SCIENTIFIC ABSTRACT ZHOLONDZ, I.A. - ZHOMOV, YU.

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SCIENTIFIC ABSTRACT
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ZHOLONDZIP 1.4; FINKELISEITMI., M.I. Protective coatings preventing paraffin deposition on the in- ternal su~races of petroleum pipes. Labikras.mat. i ikh.prim, no*4*.40-44 1624 (KIRA 16:11) .1, Leniniradskaye otda"Leniye Gosudarstwnnoy vsesoyuznoy pro- kontory po lakokrasochnym pola7tiyam Glavkhim- plastkrasi Mnicterstva khimicheskoy promyshlennosti SSSR* I 5.5210 777118 SOV/75-15-1-10/29 AUTHORS: Busevs A. 1,, Zholondkovskaya, T. N., Kuznetsova, Z.-M. TITLE: Separation of Gallium and Indium by the Diethyldithio- carbamate Method PERIODICAL: Zhurnal analiticheskoy khimii, 1960, Vol 15, Nr 1, PP 50-56 (USSR) ABSTRACTs Conditions of Ga and In separation by precipitating In with sodium diethyldithiocarbamate or extracting it filth ethyl acetate were studied. A review of the literature dealing with the determination and separa- tion,of Ga and In Is also given. The following solu- tions were used: standard gallIum nitrate solution (1 Mg Ga/i~l)j standard indium nitrate solution (2-5 rqg in/ml)j 2% aqueous sodium diet~iyldithiocarbamate solu- tion; and the following buffer solutions: 0.21l1 CH3CO01-1 + 0,2M CH.1COONa. pl-I 3,72-5,57, 0,2M KCI + 0,2AI HC1, pH 1.00-Z20. 0,2M H;180, + 0.05M Na2B407, Card 1/5 Separation of Gallium and Indium by the Diethy-l- 77748 dithiocarbamate Method SOV/75-15-1-10/29 Card 2/5 The data obtained show that quantitative precipitation of gallium with sodium diethyldithiocarbamate takes place at PH 2.7-5.0, but has no practical value since. precipitation of many other elements also takes place under the same conditions. Precipitation of indium with sodium diethyldithlocarbamate is more selective; tartrates, oxalates), and aulfoE,alicyllc acid do'not Interfere. It was found that indium diethyldithio- carbamate can be quantitatively extracted with ethyl acetate at PH 3-5 in an excess of sodium oxalate. It is proposed to separate Ga and In by precipitating indium. with sodium diethyldithi.ocarbamate or extracting it with ethyi acetate at PH 3-5- in an excess of sodium oxalate. Experimental error for In and Ga is 1-3% at a In/Ga ratio from 2tl to ltlO. The results of Ga ~rd In separation by precipitation are shown in Table 1,1*.'& Separation of In and Ga by extraction is illustrated by data shown in Table 11. There are 11 tablesj and 35 references, 8 U.S., 3 U.S., 3 U.K., 14 German, I Japanese, Separation of Gallium and Indium by the Diethyl- 77748 dithiocarbamate Method SOV/~5-15-1-10/29 Table 10. Precipitation.of In with sodiwn di.ethyldithlocarbamate in the presence of allium at pH 3-4) in excess of sodium oxalate: (a) taken M)j (b~ ratio In: Ga; (c) In found (mg)j ~d~ error of In determinationj (e) absolu-1,Je (mg); (f) relative % j (g) Ga found (mg~; (h) error of Ga de-terminationj i absolute (mg)j (J) relative A. In .-Ga 2,39 t9,68 1 2,44 +0,05 +2,1 tg,B() -!-0.2t +t,06 2,39 19,08 1 -8 2,46 +0,07 4-2.9 19,82 -,.0,14 ~0,7 2. 09 4.912 1 2 2,97 -0, W2 -0,7 4 911 +0,04 +0.8 5 98 -4,92 t 1 5,79 -0,19 -3,t 4:91 0.02 +0.4 5:08 4,92 1 t 5,91J -0,02 -0,3 4 !)o () ai +().8 .'), 0 8 4,92 1 1 6,03 +0,05 40,8. 