SCIENTIFIC ABSTRACT ZHIKHAREV, YU.N. - ZHIKIN, L.V.

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December 31, 1967
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SCIENTIFIC ABSTRACT
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" ~;:f I : I- " 1~ - IA-, " : I : 1. L ;.~ -f i !w 1 ; . ; _i F. I i# 111 iI II IIt f~&4. : I I.: "Ir. ill-L- , ~ 1 i 1; II. I I S.I., red.; SALUKYADZE, V.S., red,; ANDRIANOV, K.I., red,; VASZIYIT, A*Ye*# red,;--~~A ~G.P. red.; KRYLOV, P&I.p red.; KIMONDM,. G*L* red.; KHRA INg F*G*q 7ieds (deceased]; CHO ISINOVj MA, red, Prinimali uchastiye: ANUCHKIN, R.P., 'red., GRIGORIYEVA, M.B red.; ZHUAKOV, V.I., red.; KALTUZHNTr, N.G., red:; KMRSM7N, Zj red. KOZLOVSKAYAP A.A., red.; LAYROVA, N,P., red,; NUSOV, G.I. red.- FALI- 131VIOH, A.S.q.rq4.;.YWSHO.V, P.R.,.vq4uahch y red.; MOT&A, tekhn.red. [Safety regulations for qonatructing steel pipelines] Pravi1a takhniki bezopasnoott-pri ati6it6l'ot*.M'glattallnykh.stallnykh trWaprovodqv. -Goo.nauobmb.~tekhn..izd-vb'neft. i gorn -.t -x7o 9 Hoskvaq, 0 OPlivuOi lit 19PO 21 p0 (min 13:9) I I .~ -v.4 , I 1. Russia.(1923- U.S.S.R.) dla4zid ravleniye gazovoy promyshlenuosti. 2.-Vsesoyuznyy n Iauchno-isqAd~,v I y6 up atqUskjy inotitut tverdykh splavov (for Anuchkin, Grigorlyavai-Zh ov~'Xalyushnyyj Xamerahteyn, Koslovskaya, Lavrova, Nusov, F 11 3b, tPipqlinee)--.- (JAdgetrial-- safety~ V)A;) 0 311 AID 985 EntdLra 'MS: CONTAiNMG FMMOCENE- AAr)rcA I-S (M, qR) Tjft~o-- 1. X. K. D. Z4Mariwa.- and F. Z. Rodova. Zhurnal obshchey khimil, v. '33, -no. 3, Mar 1993, '798-804. s7o-79163/033100310031005 ThefoUlowing now compounds hav6 been synthesized: 2-methyl-6- (1) (mp, 1,55,C) An q.S-bo 21.1% yields and 2-mathA-6-fer-ocenylbenzothiazole (11) (mp, 185,C) in ,"14 to 27116 -~Ields;-vnd bip-0-im ethyl - 6 - (M) (mp. 240*0 in an 0.3110 yield and bis(2- :-methyl-5-benzothia-z*l,)Imn-on~nelM (mp, 26rc) inan OAT. yield. The synthesis was accomplished hyithe reaction of ferroo~w vAththe 1) (dim ethyltriazeno)benzothia- .:moles:, 2) benzcFth1azdj3ddiP-'z*nium P.)Alorides,-. or 3) benzothiazolyldlazonium acetates* 1/3 Z' t 7-7 IV t j_ USZ20 A ADI ~. A !D 985 Kflv*&~branch of the'Donets Institute of Soviet Trade a v! Vne 'ns"'u.1e )4 ant c Ch e.-n:' 9 eq 'i-h e rea c, i e~ 7 7--. e: t- 04 -C' as were formed 1-n al~ *-hree cas ev. Th e I- V !i e c t r a (-f 1. 11, '4 M.-and fV contamed a band Ln the 400 to 300-m4 rAnge. Compouhda 1, 11, 111, and IV were converted to the quaternlfy salts from -%vhich in -Lirn th,! following thio- carbocyanines and dtmethy1merorvarines were synthe-' sized-, 3, 3' -diethy!A-5. 6'- (V) an,-, 3, '7'-diethyl-3' -5-"-diferrocerrylthiacarbocyanine iodide (VD~ and 3-ethyl-5-13-ethy' .6- (VII) and .'3-ethYl-5-(3-ethyl--5-terrocenylbenzothiazolinyLidene-2-ethylidene'tZ-thiazolidir,e- thione-4-one (VM-)- 77be optical and photographic properties .),' V. V1, VT-., and VM'were studied to determine U their possible -use4as pliotosensitizers and 2) the ,-degree of -conjugatilondf the ~5 or 6-4errocenyll substituents in tne benzothiazole ,xing -with the bagic polymethIne ichromo?hores. 11fe.absorption maxima of N, VI. '_IM, and VM -were -at -SOEL 222~ Z43 and 535 -mli*. res ect.1vely. indicating that the--.; P V3 PMDEMO DUB GONTAMO MROCENE RAMC= (USM) AM 985 :#ia~ima In -these compounds shth ed'towmrd ;long wavelengths wtth r espec~ to the gliacarbocyanine a arid -mer'ocyanines containing no ferrocenyl substituentS. A greater/ 4athbchromic shift cyccurr ed -in thL, case of thiacarbocyanines ~-onta~,!-ing r, S'- than in those -with 5, V-ferracene substftuents. Compounds V, V1, VU, and VM are Stable dyes, soluble in alcohol:and benzene, and differ little in properties from the unsub- I.stituted thiacyaninm- lnadditlon,'.Co'ndensation of formy1ferrocene vrith 3-etlh-111-2- I :methyIbe=othiazdHum Sorn-Md tht-'de-ep =IorO_d diri~e dvf- TKI',i;_-- .801 mp. The deep color of IX Itivia-dhaa-ge -U-an6t= -to Ibrie =ethine Z=upa And -%,o theroyalopen-.~Ai or.,v, rings. V3 hj" 1 1 -,lI j I I '!. B/079/62.,"032/011/007/012 Investigations of the chemi:1'3try of ... D204/D307 ethyl-~5 I -Lbefizothia~ol7l-(211) befizothiazolinilidene-21 ethylidene thiazolidinthione-2-one-4 (compounds VII and VIII) were prepared by disso.Lving III and IV in absolute ethanol and:boil- ing for 30 minutes at 1 OOOC 'with 3-ethyl-5~-(acetanilidomethylene)- -rhodanine and triethylamine~* Compounds IX, 2-(f,-dimethylaminostyryl) .'