJ. Gluzman held the opinion that the toxigenic properties of-Coryne-
bacterium diphttieriae.determine its'virulency. A.S. Krutkova, V.S.
Suclova, N.I. Volovich,K.M.LefldaiiA.PMarlsova and Ahers -consider the
method of-cultivating the diphtheria strains on solid nutrient media
td.be'just as',effectiveand'sensitive as the method in vivo oultivation.
Subject author reports on his use of the solid media method in the
'
li6orator7r of the V detskaya infektsionnaya bo'llnitsa Saratova
(V
Ho3pital of ChildrenislInfdatious Diseases) in Saratov. The tokigenic
properties of 416 pure diphtherial strains were tested. in parallel
expIerlmentsin guinea pigs and on 3% Martin agar. 7be, results co-
inoided in 89% of the caBesj Toxigenia strains were isolated in 200
of' the 247 patients with diphtheria and in carriers toxigenio strains
Card 1/2 wore isolated in 55.8%. In nidi of diphtheria, toxigenio strains were
soy/16-59;-9-5/47
-The Toxigenicity of Corynebacterium Diphtheria Strains Isolated From Patients and
Carriers
isolated twice as often as outside the nidi, The tests showed that
it Is quite feasible t1o use mixed bacterial cultures for the rapid
detennination of Corynebacterium diphtheriae.
There are: I table and 9',references, 6 of which are Soviet, 2 English
and I Scandinavian.
ASSOCIATION: 5-aya infektsionnaya detskaya bollnitsaf.Saratov (Nr 5 Hospital of
Children s Infectious Diseases,', Sarato"
V),
SUEMITrED: anual. y 16, 1959
Card 2/2
YAGNTATIYSXjT,,_S,..O.; MMIWf N.M.
X'. ; KHAVTSOV, V,S., vedushohly reduktor;
tekhtilchaskiy redaktor.
[Automatic lines for grinding bearing parts] Avtomaticheskie linji
dlia sh'lifovanila detalei podshipnikov. Moskvpt, Gos. nauchno-tekhn.
izd-vo imshinostroit. lit-ry, 1954. 31 p. (MMA 8:1)
.(GrIinding and pollshinZ) (Roller bearings)
VECHERO N.A.9 inzh.; GMIAIDZEp 0. Ye.t inzh.;-pANFILOV, M.I., d,~-tsent;
KHILIKOI M.M.p inzho; MERSHCHIYg N.P.p inzh,; ALFEROVV X.s..t inzh.;
ANTIONOV9 S.F.; DTKSHTEYN, Ye.I.; YAGEM, M-1,; BELIKOV, K.N.;
GONCHAREYBKIY9 Ya.A.; TRIFONOrq A.G.;,SEbACHq G.A.
*OpeLa-heErth plants with.,large-capacity furnaces" by D.A. Smoliarankop
N.L Efanova.,Reviewed by N.A. Vecher and others. Stall 21 no.2:125-126
F 161. (MIRA 14:3)
~1. 6,werdlovskiy sovet narodnogo khozyaystva (for Vechery Germaidze, Pan-
fi:Lav).
~Ppen-hearth f -I)Ng and consti
urnace rtion)
(Smol-iarenko, D.A.) kzr oval, X.I.
OVECIIKISY Ye.S., kand.tekhn.nauk; SHIFMAN, R.O., inzh.; YAGODA,, L.A., inzh.
Analyzing the chemical composition of leather by the separate
topographical sections. Nauch.-issl.trudy Ukr I(IIKP no.13:222-
236 162. NIRA 183-2)
I ---- --- -- --- ---- - -- --- - :-- --
ya.1 YAGODA ots
B01301my"
ometry of color multilayer rat,,,rials- Zhur""uch'i Prikl*
Sensit . 1650 (JaRA.
10 no.3%161-169 "Y-le skoy SSR (AMU)
iskuset-7 Chekhosl0v&t
yjnofal~ulltet Akaaamii inatitut tekhni-ki zv-a'y&
izobrazhen:lya (VUZORT).
YAGODENKO, M.
ILIYASOV, Yc-':) AIZKSrY?,V, ~%V-
ImIre stl gating and comonting cimulatlOv
a hydromchanical Packer denigned by tfir, Totar
horizons Usicg 0o..24 165. (MIRA 18- '5)
Oil If6il Drilling Trust. Burenie no.4-.,
1. Gosudarstvanriyy t-rest, po net'tobtxro vym rabotam Tatarskoy ASSR.
(Mining machinery
STANISIEVSKIY, A.S.; RUDEITKO, A.P. - YAGODIN A.1-1.
14e-Vnod,:s for calculating a"heavy drill-stem bottom. Trudy
VITR no.3:319-69 161. (MIRA 15:7)
(Boring machinery)
YAGODIN J.
CU4, initial -41 fu=1 vats. tLad
tion I,w the rILI,-) 4 -he ')Y
~r s'- M12T
tp
144
YAGODIN, 0. A.
