SCIENTIFIC ABSTRACT YANIN, B. T. - YANISHEVSKAYA, V. M.

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SCIENTIFIC ABSTRACT
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YAI~TIN, B. T. : llyaa.tor Gool09-Mlnlr,'-cA0 Scl (LI1013) -- "Bivalvo :1011"Inks of V-10 Ivalandin Q~oterive of the Crimea (the order Schizodonta, Haterodonta, and. Rudiatae)". 1100cov, 1959. 12 pp (Mofscaw Order of Lenin and Ordor of Labor Rea Baniyjr State Tj Im M. V. Lowonosov, Goology Faculty), 120 copies (n, ljo 1959, 1P8) DRUSHCHITS, V.V.; YARIN, B.T. Lower Cretaceoua deposite of central Crimea. Vest.Xosk.uu.Ser. biol., pochv., geol., geog. 14 no.1:115-120 '59. (NIR,k 12-.9) 1. Hoskovekiy gosudaretyem7y univeraitet, Kafedra paleontologli. Orimea_-Geology, Stratigraphic) YANINJ B. T. Now data on the stratigraphy of the Albian otage in Bakhchlearay Diotriot (Crimea)'# Biule MOIP. Otd.geol. 37 no.3sl26-129 My-Je 162* (MIFul 15:10) (Bakhchisaray Distcict~-Geology.. Stratierapbio) AMIDT, Yu.A. YANIN T. LAte Jurassic and Early 04 Paleont. zhur. no.3:140-,'_,2 1. Paleontologicheskly Itisti-t!lt liti i ',!csko-vskly vennyy universitet. NAYDIN, T).P,l YANIN, B.T. harhc ice of the geo2of-j of the ou.-raund!ngij e-,-' Frokhladnoya (Crivrn, Bakhoblaaray Watrict"6 Billi. Moi? 9 Otd. geol. 40 no.305-81 MY~70 165. Mpl 113t,3) YANIN, F. G. loading and Unloading New scheme for unloading ships. Rech. transp. 12 no. 1, 1952. Monthly List of Russian Accessions, Library of Congress, June 1952, Unclassified. YANIN, G.I. School hotbeds heated by a stove. Rol. v shkile no.4:50-52 JI-Ag 161. (MIRA 14:7) 1. Helitopol'skiy peclago Icbeakiy institut. fHotbeds) YANIN, Ivan -Aloksoyevich; YAKOVWT,, D.Y., red.; KIIITWY, P.A., tokhn.red. -"'--~1n:r'easing the officionc7 of regenerative braking for TL22~ electric locomotives] Pov7shnnie offektivnosti relmperativnogo tormozhenila na elektrovozakh VL22m. Moskva, Goo. transp. zhe,l-dor. izd-vo, 1958. 36 p. (MIR& 12:1) 1. Starshiy mashinist lokomotivnogo depo Elatoust Yuzhno-Urul'sko7 doro~i. (Railroads--Brak"s) (Electric locomotives) - -- ------- --- --- TANIN, I.A., maohinint Regeneratiou of enarg7 b7 the JIB electric locomotive. Ilek,i, teplotiaga 14 n0-3:7-9 97 160. (MIU 13t7) 1. Depo Matoust Tiabno-Urallskojr dorogi, (Ileotric locomotives) YARIN, I.A., mashinist elektrovoza; KOVRIZMM. V.V., mashinist elektrovoxa; V.A., insh. How to check the operation of regenarative eystem. Blek. L tepl. tiaga 4 no.10:7-8 0 160. (MIRA 13:10) 1. Depo Zlatoust Yuzhuo-Urallskoy dorogi. (Railroads-Brakse) KALININ, V.K., kand. tekhn. nauk,- MIRONOV, K.A., insh.;.LBVIN, B.H., lnzb.; LIWIAN, G.M., inzh.; YERSHOV, Ye.F., inxh.; PANCHENKO, P.M., lnzh.; BOLYCHEV, N.G., mashinist elektro- voza; ZOLOTAREV, V.N., mashinist instruktor; YA~ inzh.; BOVE, Ye.G., kand. tekhn. nauk, red.11=0, takhn. red. [Electric networks and maintenance of the equipment of electric locomotives] Elektricheskie skhemy i ukhod za obo- rudovaniem elektrovozov. [By] V.K.Kalinin i dr. Moskva Transzheldorizdat., 1963. 279 p. (MIRA 16'.-7) (Electric locomotives) '31 S/107/61/000/010/005/007 D201/D304 AUTHORs Yaninj L.$ Engineer TITIZ: Exposure meter for projection photoprinting TERIODICALt Radiop no. 10, 1961) 49-50 TEXT: In the present article) the author describes the circuit of an exposure meter which permits quick evaluation of the exposure time required. It is essentially bridge circuit with a photo-emissive cell 4(:-K1 (FS-KI) as the sensing device in one of the brid * arms. The diagonal of the bridge has a microammeter type MIC -100 f-US-100) with 100p.A FSD. The bridge is zeroed by var-ying the resistance of one of the arms to give zero deflection of the ammeter) and with the illumina- tion of FS-JU, the current flowing in the meter determine& the exposure time. The power supply consists of a half-wave rectifier employing germanium diodes A'IF- (DTY*) connected in series. The d.c. supply is stabilized by a noon valve cr-in(sa-2p) which is also used as "ON" indicator# The instrument is in a rectangular metal box 170 x 110 x 80 mm with the photocell FS-11 on the outside. The FS-KI in connected Lard 1/2 S/107/01/000/010/005/007 Exposure meter for... D201/D304 to the bridge by a 500 mm length of wire. After calibration, a sample run in made with various apertures and corrections introduced if neces- V// sary. To determine the exposure time for different grades of photopaper, the relative values of sensitivity of different kinds of paper--Unibrom -30, Potobrom 209 Bromportret 12-can be used. If a leas sensitive 500-V A meter is to be used, the d.c. voltage has to be increased, remembering the maximum p.d. at the photo-emissive cell FS-1Kl is 40OV. Thor* are 3 figures. Card 2/2 YANINp Lo. lnzh. Photographic OXPOSure meter -for Printing operations. n0-10:49-50 0 161. Radio (Photographic sonsitometry) MMA 14:10) R6 M ReplacemApt of 5Ts4S and 5Ts3S kenotrons with transistor diodes In television receivers. Radio no.2:37-38 F 061. (MIRA 14:9) (Television--Receivers and reception) _-i-- --- -I - -------: YANIN,, L., inzh. Yaults in the automatic gain networko of a televiaion receiver. Radio nojt25-26 Mr 062. (MIRA 15:3) (Television-Receivero aW reception) YANIN, L.G., inzh. PPY-AM mOdulation with Ume djvjBiOj lines Vest. BvIaZi 22 Or channels in a Milo rel-,, no.11;8-10 N 162. j, (KRA 16 112) YANIN,. L.V. (Moskva) Basic trends in the activity of nd r sanitation inspection. G16- truda I'pror.,zab- 4 no, 7:3-7uJ-51t 1, 11 Minister (MIRA 13:8) stvo 2dravookh-raneniya SSSR. (FACTORY SANITATION) ~"q KOVARSK!Yy A.G.j MEDOKSj T.S.; Prinimali uchastiye: GLEBOVA, L.F.; 34MOV, S.M.; YAN10) L.V.; VIDANOV., V.H.j prof., red.1 IWISTOV0 L.N., ra.