4:71) 1): 13 -2,111 5 08 4 92 1 t P,04 +0JA + 1,0 4, 93 40.01 5:08 2:46 2 t (1,01 4.0,03 -I.o,r, 2,301 -4),1(1 -3,3 5,0 2 1 5,90 -0,()8 -1,:1 2,5(~ -10'm +0,8 Card 3/5 Separation,of Gallium and Indium by the Diethyl.- 77748 dithiocarbamate Method SOV/16'(5-15-1-10/29 Table 11. Separation of In and Ga by extracting indium diethyldithiocarbamate with ethyl acetate in an excess of sodium oxalate (,~H - (a) taken (mg), (b) ratio Int Oa, (c) found In ~d3)error of In deternination, (e) ab so- lute (mg),'(f ~Rleiat ive (%), (g) found Ga (mg), (h) error of Oa determination, (i) absolute (mg), (JI relative It, 04 _578 t: 1 74 4- - - 2, 5:78 t:2 2 85 1 1 +0,01 1 +0 2, M 02 1-5 30 +0,00 +2 2, 30:44 1 10,- 2:OG +0,02 +0 Card 4/5 :4 ,7 /7 3 5r'., 8'7) ++ 00,' (()722 ++ 0()'3 0 14,9 1::o 0(3 1 -0.4 29,0 ~O -0,2 Separation of Gallium and Indium by the Diethyl- ',7748 dittliiocarbamcte Method !:)IOV/75-15-1-10/29 1 French, I Czechoslovak, 7 Soviet, The 5 most recent U.S. and U.K. references aro: Irving, 11. M,, Rossoti, F. G. C., Analyst 77, 801 (1952); Kraus, K. A.., Nelson F., Smith, G. W., J. Phys. Chem. 58, N 1, 11 (1954~; Arden, T. W., Burstall, F. H., Davies, G R , Lewis, J. A., Linstead, P. G., Nature 162, 691 (i946 ; Carvalho, R G de, Lederer, M., Analyt. chim. acta 15, Nr 6, 543 49~6)- ~ASSOCIATION: M. V. Lomonosov Moscow State Univei-sity (Moskovsk5 gosudarstvennyy universitet imeni M. V. Lomono~ova: .SUBMITI)ED: November 11, 1958 Card 5/5 SOV-26-58-9-41/42 AUTHORS: Gibovskaya, L.D., Zholtko, Ye.A., Krasnoyarsk TITLE: Early Snowfall (Ranniy snegopad) ~PERIODICAL: Priroda, 1958, Nr 9, p 126 (USSR) ABSTRACT: A case of an early snowfall during the night of 25/26 Se p 1955 in Krasnoyarsk is described. There is I photo. 1. Snow--USSR Card 1/1 ZHOWOK.A.G.; ZABCLOTSKIYY.D. Kasters of highly productive labor N.H.Pavlov -and X.F.Plotnik-ov. Avt. dor. 18 no-3:11-13 My-Je '55. (MM 8!9) Okrthwork) ZABOLOTSKIT,, IF.D., inzhener; Z)ROLTOK, A.G., insherer. Over-all.p'reparation of roads for springtime. Avt.dor. 20 no.3:12-13 Mr (MM 10:5) (Roads-Kaintenance and repair) TT-Col F, I U, N 11 -FC I ZABOIA)TSKPY. Fedor Danilovich "nwl ch- VBYTSMM, X.I., redaktor; XALIKOVA, N.V., takhnichaskiy redaktor LLeading road graders; practices of the Inno-rators H.F.Plotnikov add,N-l.)(Atusevlchj Peredovye avtogreideristv; Is opyta raboty novatoroy M.-I.Plotnikova i K.I.Natusevicha. Moskva, banchno-takhn. isd-vo avtotransp.lit-ry, 1957. 33 p. (MIRA 10:8) kRoad machinery) (MIRA 14: 5) ~~ASM, Andrey Iosifovich; DXMCH, Xyan Stepanovich. Prinimal uchastlys ZHOLTOVSKIY, P. (ZholtoyOkyl, P.I. GAIW, Tu. (Hapon, re [Lvov; guidebook] Ltviv; putXvVk. Llvivt laphkovo-zhurnallne vyd-vo, 1939. 147 P. (mm 13:4) (Lvov--Guidebooks) ZHOLTOVSKIY, P..N. "Drevniye motivy v gutsulskoy ornamentike." report submitted for 7th Intl Coag, Anthropological. & Ethnological Sciences, Moscow, 3-10 Aug 64. ZIIOLUN=-TGV, K. I. ZJiMUBHETOVj K. I.- "Heasurea to Eliminate Spelling Mistakes in the Native Language in the V-Vl Classes of Kazakh Schools," Acad Pedagogical Sci RSFSR, Inst of Methods of Teaching, Moscow, 1955 (Dissertations for the Degree of Candidate of Pedagogical Sciences) SO.