SCIENTIFIC ABSTRACT YANIN, B. T. - YANISHEVSKAYA, V. M.
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CIA-RDP86-00513R001962030010-9
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RIF
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S
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100
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December 31, 1967
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SCIENTIFIC ABSTRACT
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YAI~TIN, B. T. : llyaa.tor Gool09-Mlnlr,'-cA0 Scl (LI1013) -- "Bivalvo :1011"Inks of V-10
Ivalandin Q~oterive of the Crimea (the order Schizodonta, Haterodonta, and.
Rudiatae)". 1100cov, 1959. 12 pp (Mofscaw Order of Lenin and Ordor of Labor
Rea Baniyjr State Tj Im M. V. Lowonosov, Goology Faculty), 120 copies (n, ljo
1959, 1P8)
DRUSHCHITS, V.V.; YARIN, B.T.
Lower Cretaceoua deposite of central Crimea. Vest.Xosk.uu.Ser.
biol., pochv., geol., geog. 14 no.1:115-120 '59.
(NIR,k 12-.9)
1. Hoskovekiy gosudaretyem7y univeraitet, Kafedra paleontologli.
Orimea_-Geology, Stratigraphic)
YANINJ B. T.
Now data on the stratigraphy of the Albian otage in Bakhchlearay
Diotriot (Crimea)'# Biule MOIP. Otd.geol. 37 no.3sl26-129 My-Je
162* (MIFul 15:10)
(Bakhchisaray Distcict~-Geology.. Stratierapbio)
AMIDT, Yu.A. YANIN T.
LAte Jurassic and Early
04
Paleont. zhur. no.3:140-,'_,2
1. Paleontologicheskly Itisti-t!lt liti i ',!csko-vskly
vennyy universitet.
NAYDIN, T).P,l YANIN, B.T.
harhc ice of the geo2of-j of the ou.-raund!ngij e-,-'
Frokhladnoya (Crivrn, Bakhoblaaray Watrict"6 Billi. Moi? 9
Otd. geol. 40 no.305-81 MY~70 165. Mpl 113t,3)
YANIN, F. G.
loading and Unloading
New scheme for unloading ships. Rech. transp. 12 no. 1, 1952.
Monthly List of Russian Accessions, Library of Congress, June 1952, Unclassified.
YANIN, G.I.
School hotbeds heated by a stove. Rol. v shkile no.4:50-52
JI-Ag 161. (MIRA 14:7)
1. Helitopol'skiy peclago Icbeakiy institut.
fHotbeds)
YANIN, Ivan -Aloksoyevich; YAKOVWT,, D.Y., red.; KIIITWY, P.A., tokhn.red.
-"'--~1n:r'easing the officionc7 of regenerative braking for TL22~
electric locomotives] Pov7shnnie offektivnosti relmperativnogo
tormozhenila na elektrovozakh VL22m. Moskva, Goo. transp.
zhe,l-dor. izd-vo, 1958. 36 p. (MIR& 12:1)
1. Starshiy mashinist lokomotivnogo depo Elatoust Yuzhno-Urul'sko7
doro~i.
(Railroads--Brak"s) (Electric locomotives)
- -- ------- --- ---
TANIN, I.A., maohinint
Regeneratiou of enarg7 b7 the JIB electric locomotive. Ilek,i,
teplotiaga 14 n0-3:7-9 97 160. (MIU 13t7)
1. Depo Matoust Tiabno-Urallskojr dorogi,
(Ileotric locomotives)
YARIN, I.A., mashinist elektrovoza; KOVRIZMM. V.V., mashinist elektrovoxa;
V.A., insh.
How to check the operation of regenarative eystem. Blek. L tepl.
tiaga 4 no.10:7-8 0 160. (MIRA 13:10)
1. Depo Zlatoust Yuzhuo-Urallskoy dorogi.
(Railroads-Brakse)
KALININ, V.K., kand. tekhn. nauk,- MIRONOV, K.A., insh.;.LBVIN, B.H.,
lnzb.; LIWIAN, G.M., inzh.; YERSHOV, Ye.F., inxh.;
PANCHENKO, P.M., lnzh.; BOLYCHEV, N.G., mashinist elektro-
voza; ZOLOTAREV, V.N., mashinist instruktor; YA~
inzh.; BOVE, Ye.G., kand. tekhn. nauk, red.11=0,
takhn. red.
[Electric networks and maintenance of the equipment of
electric locomotives] Elektricheskie skhemy i ukhod za obo-
rudovaniem elektrovozov. [By] V.K.Kalinin i dr. Moskva
Transzheldorizdat., 1963. 279 p. (MIRA 16'.-7)
(Electric locomotives)
'31
S/107/61/000/010/005/007
D201/D304
AUTHORs Yaninj L.$ Engineer
TITIZ: Exposure meter for projection photoprinting
TERIODICALt Radiop no. 10, 1961) 49-50
TEXT: In the present article) the author describes the circuit of
an exposure meter which permits quick evaluation of the exposure time
required. It is essentially bridge circuit with a photo-emissive cell
4(:-K1 (FS-KI) as the sensing device in one of the brid * arms. The
diagonal of the bridge has a microammeter type MIC -100 f-US-100) with
100p.A FSD. The bridge is zeroed by var-ying the resistance of one of
the arms to give zero deflection of the ammeter) and with the illumina-
tion of FS-JU, the current flowing in the meter determine& the exposure
time. The power supply consists of a half-wave rectifier employing
germanium diodes A'IF- (DTY*) connected in series. The d.c. supply is
stabilized by a noon valve cr-in(sa-2p) which is also used as "ON"
indicator# The instrument is in a rectangular metal box 170 x 110 x
80 mm with the photocell FS-11 on the outside. The FS-KI in connected
Lard 1/2
S/107/01/000/010/005/007
Exposure meter for... D201/D304
to the bridge by a 500 mm length of wire. After calibration, a sample
run in made with various apertures and corrections introduced if neces- V//
sary. To determine the exposure time for different grades of photopaper,
the relative values of sensitivity of different kinds of paper--Unibrom
-30, Potobrom 209 Bromportret 12-can be used. If a leas sensitive 500-V A
meter is to be used, the d.c. voltage has to be increased, remembering
the maximum p.d. at the photo-emissive cell FS-1Kl is 40OV. Thor* are
3 figures.
Card 2/2
YANINp Lo. lnzh.
Photographic OXPOSure meter -for Printing operations.
n0-10:49-50 0 161. Radio
(Photographic sonsitometry) MMA 14:10)
R6
M
ReplacemApt of 5Ts4S and 5Ts3S kenotrons with transistor diodes
In television receivers. Radio no.2:37-38 F 061. (MIRA 14:9)
(Television--Receivers and reception)
_-i-- --- -I -
-------:
YANIN,, L., inzh.
Yaults in the automatic gain networko of a televiaion receiver.
Radio nojt25-26 Mr 062. (MIRA 15:3)
(Television-Receivero aW reception)
YANIN, L.G., inzh.
PPY-AM mOdulation with Ume djvjBiOj
lines Vest. BvIaZi 22 Or channels in a Milo rel-,,
no.11;8-10 N 162. j,
(KRA 16 112)
YANIN,. L.V. (Moskva)
Basic trends in the activity of nd r sanitation inspection.
G16- truda I'pror.,zab- 4 no, 7:3-7uJ-51t 1,
11 Minister (MIRA 13:8)
stvo 2dravookh-raneniya SSSR.