..._6-[benzothiazolyl-(2)] b6nzo thiazole ethyl.p- luenesulfonatep was synthesized by boiling III.-for,20 min, with 17-dimethyl-aminobenzal dehyde and acetic anhydride. Substitution ofbenzothiazolyl radi- cals into 5P51 and 616-1-positions caused considerable shifts of the absorption maxima in the direction of longer wavelengthsq.the ef V, feet b6ing stronger for 6g6l-substituted.thiacarbocyanineEis Alcoho- solutions of thiacarbocyanines. containing 5951 or 6,61-substitu- ted.benzothiazole radicals fluoresce more strongly than,the,very .-:,T--atrongly fluorescent 6t6l-di6trylthiacarboxycyanines, There is 1 figure.and 1 table, ASSOCIATION: Institut organioheskoy khimii Akademii nauk Ukrainskoy. A SSR:(Institute'.of.Organio Chemistry.# Academy of Scien-, ces of the Ukrainian SSR) SUBMITTED: November 20, 1961 Card.2/2 S ITe.] n, 5 SOV/79-29-.8-25/61 AUTHORS:: Samokhvalovp 'G. I., Vakulova, L. A6# Men, T. V., Zhikhareva,L.T.-I Koltunovap N. Iop Preobrazhenskiy,,N. A. TITLE: Synihietic, Investigations in.the Field of Polyene Compounds,-, XV. A.'.Complete_Synthesis of Citral PERIODICAL: Zhurnal *ob s hchey khimii, .1959, Vol 299 Nr 8, pp 2575." 2 578. (USSRY: ABSTRACT: Citraljs ..the- initial product for the synthesis of.vitamin At the carotinoids, and a number of fragrant sub a tana e 9. The tranisiti.,5n.of, compound (1)*, which was also synthe sized by the: authors#'~ from acetone and acetylene (Refs 112,3) to citral-has so far been carried out by condensation with magnesium bro:mo- ethoxy~-acetylen6, partial hydrogenation, and saponification of the resultant I-ethoxy-3,"I-dimethyl-octadien-296-01-3 (Ref 09 as well as'ace-ording to reference 5. In the present paperthe synth.esio.of citral from (1) is carried.out without organo-metallic compound according to the given scheme. Othero- wise compound (II) is formed when using the easily accesuible tetraethoxy-eilane'in the presence of orthophosphdrio-acidt Card 1/2 a small quantity of p-toluene-oulfonic acid, and 0.3 mole of. -heptene-5- -methyl one-2. . 1 1 J: A - ft tf;:! ~~ .1, ;.,~ li ~ . . I i ~t ~3 :;~ I ~-., - 1 i fj t ~ V I U, 1" 1 W [ .I, .. p 11M VM i ~ f", I, I T A~t~l - q. - - I I ~~ ~" .1, u . tl- ,~15 qlvp;j~;, i :- . lev, To -i$., 1 Ru I * .I . 1: 1 ill: ~ . 1- AR6016170 SOURCE CODE.-. Un/0058/65/000/011/1)003/DO03 AMMOR i ~.'Zhikharevs Te,l 11 _31500-66, En(1)/Vq(m)/EWP(t)/ET1 - IJP(c) JD/AT_ ACC NR: :Ar6oimi SOURCE COM UP /0053/66/OP-0/004/0724/0727i AUTHOR: Zhikhar , =P T. V, ORG: none 1 TITLE: Resonant phenomena in elastic scattering of electrons buy helium atoms. SOURCE: opt i1o i opektrookopiya.. v. 2o, to. 4.. 354ap 724-727 TOPIC TAGS: helium,, electron scatteringp elastic scattering, electron energy lev-11 el,.-scatt ering cross section's ABSTRACT: :This is a:continuation of the first part of the paper (Opt. i spektr.. ve 19 851.,11965) and consider -3 1 $ s the neaj~-thrcshold behavior of the cross section i- for elastic scattering:of electronL~-by helium atoms with account of the 13,S-23S and 11~S-23B-2-S coupling of the He atoms.. The calculation was made in the Born approximation for the reactance matrix, For a better extrapolation of the Born- Oppenheimermethod o the low .40 t -energy- region, the aut r used V. L. Ochkur.'s methodt (zhETF v. 4 734, 1963),of separating the principal'term of the exchange- 5, scattering amplitude* Tables of the matrix elements with- and without allowance exchange) and plots of the elastic scattering cross sections are presented. i,The results explain the second resonance observed by Co R. KtWatt and J. A. Simpson Card ;-UM: 539.186.2.001 1 1.4 I. t 11H. 13 1 HUI tv At, IM) 13/137/61/000/012/140/149 A0061AI01 AUTHOR: Zhikhareva,'-V~ 1, TITLE: Determining'aluminum.l.ii2~,chromium steels by. the complexometric method PERIODICAL% Referativnyj zhurnal, Metallurgiya, 1961, no. 12, 3, abstract 12K17, -06 tZ,.'1U1ci.: n,,~,i. in-t metallov", 1961, no. 7, 285-288) TEXT: Vo deItermine Al in 'a teeI wIithhi-gh.Cr contents the metal batch i a iissolved in H2SQ4,(1 1 10) ~ and oxidized with WO The solution:'Is diluted' with water aqd- Cr Is oxidized with ammonium pe.rouliate. Furthermore, Al, Fe.0 Ti,, V, 'phosphate-Ion and partially Mn(0AW 2 ~aree-slngled-out by ammonia. The precipitate is.boiled together with,the solution, filtered off and repeatedly washed withwater containing-~some drops bf,WH40H. The, precipitate is washed off the filter into a container and dissolved in HC1. Separation of Al from Fe.