- Knizh~M Let2pis' No. 96) June 1955, Moscow ZMLT3DIV, A. for Inspection of venturi wings In K-M and K-81 carburetors. Ayt. tranap. 34 no-10:33 0 156. (KTBA 9t12) (Automobilee--Znginen--Carburstors) ZHOLUI)ZV, A. Reconditioning the valve aeat of the B-6 gas pump. Avt.tran8p. 34 no.9:33 5 156. OQU 9:11) (Fuel pumps) ZHDUJDBV, I. (Saratov) Scientists help to organize urban gas supl!7 systens. Zbil.-kom.khoz. -10 no.4-11-13 160. (WRA 13:6) (Baratov--G-oa distribution) ZBOLUDEV, S. "Symmetry of Tensors of Second Order and some Problems of the Point Symmetry of Physical Objects" a report presented at Symposium of the International Union of Crystallography Leningrad, 21-27 May 1959 AID P - 4617 Subject USSR/Aeronautics - training .Card 1/1 Pub. 135 - 6/23 Author Zholudev, L. V., Hero of the Soviet Union, Guards Col., -pilot Class I .Title Flightlof a flight of bombers at night Periodical : Vest. vozd. flota, 4, 30-33, Ap 1956 Abstract : The author makes some suggestions how to train the flying personnel in formation flying at night. The made suggestions are based on the experience gained in flying the Il-28 type bombers. The article is of informative value. Institution : None Submitted : No date 1,Dnepropetrovskiy khimiko-takhnologicheakiy institut. (Hydrogen) (Overvoltage) ZHOLUDEV M9.P..o kand. tekhn. nauk; KISM.'VICH, T.O.., inzh.; ELAMM, Ya*IM,p inzh.; Prinimala uohastiye OEHRAHMCH L.N. , inzh, Production of thin-vml-led pipe made by gi.Llvamplasty. Proizv. trub no.10:101-105 163. (1,11RA 17: 10) KISILEVICH9 V.O... inzh,; ZHOLUDEV.. M.D.. kand.takhn,nauk Unit for electrodepogtion of metals'6n metals on Internal our- faces of hollow cyllnd~ical bodlese Mashinostroonie no.6s64 N-B 162. (MIRA .1612) 1. Ukrainskiy nauchno-issledovatellskiy trubnyy institut, g. Dnepropetrovsk. (Electroplating) ACCESSION NR: AP4022110 S/0073/64/030/003/0287/0'289 AUTHOR: Pilipenko, 111. L.4- Zholudev, M. D. TITLE:, Chromium plating of articles made fron SOURCE:. Ukrainakiy khimicheskiy zhurnal, v.. 0, no. 3, 1964, 287-289 TOPIC TAGS: chromium plating, Nimonec, nickel alloy,, coatiu~ucuz 'Plating. chemical picklina, pobassi= f luossilicatej j4ati~g bath, stainless steel, tunasten containing alloy ABSTRACT: It was established that chromium plating of pipes and rods of "Nimonec" tungsten-containing alloys cannot be effected with the present plating Systems. A method was worked out for continuously depositing strcnaly ;~hex6t'- chrcniuz~qepoAts -5o-6o M1crcns thick by combining che.aical 34cklIA-1 and chr=-",-.,[. ium, plath~g in- -a s el-f- regulating electrolyte (Fig. 1). The chromium plating conditions aire presented. The plating bath in Sqonsistea of chrmic anhydride 25Q, strontium sulfate 5. 5- 6. 5, and potass Lum. fluoailicate 18- 20 I i i FILIPMOI, N.L.; VIOLIDEVy M.D. Chromium plated articles made of 'yLlmonie" tYpe of allQYs- Ukr. khim. zhur. 30 no.3;287-289 .164. (MIRA 17s10) GORBUNOV, N.S.; ZHOLUDEV, M-D.; PROSKURKIN, Ye.V. Zinc diffusion coatings. Zashch. met. I no.3t314-318 W-JO 165. (MIRA 1W) 1. Institut fizicheskoy khimii AN SSSR i Ukrainskiy nauchno- issledovatellskiy trubnyy institut. ~~~Cand Tech. Sci (dies) 11"Electro,(-T-~s~clu~tions, ~f~~ Dnepropetrovsk,1957. 