SCIENTIFIC ABSTRACT BLINOV, V. A. - BLIZNYUK, N. K.

• Document Type: CREST
• Collection: Scientific Abstracts
• Document Number (FOIA) /ESDN (CREST): CIA-RDP86-00513R002200410013-8
• Release Decision: RIF
• Original Classification: S
• Document Page Count: 100
• Document Creation Date: November 2, 2016
• Document Release Date: September 1, 2001
• Sequence Number: 13
• Publication Date: December 31, 1967
• Content Type: SCIENTIFIC ABSTRACT

USSR
ux 666.113.431.47-32-31.28
UDO'PENKO, N. G., NIKULM, V. KR., PRUSAKOVA, L. M. )
SOKOLEISY,TYI, A. G.., ORLOV, V. N.., VYSOTS"KIAYA, Z. I., and CIERITYSHEEV, A. V.
"Glass for Ultrasonic Delay Lines"
USSR Author's Cer-._ij-ica".-e No 366156, Filed 26 Jun 70, Published 16 Jan 73
(from Otkrytiya, Izobreteniya, Pronkyshlennyye Obraztsy, Tovarnyye Znaki, 0 7,
Mar (a) 73, Clsim NO 14531641/29-33)
Translation: A jlass for ultrasonic delay lines, including S-410.1 Z110, Bao,
Yw2O, is distiPS7,Llshea bly 1-he fact that,, in order to obtain Otable acoustic
properties it contains the above conmonents in the foLlowir,f announts,, wei~rht
sio,2 49-65; ZnO 5-27-5, aao 10.5--,,0- K 0 6-25 and furthermore Sb~,O 0-0-5-3-
3
47

USSR UDC 662.75:662.61
njXg,_V. I., LUSHPA, A. I., XHAYLOV, V. M., and KHUDYAKOV, G. N.
wBurning Rich Kerosene-Air Mixtures in a Tunnel-Type Combustion Chamber"
Moscow, Goreniye i vzry-i -- sb. (Combustion and Detonation -- Collection of
Works), Nauka Publishing House, 1972, pp 416-420 (from Referativnyy Zhurnal --
Teploenergetika, No 3, 10,73, Abstract No 3T71)
Tran~slation: The authors present the results of experimental research in the
effect of the excess air ratio (0( = 1.0-0.3), the air temperature (T. =
0-1,0000C), and the length of the combustion chamber (0-5-0.2 meters) cn the
degree of approximation of the mixture and the combustion products' parameters
to their equilibrium values in a chamber with an internal diameter of 100 mm
and at a pressure of M2. As the values of (X and T are reduced, the
1.1 kg/c
dffference between the experimental and theoretical parameters increases,
while the curves showing the change in the experimental data along the length
of the chamber have a greater slope. The authors show that the process of
achieving an equilibrium state is limited by the heterogeneous combustion of
the solid carbon given off during the thermal decomposition of the kerosene in
the initial combustion zone. (4 illustrations; 5 bibliog. ref.)
IA
- 36

USSR
UDC 629-7-036-3:536.46
WSHPA, A. I.,
BLINOV~_ V. M., and MUDYAKOV, G. N.
"The Combustion of Rich Kerosene-Air Mlixtures in a Tunnel-Type Clip-mber"
Moscow, Goreniye i Vzryv--Sbornik (Combustion and E%Tlosion--Collection of
Works), Nauka, 1972, pp 416-420 (from Referativnyy Zhurnal--Aviatsionny-ye i
Raketnyye Dv-igateli, No 2, 1973, Abstract No 2-34.26. Resune)
Translation: Results are presented of an experimental investigation of the
influence of the air-excess coefficient (CK= 1-0 -- 1-3), the air teraperature
(Tair = 0 -- 10000C), and the combustion-chamber length (0-5--2.0 m) upon the
degrk!,-! of approximation of the composition and parameters of the combustion
products to their equilibrium values in a chamber with an inner diam~,_-tcr of
100 mm at a -Dressure of 1.1 absolute atmospheres. Mhe result is obtained
that as 0( and Tair decrease, the difference between the ex-perimental and
theoretical parameters increares, and the cui-res of chanf-,c of the crr,~,,rimf_~ntal
data with respect to the chamber length become flatter. It is showu that the
process of attainment of the equilibrium state is limited by the heterogeneous
combustion of solid carbon escaping during the Itherrial decomposition of kero-
sene in the initial zone of combustion. 4 figures- 5 references.
1/1

UNCLASSIFIED pikii-EssiNG 7 0
TITLE-AUTGNATIC STR,416HTENING A~,D CUT-TING MACHINE -U-
AUTHOR-(05)- YASINSKIY, Yl).G., PCLYA.-dN, YU-N.r
V.-A.
COUNTRY GF !.:F0--UScjR 01~
SOURCE-U.S.S.A. 238517
Rl~FE'.-',ENCE--OTKkYTlYA, MBRET., PROM. OBRAZTSY, rovAkt~ycl ZNAKI NO 10
DATE PUBLISHED-31JUL70
SJ4,JECT AREAS-tiEC.H., IND., CIVIL AND MARINE ENGR
TOPIC TAGS-PATLN'T, AUTGIMAFIC CONTkOL SYSTEM, CUTTING WOL
I)CCUMENT CLASS-UNCLASSIFIED
Pili-JA'Y STEP N~)--URf
L '% L ~1_1 I: I LE L

USSR UDC 621-396.267: 15219. 0' -:'
.j J
FR I D'~~ V. V. -RLTj,'01,(1 '%7. 1
"The 2' -ne Nlavig-~ 4-onal R~-.dar System3l'
Sudo-v7,7,,e navi-gatc--'onn--,~.-e radiolahatsionn,,-ve stantsii
t1 - -
"Kivach-2* (cf. '-nFl;Sh albove.). ?,:oscow, pror-st'", 1.9-,-',
T6-8pp3 -ill. 75 1:. (fi-cm RZh-Radioteklini.,-.a, NO 7, Jul 7-` , A-bstract
1~ K
11o 7G20 I )
Translation. '71ne book contains information cii "lie rriilci-)lc~ of d-s-Ii7l,
on the o'cerat-ic--l and technIcal characteristics , cons-tru---tion and -wer',71-
ing principles c-7' the "Kivach-l" wid "Kivach-2" radar Jv.-tC-.l]-ationi;.
The wirint- connectionr., and the functian.,,Ll circuLt of thr. rtldrar
lations are -oizether -,,ith schematic dialzra---:3 ano -~he
tion of t"E: liuli2s, are giveti for
the r~:d,~r i no, +--31 atic.-.'L Q-n board the hip , drty- v r-cl!
. Lcal and r-:Iace-ent of tie
n- units- a-r4d zs3diLfi- Jn-
stallations. The dist-inctive features of the image on screen are
discussed~ are given on controllinf~
the cDerar-~~rg cc-diticn of the station. Forty-seven
twenty-five tpbleS, bibliography of thirteen titles. lunotation.
1/1
212 01 13 U7NICLASSIFIED iNG
C I a C A C L E S S I IN i-AA 1 -14 9 3 2
A-L3SIRAL1/r-X1'i~ACT--!U) GP-0- ABSTkACf. AUTOMATIC STRAi-1.'p.riTL-N1NG AND
CUTTING AACHII,& CUNTAINS CUTTING MACHANISMS I AND 2 WITH MUbILE BLADES7
MECHANISMS FOR STK.A1GHrENINGv ROD DELIVERY AND RILMOVAL OF CUT OFF
DETAILS. IN URDLIR TL; INCREASE EFFICIENCY W[iE;N FIXI,'.Q'- IT AFTE;~ THE PRE-~-S
wHICH P'EkFURMS SIMULTANEOUS PRESSING OF A ROW UF PARALLEL ;0D.51 THE
MACH]j'i~: HAS SEVERAL .14ECHA-jISMS FOR STRAIGHTENING, DELIVERY, CUTTING AINID
REMOVAL 6F CUT OFF bFTAILS, SIIUATED IN PARALLEL. T~AE MIECHAN,ISMS ENIA5Li'
THE MOVEMENT OF THE DETAILS TO A VIBEOPLATFORM (16) ,4HICH IS SITUArEo
UNDER fHE MECHANISMS. THE VIBRU PLATFORM HAS *,k DEz-BALANCLNG D;-~IVE (18)
AND HAS T60 PAIRS OF INCLINED GUIDES WHICH ARIE StrUATED ONE A.:3UVL-- THE
OTHER. IN THE CLEARANCE BETWEEN THE UPPER GUIDES MiTCH FOR A HUPIPERI
A TURNING SLIDE IS FIXED. THE SLIDE HAS TWO FIXED PUSITIONS AND DIVILD!.`-
THE DETAILS INTO TWO STREAMS WITH THE HELP OF THE L-'-jiEP GUIDES. T jj~:
AU61LE SLAOF (7) OF THE CUTTING MECHANISM (1) 15 kJAL0 01,~ A
(11) 6HICH PERFORMS REVERSE EUaWARD MOTION AND IS AFF~-CrEl`) f~)Y A
1121. T~iE SPkING CRL-ATES Aiji)[TIONAL EFFORT DURING CUTTING ANIO P-40VII'Lik-S
A REIDUCTION IN INERTIAL FORCES DUPING THE REVERSE SJRJKE.
FACILITY: TSENTPALINYY NAUCHNO-ISSLEDOVATELISKIY Jlij~"IITUT TARY i
UPAKOVKI.