~ Mn -and.T1 is'performed with a 20% KaOH solution. The preoilpitate is boiled with the solution, placed into a 500 ml retort and filled up with water to the mark; the aliquot'portion.of-the solution Is filtered into a 250 ml retort, by throwin& off the initial,portions. The filtrate in the measuring'retort Is transferred Card 1/2 1;4-~ 1, EMENERM , I iWl - 1,13 1 r , i,. I ;l- 6 : , ,l I I , " I ~?. t, 1 .111' 11111 ~ i I 1~I 41k. i I - I " V~l 1 ", I " I : i -11". Ei 1 1 t, ~ g :;i:l f I i ~~ . i ~ I I &I I'I i I t ~, " ~ E . :~,- .-~, I I i It i I,' lfjlij~f I I I -:"AHN I i:I : , ~ L . - . I . . ~, * v 11 ---~ 1 , -, -,j I , I I I i ~! 1. ~ 11 ,~ - 1, "1. f di 1 lfli~ I lfl.~ ~ ET" iil OMNI ~P I t I MIM i I ? I ; ; i I Oil li "MINITHIT 11 IN: IMIN!'11IL11. +m :, A; ". 11 1 ~ I. ~ .000 00 0000 a***#* #0:0;0099 00 0 0 0 0 *00 foe 0 9 0 O .1 1 9 6" 0 It 9090 239UNI P It 41 41 a 0! as a n r* 6 1 C 0 D 6 4 $9 L 2 W 0 P9 It I I W , g JIM-_" - T AND PWLKT f 74 VVrWl k8f) ANO #1A 90141 AW"011 10011 - -tier'"10 -04 V I 4 0 ~ 4 _4_ ; Ova 0 OR At ook "mr-k P. aL -PROOF AND KID M .' t L G.. ANWACT r. deal. krram. Gel., It rNODUM "as TROM axon. Iff lti ir 00 f Virdix, NA(m. 7hor.. S. Ill 104 *t, are dut to tile 1)(Tilgralifln -AS t of the c I IM am t M. Of Of ~ the raw materials. e.g.. firint; tile grog allil dtirills the 1 IMICk. the roAnUFMCIMM Of the Mulfte products without grog 14 conddered. Conclusiom are as follmn: (1) Refractory factu"'i without V prothfall, brick, etc., m be manu 09 'fl f b i 2 n ar. ietnanu y heat Ily adding clay nmde lean ng. ( ) deh dration h( th d i l F b h i o e re or te ent lure can. e mcc an y, y the clay. a drying druen can be u-ed. 43,? 71w drying 0 onwtaary~ (4) It is Unurcmity to ItAve rornplicuted 0 and expensive cquiptimot for preparing mistures. 5) J, 9 . The material mt of the prpdttcts it ill be lower. 11 00 a 00 it 11100, mit doov Car 91 all W WAS et 1u X TT t 0, 0 0 0 411110a IND. URI it IVA 4' A 04 0 3! At i -w a- R* 9 z 11' 1 "s, .10 0 0 a Wo 0 0 0 0 04 0 0 0 0 0 0 0 0 0 0 0 01* 0 0 0 0 0. 0- q * o 0 0 oiit 94 OIL- 2 Aar the dly 'Ailt".- 7:- .-V as k* day, 9 tog is ~Ptl bi [a viib Alto Vt 1 0 0 a We NO 0 f 4 11 a u Lu, I -I-." .I ILIA it IT INS ""OS. r--oe lot 40* 0. 0", L. x"101, OOWPWW I 11,~t t= -lartstipil" in M. Old 00 9 W - desuibcd. Swil" twap" (19-M "i4imp Wkset t for IDS Momurt ThIPWO& With= -Mbly of a tk C11" Wfth Owning point(I fir Ow. qwwts, tot$.; 00 4ust *Aft OW 0 O'C mish/sq. CM.- K be isied, Compa. d ths mitsill 1110* mw of .."to Z 111100 1 1$- H,.Wg'bda must-poeam a Wra~~ d OA,Uada ton "., It mint be iis-, wthM*cOb(fm6'eWb*fOkwx ==got tLIrd&d aw the saw ItMvAbeh ke, the wbdk ww a nhlS,., - ~C-*Msuww "A mct*g *Ape. Lind tat re4uIrcuMLS: 001 g4 IntgrW d1w.81torthit Coo g. a. stdaslovay see ot fit 60:4 fig I.. !!1AL11*4!jA1, ~1!~e - I . WOO S&Aoiso p$ Masi All 04Y aft, *JIASI ad 04. Aft W, I Od 9 9 a 0 2 0 V is 00,o * 0 0 0 00 0 0 0 0 0 0 0 0 6 0 0 0 01 :1P ~00010 go, ~106ifl ! ~160 -- - - 0 0 0 :10 00 0100 000 40 000 * O's 0 0 00 0 00 4 0 0 0 * 0 0 0 * a 0 0,111-0 0 04*41i'WO44-0 0,--,- 0.00 .0 0 0 0 0 0 0,401 0 0 * 0 -0 1. 0 -4, o, We 000, 00 0 p IU-N . 1 :1 R "0 4t* Cape A F4 40fitIVO& AU 1"M-Mcfs ion BudWko v P. P"Zbik "d LaWs. S. D. it MAT$941ALA Mir A A lit (witifs Full $0111em AtTrItly PROOMION, Chew (U.&S-R,). 7,; 13W--,3 1104)~-llw hfkk 11141uld 00 0% palorm vk1th the frAlow- 4 'AhOsotudshott1da 140 kg.laq. em.. hftt, ing Vedficmtjoft~ - CrUdring J-d 4 rermforinew (1) < Corte 32, Coarimenceine"t of defumna-, lion under a lmd of 2 kjdsq~ ens. at Mill, shtinkair m 0.- o0 far.at t'"91 1. 