17 pp. (Min of Higher Education UkSBR..Dnepropetrovsk Chemico-Technological Inst im F.B. Dzerzhinskiy. Chair of Technology of Blectrochemical ProductsO 130.copies. (KL, 8-58,. 105) -25- ZROLUDEV, M.D.; STBN=, T.V, Catbodic polarization during alectrolyois of zircate solutions. Ukr. kbim.zbur. 24 "o,5:570-574 58. (MIRA 1?-Il) 1. Dnepropetrovskiy kbimiko-tekbnolo6ichaskly institut. (Zincates) (Polarization k3loctricity)) Y, //VV/ ,~,ZHOLUDNV,_H.D,,*, STMAR, Y.Y. Potentials of hydrWn separation from alkali solutions at ind-?daQ4&-- current densities. Ukr. khim. zhur. 23 n0.31322-324 157.(KLBA lotg) 1. Dnepropetrovokly khimiko-tekhnologicheskly inatitut, (Electrolysis) (Hydrogen) SOV/ 137-58-7-14617 D Translation from: Referativnyy zhurnal, Metallurgiya, 1958, Nr 7, p 96 (USSR) AUTHOR: Zholudev M D TITLE: Electrolysis of Sodium Zincate Solutions (Elektroliz rastvorov tsinkata natriya) ABSTRACT: Bibliographic entry on the author's dissertation for the de- gree of Candidate of Technical Sciences, presented to the Dnepropetr. khim.-tekhnol, in-t (Dnepropetrovsk Institute of Chemical Technology), Dnep rope trov sk, 1957 ASSOCIATION: Dnepropetr. khim.-telchnol. in-t (Dnepropetrovsk Institute of Chemical Technology), Dnepropetrovsk I. Sodium-zinc solutions-.-Electrolysis Card I/ I 5(4) SOV/153-58-6-13/22 AUTHORS: Kisilevich, V. 0., Zholudev, 11. D. TITLE: Ization (0b izmerenii On the Measuring of Electrode Polar. elektrodnoy polyarizatsii) PERIODICAL: Izvestiya vyashikh uchebnykh zavedeniy. Khimiya i khimicheskaya ~tekhnologiyaj 1958v iTr 6, PP 79-63 (USSR) ABSTRACT: Thelirrepro ducible results on electrode polarization (Refs 1, 2) arecax1itioned by several factors. Various suggestions have been made for their elimination (Refs 2-5). However, scientific publications do not contain any well-founded experimental data concerning the economical choice of electrode eize~ shape etc. The paper under consideration serves the purpose of establishing experimentally the electrode ahapeto be chosen, the angle at which the tip of the electrolytic key should be-fixed with regard to the electrode, and finally the maximum current densities permissible at which reproduci- ble results an polarization measuring at this or that position of said tip can still be obtained. In the experimental part, table I gives the characteristics of the cathodes used (of Card 1/3 nickeled ironj rectangular I triah&ular, cylindrical, spherical, On the Measuring of Electrode Polarization SOV/153-58-6-13/22 and discoid). Figure 1 shows the dtiaign of a screening frame for theAiscoid cathode. Figure 2 illustrates the position of the tip of the electrolytic key. From figure 3 it can be aeon that the extension from 0.1 to 1-7 mm of the capillary diameter (Fig 21 position 1) results in a potential-increase withrising current density (Curves 3 and I)- Figures 41 5 and 7 show the cathode potentials with individual electrode types Figure 6 shows a turnable plate for electrode$ which turne; out to be inapplicable to the purpose. A rotating disc must be used, the potentials of which are identical at dif- ferent points. For their experiment3 the authors used the electrolytic precipitation of