(FACTORY SANITATION)
~"q
KOVARSK!Yy A.G.j MEDOKSj T.S.; Prinimali uchastiye: GLEBOVA, L.F.;
34MOV, S.M.; YAN10) L.V.; VIDANOV., V.H.j prof., red.1
IWISTOV0 L.N., ra.-;-M
' _hh11' M.T., tekbn. red.
[Collection of official materials relating to laborator..y work]
Sbornik ofitsialinykh materialov po laboratornomu del., No-
ekva, Medgiz, Book 1. (Manual for laboratory doctors., sanita-
tion doctors, and epidemiologists] V pomoshch' vracham-
laborantam, sanitarnym vracham i vracham-cpidemiologam. 1961.
462 P. (MIRA 15:2)
(1,12DICAL LABORATORIES) (BIOLOGICAL Lj1BORATNUES)
(CHWICAL LABORATORIES)
YANIN, L.V... red.; RMIANOVAt Z.A., tekhn. red.
[The most important official documents on industrial Irigieno
and sanitation]Sbornik vazhneishikh ofitsiallnfth raterialov
po voprosam gigieny truda i proizvodstvemoi sanitarii. Yo-
skva, Medgiz. No,2, 1962. 219 (MRA 15:12)
(INDUMIAL hYGIFITE~*
KLIMOVAI T.Kh.; LORMSKIY, D.E.; YAIIKOVSKAYA,
YEGOROVi Yu.L., red.; MIRONGVA, A.M., tekhn, red.
(Co3lection of the most important official data on problems of
industrial Irygiene and industrial sanitation]Sbornik vazhnei-
shikh ofitsiallxWkh materialov po voprosan. gigierg truda i pro-
izvodstvennoi sanitarii. Fioskva,, Medgiz. Vo.l. 1962. 314 p.
(MIRA 15:10)
(INDU,-,IRIAL BYGIEIM--LAW AND LEGI SLAT ION)
TAHINj N.G.;.BCHETCHIKOV. I.I.; BILISKIT, V.I., otv.red.; PEVZNSR, A.S"
zav'~iad.izd-va; GILRUSON, P.O., tokhn.red,
(Uniform time and pay standards for construction, assembly. and
repair operations in 19601 Edinye normy i rastsenki na stroi-
tellnys, montazhnye i remontuo-stroitollnye raboty, 1960 g.
Moskva, Goo.izd-vo lit-ry po stroit., arkh1t. i stroit.materia-
lam. Sbornik 13. [Installing industrial furnaces and flues)
Xladka promyahlennykh pechei i trub. 196o. 96 p.
(MIRA 13:6)
1. Russia (1923- U.S.S.R.) Gosudarstvannyy komitet po delam
stroitel'stva. Ze Normativno-iseledovateltakaya 9tantsiya No.5
(NIS-5) Ministerstva stroitellstva RSFSR (for Tanin, Schatchikov).
(wages) (Furnaces) (Flues)
VIA
S/1 93.16 1/0' 0/0 11/002/007
A0047A101
AUTHOR: Yanin, V. Ye.
TITLE: Pressure working of metals at the enterprises of the Moscow City
Sovnarkhoz
PERIODICAL: Byulleten' takhniko-ekonomicheekey informatsii, no. 11, 1961, 20-24
TEXT: The author reports on the achievements of the Moscow City Sovnarkhoz
plants in the field of forging, pressing, die forging and drop forging and points
out that, in comparison with 1948, the stock of forging andpressing machinery in
the Soviet Union had increased by 1958 nearly by a factor of 3. The development
plan for the national economy provides for an Increase in the production of forg-
ing and pressing machinery of 25% compared to 14% In 1958. The considerable
increase in the production of forging and pressing equipment can be mainly
explained by the necessity of producing precision forgings approaching the
dimensions of the finished components. To increase the forging precision and
cut the labor consumption some 20 orank-type drop-forging presses with a capacity
of up to 6,300 tons have been installed in the Moscow plants. By 1960 the volume
of precision forgings at the Moscow City Sovnarkhoz plants amounted to 34,000 tDns
Card 1/4
B/193/61/000/011/002/007
Pressure working of metals at the enterprises ... A004/A101
or 13% of the total of drop-forgings. For 1961 the rated output figure of
precision forgings is 35,000 tons, while it is planned to bring that figure up
to 80,000 tons by 1965. The introduction of advanced technologies considerably
improved the teohnological and economic indices of forging shop operations. In
1960 the metal consumption per ton of forging amounted to 1,170 kg, compared
with 1,178 kg in 1958, while rejects could be reduced to 0.3%. The author
points out, however, that still up to 30%of metal losses occur particularly In
hand forging, while the losses are still greater when machine pE--ts are manufac-
tured directly from rolled material on machine tools, where the coefficient of
metal utilization amounts to 0.3 - 0.5 only. Technological processes are being
developed at the Moscow City Sovnarkhoz plants which will increase the output
of serviceable metal in forging and pressing shops to 90%, while the metal loss
In chips in mechanical shops In the manufacture of parts of Intricate configura-
tion will be cut by 15%. The practico of the "Krassnyy proletariy" Plant and
the Moskovskiy zavod pozharnykh mashin (Moscow Fire Engine Plant) shows that
in small-batch production the cost on die-making is paid off after 3,000 to
4,000 parts. The forging shops of the "Dinamo", "Krassnyy proletariy", Vladimir
Il'ich and other plants have converted some 2,000 tons of hand forgings to die
forging, which reduces the labor consumption by 35-40 norm-hours per ton of die
Card 2/4
S11931611000101110021007
Pressure working of metals at the enterprises ... A004/A161
forgings, and saves some 80 rubles per ton. The author mentions the extensive
use of multipurpose-setting dies for small-batch and big-lot production for which
only inserts for the shaping grooves need to be chanaed to forge parts of
dif ferent conf 1guration. The author points out that at present already some
~,000 tons of forgings are produced by the impact extrusion method, which saves
up to 15 - 40% of metal, cuts labor consumption by 15 - 40% and yields forgings
attaining the 2nd class of precision without subsequent machining. The Avto-
zavod Im. Likhacheva (Automovil Plant im. Likhachev) (ZIL) in cooperation with
NIITavtoprom introduced the method of hot gear generation for the ZIL-157 truck.
The machine tool for the manufacture of these gears has been described in the
Rjulleten' tekhn1ko-ekonomicbeskoy informatsli 1961, no. 8, 33. The author
emphasizes that the use of induction heating I~ precision die forging has
increased the labor productivity, facilitated the working conditions and,created
the necessary prerequisites for the overall automation of die-forging equipment.
A deterrent of the increase in efficiency of pressing and forSing equipment Is
the Insufficient service life of dies made from the steel grades 5XHT Mhmr),
5XHB OKIW), 5xrc (5KhGS) and others which, on the average does not exceed
4,000 to 5,000 forgings. The author reports on a new non-nickel die steel
which has been tested at one of thc- Moscow City Sovnarkhoz Plants and has been
Card 3/4
S/193/61/000,/011/002,/007
Pressure working of metals at the enterprises ... AOO4/AIOl
developed by TeNlIchermet. The service life of this new steel is 4 to 6 times
higher than that of 5KhNV steel. The Stankostroitelinyy zavod im. Ordzhonikidze
(Machine Tool Plant im. Ordzhonikidze) has erected a new meohanized.line for
the production of forgings for shafts and spindles of metal-cutting machines.