0.11%. absrwpti%v eAlkicity f(w refiring fm t 10.1vteife and Chr volive-Imegimdoe brick Cilhitut ijnmujj~ .1clary (1). to too Pm! a Itt j VA -9, 0 0 -0-0--o - :0 ~ 0 0 00 a 0 wwo o -0 671 .419 A 0# A S-A-L-L-A- I * 4 Tt A A-mvpMAN of ioto "b tot tomd" fws&m to as 0 A ZhIkh i h . . o" c and R. V., Lukun. J, c 7(% f6*"Yl#X; Nb. M. C. A. Off l OC 1 .6# so o a AA 0 go* 001 SO 0 LMNATUNg CLAsSIFKATOW jj7 44t NI so ;7jp v 0 S tW 11 V1 'a, W. '3 1 :eL f 010 o 17-w- a - : :_: _a 1'# 0 0 0 0 0 0 e 0 o 0 o 0,0 0 a 0 4 0 0 0 * I *49 0,0 0 0 is *,a ago 4 *goo a 0 4 4 0 0 C. kof a a a 0 0 0 0 0 0 0 0 a'4 *'a 1 0,04 0 W- a 0 4 0,41 x If If a Id a a 0 IS a 4 a J-k P-00cel"S A-0 po"JAIII$ MCI I a 0 :a dd4u mAterfals. C 11krGill. got hikhas VIrunif,J). -KiVin. L NdiJ gopam Kistomit" 33, 113 pp (Ims). .0* ~-A wim of ratimal mgthods was dtvrk4K41 for dog. The , i MAY. Of Umfift fu AcWs. and for roc"Uring thtir d.. The, %wk was bamd.ou the XaMuner.Barts usethod moplL., mentod, by (a) diWiving, the, tiny suffuric "" by 0 ago hrftk~i tbm on a water bath (6) neutralkims I'add ' grain VW" thyl A tratgd with 11M.) 14 (IIA PfM-MV U(MT use ormulp (c) mutralfaing "'alkali" grahtA (Vains trta(rd see, 'with aC(h) in the presmt of phentilkhthakin, Kou"dy 000 too so goo see, 100A "I ISO* A 'low iM111WIF L*v )kill No a a U a 4! jp or O'b a Wit KtIff IfN YA a* 0 0 a 0 00 @is 0 0 so* a a 0 0 0 4 -~~4 : : 0 SO a 0-41 *-a 0 0 4,41 0 0 of got-* 0 1 1 v if- it it If " it, 0 0 k v a 0.0:0 a 11,ij Olle 8 FROCISSIS AW WOUSM) -tits Zhbdnm t*h and S. D. Lukm. 1. Ap- jww CAA-M~- ~' M-Mo9w),S11"M .1 the Campo. M(31% 6346-M.M (nevlj 9bove 70 0) AIA ,I r1c, Fqt% 145-IM. CAO 0.76-0.90 OV 'IJw* MOISIAMt tbX4 Mtt&Hk StIrMs. It Issftow W ww* stkm the "Utocs is Iu tog. of tberaw expumm ot cost km can Ow fttvnic% alouki to taken Into ConsIdeftil". Tbe nulaw of stwws dOU14 be Coveted wilb "bWas st points of contw with awl Tim 0: ge 0 lot" L stlitiVIRMAL LITINAURI CLA$WKATM 40 law 111#4100 =w wavo -to an# Gift. Ai I 10 Od 0 ANP 4~ ).1 0 'u a AT 00 Att" iM A 0 46 0 0 4 00 0 0 fee of v a.- 0 we 0 00 0 0 go *I* o o * 0 0 0 a 0 v 0 to 9 0 aro W V1 H X L CA "l - - Ott AND " 1,11M11 too AN* d14 "no 404401 AUTO" 1"01111 *ATINVALO OWWAV offiOAL; and Fe ' =1 M k -TT96 CZXB.Vrg AND CONCIRS. VROM A lo, 111 sea votnuffe aANL. ~ Vkraia. Na&vk.-)ijkdaPekJ. I*A Otitew 0 SIR 44, (50-010 (INS).-Ratensive, ' d l f d l t d i l uct on o o om te c tests an repor e an the pro inker. d h l1 h d b d b d li d d h d rau ca ar toe on t urne . an an e urne , on y y oothe' Dents andconcr es roduced from It Workin . e p g asturriptioA that such a clinker is stable in the pitst, ce of &.00 0 'MOs tricakinut a ' I il id llicate-periclam stud COT twits or aluminitte at li b ed f d lt k l k It 04 oft a m ar os with the ad n er w= ora urn rom var o es a. c m ditiou otchmme Iron orv and citiartifte. 71*' best of these expefimental clinkas was produced from dolo- l 7 h i 2 d f mite rom te 0 an . it was re 5. c quartifte b9o ractory alt 1M* and at a pritam of 2 kj./Fq. cm. the initial del- - ' temperature was HM Otad the final I" . A P of 7be clinker consisted o(SA C&O.7723, MgO A10. and IIM, AIA;LI2. PtiCh 7.91. CrA &777". Examituition Pee 0 tlow of a tbin sectim betoreen M 40 H 3C Bi b M 0 cal nrk- &bowed a cm I ~92CO IR OW 0 AP" 0 - oo & % a out . h i j l i - 1 V . T e water consumpt on, sett ng thme and volume were sannal. After 28 days the resi casstanq of stance to cam- oo , pression was 300 kg./sq. cra, IU densi ty was 3.412. 11'a balialad ~~ ~Uburoed brick produced:. IN 0* from such dialter showed JIM geneW the pro we* Ir 400 fig" SIP145,00110 GMT OPS13"'N't 'V y ~ # __ Tki .k i_ 01~j;.110 4 -V , 9~ 9. 1_1 I T,)~* 0 0 0 We 0 041 0 a 0:0. 0 *_* W 0 WOIS 0 0-0,0 0_0_0_9r*~~ -1 or ip ropc4lifs am -flufff"" wool Ad 00 .00 6=4 4A "d" Miss gold , Aft 4 'A on MON. ili"L for So ;~Uf. 0l a rowoult an lou dMifuse bi nMMb# Vft M"'by swats witla P&OA drJ MAlk bM- td tar 10 to ~,M ftg at temps. up t o I U. F. R. . q1t. 4 ~jjjo WO,-0:6-6 O-O"ll 0-0 0-0:0 Wo 0- We 6~0.0 0 0 0 0 0 6 0 0 6 0 0.0,00 0 W141 ,6 41,00*449416 too* foe 0 * " " " , 4. '11 " 0 0 J - r POOCIMI AV ##W##ft1# twOt I i's Ahmbw Refractories md. TWr Possible use in runwm open'" Whit Oxyra West. 000 ns d It t h e a c . er .( S. At-ZhikhaftVi Henry Bru ' .00 F N fez " rom ANO, 1948, 4 Pages. WHO, Translation (Oxyjren), V. 3, no. 2-3. 