A. *Investigation of the IsOtOPe Copposition of EquJ-lJ-br:lu'4
yAGODIN, G. Ethane, and Methane-" Kin Higher
Phases in the Distillation of Ethylene, oiogical Inst imeni
Moscow Order of Lenin Chemixotechn, Inst iment
Education USSR- Labor Red Banner PhYsicochemical
11 Mendele~ev- Order of f Candidate
D. . . . V# Moscow, 1955- (Dissertation for the Degree 0
L. Ya. Karpo
:ences.)
of Chemical 9"C-1
so. Kniz IhnaYa _qtoj3js1 No. 49 Moscow, 1956
S/078/60/005/009/005/017
B015/BO64
AUTHORS: Yagodin, G, A,,) Tarasov, V. I,
------------------------
V
TITLE:_ T~iermal Stability o,f Potassium Fluozirconat,
PERIODICAL: Zhurnal neorganicheskoy khlmii~ 1960, Vol. 5, No. 9,
pp, 1987-1992
TEXT: The thermalstability of.potassium fluozirconate was thermogravi-
metrically examined as well as by X-ray structural analysis, and by
methods of optical crystal examination. The first-mentioned analyses 'sere
carried out wi4h the Kurnakov pyrometerg the second on thermally pre-treat-
led samples in different gas media (Fig. 5)6 A* Ao Mayer carried out the
optical crystal examination. Heating of potassium fluozirconate entails
.a number of conversions Five endothermal effects occur when heating up to
10000C. The effects at ;85-3300C charaoterizethe process of reversible
'distortions of th8 crystal lattice and lead to a reduction of the crystals.
The effect at 465 C is due to the reversible decomposition in potassium
0
fluoride and zirconium tetrafluoride, whereas at approximately 600 C
melting and formation of a mixture takes place. This depends on the heating
Card 1/2
Thermal. Stability of Potassium Fluozirconate S/078/60/005/009/005M7
conditions, since thecomposition of the melt changes due to zirconium
volatility. Annealing of potassium fluo%irconate in undried air during
0
four hours over 600 C (Table) leads to the formation of zirconium dioxide.'/
Annealing at 8000C in dried argon or hydrogen does not change the, propel-
ties 61' potassium fluozirconate. V. A. Plotnikov and Ye, B, Oitman,ara
mentioned in the paper. There ara 5 figures, table, and 7 references.-
3 Soviet, 1 German, I French, and 2 US.
SUBMITTED; March 7, 1960
Card, 212
-qOV/78-3-8-42/48
AUTHORS. Yagodin, G. A., Fomin, G. S., Fisellson, L. A.
TITLE: The Determination of the Relative Volatility of the Products
of the Interaction 3etween ZrC1 41 HfC1 4' and POC13 (Opredeleni~e
otnositelnoy letuchesti produktov vzaimode.ystviya ZrC1 4 i Hf%"'l4
s POC1 3)
PERIODICAL: Zhurnal neorganicneskoy khiiiii, 1958, Vol. 3, Hr 8, pp. 1971-
1972 (USSR)
ABSTR&CT;
Card 1/2
In the present study the arnount of the relative volatility of
the products of the interaction between ZrC1 and HfC1 with
4 4
POC13 was determined by means of a re-circulating apparatus.
The hafnium content in the samples was determined by radioactive
181
Hf . The basic materials were purified bj m&qrla of the sub-
limation method. The hafnium content in the basic material Hf02
amounts to 0,8 per cent.
The relative volatility (a) of the materials inveatigated
amounts to 1,160 � 0,005 at the pressure of one atmosphere.
There are 1 figure, 1 table, and 3 references, 1 of which is
SOV/78-3-8-42/48
The Determination of the Relative Volatility of the Products of the Interac-
tion Between Z.-Cl and
HfCl4' POC13
Soviet.
ASSOCIATION. lJoskovskig khimiko-tekhnologicheskiy institut im. D. I.
Mendeleyeva (Chernical-Technological Institute imeni D. I.
Mendeleyev, Moscow) Moskovs'~iy institut tsvetnylch metallov i
zolota im. L. I. Kalinina (Institute for Non-Ferrous Metals
and Gold imeni M. I. Kalinin, 11,loscow)
SUBMITTED: December 12, 1957
YAGODIN, G.A.; MOSTOVAYA, O.A.; CHM04AREV, A.M.
Sepprating hafnium and zirconium bv extracting their nitrates with
the diisoamul, ester of methylphosphonic acid. Izv.,r/s.ucheb.2av.;
khim.i khim t.6kh. 3 no.1:135-137 160. (MIRA 13!9)
1e Knfedva tekhnologii radioaktivnykh, redkikh i rasseyannykh
elemantov Moskovskogo khimil~e-tekhnologicheskogo instituta imeni
D.I. Mendeleyeva.
(Hafnium)
(Zirconium)
(Chemical tests and reagents)
S/078/60/,005/05/10/037
~~2 AA3.2 0 BOO41B01
AUTHORS: Yegorov, G. F., Pomin, V. V.9 roloy, Yu._G#, agodin, G.