This line conslats of press-shears, merry-go-round-type gas furnace, vertical
radial forging machine with hydraulic station, annealing furnace, conveyers and
other means of mechanization. There is 1 Soviet-bloc. rsference.
card 4/4
YAMM V Ye inzli.~ OKHRIMKO, Ye-.R., doktor tekhn. nauk, prof.
i --ellhod for the deformat-lon of biwtals.
'4-w im Ve3t. mashlnostr
45 no.7:67-71, Jl 165. (MIPA 18:10;
YANIN? V.Ye.
Survey of the state of technological processes in enterprisca
of the Moscow City Economic Council. Biul.tekh.-ekon.informz.-
gos.nauch.-issl.inst.nauchJ tekh.inform. no.3:72-75 162.
041RA 15-0)
(Moscow-Industrial management)
nr
YANINY VIYO.
Review of the levels of technological processes in enterprises of
Moscow City Economic Council. Biul.tekh.-ekon.inform.Gos.nauch.-
issl,inst.nauch. i tekh.infom. no.6:84-86 162. (MIRA 15M
(Moscow-Industry)
YANINO V.ya.
PrOBOwOrking of metals In the ent8rPriden of the Moscow
Economic Council, Blulotekh,,-ekonolnfom*Goo.nauch -1801,
Instonauch.i tekh.inform. no.2:80-81 163. RRA 16-:2)
(Hoscow-Forging)
Si7dV'Ri
*Tm~
a
E
-5 M
K
. . . . . . . . . . . . .
4
IT--4 Fi 0 F-a - 4., ralliDIfi"(110 rd
1-414 At-ii, -it h,
S v L_71 V _~d u, b r a_1 4~;
uo:;WL1pr,; i'Moscow non-ierrvus metal )ro, ess-ing
ti e b i 1Fe_6T._AWi _ngo4F -of t4fi.- I - "'t P - , ,
_____ptant) devised a now method cf preparing the, 0 ". 7 x
600 mm, is cleaned with emery paper -n 6(-' rnzria side,_dia-reasedtfn a lii'17k, s~xla -)iuLion.
F,_
~vashed, coated wfflu borax fl "i, heated .4D 30- 11160C, vertic I - __ n -
aJJV in-Sert&H 1 1 apnvj~'!
cast-iron mold, and molt, 're" intu, the free space of [lie moid ad ~icen; i
UP
the c 1 ear, ed s ide of the s tingo t ~, -o obtained is (Lffus tes t.,
Lie jointF ional..' TenB i I
off strips cut across such a iho. invariably result in a rtmt ure through- 6" copp-r pa
never all the ~:olrit. I'lle hillvt ii n ~,I, 'I'l-o- I'' U"., 11nal Ql,*,,s usf,~ 1)
Cocci 1,2
-APT
-300
after'to ing. - The first reduction should not exceed m' but the last cam re A
formula describLng warping of bimetal stripq duririg rollina is derivrwf
t.SSOCIATION: none
5,
0011
11 (Olltll ( 64 -'."t6w'-.Ja(hVz z/
-k-64372-6a, IR q
-'ICCESSIOI?-.NR.- AP5018670 M/0122A5/000/OM /0067/0017~,'~-Wtvl
621-/j9.4.002.2 yx
AUTHORS yanitv~ yd. z nko Ya. -of- ted-n ical :L.~
so
(*inoer khti
v M' OL-sm-n~-
a -ax Ift- ~1;1 q/ 5
1'7'
_0 dormaiion of. bIMSIgials~-"
TITM..~: Nowiaod t d
~Neqtzak rashinostro7wilya no 7 5 677-7-17
v
TAGS baili6' qu!lp ~q_jn
yar-bime-tal.-
bv -L90__br-asi---ra-
I L
brass, GDIJ alloy.
AB8TWICT.: 0
6-,"Plas t. ic 'deformtiont of b tallic soa6imops,with tIhe d formitio Ia_
~'_forces-~ 4#vcted _-,paraIL&I ~.to -the _~2nded t~i 4- b4tudett:_ttn
rug-_ _na w-In or the moth-a
'ea
-0 -prepared aue-d:rrg,~9 d r;Wgreated by V,
It 1. AnT)i1.8IicF;4'(Spoaob iz-gotovIeniya
__janiM"
bimotallielieskikh polos liatov 'J~ ugolkov i tomi podobnykh i-.doliy. Avtvrskoye
ovidotelletvo SSSSR' 110._IJ+7A) 1960) from four bimetallic combination.- (Invar.1.1,
1136-brass -ill-ly
7:1
5 irn a
I-Ciard ti'm :-" 0.5-0.9 for uf~e
L_643-72jo~65_'
ACCESSION Va.,. AP5018616':,
aiteon 6' imens, a
ch bimoW:wrq
WO'bimetas# poo defomd 20~-40,1 -and
see--
ons- uere- stWdied Vtdudlli
9W. t 16- ~=/S a
tidrdjig and etching) and by r-radiation from isotopes. It was found that the
bulaing of the welded surface depended on the coefficient n ptat/Pa~, Wiers
I Pft .2
~4_(' t 77'
itAll
P
'4_
t -of contact -.the -'b a~ um-s--in- the A -7
n _f' the direction of the hard motal.i
1.0, a re 0
a it t van n
Tt was found that the Umotallic bonds remninad intact in all apocirnong ( u.
gwo delfarmat' TO bqf, -hqt C"', C k s'.-,T-t7ia 2. ff
Tt' Tm /A' allould 2; fc,r 2.5 it should hc~ < A.
~R-
y~
R
ACCZSSION NA: AP5018,PfO
Orig. art. 'las: 4 fiCures, 4 tables, aA forming.
Vw ii
., oz,
YANIN, V.Ye.
Effect of the shape of bimetal test pieces during upsetting
on their state of stress. TSvet. met. 38 no-5:79-V. My 165.
(MIRA 18t6)
P'.
USSR/ChOM1907 - PhnTMcQUtIOalV 21 JUn 32
'Medicine - Tuberculocia. Chow-tbara-py
Olsonlootinoyl Hydramones and Their AntItubercultir Activity," M.N. Shemkim. 0. if.
Pershin, 0. 0. Un "-yova. Yo. D. Sezonovs. Te. 13. Hikitskayn, As D. Yanina,
A. 1. Yakovleva, All-Unton Set Pat Chem-P&nr Inst I~Mal S. Ordzhonikidze
7
Olbk Alc ftuk- SSSR! Vol LMIV, 210 5, PP 981 - 984
Isonicotinoyl hydrazide has an antItubercular Potlon, but Ito thempeutic Index Is
low, A sories of substituted IsontootInoyl hydrazIde derive were,prapd and their
bactarlostatic action on tuberculosis bacilli in vitro tested. It was shown that
substituted toonicotlnoyl hydra2ones have a higher antituberculnx activity tham
Para-2kninonalicylic aeld and streptorqcin and are better tolerated'; by exptl milmls
than tho bydr!~%Ide of Iron1cotinic r-cid. Thle mdo It possibl-a t4i Oeleat froo theta
cubst,nneen for clinical stue-y on tubercular humns. A oubtatr~nce. called "2-ht1vUcids*
by the authors. vas foramrded for clinical study, which is Prorrassind, successfully.
Presented by Aaad A~.' N. Nesmeyanov 9 Apr r2.