-;-M ' _hh11' M.T., tekbn. red. [Collection of official materials relating to laborator..y work] Sbornik ofitsialinykh materialov po laboratornomu del., No- ekva, Medgiz, Book 1. (Manual for laboratory doctors., sanita- tion doctors, and epidemiologists] V pomoshch' vracham- laborantam, sanitarnym vracham i vracham-cpidemiologam. 1961. 462 P. (MIRA 15:2) (1,12DICAL LABORATORIES) (BIOLOGICAL Lj1BORATNUES) (CHWICAL LABORATORIES) YANIN, L.V... red.; RMIANOVAt Z.A., tekhn. red. [The most important official documents on industrial Irigieno and sanitation]Sbornik vazhneishikh ofitsiallnfth raterialov po voprosam gigieny truda i proizvodstvemoi sanitarii. Yo- skva, Medgiz. No,2, 1962. 219 (MRA 15:12) (INDUMIAL hYGIFITE~* KLIMOVAI T.Kh.; LORMSKIY, D.E.; YAIIKOVSKAYA, YEGOROVi Yu.L., red.; MIRONGVA, A.M., tekhn, red. (Co3lection of the most important official data on problems of industrial Irygiene and industrial sanitation]Sbornik vazhnei- shikh ofitsiallxWkh materialov po voprosan. gigierg truda i pro- izvodstvennoi sanitarii. Fioskva,, Medgiz. Vo.l. 1962. 314 p. (MIRA 15:10) (INDU,-,IRIAL BYGIEIM--LAW AND LEGI SLAT ION) TAHINj N.G.;.BCHETCHIKOV. I.I.; BILISKIT, V.I., otv.red.; PEVZNSR, A.S" zav'~iad.izd-va; GILRUSON, P.O., tokhn.red, (Uniform time and pay standards for construction, assembly. and repair operations in 19601 Edinye normy i rastsenki na stroi- tellnys, montazhnye i remontuo-stroitollnye raboty, 1960 g. Moskva, Goo.izd-vo lit-ry po stroit., arkh1t. i stroit.materia- lam. Sbornik 13. [Installing industrial furnaces and flues) Xladka promyahlennykh pechei i trub. 196o. 96 p. (MIRA 13:6) 1. Russia (1923- U.S.S.R.) Gosudarstvannyy komitet po delam stroitel'stva. Ze Normativno-iseledovateltakaya 9tantsiya No.5 (NIS-5) Ministerstva stroitellstva RSFSR (for Tanin, Schatchikov). (wages) (Furnaces) (Flues) VIA S/1 93.16 1/0' 0/0 11/002/007 A0047A101 AUTHOR: Yanin, V. Ye. TITLE: Pressure working of metals at the enterprises of the Moscow City Sovnarkhoz PERIODICAL: Byulleten' takhniko-ekonomicheekey informatsii, no. 11, 1961, 20-24 TEXT: The author reports on the achievements of the Moscow City Sovnarkhoz plants in the field of forging, pressing, die forging and drop forging and points out that, in comparison with 1948, the stock of forging andpressing machinery in the Soviet Union had increased by 1958 nearly by a factor of 3. The development plan for the national economy provides for an Increase in the production of forg- ing and pressing machinery of 25% compared to 14% In 1958. The considerable increase in the production of forging and pressing equipment can be mainly explained by the necessity of producing precision forgings approaching the dimensions of the finished components. To increase the forging precision and cut the labor consumption some 20 orank-type drop-forging presses with a capacity of up to 6,300 tons have been installed in the Moscow plants. By 1960 the volume of precision forgings at the Moscow City Sovnarkhoz plants amounted to 34,000 tDns Card 1/4 B/193/61/000/011/002/007 Pressure working of metals at the enterprises ... A004/A101 or 13% of the total of drop-forgings. For 1961 the rated output figure of precision forgings is 35,000 tons, while it is planned to bring that figure up to 80,000 tons by 1965. The introduction of advanced technologies considerably improved the teohnological and economic indices of forging shop operations. In 1960 the metal consumption per ton of forging amounted to 1,170 kg, compared with 1,178 kg in 1958, while rejects could be reduced to 0.3%. The author points out, however, that still up to 30%of metal losses occur particularly In hand forging, while the losses are still greater when machine pE--ts are manufac- tured directly from rolled material on machine tools, where the coefficient of metal utilization amounts to 0.3 - 0.5 only. Technological processes are being developed at the Moscow City Sovnarkhoz plants which will increase the output of serviceable metal in forging and pressing shops to 90%, while the metal loss In chips in mechanical shops In the manufacture of parts of Intricate configura- tion will be cut by 15%. The practico of the "Krassnyy proletariy" Plant and the Moskovskiy zavod pozharnykh mashin (Moscow Fire Engine Plant) shows that in small-batch production the cost on die-making is paid off after 3,000 to 4,000 parts. The forging shops of the "Dinamo", "Krassnyy proletariy", Vladimir Il'ich and other plants have converted some 2,000 tons of hand forgings to die forging, which reduces the labor consumption by 35-40 norm-hours per ton of die Card 2/4 S11931611000101110021007 Pressure working of metals at the enterprises ... A004/A161 forgings, and saves some 80 rubles per ton. The author mentions the extensive use of multipurpose-setting dies for small-batch and big-lot production for which only inserts for the shaping grooves need to be chanaed to forge parts of dif ferent conf 1guration. The author points out that at present already some ~,000 tons of forgings are produced by the impact extrusion method, which saves up to 15 - 40% of metal, cuts labor consumption by 15 - 40% and yields forgings attaining the 2nd class of precision without subsequent machining. The Avto- zavod Im. Likhacheva (Automovil Plant im. Likhachev) (ZIL) in cooperation with NIITavtoprom introduced the method of hot gear generation for the ZIL-157 truck. The machine tool for the manufacture of these gears has been described in the Rjulleten' tekhn1ko-ekonomicbeskoy informatsli 1961, no. 8, 33. The author emphasizes that the use of induction heating I~ precision die forging has increased the labor productivity, facilitated the working conditions and,created the necessary prerequisites for the overall automation of die-forging equipment. A deterrent of the increase