112 025 W.CLASSIFIED Pi"'OCESSINIG DATE--IIDEC70
f4TLE--IMMIELIATE AND LCNQ_ TERM RESULTS Cf- SPLENECTOMY IN HEMIOLYTIC
_u_
AUTHoF-(Qzt)-5ENGHfLCj YI.A., b~Q ~At A.[., KURALGVA, V.V., 130ULKADYROVA,
"A.S.
CCUNTFY CF INFC--USSR
SOURCE-SUV MED 33(l). 72-77. 11;70
DATE PUBLISHEO ----- -70
.-SUBJECT AREAS--BIOLCGICAL AND MEDICAL SCIENCES
TOPIC TAGS--ANEMIA, SUKGERY, SPLEEN, hORMONE, CORTICOSTEROID, TEST,
HEMCLYSIS
CCNTRUL lAtkl(lNG--.N0 RESiRICTIONS
-DOCUMENT CLP.SS--UNCLASSlFlED
PROXY REEL/FRAME--3CC7/0304 STEP t4O--UR/C399170/033/001/0')72/0077
CIRC ACCESSICIM NC-AP013571~-9
WIL, L 114, s S 1L 0

212 025 UNCLASSIFIED PROCESSING DATE---ILDEC70
CIRC ACCESSICN NO-AP0135799
ABSTRACT/EXIRACT--(U) GP-0- ABSTRACT. SPLENECTOMY WAS PERFURMFO IN 55
.PATIENTS VITH HEMOLYTIC ANEMIA, AND IN 41 IT WAS DONE FOR CONGENITAL
MICRGSPHEPOCYTIC HEMbLYTIC ANEMIA WITH GOOD IMMEDIATE OPERATIVE RESULTS.
IN 11 OF 14 PATIENTS ii-LTH ACQUIRED AUTDIMMUNE FGR.4 OF HE,'-lJLYTIC ANEMIA
IMMECIATE RESULTS OF THE OPERATIGN WERE SATISFACTORY. REMOTE OUTCO~'IES
OF SPLENECTGMY WERE STUCIED IN 40 PATIENTS. FOLLOviING SPLENECTOMY
CLINICAL i;FCOVERY IN PATILNTS) WITH C014GENITAL HEVIOLYTIC AhEMIA CCCURRED
IN 29 OUT UF 30 CASES. IN INSTANCES OF ACQUIRED ALIFOUMMUNE HEMOLYI-IC
HELPED TO !;'APROVE THE CONDITION OF THE i-)ATIE,.%TS,
ANENIA Sr
WHILE SCi'-E OF THEM [)Ef~CNSTRATEO COMPLETE CLINICAL RECOVERY. -'-lAINTENANCE
THERAPY WITH CORTICUSTEROlU HORMONES IS INDICATED POSTOPC-?AT[VELY IN
PATIENTS ~TLTF ACCUfFED AUTO[MMUNE FGRIM CF FEMOLYTIC ANEMIA PRESENIT[NG
SYMPTOMS LF HEMOLYSIS ANO CCNTINUEO POSITIVE COOMB'S TEST.
FACILITY: CLIN. SORG. HEMATOL., LENINGRAD RES. IN5T. hENATOL. BLOOD
-TRAKSFLS., LEN'INGRAD, USSR.

1/3 024 UNCLASSIFIED PROCESSING OATE--160CT70
TITLE--CONDITIONS FOR PRODUCTION AND ISOLATION OF VALINOMYCINY A REGULATOR
OF CEtL MEMBRANE PERMEABILITY -U-
AUTHOR-(04)-SMIRNOVA, G.M., BLINOVA, I.N. KOL ODT TSKAYA,
A.7S.
COUNTRY OF INFO--USSR
SOURCE--ANTIBIOTIKIr 1970, VOL 15, NR 5, PP 387-392
TOPIC TAGS--ANTIBIOTIC DRUG EFFECT, STREPTOMYCES, CELL MEMBkANE,
PERMEABILITY? DRUG PRODUCTIONr CONTINUOUS CULTURE, CHEMICAL
PURIFICATIQN/(U)VALINOMYCIN ANTIBIOTIC
DOCUMENT CLASS--UNCLASSIFIED
PROXY REEL/FRAME--1994/1362
NC--AP0115332
UNCLASSIFIED