nickel from sulfates, of zinc ,from zineates, and of hydrogen from 6N NaOH. The moat easily reproducible results are obtained oii the measuring of po- tentials at all points of the cathode, with a sphere and a small disc enclosed in a vinyl-plast frame no as to eliminate an uneven current distribution. The tip of the electrolytic key must be direoled towards the electrode from below, at an angle of 60-65 . There are 7 figures, 1 tablet and 10 references, 6 of which are Soviet. Card 2/3 On the Measuring of Electrode Polarization, SOY/153-58-6-13/22 Kafedra tekhnologii elektrokhimichaskikh proizvodstv; Dnepropetrovskiy khimiko-tekhnologicheskiy institut (Chair of Technology of the Electrochemical Plants; Dnepropetrovsk.,.Chemo-teohnological Institute) SUBMITTED: November 29, 1957 Card 3/3 ZHOLUW, K..D..; SITIMM,.Y.T. Yroportles of sodium sincate solutions; viscosity, density, and tulip.. *h1w'.23_no*2:200-207 '57. Mm 10:6) 1. Muepropetrovskly khimiko-tekhnologiohaskly inatitut. (Sodium zincate) - (Solution (Ghemistry)) cc d1c., V 73-3-6/24 AUMOR: Zholudev, M. D. and Stender, V. V. TITLE: Potentials of Hydrogen,Evolution from Alkalis with Increased Current DeasLty- (Potentsialy Vydeleniya Vodoroda iz Rastvorov Shehelochey Pei Povyshenaykh Plotnostyakh Toka) PERIODICAL; Ukrainskiy nimicheakiy Zhurnal, 1957t Vol. 23., No. 39 . pp. -322-324 (USSR). ABSTRACT: The potentials of hydrogen evolution of 9 metals (Mg, Znj Pb, Sn, Cd, Grt Sbj Ca anq Al) wese measured by the direct compensation method at 22W + Q.2 C at a current density interval of 107-' to 4.10 -La/e-m"-. These data are required for the calculation of the intensity in the bith, for the investigation of conditions of the discharge of metal ions together with the H-ions, etc, when calculating the electrolysis of alkaline solutions. 6 N and 0.6 N NaOH solutions (chemically pure) were used as electrolytes. All metals were used in the shape of discs as cathodes which were previously polarised in the inv~stigOed solution for 1 hour at a current density of 400 a/m . Measurements were cafried out in an open vessel, the electrodes being Card 1/2 at a distance of 60 mm. Results are tabulated in Table 1. 73-3-6/24 Potentials of Hydrogen Evelution. from Alkalis with Increased jP Current Density. Table 2 gives comparative data for iron, nickel and cobalt obtained by the authors in analogous experiments and data for the metals which have previously been published in literature. Discrepancies were of the order 0.01 - 0.05 V. lead differs from other metals even during a comparatively short polarisation eriod as the surface turns porous and the overvoltage georeases due to the increase of the surface. The disintegration of the surface is obviously connected with a discharge of Na,-ions. Aluminium disptegrates during cathodic polarisation, up to 600 a/m current density, at higher current density cathodic protection takes place. There are 2 tables and 6 Slavic references. SUBUTTED; November, 29, 1956. ASSOCIATION; Dnepropetrovsk Ohemical-Technology Institute. (Dnepropetrovskiy Khimiko-Tekhaologicheskiy Institut) AVAILABLE: Library of Congress. Card 2/2 AUTHDRS.oZholud6v M;D. and Stender V,V. T2j-2-9122 I----------- TITLE: Properties of sodium zincate solutl,onsi ~.,oeffioients of diffUSionq viscosity and density. 