in efficiency of pressing and forSing equipment Is the Insufficient service life of dies made from the steel grades 5XHT Mhmr), 5XHB OKIW), 5xrc (5KhGS) and others which, on the average does not exceed 4,000 to 5,000 forgings. The author reports on a new non-nickel die steel which has been tested at one of thc- Moscow City Sovnarkhoz Plants and has been Card 3/4 S/193/61/000,/011/002,/007 Pressure working of metals at the enterprises ... AOO4/AIOl developed by TeNlIchermet. The service life of this new steel is 4 to 6 times higher than that of 5KhNV steel. The Stankostroitelinyy zavod im. Ordzhonikidze (Machine Tool Plant im. Ordzhonikidze) has erected a new meohanized.line for the production of forgings for shafts and spindles of metal-cutting machines. This line conslats of press-shears, merry-go-round-type gas furnace, vertical radial forging machine with hydraulic station, annealing furnace, conveyers and other means of mechanization. There is 1 Soviet-bloc. rsference. card 4/4 YAMM V Ye inzli.~ OKHRIMKO, Ye-.R., doktor tekhn. nauk, prof. i --ellhod for the deformat-lon of biwtals. '4-w im Ve3t. mashlnostr 45 no.7:67-71, Jl 165. (MIPA 18:10; YANIN? V.Ye. Survey of the state of technological processes in enterprisca of the Moscow City Economic Council. Biul.tekh.-ekon.informz.- gos.nauch.-issl.inst.nauchJ tekh.inform. no.3:72-75 162. 041RA 15-0) (Moscow-Industrial management) nr YANINY VIYO. Review of the levels of technological processes in enterprises of Moscow City Economic Council. Biul.tekh.-ekon.inform.Gos.nauch.- issl,inst.nauch. i tekh.infom. no.6:84-86 162. (MIRA 15M (Moscow-Industry) YANINO V.ya. PrOBOwOrking of metals In the ent8rPriden of the Moscow Economic Council, Blulotekh,,-ekonolnfom*Goo.nauch -1801, Instonauch.i tekh.inform. no.2:80-81 163. RRA 16-:2) (Hoscow-Forging) Si7dV'Ri *Tm~ a E -5 M K . . . . . . . . . . . . . 4 IT--4 Fi 0 F-a - 4., ralliDIfi"(110 rd 1-414 At-ii, -it h, S v L_71 V _~d u, b r a_1 4~; uo:;WL1pr,; i'Moscow non-ierrvus metal )ro, ess-ing ti e b i 1Fe_6T._AWi _ngo4F -of t4fi.- I - "'t P - , , _____ptant) devised a now method cf preparing the, 0 ". 7 x 600 mm, is cleaned with emery paper -n 6(-' rnzria side,_dia-reasedtfn a lii'17k, s~xla -)iuLion. F,_ ~vashed, coated wfflu borax fl "i, heated .4D 30- 11160C, vertic I - __ n - aJJV in-Sert&H 1 1 apnvj~'! cast-iron mold, and molt, 're" intu, the free space of [lie moid ad ~icen; i UP the c 1 ear, ed s ide of the s tingo t ~, -o obtained is (Lffus tes t., Lie jointF ional..' TenB i I off strips cut across such a iho. invariably result in a rtmt ure through- 6" copp-r pa never all the ~:olrit. I'lle hillvt ii n ~,I, 'I'l-o- I'' U"., 11nal Ql,*,,s usf,~ 1) Cocci 1,2 -APT -300 after'to ing. - The first reduction should not exceed m' but the last cam re A formula describLng warping of bimetal stripq duririg rollina is derivrwf t.SSOCIATION: none 5, 0011 11 (Olltll ( 64 -'."t6w'-.Ja(hVz z/ -k-64372-6a, IR q -'ICCESSIOI?-.NR.- AP5018670 M/0122A5/000/OM /0067/0017~,'~-Wtvl 621-/j9.4.002.2 yx AUTHORS yanitv~ yd. z nko Ya. -of- ted-n ical :L.~ so (*inoer khti v M' OL-sm-n~- a -ax Ift- ~1;1 q/ 5 1'7' _0 dormaiion of. bIMSIgials~-" TITM..~: Nowiaod t d ~Neqtzak rashinostro7wilya no 7 5 677-7-17 v TAGS baili6' qu!lp ~q_jn yar-bime-tal.- bv -L90__br-asi---ra- I L brass, GDIJ alloy. AB8TWICT.: 0 6-,"Plas t. ic 'deformtiont of b tallic soa6imops,with tIhe d formitio Ia_ ~'_forces-~ 4#vcted _-,paraIL&I ~.to -the _~2nded t~i 4- b4tudett:_ttn rug-_ _na w-In or the moth-a 'ea -0 -prepared aue-d:rrg,~9 d r;Wgreated by V, It 1. AnT)i1.8IicF;4'(Spoaob iz-gotovIeniya __janiM" bimotallielieskikh polos liatov 'J~ ugolkov i tomi podobnykh i-.doliy. Avtvrskoye ovidotelletvo SSSSR' 110._IJ+7A) 1960) from four bimetallic combination.- (Invar.1.1, 1136-brass -ill-ly 7:1 5 irn a I-Ciard ti'm :-" 0.5-0.9 for uf~e L_643-72jo~65_' ACCESSION Va.,. AP5018616':, aiteon 6' imens, a ch bimoW:wrq WO'bimetas# poo defomd 20~-40,1 -and see-- ons- uere- stWdied Vtdudlli 9W. t 16- ~=/S a tidrdjig and etching) and by r-radiation from isotopes. It was found that the bulaing of the welded surface depended on the coefficient n ptat/Pa~, Wiers I Pft .2 ~4_(' t 77' itAll P '4_ t -of contact -.the -'b a~ um-s--in- the A -7 n _f' the direction of the hard motal.i 1.0, a re 0 a it t van n Tt was found that the Umotallic bonds remninad intact in all apocirnong ( u. gwo delfarmat' TO bqf, -hqt C"', C k s'.-,T-t7ia 2. ff Tt' Tm /A' allould 2; fc,r 2.5 it should hc~ < A. ~R- y~ R ACCZSSION NA: AP5018,PfO Orig. art. 'las: 4 fiCures, 4 tables, aA forming. Vw ii ., oz, YANIN, V.Ye. Effect of the shape of bimetal test pieces during upsetting on their state of stress. TSvet. met. 38 no-5:79-V. My 165. (MIRA 18t6) P'. USSR/ChOM1907 - PhnTMcQUtIOalV 21 JUn 32 'Medicine - Tuberculocia. Chow-tbara-py Olsonlootinoyl Hydramones and Their AntItubercultir Activity," M.N. Shemkim. 0. if. Pershin, 0. 0. Un "-yova. Yo. D. Sezonovs. Te. 13. Hikitskayn, As D. Yanina, A. 1. Yakovleva, All-Unton Set Pat Chem-P&nr Inst I~Mal S. Ordzhonikidze 7 Olbk Alc ftuk- SSSR! Vol LMIV, 210 5, PP 981 - 984 Isonicotinoyl hydrazide has an antItubercular Potlon, but Ito thempeutic Index Is low, A sories of substituted IsontootInoyl hydrazIde derive were,prapd and their bactarlostatic action on tuberculosis bacilli in vitro tested. It was shown that substituted toonicotlnoyl hydra2ones have a higher antituberculnx activity tham Para-2kninonalicylic aeld and streptorqcin and are better tolerated'; by exptl milmls than tho bydr!~%Ide of Iron1cotinic r-cid. Thle mdo It possibl-a t4i Oeleat froo theta cubst,nneen for clinical stue-y on tubercular humns. A oubtatr~nce. called "2-ht1vUcids* by the authors. vas foramrded for clinical study, which is Prorrassind, successfully. Presented by Aaad A~.' N. Nesmeyanov 9 Apr r2. 