'213 024
UNCLASSIFIED PROCESSING DATE--160CT70
CIRC ACCESSION NO--AP0115332
ABSTRACT/EXTRACT--(U) GP-0- ABSTRACT. CONDITIONS FOR BIOSYNTHESTS OF
VA.LINOMYCIN BY STREPTOMYCES SPECIES PRL 1642 UNDER PILOT PLANT
CONDITIONS WERE DEVELOPED. A METHOD'OF SERIAL TITRATION AGAINST CANDIDA
AL81CANS WAS PROPOSED FOR DETERMINATION OF VALINOMYCIN CONTENT IN
SAMPLES TAKEN OURING THE CULTURE GRO14TH AND THE ANTIBlOTfC ISOLATION.
SAMPLES OF THE FERIIIENTATION 13ROTH WERE ACIDIFIED WITH HYURUCHLORIC AC(D
TO PH 2.3-2.5, THE PRECIPITATE WAS WASHED AND EXTRACTED TwICE WITH
ETHANOL, THE VOLUME OF THE EXTRACT OAS ADJUSTED WITH DISTILLED WATER TO
70 PER CENT. THE COMPOSITION OF THE FERMENTATION MEUIUM WAS THE
FOLLUWtNG (IN PER CENT), CORN STEEP LIQUOR 0,5 (ORY WEIGHT)i AMMONIUM
SULFATE 0,4, GLUCOSE 1, STAkCH 1.5, SODIUM CHLORIDE 0.5, CALCIUM
CARBONATE 0.5. THE TIME OF FERMENTATION IN 45-, 100- AND 500-LITER
FERMENTORS WAS 4 TO 5 DAYS. THE AVERAGE CONTENT OF THE ANTIBIOTIC IN I
LITER OF THE MEDIUM WAS ABOUT 40 MG. THE ACTINeMYCETE DEVELOPMENT
PROCEEDED IN 2 STAGES. THE ANTIBIOTIC PRODUCTION wAS OBSERVED IN THE
ZND STAGE, WHEN FRAGMENTATION OF THE MYCELIUM TOOK PLACE. VALINOMYCIN
WAS ISOLATED BY 3-4 FOLD EXTRACTION OF THE MYCELIUi'-I WITH ETHANOL,
FOLLOWED BY PURIFICATION WITH BUTYLACETATE, SATURATED SOLUTION OF SODIUM
BICARBONATE,: AND CARBON TETRACHLORIDE. AFTER THAT THE SUBSTANCE rJAS
ELUTED IN AN ALUMINA COLUMN BY CARBON TETRACHLORIDE AND THEN BY ITS
MIXTURE WITH ABSOLUTE ETHANOL. ACTIV .= FRACTIONS WERE EVAPORATED,
DISSOLVED IN ETHER AND THE SOLUTION WAS PASSED T14ROUGH A CULUMN WITH
ACTIVATED CHAFCUAL AND CELITE 545. VALINOMYCIlN WAS CRYSTALLIZED FROM
HEXANE

1. 313 024 UNCLASSIFIED PROCESSING DATE--160CT70
CIRC ACCESSION NO--AP0115332
ABSTRACT/EXTRACT--A COLOURLESS CRYSTALLINE SUBSTANCE WITH A MEL-TING POINT
~ OF 185-1860EGK~-ES, ACTIVE AGAINST CANDIDA ALBICANS IN A DOSE OF 0.1
MUG-ML WAS OBTAINED. FACILITY: INSTITUTE FOR CHEMISTRY OF
NATURAL SUBSHrANCES OF ACADEMY OF SCIENCES OF THE LJSSP, MOSCOW.
UNCLASSIFIED

USSR
UDC 5417-94
YA1G!O1NT6?Y'A , L. D., KOMAROVA, M. N., PEREMSON, 14. YE., iBUNOVA, K. F.,
and TOLKACHEV, 0. V. , All Union Scientific Research Institute of Medicinal
Plants, Leningrad Chemical-Pharmaceutical Institute
"Hypecoum Erectum Alkaloids. Structure of Hypecorine and Hypecorinine"
Tashkent, Khimiya Prirodnykh Soyeclineniy, No 5, 1972, pp 624-628
Abstractj Two new alkaloids were isolated from the Fypecoum erectum L, grass
hypecorine, m.p. 154-1560 and hypecorinine, m.p. 197-1980. The structures
of these compounds were determined on the basis of their chemical reactions
and IR, UV, MR, and mass-spectroscopic data. Hypecorina was a'95igned
the structure of 7-methyl-2,3,11,12-dimethylenedioxy-g-oxahomospirobenzyl-
tetrahyclroisoquiiioline, and hypecorinine was identified as 7-methyl-2,3,11,
12-cLimethylenedioXY-15-keto-g-oxa.homospirobenzyltetrahydroisoquinoline.
Both compounds are optically inactive, probably due to the ease of the
racemization stemming from thoir spiroaminoketal structures.
i/I

USSR
UDC 576.858:616-002.77
BOCHAIROV, Ye. F. , YAVOROVSKAYA, V. Ye. , S11KU"RUPIY V. A., BLINOVA L I
and Y-A-Z'NACHEYEV, V. P., 'Llovosibirsk Mcdical Institute, and"C"zeW't`ral Order of
Lenin Institute of Advanced Training of Physicians, Moscow
"Morphogenesis of Coxsackie A 13 Virus Isolated From Rheumatic Fever Patients"
Novosibirsk, Izvestiya Sibirskago Otdeleniya Akademii Nauk SSSR, Seriya
Biologicheskikh Nauk, No 10 (190), 1971, pp 131-137
Abstract: Light and electron microscope examination of human embryonic fibro-
blasts infected with Coxsackie A 13 virus, strain 689, -7solated from rheumatic
fever patients, shoived that the nature and dynamics oL' the observed changes
were identical to those in fibroblasts infected With the prototvpe virus.
Signs of de.-oneration wc-re evident within 6 to 8 hours when the virus began
to reproduce and emerge from the cells. Two hours later eosinophiLic and
basophilic inclusions nppeared in most of the affected cells. As the infec-
Lion deVelol)(1d, the nuclttu-,; sbifted Co ant! Uf LIM poleii. "'trucLural challg~_-fl
in the cell organelles, especially the mitochondria, were prominent. Complex
membranous-vesicular structures consisting of cytoplasmic vacuoles formed
around the cells. Discrete granules were scattered about the cytoplasm.
Virus particles concentrated on the periphery of the. cells. These fi.ndin.-s
1/2

USSR
BOCHAROV, Ye. F., et al., Izvestiva Sibirskogo Otdeleniya Akademii Nauk SSSR,
Seriya Biologicheskikh Nauk, No 10 (190), 1971, pp 131-137
are in agreement with the results of morphological studies on other picorna
viruses and support the view that virus isolated from rheumatic fever
patients belongs to the enterovirus group.
2/2
- 22 -

USSR UDC 534.6
BLINOVA KOLES'~'IKOV, A. Ye., LANIGAN B.
L
"Acoustical Measurements"
Moscow, Izdatellstvo standartov, 1971, D 2
Translation of Annotation: The book c.onsiders methods of
measuring the parameters of acoustical processes in air, licuids,
and solids and evaluates methods of measuring sonic Dressure in
various media as well as the effect.of interferer.--e and diffrac-
tion phenomena on measurement results.
General problems of acoustical metrology are considered.
Descriptions are given of modern electroacoustical sonic trans-
mitters and receivers used in measurements. Problems in spec-
tral, correlational,and statistical analysis, as applied to vari-
ons cases of measurement practice, are discussed. Attenlion is
given to questions connected with measurements in physiological
acoustics. Methods of eplibrating electroacoustical converters
1/2

USSR
BLINOVA, L. P. et al, Izdatelfstvo standartov, 1971, D 2
for the reception of sound and vibrations are analyzed in detail.
Also, methods are described for estimating the measurement error,
and recommendations are made for processing measurement results.
The book is designed for workers engaged in verification
operations, for metrological organizations, for control air! mea-
surement laboratories, and for specialists in acoustical measure-
ments.
There are 24 tables, 143 illustrations, and a bibliography
of 89 titles.
212
- 36 -

'L
JSSR, 'UDC 534.6
~ILINOY~A, L. P., KO=-SNIKOV, A. Ye., LANGANS, L. B.
"Acoustical Measurements"
Moscow, Izdatel'stvo standartov, 1971, pp 270-271
Translation:
TABLE OF CONTEETF-PS
Foreword
Chapter 1. General Problems of Acoustical Metrology
1.1. Measurement units
1.2. Government standards in acoustical measurements
1'.3. Measurement transmitters and receiver-s of sonic
oscillations
1.4. 'Elect_-onic ecuinrqent for exciting electuro-
acoustical converters
1/7