TITLEt Solvate Forms of Zirconium- and Hafnium Nitrates I
butyl Phosphate
PERIODICAL- Zhurnal noorganicheskoy khimiif 1960, 'Vol. 5, No. 5,
PP. 1044-1050
TEXT: introduction, the authors mention in brief the problomo dealt
i-Itith: prepaiation,of ziiconium with a minimum hafnium content, investigation
of the mechaki-m of, ~tho (C H 0) PO (TBP) extraction, investigation of the
4 9 3
solvate forn.,11ext, thoy describn the purification of the reagents, Tho
9
Partition coe~,,ficients of Zr and Hf were determined by means of Zr ) and-
181 95 95
Hf . The resultant. Nb. was oeparated from Zr by means of Mn02- Tht, ex-
traction.s were carried.out at 200 and at'a zirconium- and hafnium con-
centration of jo-5 First of all, 'the extraction of,nitric acid by
tributyl phosphate at different acidity and concentration of the 110-
3
Card,1/3
Solvate Forms of Zirconium- and Hafnium S/07o/66/005/05/10/037
Nitrates With Tributyl Phosphate B004/BO16
ions was investigated. Intbis connection, the authors refer to papers by
A. S. Solovkin (Ref. 2), A. M. Rozen (Ref. 6), V. V. Pumin, and Ye. P.
Mayorova (Refs. 3,4,7). The existenre of the complexes TBP.11NO and
3
TBP..2111,0 assumed by the last-mentioned authors in Ref- 7, and -the values of
3
tIheir instability constants (0.2-2 and 0.00044) were confirmed experimentally
(Table 1) . Xyleno wass used as the 3olvent for TBP. The ;dependence of the
nitric-acid extraction on the concentratfan of hydrotAn ions and in the
040 ~_ is ohown in table 2. The
presence of NaNO 31 HH 41103' bilioA O-r lic- 3/'
-t a. w i -~ItLe
mechanism assumed of HHO extraction hol.ds it do r, also in the
3
PTG~3ewoc of an excess of 110- ion3. It is proved for the extruction of Zr and
Hf that the partition coefficierits darr. proportional to the concentration
se. The number of solvating TBP rioleculas wao
of~free TBF in the organic pha
~ewnd_6 9f 1r.6c< on log(TBP) org. Experimental data
determined from the- n
far zirconium are presented in table 5, for hafnium in table 4- It resulted
that partition coefficients !,,,f Zr and Hf increased with increasing TBP can-
Card 2/3
Solvate Vorms of Zirconium'- and Ila f nium 8/078/60/005/05/10/037
Nitrates With Tributyl Phosphate B004/BO16
centration in the organic phase, On the I_W'6id:~of the diagram log c~
TBP) (Pig. 1) the formation of the colvato HG(NO 3)4* TBP reaulta, for
log( I
low.TBP concentrations and the solvate Mfe(110 3 )4' 2TBP for higher TBP con-
centrations. At IINO concentrations of 5 moles/1 the formation of more com-
-thich, however, was not further investigated.
plicated complexes is assunee~, i
Figs. 2,3 depict.the dependence of the partition coefficients of Zr and Iff
on the hydrogen-ion concentration and the concentration of the added.,
nitrates, The Ck-values decrease with decreasing hydrogen-ion concentration.
Thj,1, decroase, however, depondq on the type of the added nitrate. in the
presence of UH + and Na-l', bivalent 'Lons, ZVO 2-t-, or Zr (011)2+ are dissolved.
4. 2 +
The deviabion of, the dependence of c~ from linearity in the presence of Li
2+
,.and N9 is explained by a*stronger hydration of these ions. There arc-
-1711ren, 4 tables, and 7 references* 6 of whioh are Soviet.
3.fi,
SUBMITTED: PelbruarY 4, 1959
Card
- - - - ------------------------
65445
S/080/60/033/011/002/014
00 41.1 t1l 12si AO03/AOO1
AUTHORS: yptgodin, G. A., Mostovay-a, 0. A.