223T17
p. r"I 11) f pf v1 it
Iff'o;
IT
""d ""i,
-Ir -T-
,tvp .4t F T. tit
44
1cl
IMIN
lam
--- law
v r
USSR/Chemistry - Drugs Sep 53
IlAminoalkyl Derivatives of quinuclidine," M. V. Rubtsov, Ye. S. Nikitskays., Ye. Ye. Milchlina,
A. D. Yanina, and V. Ya. 1"urshtatova, All-Union S(~I-Reqevrch Chomico-Phermaceut Inst im Ord-
zhonikidze
Zhur Obshch Xhim, Vol 23, No 9, RP 1555-1559
A number of substituted 2-aminomethyl quinuclidines and 2-aminomet-hyl-3-( -aminoethyl)-quin-
uclidinec were synthesized.
U
g "A
N
-Muf frcm VT. WA. V- I--
--f-W
E YA 7. C. --l C4- A~4
UM/Chemistry - Synthesis
1/1 Pub@ 151'- -X/1,2
'Rub sav Nikitskaya E. and Yanina,, A. D.
Synthesis of gamma-formylpyridine and isonicotinic acid
PorlOldicdl I Zhur.-ob. khim, 24/9, 1648-1651,, SOP 1954
"Abotract I 'The conditions favorable for the synthesis of gamma-fornWlpyridine by'
selectie- oxidation of. gamma-picoline, with selenium dioxide in the
presence of beta-picbline,.areIescribed. Two variants for the deriva-
tion of isonicotinic acid, with a.yield of 75-80% of the initial ga=a-
picoline, were developed, The effect of selenium dioxide, on the se-
lective oxidation of gam-na-picoline, is explained. Five references:
2-U3511; 1-S~riss; 2-German and USA (1934-1953).
Institution The S- Ordzhonikid e All-Union Scientific Research Chemical
Pharl;;ceutical Instzitute
Submitted April 14j. 1954
~M-
AUTHORS: Yanina, A. D., Rubtsov, Lt. V. SOV/79-29-2-27/71
TITLE: The Hofmann Cleavage of I-Azabicyclo-(3,2,1)-Octane (Gafman-
ovskoye rasshchopleniye 1-azabitsiklo-(3,2,1)oktana)
PERIODICAL: Zhurnal obshchey khimii, 1959, Vol 29, Nr 2, PP 485-493 (USSR)
ABSTRACT: In the 11ofnann cleavage (Refs 112) the unsymmetric bicyclic
systems react with a common nitrogen, under formation of not
one monocyclic heterocycle but 3 heterocycles which have an
unsaturated side chain or under the formation of their trans-
formation products, in dependence on the question, from which
P-carbon atom the hydrogen will separate to form the water
molecule. The direction of cleavage apparently depends both on
the stability of the bicycles and on experimental conditions.
This was proven by the experimental cleavage in the case of
1-azabicyolo-(3,2,i)-octano (III). The initial product in this
connection was 1-carbethoxy methyl-3-carbethoxy piperidine M
(Scheme 1). The intramolecular condensation of (I) into (II)
proceeded in the presence of potassium alcoholate [not with
metallic potassium (Ref 3)], which increased the yield from
30 to 71 1171o. By reduction of the ketone (II) octane (III) was
Card 1/2 obtained, which was transformed by methyl iodide into the
The Hofmann Cleavage of 1-Azabicyc1o-(3,2,1)-0ctane SOV/79-29-2-27/71
quater nary salt (IV) and further with silver oxide into the
corresponding base (V). It was found that oncleaving 1-aza--
bicyclo-(322,1)-octane under various conditions (at normal
pressure, in vacuum, in.40 01~6 potash lye, and at increased
pressure) three products are formed; 1-methyl-3-allyl
py=11dine, 1-methYl-3-(P-oxyothyl)-piperidine, and
di-[P-(l-methyl piperidyl-3)1-cthyl ether. 1-methyl-3-allyl
pyrmliline was separated in all cases and is the chief product
of the cleavage of 1-azabicyclo-(3,2,1)-octane in alkali medi-
um, in vacuum, and at normal pressure. On its heating in water
under pressure; 1-methyl-3-(P-oxyethyl)-piperidine is the
chief products There are 0 references, I of which i3 Soviet.
ASSOCIATION: Vsesoyuznyy nauchno-issledovatellskiy khimiko-farmatsevti-
,:heskiy institut imeni S. Ordzhonikidze (All-Union Scientific
Chemico-pharmaceutical Research Institute imeni S. Ordzhonikid--e)
SUB14ITTED: January 3, 1958
Card 2/2
~70 ME a 7 ~__'
HUBTSOV,, M.V.; IIIKITSKAYA,, ye.s.,. YANDa, t,.D.; USOVSKAYA, V.S.
New ganglion blocking preparations. Khim. i med. no.15:16-28 160,
(I-MA 15: 1)
1. Vsesoyaznyf nauchno-issledovatellskiy khimiko-farmatsev-tichoskiy
institut imeni, S. Ordzhonikidze.
(AUTONORIC DiWGS
5.3616 77883
SOV/79-30-2-34/78
AUTHORS: Yanina, A. D., Rubtsov, M. V.
-----------
TITLE: Hoffmann Degradation of I-Azabicyclo-(3,2,1)-Octanes.
III Cleavage of 7-Methyl-l-Azabicyclo-(3,2,1)-Octane
PERIODICAL: Zhurnal obshchey khtmii, 1960, Vol 30, Mr 2,
pp 526-533 (USSR)
ABSTRAM Quaternary base of 1-azabicyclo-(3,3,1)-nonane (VII),
on thermal decomposiltion, forms 1-methyl-3-allyl-
piperidine (VIII). The latter wan uned for the
preparation of the methiodide of 'I-methyl-l-azabicy-
clo-(3,2,1)-octane (X).
N-C11,C11,C00(%11:j
Card 1/9 (Figure continued on Card 2/9)
(Cont'd from Cat-d V9)
777893 SOV/79-30-2-34/-(8
cooell, c0
11,0
N C112CI12('OOC211,1 N
-cI12GII=CII
2
(
N:f~
N- \N1
M (VO (Vill)
Ag
N~ Ili N CII, N C I I'l
u, Oil
(I X) (X 1)
C ard 2/9
,radation of 1-A~,-ihlcyclo-
i1of fmann Dej, 77883
-(3,2,1)-Octanes. II. of' SOV/-[,)_30-2_34/78
'(-Methyl-l-Az,ibtcyclo-(.-,$,~l,, )-O(A~lllc
Synthe:As of X 13 ba.3ed on the addition of III to
Viii (af,-cordIng to Mackovirilkow) vilth formation or
1-methyl-54 P -`o(1ow'01)y1)-r)1Pcr1(J11lc (IX), and
cyc-IL:~atlon Lo compounil X. X ~ja.,,, ,iyntheolzed for the
I'Ltial M;mwtuve proof according to the 6chelne below:
C112CO011
N 1111 N
CM. -CAI Vll~j
Ml N 111tr c1l,
a r, d /9 f,u ve c on td on Card 11/9)
t!of.f.tj~,jtjn Degradation of I-Aza~)Icyclo-
-(3,2, 1 )-Octanes. II. Cleava~-,e of'
N (All
7,1-883
c 11,
CIII:,i
Theoretically, four possLble compoundq can be formed
by 11offmarm degradation OC XI.