USSR
BLINOVA, L. P., et al, !zdatel'stvo standartov, 1971, Do 270-271
1.5. Electronic equipment for am-plifying, in-a-icating,
and recording signals.
Chapter 2. Condit-ions Sol, Fundonental Acoustic 11-~easure-ients
2.1. Operation modes in acoustical measurements. Use
of harmonic, frequency-modulated, noise, and
pulse signals.
2.2. Measuring sonic pressure in air. Dampening and
reverberating ch~,mbers.
2.3. Measuring sonic pressure in liquids. Measuring
hydroacoustical basins, devices for absorption of
sound. Recuirements of measurement basins. Measure-
ments in open tanks.
2/7
- 37 -

USSR.
'BLINOVA, L. P. et al, Izdatel'stvo standartov, 1971, pp 270-271
2.4. Effect of interference and diffraction P~henomena
on acoustical measurements.
2.5. Measuring the-power of sonic transmitters, deter-
mining their e~ficiency--
2.6. Determining the directional characteristics and
the directional factors of transmitters and
receivers in various media.
2.7. Acoustical measurements in solids. Measurements
in steel, concrete, and ice.
2.8. Measuring acoustical resistance.
2.9. Measuring vibrations: acceleration, velocity,
and displacement.
3/7
0

USSR
BLINOVA, L. P. et al, Iz-da-uellstvo standartov, 1971, Dp 270-271
Chapter 3. Analysis-of-Measurement Signals
3.1. Forms of snectral analysis and types of analytic
ecuiDment.
3.2. Characteristins of tyT)ical analyzers.
3-3. Choice of optimal conditions for spectral analysis.
3-4. Mathemat-ical basis of correlation analysis.
3.5. Description of typical correlation analyzers.
3.6. Correlation analysis of acoustical processes.
3-7. Statistical analysis.
3.8. Measurement of nonlinear distortion.
4/7
- 38 -

USSR
BLINOVAJO L. P. et al, Izdatellstvo standartoy, 1971, DD 270-2271
Chapter LL. Meacurenents in Physiological Acoustics~.
4.1. Modern problems in audiology.
4.2. Psychological aspects of hearing and its quantitative
characteristics.
4.3. Audiometers and hearing equipment.
4.4. "Artificial Ear" and "Artificial Mastoid"
instruments.
4.5. Reliability of audiometers.
Chapter 5. Calibrating Measuring Acoustical Eouimment
5.1. General calibrating problems. Absolute and relat--ive
calibration. Rules for checking measuring equipment.
-5/7

USSA
BLINOVA, L. P. et al, Izdatel'stvo standartov, 1971, Du 270-271
5.2. Calibrating sonic transmitters and rec6ivers
on the basis of the reciprocity principle.
5.3. Calibrating microphones and hydrophones with
acoustical tubes.
5.4. Calibrating electroacoustical converters by the
pistonphone method.
5.5. Calibrating electroacoustical converters by the
electrostatic method.
5.6. Calibrating measuring hydrophones by the
C, . . -
piezoelectric compensation method.
5.7. Calibrating hydrophones in a liquid oscillatuinS
column.
5.8. calibration -methods based on nonlinear effects.
5.9. Calibrating vibration receiver-s.
6/7
301,

USSR
.-BLINOV.A, L. P. et al, Izdatel'stvo standartov, 1971, -Dp 270-271
Chapter 6. Conditions of Accurate Acoustical Measu'rements
6.1. Estimating measurement reliability.
6.2. Factors determining the accuracy of basic acoustical
measurements.
6.3. Automation of measurement operations as a means of
improving accuracy in measurement results.
6.4. Metrological processing of measurement results.
Appendix
Bibliography
7/7

USSR UDC 616.288-75+616.2-03,S.113-053.2-085-339:576-8581-039-71
YEM-11OL'YEVA, Z. V., a1,L-JQYA .1. FURER, N. I.I., RITOVA, V. V., KUC.~-,~Ir--~&O,
L. P., NEIILEROV3. '-'-A, B. H., 3H--ERa-kKOVA, E. G., SCiL113Ti1n~,'E. I., OHWVA,
L. N., and FAENSHTEfNi, S. L., Chair of Microbiology, Central Institute for
Advanced Training of PiWsicians, and Institute of Virology itaeni D. I. Ivanov-
skiy, USSR AcaderV of medical Sciences, Moscow
"Prophylaxis of influenza and Other Acute Respiratory Diseases Among Children
Through AcLministration of Leukocytic Interferon and a Stimulant of Interferon
Production (UF Virus)"
Moscow, Voprosy Virusologii, No 4, Jul/Aug 71, pp 442-446
0
Abstract: An ex-pross method of preventing influenza and other azute respira-
tory diseases was tested in childrens' institutions in Eoscov; during the in-
terepidemic period of V;arch-June 1968 and during the influenza epide."lic in
January-February 19601. The project was carried out undler strictly controlled,
coded experimental conditions. The 750 children, aged 10 months to 7 years,
were divided into four groups at random, and the preventive agents were ad-
ministered intlranasaliy. Ore grout) received leu.~.oc'vti~c L-iterferon t-wo ti-Tes
per day for 7 to 42 days. The second group received interferon with liquid
eem-aline. The third group received U.-F virus once daily for 3-4 days with
1/2

USSR
YMIOLIYEVA, Z. V., et al, Voprosy Virusologii, No 4, Jul/Aug 71, PP 442-44-6
intervals of 3-4 days. The fourth group received placebos. The effectiveness
index of interferon was 3.0 (frequency of diseases three tjjres smaller than in-
the placebo group) in the interepidemic period and 2.2 during the epidemic.
The effectiveness index of interferon with eemoline was 1.8, and that of UF
virus was 3.0 in the interepidemic period. All differences are statistically
significant. Since no toxic effects were observed, the method is recommended
for the prevention of influenza and other acute respiratory diseases.
2/2

'USSR UDC: 616.988-75-085-371:576.'05.23(ECHOY/-030'.-P;
V., VOROSHILOVA, M. V., =VOLIYEVA. Z. V., Centre-l
Ei V Z, I-
Institute for the Advanced Training of Physicians, Institute of' Viroloz_v in. eni
Ivanovskiy, AcadeV of Medical Sciences USSR, Instslitute of FoliorVelitis and
Viral Lhoephallitides, Acader,7 of Medical Sciences U55a, Moscow
"Study of the Epidemiological Effectiveness of the Stimulator of Interferon
Formation Diming m Outbreak, of A2 (Hong Khog) Influenza"
Moscow, &earnal ILikroggiologiii Epidemiologii i -Tirmaunobiologii" , Vol 48, 11-Yo 1,
Jan 71, pp 70-73
Abstract: More than 100 new viruses producing respiratory diseases have been
discovered during the past ten years, requiring develop-ment of new prophylactic
methods.
A study in groups of children and Wults showed that ZhV1-h (Zhiv--y--
enterovirusnaya vaktsina-live enterovirus vaccine), a stir--~LLIator of interferen
formation, had a prophylactic effect for healthy persons in contact -,rLth inf ected
persons. Per=oral immunization of chaidren b-1 vaccine (in a 1 :10 dilution) at
1/2
- 56 -