TITLE-
Extractionof Zirconium kid Hafnium From Nitrate and Sulfate Solutions
by the-Diisoamyl Ester of the Methyl~hosphonic Acid
PERIODICAL: Zhurnal prikladnoy khimii, 1960, Vol. 33, No. 11, pp. 2459-2466
TEXT: The extraction methods used for separating zirconium and hafnium are
very promising. In the experiments diisoamyl ester of the methylphosphonic acid
was used. . Chemically pure zirconium nitrate and sulfate solutions containing 1.8%
hafnium; nitric and sulfuric acids of the grade-"chemically pure for analysis" were
also emplo6ed. The distribution of hafnium was determined with the aid of radio-
active Hf1 1 with a half-life of 40 days, in some cases,the distribution of
zirconium was determined by radioactive Zr95 with a half-life of 65 days. It was
shown that the,distribution coefficient of zirconium and hafnium is higher than
,in the case of using tributylphosphate. The extraction capacity of the diisoamyl
ester of methylphosphonic acid in dependence on its concentration in Xylene was
studied. It was shown that already the 80%-ester extracts zirconium and hafnium
completely from a nitrate solution with a content of 5 g/l based on metal and 6.7
Card 1/3
65445
S/080/o-0/033/011/002/014
A003/AO01
Extraction of Zirconium and Hafnium From Nitrate and Sulfate Solutions by the
Diisoamyl Ester of the Methylphosphonic Acid
mole based on the nitric acid. The separation of zirconium and hafnium from
sulfate media.using extraction with solutions of the dlisoamyl ester in,benzene
preliminarily saturated with HCN3 was studied. The dependence of the ftCkS quantity
passing into the organic phase on the initial concentration of NH 4CNS is shown
on Figure 6. The results show that at a concentrati6n of HCNS in the organic
phase of approximately 0.5 mole/1 saturation begins. The molar ratio of the
diisoamyl ester and.HCNS at saturation is 0.79. With an increase in the concentra-
tion of the sulfuric acid to 2.5 mole/l in the aqueous phase a precipitate is
formed, prussic acid is separated and.the equilibrium acidity of the aqueous phase
drops sharply. The experiments of separating zirconium and hafnium were carried
out in a IC%-ester solution in beniene preliminarily saturated with HCNS. The
phase ratio was 1:1, the content of NH4 CHS in the solution 2 mole. In the moment
,of contact between the ester solution and the solution of zirconium and hafnium
sulfates mainly hafnium is extracted into the organic phase, The distribution
coefficients decrease with an~increase in the metal concentration. At a metal
concentration of 20 g/1 the coefficient of hafnium distribution is still high
enough for pactica.1 purposes. The effect of the temperature on hafnium extracticn
Card 2/3
b5445
S/080/60/033/011/002-/OI4
AOO3/A0O1
Extraction of Zirconium and Hafnium From Nitrate and Sulfate Solutions by the
Diisoamyl Ester'of -the Methylphosphonio Acid
01
was studied up to 60 C
.Temperature (in OC) 0 20 40,
30 50
Concentration [H] -in
the organic phase
(in mole/1) 051 0.49 0.51 0.50 0.51 0.51
The extraction of z:irconium. and- hafhium in tributylphosphate is cited for compar-
ison. it is shown that the coefficients of hafnium and zircorfium separation and
,distribution are considerably lower for tributylphosphate than for diisoamyl
ester. Even for W,~-tributylphosphate the results are lower Figure 6:
than for 10%-diisoainyi ester.
Zieyre 6- Dependence of the Quantity of HCNS Passing Into
the Organic P~ase on the Initial Concentration of NH NS.
4C
The, Initial Acidity-is, 2 m. H2304'
A - concentrdtion (Hf) in the organic phase (in moles),-
-concentration(14H4CNS).(in g/1),.. 02.
There are 11 figures, 3.tables and 11 references: 6 Soviet,
3 English, 2 American.
ST 80 /'?0
M4ITTED: April 41, 1960
Card 3/3
89662
S/149/61/OW/002/008/017
A0061AOol
AUTHORSt Yagodin, G.A,., Orlov, K.V.
TITLEi Investigating Zirconium and Hafnium Separation on Anion-Exchanging
Resins
PERIODICALt Izvestiya vyBshikh uohobnykh zavedeniy, Tsvetnaya metallurglya,
ig6if No. 2, pp, 92 - 96
TM: The use of anion-exchanging resins for separa~tlng zirconium and
hafnium, is of interest, since fluoro-zirconate solution may be directly used,
which is a technical product of the fluoro-silicate method of z1roon decomposition.
There are several literature data available on the separation of zirconium and
hafnium using Dowex-1 and amberlite TRA-400 resins (Ref. 1 - 5). The authors of
the present article used domestic anion-exehw!ging resins such as HO(NO) ~A a -lCn
(EM-10P)'# MMF -1 (MMO-1) A (~_16 (Av-16) and I H (TN). The American IRA-400 re-
sin was used as comparison element. V.V. Novikov participated in the experiments,
which were conducted-to determine the fg1l exchange capacity of the aforementioned
ion-exchanging resins in respect to ZrFg ions by the follaxing method. A batch
of 3 g dry resin of -0.25-+0.15 mm grain size, was subjected to triple treatment
Card 1/ 5
89662
S/ 149A 1/000/00 2PO 8/
A17
Aoo6/Aoo i.
Investigating2iroonium and Hafnium Separation on Anion-Exchanging Resins
during mixing 500 ml of K.;)ZrFg solution saturated at 1800. Each contact lasted 3
hours. Y,2ZrP concentratIon Iduring the second and third contaot was checked by
the weight meqho4 and was equal to the initial concentration. The resin was then
filtrated and waahed until,& negative reaction on fluoro-ziroonate ions took place.
The sorbed fluora-zirconate ions were washed out of the resin ifith 2 n. Oulfluric
acid. Zirconium.hydroxide was precipitated from the solution by a nia, roasted
rFj0
to Zr02, and weighed. The full exchange capacity in respect to ZrF per gram of
dry re6in (in sulfate form) was (in grams of Zr02). o.o74 for TN; 0.0093 for
MMO-1; 0.142 for NO; 0.260 for AV-16; o.262 for EDE-10P, 0.193 fvr IRA-400;
and 0.149 for AKi_9F. Zirconium and hafnium separation was'investigated'on columns
of 45 m length and 1 cm diameter ahd 1.7 in length and 2.5om diameter. The resins
were preliminarily converted into sulfate form and washed up to PH--4-5. A cer-
tain amount of KZrF solution of 18.4 g1l concentration was passed through the
column at a rate of q ml/cm2 per minute. Subsequently the col r was washed and
1:n. sulfuric.acid was passed through it, at a rate of I ml/cm . The solution
flowing out was divided into fractions. After completed washing-out of zirconium
and hafnium the column was washed with 1.5 liters of distilled water to pH=4.5.