1946, P. 65-66. Kislorad 4 . - - -Kith- - ,I i~ a refrac bes &velopm7ent OT -Alumin tatift aft basis of synthetic aluminum oxide. sit goo it for Refractories, Pyt-Pents Leningrad Institu rues of a 66% alumina blamt. some data on prope COO furnace brick developed at Institute., and on wml- dry proctax For brick to show resistance to abra. 0011 -deposition *tTects. so give war, and to carbon Me 0 , A O"AL1.061COL 1617CRATMe CLASSWWAV" __ U 71S x At scab K ~st 5, x a a W j 1 islo 0,1 6 0006* 0 0 0 o 0 1 i - $e 0 q 0 0 0 00 4 7 L71LO - 0- 0 - 0 - W-GA 4k- 0 0 000000 0 0 a A. 0 6-9 0 0 0 a of 0000600 a Soo fu. A's a v N 0 a of #t af-kv: a roLce'"s'AND Pe"Iffivots mot# - I - - : 0 r t i .. - ~ -4 0 di of UIS *00 of ttpresentative blast-furnace brick made In the V. S. 4~69 and In the Soviet Upion am compartd., Rm"lau bfick .00 are inferior to the American lwWuct becauxe of Interior a tmajecials *od backirurilum In tuanufacturint "v"m- "0o Tvi improve tht proevOM tl* (LAAK(URMUIlk-A WTO WMIC & properties and wi poctaftia. (2) tfft%t of lwv"utv on corapsonew of brick. (3) selection of optimum ratio lw~ iwern v~wd sny. and t4) preliminary treatment 0, see 4 00 charge. follovv n# sug". lona are madr: (1) Clay, r W: and part of the VM Ahwld be crotind Invo her. 12)Tul mills rot Vlading the components of the charge toltrther, should be Installed.' (3) Mr .Iowctful preafts should be 004 0,21 UW. ' (4) The Vft fraction 0. to 2 turn. should be ht(wed' SOW wparately and dampened before the ground mixture of too Fin and pan of the a" 1e added, I.Z.K. I ago 0 P IMP~o _w- ISoo C 44 7 to 4D X iA-fi4M11:jn##jATt logo &T rw o P1 v of 0 J3 4, 3 1 a bit 0 xv-ii:kil t! IN 46 A I U 0 0 01;:~ ; 0 0 fool* w* 6 0 o 0 0'o e 0 0 go go :10 0 0-0-0-0 : : : : 0 -.0 00 -- 1 0 *-0 0 0 0 0 6 0 *-* 0 0 411 6i 3 Kvtw4ae Im~i*;,uiwp-mm-il--;-4FW-Zwti3-,,~w44 a WAFF25ZAH I 9.~Tlf ME Ili MINRXII I w~WJIWNW -.11; !; ~ ok ,I, I . . at Wq-2 ME IF WR411 ?I U Fri V tit 13 -31 P -r 1 1111, V 66-VO gooses 0 F- VC-AF-4 $00 a 66 a too 009*016 1-j, a a a a IL V w ir L-- --k j '00 1 lip A p ELP I Kelm* W99111 W &to over Ir'll E- A use Of WA" do"" for, kili"mutim a"" z 0 11H# Pn"rW ftntal,11104 IP% Alsth (411maw -40 00 C too! tylw), 72% tooWlitip 41 "04 jewwwal" i type), UQ" H If mAx" W oft bon Aftl clay ~00 amt 4 Ift"A of clay or vuy tsvw kbow, cpiupmkkpn 0 the P" Whietkiii alumhu *M ^ .1k 2k miml clays! &NOW" W powd"vd atumbw mot clay see go fu Ino le" lb" 0.&1 j" 41116 OffivAle --. 6- mitt, tit dw 11ttil Aimmitittif to 40 to 141%, 111ch"llut N Ili 17% wire. lima P(MIN111J. IN 0 -0 tit by:mViming Itmi filtntrillts wm firod At Obw *W Sao of MIT, vAtalwa firw of foul't ww*"I It poroitity is MRAllis pirtuffth W Oto In OXI bs.,jew"S, am Mint Morift. 1144mindor2lill./m.tat 10)6 (1111140- In tlw cfw of Moro Als(h), P 10 sew J~~ Ain r(MMant L VOIUSASS dUlat watikV AlW_ ]&**. lh&pn go., 'To am Sit mhmt sbdvkkRp Ommki top Aml and Irl.1 for 6 to I hr. 0 1W. see At 1001 Pf Stbaptit MOWWA",00 44% Is OJ to 04%, 40-0 Vm"Ktrft~lk-* OVAtimm 'AnIf up"to M% At^ w"* an lot, low Itut tims"lly 91:2 (to 24%. foerk-Iml of 14* pri"iAlAtily 00 We of th"tinal t"o"m (21 in It"'14JO12 x lifts corAw-kivity lit "12.1; torotallift 61 twks After fifivir #A er", . . I III *Sk'abock OVIN (*If) Willa no tiffilthILlo" logo N hittitaittlam of viracU tiltirr I bralAhmit Orle (wattO with 6110411 WriShl JOS* ditirt 10 cycl" *#%I Shjr-j 1d,"4 ~Jfjtf if CyVk%, and St. to e *00 IF .7 014111 &A 0" Lot x 411f4ij if$# #4q Olt owl 19 'fm a it a I Sir a 0 El: u 111 jig, -0 111! of A v Cts 9, 1 0 0 a e so 0 0a se W- ionvi so -0-9 *'W-0-0~W9 GLO 9:Q 0 0 -so- 0 0 0 0 0 0 00 as 00 90 heol Abrinkow diet 2-4. 41 IM, I-V",, clit-cKst md6do a 1 7 1 4 4, 41 . all wvOinq 44ve Ir.4timl et. 1741110 amt IMOT, At 1 halw* dwww"I OwwOollity mo vh4" nee woo riot dr,O jr, awl &A#W anql plo ~ ham"i to hiwd;. at'INO . ouly %bow k&Vtng W4V thOl 1111% l od h k & m 4 kw f I m- arm Ow I e Il d". &w tdt t AIM, wm tint g ' dmvd relalIVOY WtWl Wavift W% AWhwO Ond it IbNI T"Jume chanvi arter*m as 174V v"d ISID'. but nMr of l1w v I wwwro ttutd I's lbo afth of sit oll. i r ast whe"ll am opm porodty to d deplie .1 w t of powiWir all Am"*k F"t""i to A to dN" 4*1 the MAI*. 00 W(fwttft uwkfw~M vW S6p" W It I % AIM sho"I lbt 0 w"alkit.vohmm ch~l, lWW ditmask"m on lbe b" suclacm . 40 1.3 to 13%. ~rmlpnwjurr "W%kilml of emodum chqiw . 