USSR
BLINOITAJ M. I., et al., 7jiurnal Mikrogiologii Epiderniologi-I i lim-,iunobiologii,
Vol 48, No 1, Jan 71~ PP 70-73
Uw-wc--k intervals reduced incidence by a factor of 2.8; the protective coeffi-
cient was 0-0. The same results were obtained with adults. After intranas-I
administration of the vaccine, the incidence of influenza dropped by a factor
of 2.6 and -the protective coefficient was 61%. Persons i-i-~o received a single
vaccine administration bad a rdld foria of flu. Mhen people received the vaccine
twice or three times, only isolated cases were observed. There were no incidents
af allergy or side reactions. The best effect was observed when the i-accine
was used in a 1 :10 dilution perorally.
2/2

112 _027 UNCLASST F I ED PROCESSING DATE--115,r-P.,
TITLE---;-A,v,YLXSE INDUCTION IN L CELLS. EFFECT OF THE MOOE OF CELL
HARVESTING ON THE AMOUNT OF REGISTERED AMYLASE ACTIVITY -U-
.AUT4H0R--PODG7AYETSKAYA? D.YA-r GERSHUN, V.A., IGNATOVA, T.N,., BLINOVA,
M.I., PRIDLYANSKAYA, I.I.
ZOUNTRY OF TNFO--USSR
SOURCE--TSITOLOGIYA 1970, 12(2), 253-6
DATE PUBLISHED ------- 70
SUBJECt AREAS--BIOLOGICAL AND MEDICAL SCIENCES
TOPIC TAGS--TISSUE CULTURE, CULTURE 4EDIUMv AMYLASE, BIOSYNTHESIS
CONTROL M4RKING--N'? P(~STRICTIONS
DOCUMENT CLASS-LINCLASSIFIED
DROXY CF~L/FRA4F-1986/0943 STED klkl--UP/qO53/70/011-)IOC)2/025.1/o256
CIRC ACCESSION NO--AP0102884
0',"LASS IFIED

N01i)noNi ".lNIIS3AkJVH 31dWIS bO -H03W ONidna ssvig ~iHi hob=, sii.33
Dr-.IiIS--')AbVH n0 SOOH13W IN3b~i~JIG A@ 0;!)NVH) 99 OlnOO 13~iJ=O 03b31S153~3
~Hl JU AZIS :~;k.!J- 'SIS3HINAS 3~%AZN3 :io Noi-onONI 31vcisgns -ivDio-
N
N]SdA~il IN31;dinN 'SISHI 01 HOevIS JCi'NUGV b3ljV S113D
I NI AIIAIIOV 3SVIAWV G3SV31IONI 'IDVbiSbV -0-dO
-IjS8eOlOdV--3N N(jJSS33:)V Obl'~
Oto~Sll--31VO ~MSSJDOU 0313ISSVIONn 120 Z/2

Inorganic Compounds
USSR UDC 5412-6lz 46-791-31
BUNOVA, N. I., KOZHIMA, I. I., RODIONOVA, L. P., and SOUM3EV, V. I.%
"Solution of Some Uranii-im Oxides in Sulfuric Acid"
Leningrad, Radiokhindya, Vol 15, NO 31 1973,, PP 391-397
Abstract: Chanp_es in the composition and structure of tetragonal and cubic
uranium oxides durinG solution at 900 in 2.0, 10.0, and 15.0 N 112S04 were
studied. Solution was carried out in an Ar atmsphere. Solution of U1,00 and
beta-U (~ -oroceeded with an ingignificant chanCe in the chendeal corl-mosition.
Other oxide phases did not form, in the process. The concentration of H2S04 had
no effect on the liird-ting composition of the two oxides. The lower lirlit of
the existence of the U409 phase was at a con.T-osition in the-vicinity of
and that of the beta-TJ phase at a co=osition in the vicinity
UC~2-231+0-005 307
of U02.287+0.0051 "or 90`-"UY~ and tetragonal and pseudocubic oxides vith the
_U the limiting compositions variet-1 ~dth the con-
cor-Mosi'ions UO - to U02.401
2-3f
centration of" F12SO4 and with the method b~,, which the initial oxide had been
.112

USSR
BLINOVA, N. I. et a! Radiohhimiya 7 97
j Vol 15, No 3, 10 3, PP 391-30
prepared. As shown by the compositions on solution first in 2 11 1 SO). and
~2 1
then in 10 N H2SO4. the changes in composition were rever-.:ible fo-r these
oxides. The lower Limit of existence of the gamm-UV7 phase at 900 was at
a composition in the vicinity of TJO2.-3)t6+o-005' In 'he case of the Oxi(3-08
the behavior of which varied irith the r.Jhod of prepLIrn-'-..ion, one coulO
assilme a lack of uniformity in the phase composition of the sw:-,imles, I'thich
were apparently inhomogeneous in that respeci. 'Bie aut'nors thank Prof.
U. bl. Thlmachev for his help in the investigation.
2/2
- 14 -

USSR
UDC 576-85531.1-~9-097.21.07
PETROVSKAYA, V. G. and BT.TNgg4_ Institute of Epidemiology and Micro-
biology imeni Gamaleya, Academy of-Hedical Sciences USSR
"Assessment of the Significance of Type-Specific Antigen in the Virulence
of Shigella. flex-neri 2a in Studies of Recombinants of Certain Genetic
Classes "
Moscow, Zhurnal Mikrobiologii, Epidemiologii i Immunobiologii, No 10, 1971,
pp 69-74
Abstract: Conjugation of the virulent S. flexneri 516 2a strain vith the
nonpathogenic E. coli K12 HfrC, Ab 312, and AB 732 strains produced dif-
ferent classes of hybrids with definite genetic characters and antigenic
structure. The virulence of these hybrids was studied in different bio-
logical models. After intraperitoneal infection of white mice, it was
impossible to differentiate the rultures from the results of the kerato-
conjunctival test. However, extremely virulent strains could be differen-
tiated from attenuated ones in chick embryos. The virulence of the
attenuated hybrids that included the rha+xylt region was rcgularly reduced
by a factor of two compared with virulent cultures. Shigella strains can
be differentiated more accurately with respect to virulence by using the
1/2

USSR
PETROVSKAYA, V. G. and BLINOVA, N. I., Zhurnal Mikrobiologii, Epidemiologii
i Immunobiologii, No 10, 1971, pp 69-74
"pulinonary" model, quantitative keratoconjunctival test, and Forrial model.
Loss of the type-specific antigen by lactose-positive hybrids did not affect
the virulence of the strains. Loss of the type-specific antigen by previously
attenuated hybrids resulted in behavioral differences in the models studied
compared with attenuated recombinations possessing the type-specific antigen.
The authors concluded that type-specific antigens play a secondary role in
the virulence of S. flexneri 2 a and that some still unknowil. factor is of
decisive significance in this respect.
2/2
5

USSR UDC 541.451:546-791
RODIONOVA, L. P., and TOLMACHEV, YU. M.,
&I-PYA-1te N E
"Reactions of Vixed Uranium Oxides With Acids"
Leningrad, Hadiokhimiya, Vol 12, No 6, 1970, pp 835-838
Abstract: '.Then U308 is dissolved in acetic acid at 600C in concentra-
tions ranging from .3 to 17.2 M, the lower equilibrium oxide formed
in 7.0 M, CH)COOH is U02 57' In perchloric acid U~08 yields U C,
(U02. e i e range' 8.25 to
,,~O)Was the low r e ullibrium oxide in conc n ration
2.0 hen U205 is dissolved either in acetic or perchloric acid at
900. the same oxides are formed as in the case of U308. Reaction of
U308 with 1 N nitric acid at 400 or 600 in presence of anthranilic
acid yields the pentoxide U205- X-ray analysis showed that in the
equilibrium oxides (up to U02.g7) there exists the hexagonal phase,
characteristic of the U205 oxi e.