The summary content of Zr and Hf in each fraction was determined by weight nnalysis
Card 2/5
89662
s
/ 61/000/002/008/'017
149/
fi-0061AGOI
Investigating Zirconium and Hafnium Separation on Anion-Exohanging Resins
on the AC fl -22 (ISP-22) spectrograph. Table 2 shows the results of one of the
experiments, which was performed.ufider the following conditLons: resin weight
g~ height of layer - 43 am; amount of Zr02 equivalent to the sorbed amount
of ZrFg- - o.448 g; content of HfO in Zr02 4%; desorbtion rate I ml/om2 per
minute. It was found that all the anion-ekehanging resins can be used to obtain
partial separation of Zr and Hf during one cycle. FDE-10P resin was found to be
the most effective one. During washing of sorbed ions with n H S04 at a rate of
0.5 ml/cm2 per minute, the hafnium content In the initial fr;oJon was 30% with
52% yield of hafnium oxide; in the subsequent fractions zirconium oxide of high
purity was obtained (.e" 0.05% HfO It was found that the order of washing Zr
and Rf with sulfuric acid changed the presence of KC1 in the solution (Table
4). This is apparently connected with the formation of mixed fluoride-chloride
Zr and Hf2 complexes.. When washIng the sorbed -ions w�th 0.5 n ' HS04 at a rate of
0.5 mllam per minute, the Hf02 content in the last fraction was 40 - 50%with
60 - 90% yield. On the basis of results obtained the EDE-10P anion-exchanging
resin can be recommended for the partial separation of Zr and Hf and for the re-
latively simple production of Zr_Hf concentrates with up to 50% HfO2 content in
relation to,Me02.
Card 3/5
89662
sli 49/6 1/000/00 2/tO8/017
A006/A001
Investigating Zirconium and Hafnium Separation on Anion-Exohanging Resins
Table 2 g
Separation of zirconium and hafnium on EDE-10P resin during desorbtion with mono-
normal sulf'uric acid
Volume of fractions Amount of washed out Hf02 content HfO2 yield in %
by tl~e order of Meo~) in MeO 2% from sorbed on
washing, nil % from sor- resin
bed on resin
50 - 130 o.o66,3 15 ~14 52
130 - 170 0.1271 1.,5 7
210 - 41o 0.1507 35 0,7 6
89662
8/149/61/000/002/'008/017
A006/AO01
Investigating.Zirconium and Hafnlum Separation on Anion-Exchanging Resins
Table 41
Dependence of full exchanging capacity of EDE-10P resin on the presence of XCl in
the solution
KgrF 6 g/l KC11 9/1 Full exchanging capacity of 1 g dry resin
(in grams of Zr02)
5,45 35 o,116
i3j,4 35 0,217
13 4 23 0.0262
13:4 00267
There are 5 tables and 5 references: 3 Soviet and 2 non-Soviet.
ASSOCIATIONS: -Moskovskiy khimiko-tekhnologicheskiy institut (Mose-ow Chemico-Tech-
nological Institute). Kafedra tekhnologii redkikh elementov (De-
partment of Technology of Rare Elements).
SUBMITTEDs February 19, 196o
Card 5/5
5/828/62/000/000/001/017
E039/9420
AUTHORS: Kaplan, G.Ye., Yagodin, G A., Moiseyev., S.D.,
Dm�triyeva, L.P., Mostovaya, O.A., Chokmarev, A.M.,
Sevostlyanova, E.N.1 Udovenko, V.F.
TITLE: The separation of zirconium and hafnium bv means of
organophosphorous compounds, amines and other
extraction agents
SOURCE: Razdelaniye blizkikh po svoystvam redkikh metallov.
Mezhvuz. konfer. po motodam razdel. blizkilsh po
svoyst. red. metallov. Moscow, Metallurgizdat, 1962,
28-41
TEXT: Although large separation coefficients can be obtained by
tho use of mixed nitric and hydrochlor1c acids tho process is not
Pavoured because of corrosion difficulties and the largo quaniity
of acids required. The results of experiments on the extraction
of these elements from a sulphu'ric acid medium in the presence of
different extraction agents is therefore examined. It is shown
that diisoamy.1-ether-niethylphosphonium acid ( i C H110) 2POCH3
(DAMPA) is a inore powerful complex forming agent than
Card 1/2
S/828/62/000/000/001/017
The separation of zirconium ... E039/E420
tributylphosphate (TBP). The separation and distribution
coefficients for Zr and 11f are 24.6 and 3.2 respectively when
using 100/'o DAMPA in HpSOij solution in the presence of thio-cyanic
acid, while for 40%-TSP in the -same.modium,the corresponding
coefficients are 21.6.and~~.6.~Axi increase in the concentration
of TBP is undesirable as it leads to increased viscosity and a
large loss of extraction agent. It should be noted however that
the re-extraction of DAMPA is more difficult than for TBP.