1 -1 : - h l i : Women nal 0 % 01)" to 0,112) monj wit (cryslak -,so 0 00 , 4 6, i, - 0 0 400 0 10 sl P0, Ill 11-11RHH-di- 11 W U Alt~, I-M I dill ill i I ;;~ .3 11111 H F, 1.11! 1 11 ~Rll - hi ~] -1. IP14 AUTHORS., Zhikharevich) S.A., Geimank I.A., Kozyreva, L.A., 131-5e-4- 47- ~avev ~0, m~jls .3nko, R.S., Konetsidy, U,V,, TITLE% The Production'Teohnology of Highly Aluminoua Dense Prodnots Yffitu Using the',Dispersea Concentrati of the AktaBb Occurrence k delty (Tekhnolog3,ya.proizvodstVa vy4off-oglinozemistylen plotnykh iz a primeneniyem aktashakogo diasporovogo kontsentrata) PERIODICAL, Ogneupory* 15158, Nr 4, pp. 1755-179 (USSR), ABSTRACT: Experiments'showed that this diaperaed concentrats is not easily caked 4logether at. high temperatures even if previously f inely crushea. , Furtherip. the result of petrographic investigations car- ried out.by:.N.V. Gul'ko is given..An illustration jhows the prop- erties of:-samples f rom 100% dispersaa concentrate of the )Jct"hak occurTlence at a -pressure of 200 kg/=2- anl a burning tempereture o 17009. If 4-he disparsed co-acentrate Is burned twice its of up t quality is improved but the working process is rendered more 00M_ Plicated. EVeriments were therefore carried out in.,*hich, previ- ously bu rned sma f inely ground al-spersed concentrate is used &e.a. Card 1/3 dust-like component of the fire-Y19,y mass (dispersed f ire caay). The Production Technology of Highly Aluminous Demo. 131-38-4,10/17 Products When Using the Dispersed, Concentrate of the Aktasb Occurrence ~The properties of dispersed f Irv. cley and of such made of teanical alumina and, clay are: given in table -1. The characteristic of the masses and the'properties of the arrude samples way be seen fram b'le Further- table Zp~ and -those of sample-3 burnt at i5200 f rom taL more, an inaustrial quanti-~y of blast farnace brick3 of -the type D-2 was made. Thl- granula tion of the f ir-a alay is shown in table io of 4 mass and -hhe raw pmauata a showa and the chamoterist he re in table 5. Conolusionst 1.) By a Joint application of the dia- aal alundna it is.possible to obtain persea concentrate and technic highly alumino-w. dense 2.) The dispersed 4.uwinous pro- duots with a porcsity of less than 12% ha-ve a good stmoture, thv are of low penaeabilit~ f or amelti and gaaes, arA havc a vollme stability at 1500-1550 . It Is r.Accmendad to intensify the search for dispersed ores on the condition that costs are considerably n-, duced. There are I figures 5 tablea, and 5 references$ 4 of which are Soviet. Card 213 illi -MIT 1; I I 11! IRI;~ " 1 ! WMATII N, tq ~! !'I ~! I I f~ - , 1 ~ A.UTHORS: 1Zhikharev.ich,'S. -A.o Getman, 1. A., SOV/131-58-9-1/11 TITLE:.~ -Constant, High-Alumina Products Technology of Denseo,.Volume~ , for the _~Brick: Lining of Mast Furnaces (Tekhnologiya plotnykh. obl'yem opo.stoyannykh vysokoglinozemistykh izdeliy dlya kladki l domennykh pechey) 13 P -ERIONCAL:.. OgneuporYp 19 58 qi~ Nr go pp. 385 395 (USSR) ABSTRACT: The fireproof~brioks in the well of blast furnaces are exposeVto a longlasting influence of liquid crude iron 0 as well as to a static kept at,~-a temperature of 1500 , 2 pressure.of:4-5:kg/cm ..The conditions of the heat conduction, part of the well, are unfavorable as well..',Proviously, the bricke were'manufactured from, raw ka,olin,%but.they developed a considerable-shrinkage* For the improvement of1the stone quality a.significant increase of the Al 0 content.(within the limits 65-75%) is necessary. High~alumina products comply with these requirements..Table,I shows the composition and properties Card 1/4 of thehigh-alumina, fire-clay. From Table 2 the porosity, -_7 Nchnology of Dense, Volume-Constant, High-Alumina ''SOV/131-58-9-1/11 Products for the Brick Lining of Blast Furnaces density and shri~kage~,of the products under a press;ng force o :k f:1000 g cm' and a burni ng temperature of 15500 6. ta durat ion of 10 hours is,seen. Intable 3 the composition of the batch and.the. porosity of the raw material are presented.,'The influence of thefine-grained parts of the batch on the quality ~of.samples from highly aluminous batches a e, iv in tabl and the shrinkige in table 5- Figures 3 r g en e 4 and 4 show the properties,of,samples produced from this batch. Table,.6,contains.the chemical composition and the heat resistance-of.the samplesand table 7 the fire properties. 