11, CA I -C. I I -C I Ij
,N/
CI 13 1"11, c11,
Card 4/9
(Figure cont'd on Card 5/9)
10 ff r*," u 1) Dej rl fli t, 10 n 0 [,:.-1 0- 7 7
IAl
W tt! ,]it llw-~l 1 11,11, of I I I thy L - 1 1 :11 1 -
I tic Cclt,~!Iflzl 1,1,,, or XT
I'd
Th4~,
o
S t'... a 0 b t a
o
n L
t h
anhyd rous IV
I
+
oh o 1
17 KOH
4-
V + 11 G
2
v T.I. 'i, 0
j
VIII + fli
.(Table cont'd) 77883 30V/19 -30-2 -311/78
Thc, ObLAr)~-(j C omp ou rifto and Their, Pr,operti,~.;
U1, Starting
0 i) t" a 1, rl e d
Y 1.11 20
1) p /Mm 1) r,
ic D
6 IX + lf;~O + cthcr v ~W)%, Mp )POO((Ic":!)
solutton of' 1("co ~
1.
VIII + IL'o
Y I '15110
4, M11O)t -me I'lly 1.
1) p c 1,
8 ethyl -1. -rile thy IpI pe. I-
X'I 1
90 o
Mp 188-111,110
+ IICI
X)'I 1, allhydvotlo
MIX0014a + acetic
YJIT
0 it 6
-32
e c 0 n t , d 77883 SOVIf 9 -,',0 -2 - 34 /~-tB
The Obtained Cornpoun d's, and Their, Pz,operties
Starting l"lateri-
I Obtained Yteld P r
r) ror4 wc t D
4
'0! 1 X I L r,
Four '-.1ttempt"; wer-0 mode at; a. Itot'I'mann of
'-'oflinounal ~XI: (I-) it 0 + AgOll undev not'nial
f, fli"MIl~,"I'lOrl under, Vacuum; (3) hen.tlut-, In the
pr-'--c~nce llp-'Atlllj~ 'm "'ho of'
"",,'~tev' onfl~~"" III all Only VITI
01',Utitwd In
D 1. . 'I -,'10 IF) i o ve -ve
w! th lip n
r, ('~ 1, z' en c o: IJ , S 'Phe I j . .5 . v e 1, e I,n
1, r ~rl "i" ti- I i , t J Am . C1,01ri
vp
Cnr-l l.". h. ot'ho I
Hof.fmann Degradation of :~-Azablcyclo- 77883
-(3,2- l)-Octanes. II. Claavage C)f sov/1',,q-3o-2-34/j8
7-Methyl-l-Azabicyclo-(3,2,1)-Octarle
ibid, 71, 3098 1949 ; A. Bugger, C. R'. Waltev,
ibid, 72, 1988 H950~-
ASSOCIATION:, Ovdzhonikidze All State Scientific-Reseat-ch Chemical-
PhIarmaceutical Institute (Vsesoyuznyy nauchno-Issledo-
vatellskiy khimiko-farmaL~.cvticheskly Institut
imeni S. OrdzInonikidze)
SUBMITTED: February 21, 1959
Card 9/9
7~
R
TANINA, A.D.; RUBTSOV, M.Y.
Hofmann cleavage of 1-azabioyclo 0.3.13octanes. Part 3: Hofm-ann
cleavage of a quaternary base of 2-methyl-l-azabicyclo[3.2.lloctane-
Zhur.ob.khim. 30 -no.8:2544-255OAg 16o. (MIRA 13:8)
1. Voesoyuznyy naachno-iseledovatellskiy khimiko-farmatsevtichoskiy
iustitut imeni S.Ordzhonikidze.
(Azabicycloootane)
YARBA.9 A.D.; RUBTSOVs 14.V0
Hofmann degra&lUn of I-azabicyclo'(3i2.,I) octanes. Part 4: Hofmann
degradation of 4-methyl-l-azabicyclo' (3,,2..l) octane. Zhur.ob.khim.
32-no.6:1789-1798 -Te 1621. (MIRA 15:6)
1. Vsesoyuznyy nauchno-ist3ledovatellokiy khimiko-farmatsevticheakiy
institut im. S.Ordzhonikidiep
(Bicyclooctane-) (Hofmann reaction)
YANINA A D . RUBTSOV, M.V.
Hofmann degradation of I-azabicyclo(3,2,1)4ctams.
Part 5: Hoftann degradation of 6-mothyl-l-azabicyclo(3,2,1)
octane. Zhur.ob.khim. 32 no*10;3151-3158 0 162. (MIRA 15:3-1)
1. Vsesoyuznyy nauchno-isaledovatellskiy khimiko-
farmatsev-ticheskiy institut imeni S. Ordzhonikidze.
(Azabicyclooetane) (Degradation)
J.
YAVINA,, A.D.; RUBTSOV,, M.V.
Hofmann degradation of I-azabioyclo(3a)j)*cttM#-,.
Part 6: Hofmann degration of a quaternary ammoni= bass
of~8-mothyl-l-azabicyclo(3..2,1)octane. Zhur.ob.khim.
32 no.il:3693-3698 N 1629 (MIRA 15:U)
1. Voesoyuznyy nauchno-issladovateltakiy khimiko-
farmatsevticheskiy institut imeni S. Ordzhonikidze.
(Azabicyclooctane) (Hofmann degradation)
_A~,_Dq ~"TSOV, M. V.
Hofha= dagradation of I-aublayo~o(3,2#1)octanes, Part 71
Hoftann. degradation of 3-mtb3rl-l-azabicyclo(3#2.1)octans.
Zhtw. ob. khim, 32 no.12.*3941-3945 D 162. (MIRA 16t1)
1. Vsesoyuznyy nauchno-iseledovatellski)r khimiko-farmatsev-
ticbeskiy institut imeni.S. Ordzhonikidze.
(Azabicyclooetane) (Hofmann reaotion)
ACC NRs AP6031301 BOURCE:-C-Odt~--ifR/6j66-/66/do2/009/1'707/171 I
AUVORt Yaninap A. D,; Mikhlinap Ye, Ye.; R*tsovp He V.
0-W; All-Union Scientific Research Chomical-Pharmacoutical Institute imoni S. Orzho-
nikidzo (Vsesoyuznyy nauchno-issledovatellskiy khimika-farmatcov-tichookiy inatitut)
TIMS Pinacolone rearrangement in the series of I-azabicycloalkancls. Part 2
SOURCES Zhurnal organicheskW khimiip ve 29 no. 99 1966, 1707-1711
TOPIC TAGSs pinacolono rearrangemont, pinacol IGr0Yx%)'%c
V,,-,Aexcc.~jck~c VNse
ABSTR4CTS The roaction of 3-hydroxy-3-oarbothoxyquinualidino (1) with butyl and
p-tolyllithium was used to synthasizo 3-hydroxy-3-fa,crt-di(p-talyl)-ct-hydrovmothyl]-
quinuclidino (11) and 3-hydroxy-3-(a,c~-clibutyl-a-hydrox;ymotlwl)quinualidine (111)S'
OH OH
C=1146 C/R
oil
The following roactions were also carried'outi
Q-,
ACCW~ F--Ai~6631301
0 OR
CS"t-c"I
n.5C.H.C.,
HOD% VA."Ll
Z" NS C t46r,4% CIIH Cjf3
(Vito R AN t
CH ,IH,,Dfl RMC0011.