Diplienylphosphoric acid extracts Zr and Hf from H2SO4 solution with
a separation coefficient 3 to 10. Other extraction agents of
this typo are also tostod. Testa aro also made on the use of
tri-n-octylamine and in this case as the concentration of UpSO11 is
increased the separation coefficient for Zr and Hf passes through
a maximum value of 12 at about 1 normal H2SO4 and then falls to a
steady value of about 10 for further increase in the H2S04
concentration. Details tire givan of tho constitution of the
,organic and aqueous phases and the effect of acidity on the
separation coefficient. There are 11 figures and 3 tables.
Card 2/2
3/830/62/000/002/002/002
DV4 308
AUTHORSt Yagodin, G.A. and Chekmarev, A.M.
The extraction of ziroonium and hafnium
TITLEt
by tri-n-octylamine from metal fluoride
solutions
-SOURM Ekstraktsiya; teoriya, Primeneniye,
Zefirov
apparatural-no# 21. Ed. by A.P.
and M.M. Sdnyavi*n. Moscow, Cosatomizdat,
i962, 141 1531
'XT:
TL The extraction of Zr*and Hf from K
2MF6
(where M Zr, Hf) by a solution-of pure. tri-n-octylamine (TOA)
in benzene is discussed. TOA will extract Zr and Hf only from
weak acid solutions since more* acid7solutions tend to form
R N.HX (where X - HSO C1, NO ). Highest values for the dis-
3 4' 3
tribution coefficients, D and D. , were obtal'ned
Zr f with 0.2 M
H2SO4 while HNO 3 leads to the lowest D M values. With H 2SO49
Card 1/2
S/830/62/000/002/002/002
The extractionof zirconium ... D214/D308
D but with HNO, Zr is preferentially extraotod, The in-
Hf >')Zr
fluence of additions was also studied. The values of D M decrease
as the concentration of the addition in the aqueous phase increases.
With small additions of XCL of KF D Hf > DZr but at higher con-
centrations > 6g11 for M 1% for KP) D Zr _ND... Addition of
K2SO4 make D Z r~~- DHf but with NH4NO 3 *D Hf > DZr Extraction from
K2ZrF6 (10 1;/1) acidified with 0.2 M (COOH)2 b.Y 5% benzene solu-
tion of TOA gives D 47 and D - 10. Both D values decrease
Zr Hf
as the molarity of the acid in decreased. The extraction mechanism
is sum ari .zed bys 2(R3NH)HSO 4org. + ~K2Z TI.. F6aq. *=L- (R3NH)2 ZrF6org. +
-2KH504a Evidence for this, mechanism is discussed in,detail.
+
q -
There are 12 figures and 6 tables.
Card 2/2
---- - ------
'.ACCESSION NR:1 AR40l5645 8/0081/63/000j022/0384103841
SOURCE: RZh. 10,imiYa, Abs. 221,93
AUTHOR: Pushkav, A. A.; Tarasov, V. V.
TIT1,E: Separation of zirconium and hafnium by extraction in a packed pulBating
column
CITED SOURCE; I.V. Mos. khim.-tekhnol. in-ta im, D. 1. Mendeleyeva, vy*p. 40,
1963s 142-144
TOPIC TAGS: zirconium hafnium, chromatography, column chromatography, zirconium
purification' pulsating column
TRANSIATION: ~A:good degree of purification of Zr from Hf can be obtained by
extraction with a 10%,solution of diisoamylmethylphosphinate in keirosene on a
packed pulsating column. N..Shiryayeva
DATE Aft. 07-Jan64 SUB CODE;' CH ENCL: 00
Cd'r-d -
[j YA".-t DLN 'G
.4):32--3 5 163,
rigtIcin of lwir,
1-onn in
Y/ LO
L 1743 ~-63 EPF(n)-2A W/ (m)/~DS AFFTG/ASD/SSD Pu
WW/JD/JG
77-1~
HOSTOVAYA, 0,.A.; WIM, T.V.; YAGODlN, G.A.--_
Distribution of water during the -1-nation of some P-cJe,!3
and valts of zirconium. Zhur. reorg. khIm. 9 no.5;1280-
1284 My "649 OUMA 17S9)
TP(c) WW/JW/JG/JD
pu 17 1.
ACCESSION YFU AT5012664 UR/2539/63/000/044/0035/0036
-~AUTHOR!lz C
1&d
hii x ro na Ujj~hejtj~g
_q, -TITLM,~_Be 4o
U _f- -TtOk!'