223T17 p. r"I 11) f pf v1 it Iff'o; IT ""d ""i, -Ir -T- ,tvp .4t F T. tit 44 1cl IMIN lam --- law v r USSR/Chemistry - Drugs Sep 53 IlAminoalkyl Derivatives of quinuclidine," M. V. Rubtsov, Ye. S. Nikitskays., Ye. Ye. Milchlina, A. D. Yanina, and V. Ya. 1"urshtatova, All-Union S(~I-Reqevrch Chomico-Phermaceut Inst im Ord- zhonikidze Zhur Obshch Xhim, Vol 23, No 9, RP 1555-1559 A number of substituted 2-aminomethyl quinuclidines and 2-aminomet-hyl-3-( -aminoethyl)-quin- uclidinec were synthesized. U g "A N -Muf frcm VT. WA. V- I-- --f-W E YA 7. C. --l C4- A~4 UM/Chemistry - Synthesis 1/1 Pub@ 151'- -X/1,2 'Rub sav Nikitskaya E. and Yanina,, A. D. Synthesis of gamma-formylpyridine and isonicotinic acid PorlOldicdl I Zhur.-ob. khim, 24/9, 1648-1651,, SOP 1954 "Abotract I 'The conditions favorable for the synthesis of gamma-fornWlpyridine by' selectie- oxidation of. gamma-picoline, with selenium dioxide in the presence of beta-picbline,.areIescribed. Two variants for the deriva- tion of isonicotinic acid, with a.yield of 75-80% of the initial ga=a- picoline, were developed, The effect of selenium dioxide, on the se- lective oxidation of gam-na-picoline, is explained. Five references: 2-U3511; 1-S~riss; 2-German and USA (1934-1953). Institution The S- Ordzhonikid e All-Union Scientific Research Chemical Pharl;;ceutical Instzitute Submitted April 14j. 1954 ~M- AUTHORS: Yanina, A. D., Rubtsov, Lt. V. SOV/79-29-2-27/71 TITLE: The Hofmann Cleavage of I-Azabicyclo-(3,2,1)-Octane (Gafman- ovskoye rasshchopleniye 1-azabitsiklo-(3,2,1)oktana) PERIODICAL: Zhurnal obshchey khimii, 1959, Vol 29, Nr 2, PP 485-493 (USSR) ABSTRACT: In the 11ofnann cleavage (Refs 112) the unsymmetric bicyclic systems react with a common nitrogen, under formation of not one monocyclic heterocycle but 3 heterocycles which have an unsaturated side chain or under the formation of their trans- formation products, in dependence on the question, from which P-carbon atom the hydrogen will separate to form the water molecule. The direction of cleavage apparently depends both on the stability of the bicycles and on experimental conditions. This was proven by the experimental cleavage in the case of 1-azabicyolo-(3,2,i)-octano (III). The initial product in this connection was 1-carbethoxy methyl-3-carbethoxy piperidine M (Scheme 1). The intramolecular condensation of (I) into (II) proceeded in the presence of potassium alcoholate [not with metallic potassium (Ref 3)], which increased the yield from 30 to 71 1171o. By reduction of the ketone (II) octane (III) was Card 1/2 obtained, which was transformed by methyl iodide into the The Hofmann Cleavage of 1-Azabicyc1o-(3,2,1)-0ctane SOV/79-29-2-27/71 quater nary salt (IV) and further with silver oxide into the corresponding base (V). It was found that oncleaving 1-aza-- bicyclo-(322,1)-octane under various conditions (at normal pressure, in vacuum, in.40 01~6 potash lye, and at increased pressure) three products are formed; 1-methyl-3-allyl py=11dine, 1-methYl-3-(P-oxyothyl)-piperidine, and di-[P-(l-methyl piperidyl-3)1-cthyl ether. 1-methyl-3-allyl pyrmliline was separated in all cases and is the chief product of the cleavage of 1-azabicyclo-(3,2,1)-octane in alkali medi- um, in vacuum, and at normal pressure. On its heating in water under pressure; 1-methyl-3-(P-oxyethyl)-piperidine is the chief products There are 0 references, I of which i3 Soviet. ASSOCIATION: Vsesoyuznyy nauchno-issledovatellskiy khimiko-farmatsevti- ,:heskiy institut imeni S. Ordzhonikidze (All-Union Scientific Chemico-pharmaceutical Research Institute imeni S. Ordzhonikid--e) SUB14ITTED: January 3, 1958 Card 2/2 ~70 ME a 7 ~__' HUBTSOV,, M.V.; IIIKITSKAYA,, ye.s.,. YANDa, t,.D.; USOVSKAYA, V.S. New ganglion blocking preparations. Khim. i med. no.15:16-28 160, (I-MA 15: 1) 1. Vsesoyaznyf nauchno-issledovatellskiy khimiko-farmatsev-tichoskiy institut imeni, S. Ordzhonikidze. (AUTONORIC DiWGS 5.3616 77883 SOV/79-30-2-34/78 AUTHORS: Yanina, A. D., Rubtsov, M. V. ----------- TITLE: Hoffmann Degradation of I-Azabicyclo-(3,2,1)-Octanes. III Cleavage of 7-Methyl-l-Azabicyclo-(3,2,1)-Octane PERIODICAL: Zhurnal obshchey khtmii, 1960, Vol 30, Mr 2, pp 526-533 (USSR) ABSTRAM Quaternary base of 1-azabicyclo-(3,3,1)-nonane (VII), on thermal decomposiltion, forms 1-methyl-3-allyl- piperidine (VIII). The latter wan uned for the preparation of the methiodide of 'I-methyl-l-azabicy- clo-(3,2,1)-octane (X). N-C11,C11,C00(%11:j Card 1/9 (Figure continued on Card 2/9) (Cont'd from Cat-d V9) 777893 SOV/79-30-2-34/-(8 cooell, c0 11,0 N C112CI12('OOC211,1 N -cI12GII=CII 2 ( N:f~ N- \N1 M (VO (Vill) Ag N~ Ili N CII, N C I I'l u, Oil (I X) (X 1) C ard 2/9 ,radation of 1-A~,-ihlcyclo- i1of fmann Dej, 77883 -(3,2,1)-Octanes. II. of' SOV/-[,)_30-2_34/78 '(-Methyl-l-Az,ibtcyclo-(.-,$,~l,, )-O(A~lllc Synthe:As of X 13 ba.3ed on the addition of III to Viii (af,-cordIng to Mackovirilkow) vilth formation or 1-methyl-54 P -`o(1ow'01)y1)-r)1Pcr1(J11lc (IX), and cyc-IL:~atlon Lo compounil X. X ~ja.,,, ,iyntheolzed for the I'Ltial M;mwtuve proof according to the 6chelne below: C112CO011 N 1111 N CM. -CAI Vll~j Ml N 111tr c1l, a r, d /9 f,u ve c on td on Card 11/9) t!of.f.tj~,jtjn Degradation of I-Aza~)Icyclo- -(3,2, 1 )-Octanes. II. Cleava~-,e of' N (All 7,1-883 c 11, CIII:,i Theoretically, four possLble compoundq can be formed by 11offmarm degradation OC XI. 11, CA I -C. I I -C I Ij ,N/ CI 13 1"11, c11, Card 4/9 (Figure cont'd on Card 5/9) 10 ff r*," u 1) Dej rl fli t, 10 n 0 [,:.-1 0- 7 7 IAl W tt! ,]it llw-~l 1 11,11, of I I I thy L - 1 1 :11 1 - I tic Cclt,~!Iflzl 1,1,,, or XT I'd Th4~, o S t'... a 0 b t a o n L t h anhyd rous IV I + oh o 1 17 KOH 4- V + 11 G 2 v T.I. 