0 a a ,
N 0 N OR
M
Ckliq
C Cli - C3H, H, Cli Col
a H Pt
fC 4HP W W
IC%Hq
C
N OH C OCOCH3
jilt) W [al I ("' + (XI ci.~)
OCOCHS
N C4H#
The pinacolone rearrangement of compound (II) in 50% H2SQ~ leads to the fomation of
a mixture of two ketonost 3s3-di(p-tolyl)-4-keto-l-azabicy--lo[3.2.2.lnonano (IV) and
.3-(p-:tolyl)-3-(p-mothylbenzoyl)quinuolidine (V); on heating pinacol, (II) with zinc
chloride in acetic anhyc!addep only ketone (Y) is formod. Under the same conditions$,
in the case of pinacol (M)o whose alkyl radical is longer than that of (11)9 only
Card 2/3
7
!, 4cc N'R: AP6031301 - '-
I t
i procccsoG of dehydration and convor3ion of the unsaturated co=pounds formed are 61b-
I zorvod. It is concluded that tho introduction of a mothyl radical into the ph6rql i
1 icing of 3-hydroxy-3-(a,a-diphonyl-cL-hydroxymothyl)qu:lnualicuno facMtates tho course I
YANINk, S.P.; HITSLI, V.I.
OP-10 foaming agent for synthetic glues. Dereprome 9 no*2:
20-21 1 16o (MIA 13t6)
(Glue5 (Jfoam)
a I a i h- DVOSKIH, Baniamin Takoylevich; SAVICH, M.P.,
Zp"'magn
ktor; W-= = , V., takhnichaskiy redektor ' -
[Talks aboat Kazakhstan] Besedy o lizakhatane. Alm-Atm.
razakhokoe gomoizd-vo, 1957- 154 p. (HLRA 10:9)
(Uzakhoton)
14-57-7-15386
Translation from: Referativny zhurnal, Geografiya, 1957, fir 7,
(USSR~
AUTHOR:
TITLE:
PERIODICAL:
ABSTRACT:
Card 1/1
p 184
Yanios, N.
Specialized Agriculture of Southern Kazakh SSR (0
spetsializatsii sellskogo khozyaystva Yuzhnogo
Kazakhstana)
S. kh. Kazakhstana, 1957, Nr 1, pp 16-20
The author discusses logical distribution of various
branches of agriculture and more efficient local
specialized methods for agriculture and animal husban-
dry in the southern oblasts of Kazakh SSR. These are
th*c Y1=o,-Yazakhstmdcaya Alma-Ata, Dzhambul , Taldy-
Kurgan, and htyi-Orda 6blast, containing approximately
85 percent of the total land under irrigation.
-.TAN IOS#.,1X1tDW, Iva vioh, kazd. ekon, nauk; WRIMO Te,AO, redo; TROPIKOV, A.,
.110
red,
(Resources for increasing labor pi,oductivity in nonferrous Metal-
lurgy (based on the emurple of Xazakhetan enterprises)) Rezerv7
rdsta proisvoditellnosti truda v tffvetnol metalluigii (X~ primers
predpriiatli lazakhotam). Koskya, Izdvo "Znanie," 1958. 45 p.
(Vseso1nznoe obshchesiv6 po"raep'rostranentiu, politicheakikh i
uauohnykh znaull. Sor.36 no.14)0 (KIU 1118)
(Nonferrous metal industries)
SOMOVA, S.Ys.,
AYAV, Oaziz Khismatovich; YANIOS, Ilik la XyglaqZ12h: NA
red.; HAICAROV, I.I., red.izd-va; UUbl-N, H.I-, tdkhd.red.
[Economic and cultural developnent of the Xszakh S.S.R.] Pastsvet
akonomiki i kulltur7 Kazakhokot SSR. m:)skva, Izd-vo "Znania,*
1958. 46 p. (Vsesoyuznoe obsbchestvo po rasprostranentiu pollti-
clieskikb i nauchnvkh znanii. Ser.1, no.40) (HMA 11:2)
(Kazakhatan-41conomic conditions)
;,jw
yAj,jjS. 11. DILIC, A. K.
V. I., na PO 1,
"Investigation of the Action of modif~inG agents in flotation by means
of radioactive tracers," a paper stfomitted at thie International Conference on
Radioisotopes In Scientific P~esevrch, Paris, 13-20 SeP 57,
SOV/1 37-58-10-20395
Translation from: Referativnyy zhurnal, Met;xllurgiya, 1958, Nr 10, P6(USSR)
AUTHOR: Bogdanov, 0. S., Podnek, A. K. , Khaynman, V. YanisN_1A..
TITLE: Studies by the Mekhanobr Institute in the Field of Flotation Theory
(Raboty instituta Mekhanobr v oblasti teorii flotatsii)
PERIODICAL: Obogashcheniye rud, 1957,,,Nr 5, pp Z5-28
ABSTRACT: A brief examination is made of the major sttidies conducted
at the Mekhanobr Institute in the field of study of the physical
and mechanical foundations of flotation and the reaction between
flotation reagents and minerals.
1. ores--Flotation 2. Flotation--Theory
4. Minerals--Chemical reactions
Card 1/1
M. M.
3. Reagents..-Chemical reactions
YAIIJIS; N. 0 (Meldianobr)
"The investigation of various flotation modifiers for non-sulphide minerals
with the aid of radioactive isotopes"
repr PrOWOW at the 4ft SaIgmt1fle and TeabUIC&I Smajou of t1is lbld*D*r
IWtP LealnSMAR 15-1.8 JTW4 1958
MIKHAYLOVA, M.S.; KHAYNMAN, V.Ya.; YANIS, N.A.
.Z~~
Use of liquid scintillation counters to determine the sorption of
flotation reagents. O'bog. rud 5 no.5-.28-41 160. (KM 34:8)
(Flotation--,Equipment and supplins)
S/137/62/000/005/022/150
A0061AI01
AUTHORS. Bogdanov, 0. S., Haing Wei-chung, _Yanis, tt,_A,_
TITLE: Studying the effect of sodium oleate and flotation modifiers under
conditions of flotating beryl, spodumene and fluorspar
PERIODICAL: Referativnyy zhurnal, Metallurgiya, no. 5, 1962, 7, abstract 5G42
("Tr. Vses. n.-i. I proyektn. in-ta mekhan. obrabotki poleznykh
iskopayemykh", 1961, no. 128, 26-36)
TEXT: Results are given from investigating the interaction of beryl, spo-
dumene and fluorspar surfaces with oleic acid (I) containing radioactive Isotope
C111, ferric chloride with pe59 isotope, and H?.S04 with s35 isotope. The quantity
of a reagent sorbed by minerals, was determined on flotation products by direct
measurement of the radiation Intensity of the mineral powder. To measure the
intensity of preparations 1, the method of scintillation reading was employed with
the aid of liquid scintillators. Flotation experiments were carried out with
a laboratory mechanical-type machine of 160 ml volume, at 1:8 aalid-liquld ratio.;
The studies were appli6d to the existing acid and alkaline schemes of separating
beryl. spodumene and fluorspar. Prior to flotation, the mineral batch was mixed
Card lp
S/137/62/000/005/022/150
Studying the effect of sodium oleate A006/AlOl
in a cup with a solution of required flotation reagentn at a given liquid-solid
ratio. To study the naturecf I and sodium oleate (II) fixhtion on beryl and
spodamene, the method of infrared spectroscopy was used. The joint proceasing of
the minerals with reagents was performed in a special adsorption column. As a
result of investigating sorption of I and II; the effect of p1l; processing with
IIF and H2SO4, and with a mixture of these acids; process-Lig with NaOI1, on
flotation of beryl, spodumene and fluorspar, and sorption of oleate by their
surfaces, the conclusion is drawn that during the interaction of II with beryl,
spodumene and fluorspar, both physical sorption of I molecules and chemical
sorption of oleatei ions take place. Highest sorption capacity is shown by
spodumene, which corresponds to its better flotability. Optimum beryl flotation
and sorption of beryl oleate occurs in the neutral range; and those of spodumene
in the weakly alkaline range. The activating effect of HP upon beryl and of
NaOH upon beryl and spodumene, is predetermined b~ more favorable conditions
developed on the mineral surface for the chemosorptional. fixation of the ion
collector; this is connected with the selective dissolving in HF of silicate
groups. Beryl depression, non-activated and preliu&mu* activated with HP, after
processing with H2SOIJ is explAind by reduced sorption of the collector and its
fixation prevalently in molecular form.