khn-
-e
tji
WflIft- u lektrolzhimiL - -
lya V oblastl fizi &eskoy
field of physical chemistry, analytical chemistry and electrochemistry), 35-36
I TOPIC TAGS: jotassium fluorohafnate, potassium fluorozircoliat fluorohafnate thermal
property, fluoroHrconat Termal property, Fxurnakov pyrometer
ARSTRACT: The authors briefly review the studies an potassium fluorohafnates and their
analogs. the potassium fluorazirconates, reported in the literature. The thermal behavior
cf the potassium fluorozirconates is a complex physicochemical proce83 which involves
changeq in their crystal structure, peritectic processes, and changes in their state of
aggre,gation. Certain differences in the determination of the melting pcirits may be due to a
varialAe cxmpo 3ition of the phases obtained wid to different heating rabm due to the con-
version ol'a p&t of the product to the gaseous phase. In this paper, data on fluorozirc*a-
ates are compared with data on the correepondirg fluorohZnatea, whic.'i were studied by
"":J, the -differential. -the. mal method with a PK-55 Kurnakov pyrometer. Endothermic effects
ard 1/2
til Al
ACCESSION NIR: VU5012664
were note(I In the oase of KfffF5-0,75H20 at 96, 340, 414, wid 475C; the first effect cor-
responds to the lovs of water, and th,(-- last to the fusion of the salt. It is concluded that
i -, e zido
water is bound me ~hanically in the KHfFr, molwnil-. In the case of K211fF6, f ' e -
thermic effects were observed at 235, 32,14, 424, 500. cuid 5iAC, the latter N~-;119 the melting
print. In the case 3f k3lifr7.1120, endothermic effecta were -ibserved at 116. ?.30, 400. and
90OC; Uie first corresponds to the loss of water. and the last to the fusion qf -Ine sait, Orig.
art. has: I formu.
ASSOCIATION: Moskovskiy kh1m1ko-tekhnologtcheskiy institut (1vtos w C11jen-deal
Engineering Institute)
ff"M D
TT
M - -e 4A,
07
LAT /EPW EWP(
t3&--~.I'40TI49'R- APS)12975 UP/0078/65/010/'005/1250,-'1253
Sinegribo-ta, 0. A.; Y4godin, G. A.
AUTHOR.,,
phin
soamy methylOhos dtL-: extraction of hydrothiceyanic
acid, zirconium thLocyanate and hafnium thiocyanate
-MijItal- 'A_30tZ&jCh06I~6y 10'' ~-5~* 1965-.7 5 M -
'khif 12 0(,42
Or
- - - - - - - - - - -
---~-TOP -TAMw'--.~hydrothid ii~66fiiiiyi,~ thi qanate: extract dn- h4fti
cyanic~-- i z 0 UM
atid
e e tion, dI;i6oa*3.`,meb 11
anat i at
o_
~ABSTRACT: Ursina the method of sature-ion and a graphical method (exi:raction iso-
.~ - 9 ~. -'.- ' 7 9_~ ~. -1 - -~UF-4kttadtod--by diisoamy
t erm 6tchdz-tlydt~ y --o6Fan -~-71iad--HLM
a ~au~ M
Imethylphosphinate (DAMP) via the foll!3wing met:hanism:
H + CJIS- + DAMP:t HCH" DARP,
0 Pp eqa3 ibrium constan't baing dqual to IM t Oi 8-.- Extraction of zir-
:conium quifate an~- hafnium stlfate fmm sulft-ric acid solutions contalning ammonium
T, -M C)
-w z! - a ~ ~A '~.P (- x,- rac-, ~he +,w -T h e fo. f -:i comp-Dun,
Card 1/2
14R: Ap5,012975
SsIoN racted by DAW saturated
-SSI
r
IIA
ACCE s ext
orSanic phase. The
v,(OH)2(CNS)2*2 DA8P. When the uletal thiocyanate from the and that twO
1c acid, the latter is not displaced
(OR ?2
drothlocyall a fairly stable 501vate, hydroxv-
with hy ar,,j DAMP f Or'm of (haf
th hV
"'~r H CjN lecule 0 r F, ar"I C
aut-l-lors P057ula'el .n turl civate a mOi t"Us formed t.-he
't -'0r
u
04-- the 3. S) 2 - 2 (H'--NS - DI,9P)
le'u
jrolecules ~ ~~o upound Me (OR) 2 (CI"
tniocyana,,, The
-0cy
'g. art. has- 3 f1gures and 2 tabies.
phase.
pn a-se
SSOCIATION' none SUB CODE: IC, C"o
hSSOCI
MICL: 00
'UBIIT
000
N,10 REF SOV: 005
-*~r- I'Car-d 2/2_-
ME
&',T /E','IP (t)/E'
IJP(c)
JD
uglou?5/66/021/007/08?2/0874
ACC NRi 4W6024292 5uuns cw~;:
AUTHOR: Sinegribova, 0. A.; Yagodin,'G. A.
Chemico~-Technol~ogicd
ORG: D. I. Mendeleev Moscow
TITLE: Determination of zirconium and hafnium concentration in solution by titration
with a diethylamille solufl-o-n7
SOURCE., Zhurnal analitichoskoy khiriii, v. 21, po. 7, 1966, 872--874
TOPIC TAGS: zirconlum, hafniump diethylamine2 titrimetry ev"er,v rf!pjro,0A)
ABSTRACT: A simplifled weftd of detamk-dnp the conccntmtion of zirconium (or hafnium) in so-
lution has been doveloDed. It is based on the fact. that diethylamino precipitates a
hydroxide of constant conposition from Zr (Hf) solutions, so that the total molar con7l
cent,ration of the anions in the solution of Zr (Hf) salt can be determined. The meth-,
od also involves *Dhe determination of 0,T* groups in Zr compounds. The molar concen- ~1
tration of Zr is determined by two titrations of theZr sait with.diethylamine: the
first in the presence of excess KF, and the second in the absence of KF. The accurac.Vi
of the determination is 0.003 M. Orig. art. has: I table. [271~
q
SUB CODE: 071 SM4 DATE; 08Se-p65/ ORIG REF: 003 / ATD PRESS:
UDC: 543-70
YA"JOHN, ri.A,,y Pli"MFOV, A.A.; TARASOV, V.V.