'i, 0 j VIII + fli .(Table cont'd) 77883 30V/19 -30-2 -311/78 Thc, ObLAr)~-(j C omp ou rifto and Their, Pr,operti,~.; U1, Starting 0 i) t" a 1, rl e d Y 1.11 20 1) p /Mm 1) r, ic D 6 IX + lf;~O + cthcr v ~W)%, Mp )POO((Ic":!) solutton of' 1("co ~ 1. VIII + IL'o Y I '15110 4, M11O)t -me I'lly 1. 1) p c 1, 8 ethyl -1. -rile thy IpI pe. I- X'I 1 90 o Mp 188-111,110 + IICI X)'I 1, allhydvotlo MIX0014a + acetic YJIT 0 it 6 -32 e c 0 n t , d 77883 SOVIf 9 -,',0 -2 - 34 /~-tB The Obtained Cornpoun d's, and Their, Pz,operties Starting l"lateri- I Obtained Yteld P r r) ror4 wc t D 4 '0! 1 X I L r, Four '-.1ttempt"; wer-0 mode at; a. Itot'I'mann of '-'oflinounal ~XI: (I-) it 0 + AgOll undev not'nial f, fli"MIl~,"I'lOrl under, Vacuum; (3) hen.tlut-, In the pr-'--c~nce llp-'Atlllj~ 'm "'ho of' "",,'~tev' onfl~~"" III all Only VITI 01',Utitwd In D 1. . 'I -,'10 IF) i o ve -ve w! th lip n r, ('~ 1, z' en c o: IJ , S 'Phe I j . .5 . v e 1, e I,n 1, r ~rl "i" ti- I i , t J Am . C1,01ri vp Cnr-l l.". h. ot'ho I Hof.fmann Degradation of :~-Azablcyclo- 77883 -(3,2- l)-Octanes. II. Claavage C)f sov/1',,q-3o-2-34/j8 7-Methyl-l-Azabicyclo-(3,2,1)-Octarle ibid, 71, 3098 1949 ; A. Bugger, C. R'. Waltev, ibid, 72, 1988 H950~- ASSOCIATION:, Ovdzhonikidze All State Scientific-Reseat-ch Chemical- PhIarmaceutical Institute (Vsesoyuznyy nauchno-Issledo- vatellskiy khimiko-farmaL~.cvticheskly Institut imeni S. OrdzInonikidze) SUBMITTED: February 21, 1959 Card 9/9 7~ R TANINA, A.D.; RUBTSOV, M.Y. Hofmann cleavage of 1-azabioyclo 0.3.13octanes. Part 3: Hofm-ann cleavage of a quaternary base of 2-methyl-l-azabicyclo[3.2.lloctane- Zhur.ob.khim. 30 -no.8:2544-255OAg 16o. (MIRA 13:8) 1. Voesoyuznyy naachno-iseledovatellskiy khimiko-farmatsevtichoskiy iustitut imeni S.Ordzhonikidze. (Azabicycloootane) YARBA.9 A.D.; RUBTSOVs 14.V0 Hofmann degra&lUn of I-azabicyclo'(3i2.,I) octanes. Part 4: Hofmann degradation of 4-methyl-l-azabicyclo' (3,,2..l) octane. Zhur.ob.khim. 32-no.6:1789-1798 -Te 1621. (MIRA 15:6) 1. Vsesoyuznyy nauchno-ist3ledovatellokiy khimiko-farmatsevticheakiy institut im. S.Ordzhonikidiep (Bicyclooctane-) (Hofmann reaction) YANINA A D . RUBTSOV, M.V. Hofmann degradation of I-azabicyclo(3,2,1)4ctams. Part 5: Hoftann degradation of 6-mothyl-l-azabicyclo(3,2,1) octane. Zhur.ob.khim. 32 no*10;3151-3158 0 162. (MIRA 15:3-1) 1. Vsesoyuznyy nauchno-isaledovatellskiy khimiko- farmatsev-ticheskiy institut imeni S. Ordzhonikidze. (Azabicyclooetane) (Degradation) J. YAVINA,, A.D.; RUBTSOV,, M.V. Hofmann degradation of I-azabioyclo(3a)j)*cttM#-,. Part 6: Hofmann degration of a quaternary ammoni= bass of~8-mothyl-l-azabicyclo(3..2,1)octane. Zhur.ob.khim. 32 no.il:3693-3698 N 1629 (MIRA 15:U) 1. Voesoyuznyy nauchno-issladovateltakiy khimiko- farmatsevticheskiy institut imeni S. Ordzhonikidze. (Azabicyclooctane) (Hofmann degradation) _A~,_Dq ~"TSOV, M. V. Hofha= dagradation of I-aublayo~o(3,2#1)octanes, Part 71 Hoftann. degradation of 3-mtb3rl-l-azabicyclo(3#2.1)octans. Zhtw. ob. khim, 32 no.12.*3941-3945 D 162. (MIRA 16t1) 1. Vsesoyuznyy nauchno-iseledovatellski)r khimiko-farmatsev- ticbeskiy institut imeni.S. Ordzhonikidze. (Azabicyclooetane) (Hofmann reaotion) ACC NRs AP6031301 BOURCE:-C-Odt~--ifR/6j66-/66/do2/009/1'707/171 I AUVORt Yaninap A. D,; Mikhlinap Ye, Ye.; R*tsovp He V. 0-W; All-Union Scientific Research Chomical-Pharmacoutical Institute imoni S. Orzho- nikidzo (Vsesoyuznyy nauchno-issledovatellskiy khimika-farmatcov-tichookiy inatitut) TIMS Pinacolone rearrangement in the series of I-azabicycloalkancls. Part 2 SOURCES Zhurnal organicheskW khimiip ve 29 no. 99 1966, 1707-1711 TOPIC TAGSs pinacolono rearrangemont, pinacol IGr0Yx%)'%c V,,-,Aexcc.~jck~c VNse ABSTR4CTS The roaction of 3-hydroxy-3-oarbothoxyquinualidino (1) with butyl and p-tolyllithium was used to synthasizo 3-hydroxy-3-fa,crt-di(p-talyl)-ct-hydrovmothyl]- quinuclidino (11) and 3-hydroxy-3-(a,c~-clibutyl-a-hydrox;ymotlwl)quinualidine (111)S' OH OH C=1146 C/R oil The following roactions were also carried'outi Q-, ACCW~ F--Ai~6631301 0 OR CS"t-c"I n.5C.H.C., HOD% VA."Ll Z" NS C t46r,4% CIIH Cjf3 (Vito R AN t CH ,IH,,Dfl RMC0011. 0 a a , N 0 N OR M Ckliq C Cli - C3H, H, Cli Col a H Pt fC 4HP W W IC%Hq C N OH C OCOCH3 jilt) W [al I ("' + (XI ci.~) OCOCHS N C4H# The pinacolone rearrangement of compound (II) in 50% H2SQ~ leads to the fomation of a mixture of two ketonost 3s3-di(p-tolyl)-4-keto-l-azabicy--lo[3.2.2.lnonano (IV) and .3-(p-:tolyl)-3-(p-mothylbenzoyl)quinuolidine (V); on heating pinacol, (II) with zinc chloride in acetic anhyc!addep only ketone (Y) is formod. Under the same conditions$, in the case of pinacol (M)o whose alkyl radical is longer than that of (11)9 only Card 2/3 7 !, 4cc N'R: AP6031301 - '- I t i procccsoG of dehydration and convor3ion of the unsaturated co=pounds formed are 61b- I zorvod. It is concluded that tho introduction of a mothyl radical into the ph6rql i 1 icing of 3-hydroxy-3-(a,a-diphonyl-cL-hydroxymothyl)qu:lnualicuno facMtates tho course I YANINk, S.P.; HITSLI, V.I. OP-10 foaming agent for synthetic glues. Dereprome 9 no*2: 20-21 1 16o (MIA 13t6) (Glue5 (Jfoam) a I a i h- DVOSKIH, Baniamin Takoylevich; SAVICH, M.P., Zp"'magn ktor; W-= = , V., takhnichaskiy redektor ' - [Talks aboat Kazakhstan] Besedy o lizakhatane. Alm-Atm. razakhokoe gomoizd-vo, 1957- 154 p. (HLRA 10:9) (Uzakhoton) 14-57-7-15386 Translation from: Referativny zhurnal, Geografiya, 1957, fir 7, (USSR~ AUTHOR: TITLE: PERIODICAL: ABSTRACT: Card 1/1 p 184 Yanios, N. Specialized Agriculture of Southern Kazakh SSR (0 spetsializatsii sellskogo khozyaystva Yuzhnogo Kazakhstana) S. kh. Kazakhstana, 1957, Nr 1, pp 16-20 The author discusses logical distribution of various branches of agriculture and more efficient local specialized methods for agriculture and animal husban- dry in the southern oblasts of Kazakh SSR. These are th*c Y1=o,-Yazakhstmdcaya Alma-Ata, Dzhambul , Taldy- Kurgan, and htyi-Orda 6blast, containing approximately 85 percent of the total land under irrigation. -.TAN IOS#.,1X1tDW, Iva vioh, kazd. ekon, nauk; WRIMO Te,AO, redo; TROPIKOV, A., .110 red, (Resources for increasing labor pi,oductivity in nonferrous Metal- lurgy (based on the emurple of Xazakhetan enterprises)) Rezerv7 rdsta proisvoditellnosti truda v tffvetnol metalluigii (X~ primers predpriiatli lazakhotam). Koskya, Izdvo "Znanie," 1958. 