L. Glazunov
[Abstracter's note: Complete translation]
Card 2/2
. ..... RAR
S/08'/12/000/001/027/067
B151/001
AUTHORS: YLikhaylova, N. S., Khaynman, V. Ya., Yanis, N. A.
TITLEt Application of liquid scintillation counters for the
investigation of the interaction between flotation
reagents and minerals
PERIODICALs Referativnyy zhurnal. Khimiya, no. 1, 1962, 302-303,
abstract 11155 (Tr. Vses. m-i.i proyektn. in-ta mekhan.
obrabotki poloznykh iskopayemykh, no. 128, 1961, 37-44)
TEXT: A description is given of methods, measuring equipments and results
from the application of scintillating soluti)ns and gels. These methods
make it possible to increase by 200 - 250 times the.sensitivity of the
measurement of isotopes with soft ~"-radiation, on the surface of mineral
powders and in dilute aqueous solutions. This method opens up now
possibilities for investigation and also makes working with such radiators
safer and cheaper.'(Abstracter's notei Complete translation.j
Card 1/1
BOGDANOV, O'.S.; SIN VEY_CHZ11UN [Hsing Wei-cbung]; YANIS, N.A*
Studying the action of sodium oleate and flotation modifierz during
the flotation of beryl, spodumene, and feldspar. Trudy Mekhanobr
no.128:26-36 161. WRA 15:1)
(Flotation--Equipment and supplies) (Beryl) (Spodumene)
RAZUMOV, K.A.; SIN VB'Y.-CHZHUM [Heing Wei-chungl;_YANIS, N..&.
Effect of~calcl= Aid iron cations on the flotatiol'i of beryl and blotite
with a cation collectors Obeg, rud 1 h0,3:3-5 162. (MMA 164)
(Flotation) (Catifts)
A, -J,
YANISHICYSE-AYA, I.
Polish vown, builders of a better future. Yesm.prof.drith.
no.8:37-39 Ag '57. (KLRL 10:8)
l.Sakrotarl TSentrallnogo soveta profsoynsoT Pol'shi.
(Poland-women)
YANISBEVSKAYA, I.A.
I
Alkali and nephel-ine syenite, in the Hatyr section.. Mat.po-
geol.Zap.Sib. no.64:160-173 163. (HM 17:4)
I
t , i., z I ~ I i A-.- I
ISILW5KAYA, M. F.
YAN7SHF,VSKAYAj M. K. - "Microflora In Pneimonla 6f Children." Tashkent
State Medical Inst Imeni V. M. Molotov. Tashkent, 1956
(Dissertations for the Degree of Candidate In Medical ~;ciences)
SO: Knizhnaya Iotopis', No 9, 1956
S/0 16/60/000/06/i4/0r~:l
AMOM Samsonov, P.P. and Y&nlshevzkaya, M.N.
TITIE-. New Varieties of Shigella Djzenteriae In T-AshRent
PERIODICAL3 Zhurnal mikrobiologii, epidemlologli I immunobiologli, 1960, No. 6,
pp,- 52 - 57
TEXr: Fifteen.mannitol-negative strains were isolated from dysentery
patients aDd carriers in Tashkent. Although similar to Shigelia dysenteriae
by their biochemical, cultural and morphological characteristics and their
,V/
ability to provoke specific kerato-conjunctivitleb in guinea pigs, they did
not agglutinate with any of the specifle dysentery antisera and were therefore
classed as atypical Shigella dysenteriae. They appeared rel ated to Shigella
ambigua. Ihe strains had a distinat antigenic structure and constituted an
independent serological group with sub-groups. Further research is needed
for precise classification of the strains and to determine their pathological
role. There are 2-tables and 12 references, 10 of which are Soviet, 1 H-.mgarian
and 1 English.
Card 112
,9/016/60/000/06/14/051
Now Varieties of Shigella Dysenterlae In Tashkent
ASSOCIATION: Tashkentskiy gosudarstvennyy meditsinskiy institut (Taslikent State
MpAlnal Tnt:tltii+.A)
SUBMITT -~ June 16, 1959
Card 2/2
SAHSONOV, P.F., prof.jy MN_,., oosistent
Shigella ambigua. Mauch.trudy uch.i prak.vrach. no.2:15-21 161.
(MIRA 15:8)
1. Iz kafedx7 mikrobiologii Tashkentskogo gosudarstvennogo
meditsinskogo instituta (zav. kafedroy ~- prof. P.F.Samsonov).
(SHIGELU AMXIGUA)
UNISH,EVSKAYA.j M.N.
Haterials on the diagnoois of bacillaz7 dyaontery, Mod, zb=,
.Usb. no. 246-18 P 161. (KEU 34: 2)
1, Iz kafedry mikrobiologii.(Zav,.'- prof, P.F. Samonar)
TaAkentakogo gosudarstve=ogo maditainakogo instituta.
YANISHEIISKAYA. M.N.
Keratoconjunctival test in the detection of dysentery bacteria.
Nauch.trudy uchA prak.vrach. no.206-43 161. (MM 15:8)
1. Iz kafedry mikrobiologii Tashkentskogo gosudarstvennogo meditain-
skogo institute (zav. kafedrov - prof. F.F.Samsonov).
(DYSENTERY) (dRATOCON-TUCTIVITIS)
SAMSONOV,, P*Fop p~rof.j ?~~ILH "SRAj!!.N-j assiatent
Shigella ambigua in Taahkent. Report No.21 Serological abaracteristica.
Mod. zhur. Uzb. no.3t47-50 Mr 161. (MIRA 1425)
1. Is kafedry mikrobiologii Tashkentakogo gosudarstvennogo medit-
ainskogo institut4.
(TASHKENT-ZHIGELIA AMBIPUA)
WC
N.
M-S1TFV,SUj&,-M.~N.- DUBOVITSKAYA, N.K.; KLYUCIIRWA~ Me.; 141TRIKINA, P.Ye.;
PEKSHEVA,, M.N.; SAMOYLOVA, Z.Ye.; TYUNEYEVA., G.A,.
Diffictaties In diagnosing some atypical dysenterial bacteria. Mod.
zhur. Uzb. no.2t2O-22 F 162. (MIRA. 15:4)
1. 1% kafedry mikrobiologii (zav. - prof. P.F.Sanwonov) Tuhkontskogo
gosudarstvonnogo moditainnkogo instituta I labore.toriy gorodskoy I
rayonnykh sanitarno-opidemiologichoskikh stantsi3, Tashkenta.