:,~~-paratioa of zirconi-wra ax2d hafnium by rzzeane of extraction An
a pulsed packed tower. Trudy MKhTI no.,'0:142-144 163.
(MRIi. 18: 12)
7~
621.311 A
UM& E, A. BWFIMV MD G. W. 11-A01410.
Eleeti4jal I in"Ang Albet, Mr. stowisa, tM yo. 6. 26-3D. :in RwA,=.
ReIrabir indoor substations I 10
'(~10 kV f
t
vv ,
or up
o
MVA and up to 26 outgoing &6* cabks have.
MAIN I* been designed ror the supply or the ci:rdral am" of
bwp to*=., In the ftr%t of thew statiomt, the 110 kV
-it
$Mtchpbnt b arnnpd abow the 6 kV switchpla.
In a 4-storcy buildiul; or 21 -? ir '-,-vzY ind 12-3 m
%vidth. Tht transronner3 staul Dutdonrs in the yard.
Other buildinp for control, vamformcr se
ecluipfnent store and the cmerg.-ricy oil pit bling 111c
tot-M area up to 30(M)m' which Is, 10-15 fitnes lcs%
than the am of (-~J-Ating outdoor stations of similar
capacity. 1* ar6itectural styl: b adaptcd to the
surroundirtr. F. HUSMANN
YAC6DWIC-Al
124-11-13216
Translation from: Referativnyy Zhurnal, Mekhanika, 1957, Nr I I. p. 135 (USSR)
AUTHOR: Vyazemskly, 0. V. , and Yagodin, G. N.
TITLE: On an Approximate Calculation Method for the Stability of Earthen
and Concrete Hydrotechnical Structures on Circulax-Cylindrical and
Otherwise Arbitrarily Shaped Slippage Surfaces. (O*priblizhennom
metode rascheta ustoychivosti zemlyanykh i betonnykh gidrotekhni-
cheskikh sooruzheniy po kruglotsilindricheskim i inym proizvollnym
poverkhnostyam skollzheniya)
PERIODICAL: Izv. Vses. n.i. in-ta gidrotekhn. , 1957, _V01 57, -~_77-90
p
ABSTRACT: An analysis is shown of two methods of derivation of the forces-
in the calculation of the stability of rigid structures and ea rthen
slopes on c i rcular -cylindrical or other slippage surface: Terzaghi
(wherein the di~rection of the forces of interaction between the soil
sectors is directed along the tangent to a segment of a circular-
cylindrical slippage surface) andiCrea (wherein the direction of the
interaction fo,.-ce between-the soil sectors is horizontal), with pre-
ference given the Crea method. In connection therewith, the Authors
Card 1/2 have developed a proposition relative to the calculation of the coupling
124-11-13216
On an Approximate Calculation Method for the Stability of Earthen and Concrete
Hydrotechnical Structures on Circular-Cylindrical and Otherwise Arbitrarily Shaped
Slippage Surfaces. (Continued)
force exerted within the soil. Also provided is a number of compu-
tational examples, and recommendations are made on certain practical
aspects of the calculation for rigid structures as well as for earthen
embankments.
(P. D. Yevdokimov)
Card 2/2
YAOODIN, ON.
14ILOVIDOV) yAGoDM, G.V.
G'ERASIMOVY V.V-P
iki). Text-
ItFundamentals j:)f Electrical Engineering" (Osnovy elektrotekhn
book for military Ischools and the officer component of communications troopap
edited by G.V. Yagalin, 2d edition, revised. Voyenoye lzdatelletvo, 464 pp.,
1947.
77".11
.D32
Yacyodin
iva V SSSF,
shellen
'1;j,.njrovanjye DenezhnOgO Obva
organizatsiya I r in the USSR~ T~Y)
f circulation of GiirrencY
(organization and planning 0
I I. Yagodin.
V. i.,, Batyrevi, JSRLanov)
Vjosjva3 Gosfinizd4it) 1955.
16h P. Tables-
YAGMIN, i.culation Pnong enterpris68-
rencY (KlaA 9:9)
to ]38nk tasks in OTgAnising cur
Sta, -60 J1 '56.
Den. I kred. 14 no-7:53
-B&nks pLnd ballyll)
'/A (,Ob I 1~,f i - ~r- - - --- -- ---- -- -------
B.ATYUV, Vladimir Mikheylovich; T-AGANOV, Gdaliy Vullfovich; YAGOD11T,--r----
Ivan Tevgenlyevich; K=YAVTSXV, A.A., red.; NAIZZHDI A, Avg
tekhn.red.
[Organization and planning of currency circulation in the
U.S.S.R.] Orgeni28taita i planirovanie dene2hnogo obrashche-
nlia v SSSR. Pod red. A.A.Kurdiavtoeva. Koskva, Gonfinizdat,
1959. 183 P. (MIRA 13:1)
(money)