USSR
UDC 376.851.49(Shigella).097.21.07
JUN nd im ni ma
L,9.jA.j._ I., Institute of Epidemiology a Microbiology e Ga leya,
f1i6d-cal Sciences USSR
qUse of a Pulmonary Model for Determining the Virulence of Shigella Hybrids With
Various Genetic Characteristics"
Moscow, Zhurnal Mikrobiologii, Epidemiologii, i Immunologii. No 9, Sep 70,
pp 32-36
Abstract: The "pulmonary model" was developed by Voyno-Yasenetskiy in 1957 to
study the virulence of pathogenic intestinal bacteria. The irodel was considered
to represent in excellent means for studying the virulence of Shigella flexneri
recombinants with various genetic characteristics. It indicates the specific
capacity of Shigella strains to enter a given type of epithelium, is suitable
for quantitative determination of their multiplication in cells. and may be
applied In studies with readily available animals. In the present study a viru-
lent strain of Sh. flexneri (516 2a) was used as a recipient, and two strains of
E. coli (HfrC and Hfr AB 31Z) were used as donors. The animals were infected
intranasally. Distinct differences were noted in the propagation of virulent
attenuated and avirulent hybrids of Shigella. The "pulmonary model" is an ex-
pedient means for characterizing the vir-alenoe of Shigella hybrids. which could
not be differentiated distinctly by the keratoconjuctival test.

LTDC 6-2-95
NUMSDANYAN, K. A., B NUA'.A-a., STONOV, L. D., DAKU11:2,14-KO, L. A.., and
UEAM-NA, 11. 1-1.
"Concerriing the Herbilcidaa Activity of Certain layl- and Allt~yl-Conl'alriing
Thioureldes, Thiou,-eaz and Thiouriacils"
V ab. Khim aredstva zazhchity rast. (Chemical Agents for Pl-.~Lrvt Protection
collection of wo=:-~;), vyp 1, N'oscon, 19?0, pp J.97-200 (fron
Ho li, Jun ?-2, ,otialiractl Ito 1!1~44j)
Translationt The fc1lcWLrj-' 00,1POLMOIS v--ro zYnthesizocip.
0
racils (I) (R and the melting point in OC are cited)i Pie, 2611-51 Et, 202-3;
Pr, 172-3; But 16'3-4; iso-Eu, 2141 M; Ph, 2.561 -C.'C"141
COO' 0
with the formula PliCONTIC51,71M (H) (R and the melting peoint in OC are eitcd)l
Mat 1501 Et, 133r Pr, 133; Iso-Pr, 113-4; But 51-Z; t,:xt--1-'u, 127--8i CUNInt
152-31 Ph# 14,'~j o-CIC6114, 145-6; 1>-021"C6"41 182; P-'!'j2"'C6"W 166-?; and
s U b-
Stances with the formula Ii2NCSHR (III) (R and the meltinr: point in OC are cited).
J.
110, 108; Et, 1081 15?; But ?9; iso-Bu, 9,3-5- Urt-r3u, 1.65; 83;
1/2

USSR
-hIJRIDZWJIYAN, Y. A. , et al., V sb. J~hjm, eredstva mshchity x-ast., Vyp -1,
MOSCOW, 1970, pp 197-200
97; Ph, 1541 o-CIC6H4, 142; p-0 p- Y'e -2-3-
COW 21.' 'F4' 190; 2"C6'T',4- 18
Cozpounds 1 slhow I-A-hu hcrbicidal activity with res met to ronocotylcd,,)r!3
c -
and dicotyledons than -Lha corresponding uracils. Data aze presented from
tests of cor-Doimds 11 and 11I.
2/2

USSR
UDC 632.95
BLINOIYA,__Y,,G., IVANOVA, S. W., KLIMKINA, L. G., SHVETSOV-SHILOVSKIY, N. I.,
--~;d-MEIDNIKOV, N. N.
"Method of Preparing 2-Oxo-3-chrysanthemoylhvdroxymethylbenzoxazoline or
2-Thio-3-chrysantliemo,,,lhydroxvmethylbenzoxazoline"
USSR Authors' Certificate No 259891, filed 2 Aug 68, published 1.2 May 70
(from RZh-khimiya, No 1, 10 Jan 71, Abstract %'o LN597P)
Translation: Compounds of the general fonaula ~(-~~Y)OC,1130:%CII20COC11C~le2t!ICFI
-::--=Gfe2 [I; C03 W -- substituted o-phenylene; X-===Il, halogen; Y~~O or S1
are obtained by the reaction of benzoxazolinones or benzoxazolinethiones
with acid chloride of chrysanthemumic acid (11) in the Presence of an ]ICl
aCCeDtor, e.g. C5115~1, at temperature 0-90 in an organic solvent or without
it. ExamDle. To a suspension of 0.01 mole 3-hydroxNi-riethylbenzoxazoline-
thione in 10 ml anhydrous PhMe are added 0.04 mole C5fI5N with stirring and
then, drop'7ise, at temperature 5-9' a solution of 0.01 mole II in 10 ml
PhMe. The reaction mixture is stirred for 5 hr at,-v20*, after which
C5H5N-HC1 is filtered off. The solution is extracted consecutively wich
a 5% IICl acid solution, an NaIIC03 solution, an NaCl solution, and dried
over Na2SO4. The solvont is distilled off in vacuum, and the residue is
1/2

USSR
BLINOVA, V - G. , et al. , USSR Authors' Certificate No 259891, filed 2 Aug 68,
published 12 May 70 (from RZh-Khimiya, No 1, 10 Jan 71, Abstract No 1N597P)
crystallized f rom heptane, to vield 2.9 g I (X -11, Y -::= S) , melting point
91-2'. The following I's are synthesized Tindicated here are X, Y, 1". vields,
melting point, 'C)- ff-, 0, 90, 85-6 (heptane); 6-Cl, 0, 93, oil; 6-Br, 0,
91, 78-9 (heptane); 6-Br, 95, S, oil. Compounds possess high fungicidal
activity.
212

1/2 013 UNCLASSIFIED PROCESSING DATE--230CT70
TITLE--LARGE SCALE PROCESSES AND NUMERICAL SIMULATION OF THE GENERAL
CIRCULATION OF THE ATMOSPHERE AND LEING RANGE WEATHER PREDICTION -U-
AUTHOR-BLIN9VA, YE.N.
COUNTRY.OF INFO--USSR
SOURCE--METEGROLOGIYA I GIDROLOGIYA, 1970, NR 6, PP 3-15
DATE PUBLISHED ------- 70
SUBJECT AREAS--ATMOSPHERIC SCIENCES
TOPIC TAGS--ATMOSPHERIC CIRCULATIONt LONG RANGE WEATHER FORECAST
CONTROL MARKING--NO R6STaICTIOUS
DOCUMENT CLASS--UNCLASSIFIED
PROXY REEL/FRAME--2000/1744 STEP NO--UR/0050/70/000/006/000310OL5
CIRC ACCESSION N(]--AP0125362
UNCLASSIFIED