'In table,8 the properties of products which were manufactured in the testing plant UNI,IO,' are tabulated. The experience gained.in laboratory- and experimental work were introduced in the SemilWd PlOnt. of refractories. In this work parti- cipated: ~rom'the,Inatitute,,Ye.A.Ginlyar, A.P.Kochetova; from the plan't-T.A.Fitkalenko, I.A.Savkevich, R.S.Millohenkot Ye.G.Volodarskaya, Ye*V.Rachkoval S.I.Pedosovo N.V.Konetskiy and others (Ref ',I). In table 9-the granulation of the batches is given and in table 10 the pressing process. Table 11 shows Card 2/4 the properties of.the-bricks. Conclusions: It is possible A .Technology of Dense, Volume'-Constant, High-Alumina SOV/131-56-9-1/11 __ Producis for ~Blast Purnaces the.Brick Lining:of to produce..fireproof :highly aluminous bricks with low .,porosity and high~stability as well as with a volume constancy at 1550-16ooO. Th technological parameters e of this -ware are presented. Together with an inoreased golialty of the stones also theconstruction of the well must be improvedy in order to avoid a vaulting of the stones. It'is-'recommended to enlarge the dimensions of the stones In, order toreducethe, number of joint. There are 4 figurest 1i tables and 4.referencesp 4 of which.are Soviet. ASSOCIATION: Ukrainskiy niuchno-issl 'edovatellskiy institut ogneuporov .(Ukrainian Scientific Research Institute of Refractories) Card 3/4 1 r1l ll I ~, ", i f 3, IN I "N A I I i t . I I - ii h, 1. ~ I ~131 IM"ili'llillf"ll 111111; 1 RN Tiff .. , ttht 1: 1 ~j 'I 1~41'fv - 11 t 1 111 H ~ - 1".) , . 15--(2), 15,(6) AUTHORS: ikh i8ch Ao*z7ROyzens A& Jay S. -77-6/14 eval Is A., Kablukovskiy, Ai POP- Skorokhbdl-'S*-D' TITLEt ~'Refractory Concrete as Electric Insulating Material for Electrode Coolers, of Electric aro Furnaces (Ogneupornyy beton kak alektroizolyatsionnyy material dlya bkhladiteley elektrodov.dugovykh etale~lsvillnykh peche PERIODICAL: Ogneu o ~1 19 (USSR) p.ryt -959, Nr-7, PP 309-13 ABSTRACT:- The~magnqsite-chromitetiles iu.the.aroh of a steel-Melting a ou furnaoe--are satyr tedf during-operationg ~y iron-'and'ohrom a oxlder*~~and-become more conductive in this way, vhich oftd~'leade to;short:.circuits andla burning through of the coolers'. pigUre i shows the.depend6nceof'tho -logarithm of,the'specifio~eleotric-'. resistance on the temperature forsome industrial refractoriesi, At 'the experimental plant of tho.Mcrainakiy-iiauchno.ioslodavatellskiy, institut ogneuporov (U.'kIO) (U*W41M- 3oientific Rosearoh Institute of Refractories (ukiio)) and at the Semiluki Workso' experiments .with highly~aluminous refraotoTiesp*the original materials of which are indicated in a table, were carried out. The microscopic, 'Card 1/4' investigations were carried out by.N.-Ye. Drizheruk (Fo'oinote,:2).- Refractory,ConcreWas Elootrio,lnsulating Material ~SOV/131-59-7-6/14 for BleotrodeCoolero of ~,Electrid-aro Furnaces The'mass composition and.the properties of the samples are indicated in table 1. Figure,2 shows the thermal expansion, and,,- .f igure. .3, the dependence' of the logarithm of the specific electric resistanoe~bf the samples. It was not poosibles howevert tc ensure theelectrio insulation of the coolers in this way. Righly aluminous cement was-also prepared at the experimental plant-of' the-UNIIO. Highly aluminque fire clay with...a grain' size of.fr6m 3 to.below o*.0 mm.wae used,as a filler* The.chemical composition and refractorineas of.the cement.and of the f ire clay are Indicsted in table 2. The petrographic. investigation was carried out -by LO As- Kuzlmina' (Footnote 3), the-X-ray examination-by B.:Ya. Dikhem7ady (Fooinoe 41 and the thermal analysis by Ya, V. Pustoval6v Odnote,5 and'Fig Further experiment S were car#ed out"w'ith leaned masses, the composition density azid strength values of -qhich.are indi- catedin'table 3, The characteristic of the sampiis-is shown--in, table 4i Figure 5 shows the cohesion of the concrete:with a re- fractory product and an iron tube, and figure 6 shows the cohesien of the concrete witha Ma'gnesite-chromite tile. But also this experiment did not ensure an adequate electric ineulation.of the Card 2/4 coolers. kbTadmenW wM h%hly Oniums cement mdbigbly 931ldnow tUs of a -f 11"T V 17 Refractory ConcreteasMactrio Insulating Material- SOY/131-59-7-6/14. f or, Electrode Coolers, of Eleotric-ara. Furnao muMte-ccrunft -comImsitlanwre also carried out at.the experimental plant,of the UNIIO* The properties of.