(SHIGELLA) tjv%
(DYSENTEM,
AKHnWV'l N.A.;KLYUCHAREVA, T.Ye.; SAMSOROV, P.P.; XW*XZqKAYA, M.N.
Specific pbageo in the diagnoolo of Imoterial dyoentez7. Report
No,L Naucb.trudy uch.i prak.vraob.Usbo no*31151-157 162.
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meditsinskogo inatituta ~zav. - prof. P.F& Samsoncv) I Oblastnoy
sanitarno-apidemiologicheskoy stantaii Taalikenta (zave Sol*
Eydelinant) ;YSHNxm) (BACTMUOPHAaZ)
KOSOVSKIY. A.A.,insh.; YANISHEVSKATAjLY-.inzh.
Operation of tFz ~former oil. Elsk.sta.29 no.1:87-88 Kr 158.
(Insulating olls) (KIRA 110)
SHCREGLOV, A.P. ,inzh. A M.V. , Inzh.
Use of the trannformer insulating oils of munIcipal clectric
power distribution networks. Elek. ata. 35 nc.6:77-79 Je 164.
1. Leningradskaya kabellnaya 5et'.
IANISHLTSKAYA,LL~
Treat=ent of infectious polyarthritis of indeterminate etiology
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inst. kur. i fiziotorno.15:193-201 159. (141RA lj~: 9)
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A 05 1 /J.029
AUTHORSa Bozhevollnov, Ye.A., Yanishovskays, V.M.
TITLEa Aluminum Determination by the Luminescent Mothod
PERIODICAL& Zhurnal Vessoyuznogo Xhimicheekogo Obahohestva Im. D.I.
Mendeleyeva; 1960; Vol- 5, No- 3, PP- .556-357
TEXTR Luminescent methods for datermining_aluminum were developed in varl.-
ous objects according to standards of 1110 -1010-5%. The method suggest-
ed in (Ref.1) using salicylal-c-aminophanol for the deteotion and semi-
uantitati-re determination of aluminum was 1mvestigated by the authore
Ref.2). The sensitivity of the reaction wat evaluated as 0-05,y Al/5 ml
Z
of solution. The oPtim"m PH value is 5.6-6.2. The reagent is introduoed
in the form of a 0.01% solution in acetone- An a quantity of 0.15 ml to 5 ml
of the solution being analyzed. The proportional relationghip betvaen the
intensity of the fluorescence and the aluminum concentration is observed
prior to its content attaining O*5W in 5 ml of solution. Besides aluminum,
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A051yi-029
Aluminum Determination by the Luminescent Method
no other cations cause fluoraso enea in quantities of 251 in 5 ml of solu-
tion. Only coppor and iron in quantities more than 0.11 in 5 ml are able
to extinguish the fluorescence of the salioylal-o-phenol and aluminum com-
plot. The sensitivity of the given reaction dependa to a greater extent
on the purity of the applied buffer solution and as a result of its puri-
fication lby the chromatographic method using the co;:plex-forming agent
2921,41-trioXY-5--chloro~,19"#I-azobenzene-3-oulfo-.aci~ (Ref. 3) It to possible
to form a buffer solution containing 5*10-'3~ alumiwam in it. Such a purity
in the buffer solution yields a sensitivity of the resotion of 0 00251 in
5 ml. The baffer solution is purified by introdueiag 5 ml of 0-;% of the
above-mentioned oomplex-forming agent to 100 ml of the solution being puri-
fiedg and this is left to stand for one hour, eo that the internal aomplex
formation of the cvmpound vith aluminum can take place. 20-25 1 of the
buffer solution can be purified on a ;,olumn having a volume of 20-25 ml-
The ~VL*3-10 (EDE-10) anionite, which fills the column, absorbs 2,2194*-
trJ.OxY,-5-chloro--4,pll-azobenzeDi-3-sulfo-ao-l~d and acquires a Urk brown
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A051~J-029
Aluminum Determination by the Luminescent Method
color in the top portion of the column. The distritution of this coloring
doyn the column In the purirication process is the c.riterion or the degree
of anignite ooneumptign. When the colorleae zone of' the anionite becomes
less than 3 am the anionite in the column should be replaced by a fresh
bateh. The addition method is used in all cases due- to the extinguishing
effeot of copper and iron, which onables one to perform the analysis with-
out first eliminating copper and iron from the solution being analyzed.
the increment of the fluorescence ititensity was dete,rmined after the intro-
duction of a known quantity of aluminum into the solution and the unknown
quantity of aluminum was determined from the intensity of the fluorescen-.e
of the solution in 10 ml of solution according to the formulat
LC
AI(Ix' I'o)
A17/1 0 ml - -- Y - - -1 9
60 x
Al
where AC Al is the quantity of Al in Y introduced Into 10 ml of the ana-
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Aluminum Determination by the Luminescent Method
lyzed solution; I x is the intensity of fluorescence of the analyzed samplej
1 AO is the intensity of the fluoreseenoe of the i;olution with aluminum
Al
introduced Into itj 1 0 is the subtrE.cted value of the control test. The
fluoreseenoe intensity was measured with a YM-2 (Ulf-2) monochromator,
49-M
where a 4t>9Y 19-M (FEU , ) photomultiplier was usad as the emission re-
oeiver. The determination of aluminum in sodium ao&tate was performed
direetly In its aqueous solutiong &I ,'ter the pH was 'brought to 5.6-6.0. The
analyzed solution was bri~ught to 100 ml with waterfour 9 ml samples were
removed, into two of which additionji of aluminum were added in quantities
of 0-05 and 0 -08 iato the third ample - 2 drops of 0-05 a solution of
trilon B. The voLme of all four sif)llutions was brought to 10 ml with water
and 0.3 ml of a 0.01% solution of salioylal-o-amino-phanol was added into
eaoh. After 60 min the intensities of the fluorescence of each solution
were recorded photometrically. The percentage of aluminum in the sodiur
acetate was calculated according to the formulas
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Aluminum Determination by the Luminescent Xethod
Content of A'lq % . ACAI(ix-;T) where X is a weighed portion of
X(I I )-goo
x
Al
sodium acetate dissolved in 100 ml of water; I Tis the subtracted value
corresponding to the solution with trilon B. The determination of the alu-
minum percentage with an addition-of aluminum of OiC-5 and 0.08 1, did not
deviate by more than 20%. Aluminum was de+ermined Ja acids azid hy4rogen
peroxide after these had been evaporated. Neutral calts were added in order
to ensure a complete transfer of the residue to the buffer solution after
evaporation, The.determination of aluminum in hydrofluorie acid can be
accomplished only in using acidic decomposition of !;he residue after evapo-
ration of HC1. Table 1 lists examples of aluminum determinations in solu-
tions of HClp HNO39 HP H 2S0 and H 0 . The determ:Lnation error did not ex-
ceed 20%. Table 2 li;ts ex imples 2f2&luminum dete=ination after prelimina-
0
ry introduction of Al. Table 3 lists the degree of agreement between the
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A051/A029
Aluminum Determination by the Luminescent Method
results for Al-determination by the two methods on am example of HF analyses.
There &re three tables and 3 referencess 2 So-vietq 1 Czechoslovakian.
ASSOCIATIONs VNII kbimicheskikh reaktivov (All-Union Scientific Research
'Institute of Chemical Reagents)
SUBMITTEDs October 219 1959
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