212 013 UNCLASSIFIED PROCESSING DATE--230CT70
ClRr- ACCESSION NO--AP0125362
ABSTRACT/EXTPACT--(U) GP-0- ARSTRACT. PROSPECTS OF THE DEVELOPME,4T OF
INVESTIGATIONS ON LARGE SCALE PROCESSES AND NUMERICAL SIMULATION nF THE
GENERAL CIRCULATION OF THE ATMOSPHERE AND LONG RANGE WEATHER PREDICTION
ARE STATED. FACILITY: GIDROMETEOROLOGICHESKEY NAUCHNO
ISSLEDOVAT-ELISKIY TSENTR SSSR.
"NCLASSIFEE-0

USSR
BLIOKH, ZH. L., and LIBEWAN, V. A. Institute of Problems of Information Trans-
ssit-.n, - 'ML-my of Sciences, USSR, Macaw
"The Influence of Beryllium Ions on the End Plate Potential and Frequency of Minia-
ture End Plate Potentials at ~Voneural Junctions in the Frog"
Moscov, Biofizika, Vol 15, No 3, MY/Jun 70, pp 447-452
Abstract: The addition of 0-05-0.1161 of beryllium to Ringer's solution, containing
a muscle-nerve preparation from a frog, results in a block at the myoneural Junction
caused by inhibitioa of the release of mediator quanta. Analysis of end plate
potential amplitudes during Be-block Indicates that Be++ reduces the probability of
release of mediator quantum in response to a nerve impulse. There is evidence that
Be ++ in a competitive antagonist to Ca++ in this process. The mechanism of this
competition correlates with the decrease of Ca-influx into the nerve endings in
response to nerve impulse.
1/1

UDC 535.421:62-86(088.8)
BLOM A. A., Leningrad Opticomechanical Association
"Device for Scanning a Diffraction Grating"
USSR Author's -Cer-Lificate No 234704, filed I Apr 67, published 30 May 69
( from RZI-Met-rolopiya i Izmeritellnaya Tekhnika, No 1. Jan 70, Abstract
1.32.1343 P)
Translati;o~,: The proposed device for scanning a diffraction gorating con-
sists of a rotacing stand, mechanism for changing the grating, and a
mechanism for turning operations -othich is made up of levers with rulers of
cosecant -mechanism and a roller with an actuator screw with a nut. in order
11-o increase the accuracy of angular displacement of diffraction gratings, a
correcting mechanism is installed in the device which consists of a guide
bar ,r_-.h carriage to which a roller is fastened, which, in turn, is connected
LO a d;ive mechanism in such a manner that the carriage can receive MoLion
only along the axis of the guide bar. The mechanism for changing gratings
C,
A~ -
,as cz-chea, connected through a verlical shaft -?~~ith levers, which shift
simultaneously with the changing of gratings*
1/1
- 153 -

1/2 029 UNCLASSIFIED PRCCESSING DATc--IBS-:P70
TITLE--THERMALLY ACTIVATED SLIP lN LITHIUM FLUORIDE CRYSTALS -U-
AUTHOR-(03)-GAYDUCHENYA, V.F., BLISTANOV. A-A.9 SHASKOLSKAYA, M.P.
COUNTRY OF INFO--USSR
SOURCE--FIZ. TVERD. TELA 1970, 12(l), 35-41
DATE PWiLISHED ------- 70
SUBJECT A,,,EAS--M4TFr-%IALS, PHYSICS
TOPIC FFFECT, RELAXATION PRCICESS, SlINGLE C,YSTAL, ACTIVAT11-;'i
Ell';_--VGY, Cw~YST.,,L L.%TTI(-.F STkUCTU,--,,E, LITHIUM FLI_llj~~IL)Z:
CC".'Tkf'L %IAFK I NG-k~l RESTR ICTION'S
D0C*j'~-rl;T CLAS.S--!,":rL_'SS!FIP0-
PP'U"XY kEEL/FRA~vE-1 STrP
GIPC AC~--SSinrq %1;1--AP004,9519
UNCLASSIF-IED

OS3SV3N)Nl *dW31 ONIIS31 -1HI SV
H31HM, SWGIV AlmdWl A2 S3SS3dIS :10 MO1iVXV19'd -Ab SS3:)u-td
3ril ~~A SN,01111~)Olslo tio ONIN00,19 :!HI 01 031V-1-~ 3tN 'N53:3~!O-CUIZ-0141
-v :dS3 '(nVI)ACINV UIVI)H S;I' -
IV r?411'dV-LS 03DNnONO-ed 0 N -'C N 3 d ~1 0
JH1 =i~! A~iC-3Hi 3H1 hO6A SP4011VIA30 'U520 :3HI '-~IVIS 0:-:iTV3?qNV 3H1 N1 C;4
'9iNf',3 :111 >,LIJ ONV 'NONG) AlihndWI MOI V HIPA SIV'.LSk*d*) :Al doi IGSVC svm
AbFj:-;Hi ~AOOV :-;HI JO A GNV H :10 33N9(1NOdS3b*dO3 ?3ii3g V *NSj3b93C1OUZ-LL
14 Ab'01-3141 aill HIP't 119M AlIN313I 3=in3 3-3,30V A 35~~VHXI 3h'i
ONV H SNOIIVOOISIG AO N011OW 3HI 30 N'OIIVA113V -30 Aq-b9N3 3HI *(AdOgHl
.~3HOS13-13 3HI) 33111VI 3HI AO SNOII'dDISIO IVNODV'dl=i 30 30NV-V3ddV
3H1 JO llflS=-),) V SV A11'dFJdWl 3HI JO SWOIV Ag SIVISA~ID :10 9NJN3HI!)N-~tJ,-LS
30 A809HI 9141 HIIM 11=11M S301t,'OV nV1 INIOd 0131A 3HI 30 IN:-'iNGdWCO IVW'-'13HI
3H1 30 90N3(1Nad3G *d1131 ~Hl *S31VIS 03d3dW-~I ONV 03Hngn
IN93~-,13d *IV T'D '91N03 All owv ill IVISkgo 319NIS 9-~ind NI 031V',)IIS3ANI
SVM dTIS :10 tNSMVH3-3:W' gHi 'NS99-d9300947-LL IV SN:~6133t'~S IVISPi3 3ITNILS
:36 NIGISS~~*ddk,03 ND (.n"vl) NDIIVX713d SSTdIS :3C1 31V~l 3HI. GNv invinvi)
IN'10d 0-131A 9H.1 ONi ~jnsV 3.q A'd -C-dc)
OLdi-SRT---41VJ 4-DNISS3DOdd o9ji issvi).\,n &ZC Z/2,

USSR
IILTT-S-YlTUjjj~t. IM. Voronezh
UDC 539,376:532.135
"Deternination of Rheological Parameters iii Quasistatic Problems Of the
Nonlinear Theory of Visco-clasticity"
Priklachnaya Mckhanika, Vol 8, No 3, 1972, pp 68-72.
Abstract: The rheological relationships betwoen stresses and, strains; al-C
studied oil the basis of the -eneralized conditions oil isochronism of creep
curves for a complex stress state. These relationships are used to solv(?
PI-Oblevis of tor..;ioll (if ar- isotropic, visco-elastic stl.aighL Circul'-'r Cyli"l-
(ter. The I~or di, telilli 11'al Oil of vJ.,--CO-(!],'L!;LIC' Panmicters ;jie
discusscd.
1/1