45 p. (Vseso1nznoe obshchesiv6 po"raep'rostranentiu, politicheakikh i uauohnykh znaull. Sor.36 no.14)0 (KIU 1118) (Nonferrous metal industries) SOMOVA, S.Ys., AYAV, Oaziz Khismatovich; YANIOS, Ilik la XyglaqZ12h: NA red.; HAICAROV, I.I., red.izd-va; UUbl-N, H.I-, tdkhd.red. [Economic and cultural developnent of the Xszakh S.S.R.] Pastsvet akonomiki i kulltur7 Kazakhokot SSR. m:)skva, Izd-vo "Znania,* 1958. 46 p. (Vsesoyuznoe obsbchestvo po rasprostranentiu pollti- clieskikb i nauchnvkh znanii. Ser.1, no.40) (HMA 11:2) (Kazakhatan-41conomic conditions) ;,jw yAj,jjS. 11. DILIC, A. K. V. I., na PO 1, "Investigation of the Action of modif~inG agents in flotation by means of radioactive tracers," a paper stfomitted at thie International Conference on Radioisotopes In Scientific P~esevrch, Paris, 13-20 SeP 57, SOV/1 37-58-10-20395 Translation from: Referativnyy zhurnal, Met;xllurgiya, 1958, Nr 10, P6(USSR) AUTHOR: Bogdanov, 0. S., Podnek, A. K. , Khaynman, V. YanisN_1A.. TITLE: Studies by the Mekhanobr Institute in the Field of Flotation Theory (Raboty instituta Mekhanobr v oblasti teorii flotatsii) PERIODICAL: Obogashcheniye rud, 1957,,,Nr 5, pp Z5-28 ABSTRACT: A brief examination is made of the major sttidies conducted at the Mekhanobr Institute in the field of study of the physical and mechanical foundations of flotation and the reaction between flotation reagents and minerals. 1. ores--Flotation 2. Flotation--Theory 4. Minerals--Chemical reactions Card 1/1 M. M. 3. Reagents..-Chemical reactions YAIIJIS; N. 0 (Meldianobr) "The investigation of various flotation modifiers for non-sulphide minerals with the aid of radioactive isotopes" repr PrOWOW at the 4ft SaIgmt1fle and TeabUIC&I Smajou of t1is lbld*D*r IWtP LealnSMAR 15-1.8 JTW4 1958 MIKHAYLOVA, M.S.; KHAYNMAN, V.Ya.; YANIS, N.A. .Z~~ Use of liquid scintillation counters to determine the sorption of flotation reagents. O'bog. rud 5 no.5-.28-41 160. (KM 34:8) (Flotation--,Equipment and supplins) S/137/62/000/005/022/150 A0061AI01 AUTHORS. Bogdanov, 0. S., Haing Wei-chung, _Yanis, tt,_A,_ TITLE: Studying the effect of sodium oleate and flotation modifiers under conditions of flotating beryl, spodumene and fluorspar PERIODICAL: Referativnyy zhurnal, Metallurgiya, no. 5, 1962, 7, abstract 5G42 ("Tr. Vses. n.-i. I proyektn. in-ta mekhan. obrabotki poleznykh iskopayemykh", 1961, no. 128, 26-36) TEXT: Results are given from investigating the interaction of beryl, spo- dumene and fluorspar surfaces with oleic acid (I) containing radioactive Isotope C111, ferric chloride with pe59 isotope, and H?.S04 with s35 isotope. The quantity of a reagent sorbed by minerals, was determined on flotation products by direct measurement of the radiation Intensity of the mineral powder. To measure the intensity of preparations 1, the method of scintillation reading was employed with the aid of liquid scintillators. Flotation experiments were carried out with a laboratory mechanical-type machine of 160 ml volume, at 1:8 aalid-liquld ratio.; The studies were appli6d to the existing acid and alkaline schemes of separating beryl. spodumene and fluorspar. Prior to flotation, the mineral batch was mixed Card lp S/137/62/000/005/022/150 Studying the effect of sodium oleate A006/AlOl in a cup with a solution of required flotation reagentn at a given liquid-solid ratio. To study the naturecf I and sodium oleate (II) fixhtion on beryl and spodamene, the method of infrared spectroscopy was used. The joint proceasing of the minerals with reagents was performed in a special adsorption column. As a result of investigating sorption of I and II; the effect of p1l; processing with IIF and H2SO4, and with a mixture of these acids; process-Lig with NaOI1, on flotation of beryl, spodumene and fluorspar, and sorption of oleate by their surfaces, the conclusion is drawn that during the interaction of II with beryl, spodumene and fluorspar, both physical sorption of I molecules and chemical sorption of oleatei ions take place. Highest sorption capacity is shown by spodumene, which corresponds to its better flotability. Optimum beryl flotation and sorption of beryl oleate occurs in the neutral range; and those of spodumene in the weakly alkaline range. The activating effect of HP upon beryl and of NaOH upon beryl and spodumene, is predetermined b~ more favorable conditions developed on the mineral surface for the chemosorptional. fixation of the ion collector; this is connected with the selective dissolving in HF of silicate groups. Beryl depression, non-activated and preliu&mu* activated with HP, after processing with H2SOIJ is explAind by reduced sorption of the collector and its fixation prevalently in molecular form. L. Glazunov [Abstracter's note: Complete translation] Card 2/2 . ..... RAR S/08'/12/000/001/027/067 B151/001 AUTHORS: YLikhaylova, N. S., Khaynman, V. Ya., Yanis, N. A. TITLEt Application of liquid scintillation counters for the investigation of the interaction between flotation reagents and minerals PERIODICALs Referativnyy zhurnal. Khimiya, no. 1, 1962, 302-303, abstract 11155 (Tr. Vses. m-i.i proyektn. in-ta mekhan. obrabotki poloznykh iskopayemykh, no. 128, 1961, 37-44) TEXT: A description is given of methods, measuring equipments and results from the application of scintillating soluti)ns and gels. These methods make it possible to increase by 200 - 250 times the.sensitivity of the measurement of isotopes with soft ~"-radiation, on the surface of mineral powders and in dilute aqueous solutions. This method opens up now possibilities for investigation and also makes working with such radiators safer and cheaper.'