4.Svoystva rastvorov tsinkata natriya: koeffital-yenty diffuzii, vyazkost' i plotnostl)'. nRIODICAL: "Dkrainskriy Xhimicheskly Zhu:rnr2," Mrainian Journal of ch-e-MR-r-y 19579 pp.200-207 (USSR). ABSTRACT: Various methods have bee.a described in literature fox the determination of the above coefficients. The optical m-ethod devised by K.V,Cbmutov and I,Yfi.Slonim (Ref.6; X.V.Cbmutcv and 1'.Ya.Slonim7 U5p',Kt1im'.,l950.,2_2,142),_ the diffraction method described by Ya.P.GoklLshtein (Ref'.7: Ya.P.Gokiiskitein,Zh:,,Fiz'.Khim,, 1918, Vol.229 871 and 19521 Vol.26)224)336) and other methods are critioally examined. The authors determined the coefficients of diffusion on a rotating disc electrode which had porous diaphragms with straight channels. They used an equation expressing the limi",* current on the rotating disc- electrode and discuss the particular case of electroplating of metals, The Card 1/3 apparatus for this 'purpose is described in detail and illustrated in Fig,'l. The dependence of the electrode Mrl 2/3 73-2-9/22 Properties of sodium zincate solutions: coefficients of diffusion, viscosity and density. (Cont'.) potential of 0'.05 mof.sodium zincate and the log of the current density at various speeds of' rotation of-the electrode is given in Diagram 2. The diffusion ooeffic.- ients of zincat6 ions calculated by the above mentioned formula are tabulated (Table I ,Y. TLe obtained experimental values for the diffusion coefficients for various concen- trations of zinc and free alkali in the solution are in,- dicated in Diagrams 4 and 5t, It can be seen (Diagram 5) that the coefficients decrease with increasing alkali concentration. This is demonstrated.by the increasing viscosity. During the electrolysis of zinoate containing 30 gA zinc and free alkali (in one case 120 g/1, in the second case 480 gA) the limit current should decrease in t'he same'proportion as the. diffusion coefficient, i :se:0 4.8 fold. Thi's was proved by carrying out practical ex- periments. The viscosity of the solution was determined with an Ostwald viscosimeter and values obtained are shown in Diagrams 6 and 7. The density of the sodium zincate solution is determined in relation to the density T3-2-9/22 Properties of sodium zincate solutions: coefficients of diff-usiong viscosity and density. (Cont.) of water. (Diagrams 8 and 9). There are 2 drawings, 7 diagrams, l table, and 16 references, 12 of which are Slavic. ASSOCIATION: Dnepropetrovsk Chemical Technology Institute. (Dnepropetrovskiy Xhimiko-tekhnologit"%heskiy Institut). SUBMITTED: September 15, 1956*. AVAILABLE: Library of Congress (,'axd 3/3 ACCESSION NR: AR4041594 S/0137/6,1/000/005/D038/D639 SOURCE: Ref. zh. Metallurglya, Abs. 5D226 rAUTHIPR: Zholudev, M, D. Kisileyich, V. 0.; Balmlyuk, Ya. Kh. TITLE: Production of thin-walled pipes of galvanoplasties CITED SOURCE: Sb. Proiz-vo trub. Vy*p. 10. M., Metallurgizdat, 1963, 101- 105 TOPIC TAGS: thin walled pipe, galvanoplastic, pipe production TRANSLATION: Possibility was-studied of obtaining (by method of galvn noplas tics) special thin-walled pipes (with thickness of wall