-the cement-and-concrete with the fill or of hig4ly alumin" fire alay, are indicated in table, 5- some data,characterizing the qualityof the'hi#hly aluminous arch tiles and of the.fire clay axe indicated in table 6. The insulation of the coolers by refractor7 concrete is carried out in.2 variants (Figo, 7 and"S)., The oh.emical composi-,~ tion,.of the concrete zone and of the slag Orustis shown in table 7 'The petrogra hio investigation was carrie& out by Me Yoo Drizhe:~*-(Footnote T Figure 9 shdwela, conorete'pioce after. 72 melts, The experiments carried out showed that the use of concrete eliminate's the burning through of the coolers by.short circuit, and extends the working period of the -furnace arches by 12-15 %- C6nolusions: The satisfactory application results of the concrete insulation for electrode abolors should,be introducea,-as soon as possible, in all electrometaillurgie plants, particularly in the furnaces working witli 6xygen. Tlie ~ series production ofthe material needed for the insulation should be organized, There are 9 figurest~B tables, and N references, Card 3/4 10 of whioh'are,. Soviet* 9I.M. "W I I : P f; I H 1 1. 1 1 if q~ : E 1, m ! 11 VII 1. 11-1] rl ld i i ~rll--. . v , I 1 3-F --l'. T-1-11-law-muglum t 9 lia4lilk. , 4,1114~i " : .`4f! . .: 1 i . i I i .. V! I i: , , I i . I M ~ i. I ff` p i PH 1314P; 11 ~ -1 1 i 11 : I Al lu: .1 911111"1111111 1 1 I JI 3 1 i,~ H 1 T, AQ(;~ 'V-AA016879 SaM COM UH/0198/65/001/009/0020/009il AUTHOR t ~- ahikhWAgh.-Ye.. VDnepropetrovsk.) 0RGt-Dne=opotrMMk Braneb, (Dnepropetrovildyfilial x1i A-11 ftgtMcgtio~ XndixAry st.roitallnogo proizvodstva) TITLIMI.-Caloulating the effect of concentrated loads on cylindri-cal ka- not 9# 1965; 20-i.25 ~1AGSIG Lai 6:-shi3l,stiructure. uiaieriii diformaiion. ABSTRACT: An approxiiate method Is given or ca culdting drical shells for any concentrated loads. The calculation is --done In two stages to assure satisfactory convergence In th6 so- lution. In the first stage* the zero-monent convolution IsIcalw laulated arA the normal atresses are 4etermined together ulth the resultant angular deformations. The seoond stage Involves analy- sis of the moment state of the shell as a folded eyetem loaded by the angular deformations found In the first stage. The method may be used for shell caloulations involving longitudinal, distributed and concentrated foraseq as wall as for computing the setting of .one_or several euppq;~~# _for any given boundary conditions at the -ends ~f the afiki.* Orig.art-v- 6st 2 f1gures# 7 for=las, and 3 tables. CiPHS] SUEK DATE: aCODE:~ 13 /~-ORIG IMS M OTH MFI: 002 Z i p;~!~ .-Jr. -X.40~0_rA ~V_W'41rWf!/q1 0AAmt, JV 6- 1 Jn .A"; AP6012217 SOURCE CODE.& UIR/0032/66/032/004/0438/OW AUTHIORt Bo.kshteynj Bm S.;.ZhikbovitskiTj A -0 A. Surmava, G..- Gli" ORIG; Moscow Steel'and AlloZ , InstitutIe(Moskovskiy inatitut stall i splavov).. TITLE: :Method for study of 'diffusion, in,wbisker crystals'. SOURCE: Zavodskays. laboratori7a., v..32, no. 4? 1966JI.436'442 TOPIC TAGS: metal whisker,,me.tal diffusion ABSTRACT: It Is Proposied.to'_~deiteimlne,.the coefficient of diffusion of a. component-in a wbisker,crystal',by measurement of its transverse, I dimension. The results of,s study of:tbe diffusion of zinc In whisker crystals of c9mr hAve shown that the rate of the diffusion mobility of the zinc aEoms.id whiskers is I to 1.5 orders or magnitude less than. ii) ordiii-aryzr1nocrystalline, Icoppers. The article given a detailed flow sbeet,of the equipment used to study this phenomenon* Experimental results,gre given in a series of curves, The results indicate that the rate of growth of tbe.wbiskers.actually limits diffusion* Orig, art*. has: 15 formulas and 3 figureat SUB,CODE: 07. 20/ SUBM DATE: none/ ORIG REF: 002/ OTH REF: 005 Card 1 /1 zoe/v- UDC: 532,72 difficulti Mast. ugl. 8 no.8:6 A-g '59* To work where work iL ()GRA 12:12) I.Birgadir rabochikh-,ochlatnogo zaboya shakhty iment ulinina. 1~ :-D IP!", H 'IH 1 :f