(Abstracter's notei Complete translation.j Card 1/1 BOGDANOV, O'.S.; SIN VEY_CHZ11UN [Hsing Wei-cbung]; YANIS, N.A* Studying the action of sodium oleate and flotation modifierz during the flotation of beryl, spodumene, and feldspar. Trudy Mekhanobr no.128:26-36 161. WRA 15:1) (Flotation--Equipment and supplies) (Beryl) (Spodumene) RAZUMOV, K.A.; SIN VB'Y.-CHZHUM [Heing Wei-chungl;_YANIS, N..&. Effect of~calcl= Aid iron cations on the flotatiol'i of beryl and blotite with a cation collectors Obeg, rud 1 h0,3:3-5 162. (MMA 164) (Flotation) (Catifts) A, -J, YANISHICYSE-AYA, I. Polish vown, builders of a better future. Yesm.prof.drith. no.8:37-39 Ag '57. (KLRL 10:8) l.Sakrotarl TSentrallnogo soveta profsoynsoT Pol'shi. (Poland-women) YANISBEVSKAYA, I.A. I Alkali and nephel-ine syenite, in the Hatyr section.. Mat.po- geol.Zap.Sib. no.64:160-173 163. (HM 17:4) I t , i., z I ~ I i A-.- I ISILW5KAYA, M. F. YAN7SHF,VSKAYAj M. K. - "Microflora In Pneimonla 6f Children." Tashkent State Medical Inst Imeni V. M. Molotov. Tashkent, 1956 (Dissertations for the Degree of Candidate In Medical ~;ciences) SO: Knizhnaya Iotopis', No 9, 1956 S/0 16/60/000/06/i4/0r~:l AMOM Samsonov, P.P. and Y&nlshevzkaya, M.N. TITIE-. New Varieties of Shigella Djzenteriae In T-AshRent PERIODICAL3 Zhurnal mikrobiologii, epidemlologli I immunobiologli, 1960, No. 6, pp,- 52 - 57 TEXr: Fifteen.mannitol-negative strains were isolated from dysentery patients aDd carriers in Tashkent. Although similar to Shigelia dysenteriae by their biochemical, cultural and morphological characteristics and their ,V/ ability to provoke specific kerato-conjunctivitleb in guinea pigs, they did not agglutinate with any of the specifle dysentery antisera and were therefore classed as atypical Shigella dysenteriae. They appeared rel ated to Shigella ambigua. Ihe strains had a distinat antigenic structure and constituted an independent serological group with sub-groups. Further research is needed for precise classification of the strains and to determine their pathological role. There are 2-tables and 12 references, 10 of which are Soviet, 1 H-.mgarian and 1 English. Card 112 ,9/016/60/000/06/14/051 Now Varieties of Shigella Dysenterlae In Tashkent ASSOCIATION: Tashkentskiy gosudarstvennyy meditsinskiy institut (Taslikent State MpAlnal Tnt:tltii+.A) SUBMITT -~ June 16, 1959 Card 2/2 SAHSONOV, P.F., prof.jy MN_,., oosistent Shigella ambigua. Mauch.trudy uch.i prak.vrach. no.2:15-21 161. (MIRA 15:8) 1. Iz kafedx7 mikrobiologii Tashkentskogo gosudarstvennogo meditsinskogo instituta (zav. kafedroy ~- prof. P.F.Samsonov). (SHIGELU AMXIGUA) UNISH,EVSKAYA.j M.N. Haterials on the diagnoois of bacillaz7 dyaontery, Mod, zb=, .Usb. no. 246-18 P 161. (KEU 34: 2) 1, Iz kafedry mikrobiologii.(Zav,.'- prof, P.F. Samonar) TaAkentakogo gosudarstve=ogo maditainakogo instituta. YANISHEIISKAYA. M.N. Keratoconjunctival test in the detection of dysentery bacteria. Nauch.trudy uchA prak.vrach. no.206-43 161. (MM 15:8) 1. Iz kafedry mikrobiologii Tashkentskogo gosudarstvennogo meditain- skogo institute (zav. kafedrov - prof. F.F.Samsonov). (DYSENTERY) (dRATOCON-TUCTIVITIS) SAMSONOV,, P*Fop p~rof.j ?~~ILH "SRAj!!.N-j assiatent Shigella ambigua in Taahkent. Report No.21 Serological abaracteristica. Mod. zhur. Uzb. no.3t47-50 Mr 161. (MIRA 1425) 1. Is kafedry mikrobiologii Tashkentakogo gosudarstvennogo medit- ainskogo institut4. (TASHKENT-ZHIGELIA AMBIPUA) WC N. M-S1TFV,SUj&,-M.~N.- DUBOVITSKAYA, N.K.; KLYUCIIRWA~ Me.; 141TRIKINA, P.Ye.; PEKSHEVA,, M.N.; SAMOYLOVA, Z.Ye.; TYUNEYEVA., G.A,. Diffictaties In diagnosing some atypical dysenterial bacteria. Mod. zhur. Uzb. no.2t2O-22 F 162. (MIRA. 15:4) 1. 1% kafedry mikrobiologii (zav. - prof. P.F.Sanwonov) Tuhkontskogo gosudarstvonnogo moditainnkogo instituta I labore.toriy gorodskoy I rayonnykh sanitarno-opidemiologichoskikh stantsi3, Tashkenta. (SHIGELLA) tjv% (DYSENTEM, AKHnWV'l N.A.;KLYUCHAREVA, T.Ye.; SAMSOROV, P.P.; XW*XZqKAYA, M.N. Specific pbageo in the diagnoolo of Imoterial dyoentez7. Report No,L Naucb.trudy uch.i prak.vraob.Usbo no*31151-157 162. (MMA 16t2) 1. Iz kafedry mikxobiologii Tanhkentskogo gosudatst7ennogo meditsinskogo inatituta ~zav. - prof. P.F& Samsoncv) I Oblastnoy sanitarno-apidemiologicheskoy stantaii Taalikenta (zave Sol* Eydelinant) ;YSHNxm) (BACTMUOPHAaZ) KOSOVSKIY. A.A.,insh.; YANISHEVSKATAjLY-.inzh. Operation of tFz ~former oil. Elsk.sta.29 no.1:87-88 Kr 158. (Insulating olls) (KIRA 110) SHCREGLOV, A.P. ,inzh. A M.V. , Inzh. Use of the trannformer insulating oils of munIcipal clectric power distribution networks. Elek. ata. 35 nc.6:77-79 Je 164. 1. Leningradskaya kabellnaya 5et'. IANISHLTSKAYA,LL~ Treat=ent of infectious polyarthritis of indeterminate etiology at the Tashminvody Health Resort. Trudy Uz,- gos, nauch.-issl, inst. kur. i fiziotorno.15:193-201 159. (141RA lj~: 9) (ARTHRITIS) (IIIIIERAL ATM.) Aj I Alf, 1 91 REV 4;L 14 2 P,R i 4 ELI rc v -vie 7 fl 2 t;; Fg ~.q He 1.1. g i nr I H i r,,q. N Ell" 8/063Y60/005/003/010/011AX A 05 1 /J.029 AUTHORSa Bozhevollnov, Ye.A., Yanishovskays, V.M. TITLEa Aluminum Determination by the Luminescent Mothod PERIODICAL& Zhurnal Vessoyuznogo Xhimicheekogo Obahohestva Im. D.I. Mendeleyeva; 1960; Vol- 5, No- 3, PP- .556-357 TEXTR Luminescent methods for datermining_aluminum were developed in varl.- ous objects according to standards of 1110 -1010-5%. The method suggest- ed in (Ref.1) using salicylal-c-aminophanol for the deteotion and semi- uantitati-re determination of aluminum was 1mvestigated by the authore Ref.2). The sensitivity of the reaction wat evaluated as 0-05,y Al/5 ml Z of solution. The oPtim"m PH value is 5.6-6.2. The reagent is introduoed in the form of a 0.01% solution in acetone- An a quantity of 0.15 ml to 5 ml of the solution being analyzed. The proportional relationghip betvaen the intensity of the fluorescence and the aluminum concentration is observed prior to its content attaining O*5W in 5 ml of solution. Besides aluminum, Card 1/10 31063'60100510031010101"-Ixx A051yi-029 Aluminum Determination by the Luminescent Method no other cations cause fluoraso enea in quantities of 251 in 5 ml of solu- tion. Only coppor and iron in quantities more than 0.11 in 5 ml are able to extinguish the fluorescence of the salioylal-o-phenol and aluminum com- plot. The sensitivity of the given reaction dependa to a greater extent on the purity of the applied buffer solution and as a result of its puri- fication lby the chromatographic method using the co;:plex-forming agent 2921,41-trioXY-5--chloro~,19"#I-azobenzene-3-oulfo-.aci~ (Ref. 3) It to possible to form a buffer solution containing 5*10-'3~ alumiwam in it. Such a purity in the buffer solution yields a sensitivity of the resotion of 0 00251 in 5 ml. The baffer solution is purified by introdueiag 5 ml of 0-;% of the above-mentioned oomplex-forming agent to 100 ml of the solution being puri- fiedg and this is left to stand for one hour, eo that the internal aomplex formation of the cvmpound vith aluminum can take place. 20-25 1 of the buffer solution can be purified on a ;,olumn having a volume of 20-25 ml- The ~VL*3-10 (EDE-10) anionite, which fills the column, absorbs 2,2194*- trJ.OxY,-5-chloro--4,pll-azobenzeDi-3-sulfo-ao-l~d and acquires a Urk brown Card 2/10 S/063 '601005100310-010111AT A051~J-029 Aluminum Determination by the Luminescent Method color in the top portion of the column. The distritution of this coloring doyn the column In the purirication process is the c.riterion or the degree of anignite ooneumptign. When the colorleae zone of' the anionite becomes less than 3 am the anionite in the column should be replaced by a fresh bateh. The addition method is used in all cases due- to the extinguishing effeot of copper and iron, which onables one to perform the analysis with- out first eliminating copper and iron from the solution being analyzed. the increment of the fluorescence ititensity was dete,rmined after the intro- duction of a known quantity of aluminum into the solution and the unknown quantity of aluminum was determined from the intensity of the fluorescen-.e of the solution in 10 ml of solution according to the formulat LC AI(Ix' I'o) A17/1 0 ml - -- Y - - -1 9 60 x Al where AC Al is the quantity of Al in Y introduced Into 10 ml of the ana- Card 3/10 ~S1063'6010051003101010111XX 1051yi-029 Aluminum Determination by the Luminescent Method lyzed solution; I x is the intensity of fluorescence of the analyzed samplej 1 AO is the intensity of the fluoreseenoe of the i;olution with aluminum Al introduced Into itj 1 0 is the subtrE.cted value of the control test. The fluoreseenoe intensity was measured with a YM-2 (Ulf-2) monochromator, 49-M where a 4t>9Y 19-M (FEU , ) photomultiplier was usad as the emission re- oeiver. The determination of aluminum in sodium ao&tate was performed direetly In its aqueous solutiong &I ,'ter the pH was 'brought to 5.6-6.0. The analyzed solution was bri~ught to 100 ml with waterfour 9 ml samples were removed, into two of which additionji of aluminum were added in quantities of 0-05 and 0 -08 iato the third ample - 2 drops of 0-05 a solution of trilon B. The voLme of all four sif)llutions was brought to 10 ml with water and 0.3 ml of a 0.01% solution of salioylal-o-amino-phanol was added into eaoh. After 60 min the intensities of the fluorescence of each solution were recorded photometrically. The percentage of aluminum in the sodiur acetate was calculated according to the formulas Card 4/10 S10631601005100310,010111XX A051/AO29 Aluminum Determination by the Luminescent Xethod Content of A'lq % . ACAI(ix-;T) where X is a weighed portion of X(I I )-goo x Al sodium acetate dissolved in 100 ml of water; I Tis the subtracted value corresponding to the solution with trilon B. The determination of the alu- minum percentage with an addition-of aluminum of OiC-5 and 0.08 1, did not deviate by more than 20%. Aluminum was de+ermined Ja acids azid hy4rogen peroxide after these had been evaporated. Neutral calts were added in order to ensure a complete transfer of the residue to the buffer solution after evaporation, The.determination of aluminum in hydrofluorie acid can be accomplished only in using acidic decomposition of !;he residue after evapo- ration of HC1. Table 1 lists examples of aluminum determinations in solu- tions of HClp HNO39 HP H 2S0 and H 0 . The determ:Lnation error did not ex- ceed 20%. Table 2 li;ts ex imples 2f2&luminum dete=ination after prelimina- 0 ry introduction of Al. Table 3 lists the degree of agreement between the Card 5/10 S/063J'60/005/003/010/011/Xx A051/A029 Aluminum Determination by the Luminescent Method results for Al-determination by the two methods on am example of HF analyses. There &re three tables and 3 referencess 2 So-vietq 1 Czechoslovakian. ASSOCIATIONs VNII kbimicheskikh reaktivov (All-Union Scientific Research 'Institute of Chemical Reagents) SUBMITTEDs October 219 1959 Card 6/10