Z. -1~( 1 4 a
6 R e
,-1.;..-- -11-- .. - --',
I F~ i
IV,q (V 5 C~;~ E
/3 L U. , - - -
-

USSR
!MC 632.954t631.445.2
B%Y~Ev.~)~,, KOZLOVA, L. M., Candidate of Biological Sciences, Leningrad
Sc entific Research Institute of Forestry
"Effect of Various Doses of Herbicides on Soil Fertility"
Moscow, Xhimiya v sel'skom Khozyaystve, No 11, 1972, pp 50-53
Abstracts Results are presented from laboraotry tests in 1968-10.70 conducted
to study the effect of ordinary and increased doses of herbicides recommended
for application in forest nurseries on the nutritive regime of the soil.
Tabulated dataare presented for simazine, dalapone, and sodium trichloro-
acetate Indicating their effect on the nitrate and ammoniacal nitrogen con-
tent in the soil, the hl=us and total nitrogen content In the soil and the
P205and K20 content. The soil mechanisms giving rise to the results are
discussed. Wken used in the recomrgnded doses, the herbicides resulted in
A
Increased accumulation of nitrates after a month with maximum nitrate content
In the version with a mixture of dalapone and 2,4-D. Twenty days after
Injection of the herbicides the ammon-Jacal nitrogen content increased some-
what. In increased doses the herbicides inhibited the nitrate accumulation
process in the soil for the first month. The strongest inhibiting effect
resulted from a mixture of sodium trichloroacetate and 2,4-D. Intensifica-
1/2

BInvirormental C'r Eco--.otdcal Prnblers
IUSSR
T-2-1 -1 17 7 %IP
D' U FUM R, I . B
DDV'.'.GVAw.) IZE. F., and 1,LLMONGNIA, R. Ye.
joint S`Iu.-~y of A-'.,-:,j,-,Thcr4Lc -Polluidon in Certain lt-~clustlial Centers of
the Central Vol.--- Rcj~ion"
Sb. nauch. tv. Kuybyshev, [~-;--iyeny (collection of Scien'ClIfte '"'Orks of 'ile
Ku,llbyshev Scientific lIcsca.-_-clt InGtitute of No 7, 1972, pp 192-93
(f 0111 Fi_711-GeoTiZ' 'a t No c
11, _L3 . , svodxrrw ton, No 5, 1`973, Xbstrac ~).cj,
Tmnslaticn: A stu*p ~fat; ri3de_ Of the coll'ami.
ac Uv,~ by
ical anul oll-Ofinin.- .-u-nd of thta i~avnct c)-.'
and ss_iclme_~;s ral-le of ciii-I-ciren a--,,(1 on indox,~s of anirals.
L%_'-asures hwe- buun claborated for the elindnation and rec'ouction of' srec-ific
dischar,-cs -into _'W;.,.jsDh-are, for t-lie or;Trmization of sanitary chiciding of
industrial oites, a.-d for 17,7,rovint; the health of th~_~ child po,pula~,J_ori.
1/1

Org&nophosphorous Compounds
USSR
UDC 632-95
a"nYUKI ZA--K-, KVASHA, Z. N., SPLNTSEVA, L. M., FADEYEV, YU. N., UNTERBEIRGER,
and YOLOVA, M. K. , All-Union Scientific Studies Institute of Phytopathology
VProcess for Preparing Mixed Dialkyl Esters of the Higher Alkylphosphonous
Acids"
Author's Certificate No 340665, filed 22 Jun 70, publsihed 29 Jun ?2, (from
Referativnyy Zhurnal -- Khimiya, No 8(11), 1973, Abstract No 811470P by T. G.
Chekareva)
Translationi Compounds having the general formula RP(OXOR')OB" (1)(5- alkyl,
R' and R!' - CIto C6) have acaricidal activity to the stable and sensitive
form of vegetation mites. They are prepared by the reaction of RP(O)(0R')0H
(11), with a 5-10-fold excess of R"OH. For example, C12 is passed through a
solution of 0.03 moles of II (R-C 9H01 R'-c6H13 ) and 0.15 moles of absolute
BuOH in 20 ml of C112C12 luntil the appearance of a yellow-green color. It is
then concentrated and product I (R-C H19, RW H13, R"aBu) is obtained, having
20D _ 20 9 6
a 1.4435, `14 -0-92111 a boiling temperature of 176 to 1780 at 1 Mmm,
a/iold of about 100%. Other analogous compounds were prepared. R,R1 and R"

USSR
UDC 632.95
W W, Yu. I.,
KVASHA, Z. N., VARSHAVSKIY, S. L., BARAN I
BLIZML
LIBMAN, B. Ya., STREL'TSOV, R. V., PROTASOVA, L. D., MARKOVA, L. I.,
MIOKHLOV, P. S., MADZHARA, G. A., KIRILINA, L. E., All-Uuion Scientific
Research Institute of Phytopathology
"A Method of Making Thiophosphonyl Dihalides"
USSR Authorrs Certificate No 337384, filed 31 Oct 69, published 2 Jun 72
(from RZ)i-Khimiya, No 9, May 73, abstract No 9N500 by T. G. Chekareva)
Translation: Compounds of the general formula RP(S)X2 (1) (R = rl-C,2-alkyl,
cycloalkyl, aryl, unsubticituted alkyl or alkyl containing substituents, Cl
or Br; X = C1, Br) are synthesized by reacting (RS)3P (11) with a 2-10-fold
exces s of PX3 with heating to 250-330'C in an autoclave, Example. A mixture
of 0.07 mole of Il (R = Me) and 0.7 mole of PC13 is heated in an autoclave
test tube of stainless steel at 290-320*C for 5 hours. The excess PC13 is
driven off at atmospheric pressure and distillation of the residue in a
vacuum gives I (R=Me, X=Cl), boiling point 70-3"180, n20D 1.55,10, d4 20 1.4421,
yield 52%. Similar methods are used to produce other compounds of type I
(given are R, X, boiling point in *Clmm, n20D, d4 20, yield in %): Et, C1,
64-8/15, 1.5418, 1.3527, 58; Pr, Cl, 85-8/15, 1.5285, 1.2942, 40; iso-Pr,
Cl, 72-5/15, 1.5290, 1.3017, 47.5; Bu, Cl, 111-13/25, 1.5269, --, 65;
1/2

USSR
SUKHOMLINOV, B. P., Vopr. tekhnol. ulavlivaniya i pererab. produktov
koksovaniya, Kharkov, 1972, pp 50-56
sulfur with a sufficient amount of powdered SL. A SN screw mixer is recom-
mended for bringing the components into contact under pressure and pulveriz-
ing them at the same time.
2/2
- 30 -

USSR UDC 632.95
4LjPP[UK,-N,-K,t, KOLOIaYETS, A. F., GOLUBEVA, R. N., GRANIN, Ye. F.,
FADEYEV, Yu. N., VRUBLEVSKAYA, L. S., VARSHAVSKIY, S. L., KOnf&N, L. P.,
VnMANSKIY, K. N.
"A Method of Making Derivatives of Aryl Esters of B-Isothiuronium
Ethanesulfonic Acid"
USSR Author's Certificate No 337381, filed 1 Aug 63, published 1 Jun 72
(from RZh-nimiya, No 9, May 73, abstract No 9N522P by T. G. Chekareva)
Translation: Compounds of the general formula R03SC2H4SC(NII,)=NIH-HA (1)
(R - aryl un-substituted or substituted by Cl, No2, Me; A = CI or an organic
acid radical) are synthesized by reacting Ch2-CIIS03R (II) with salts of
thiourea or a mixture of thiourea with inorganic or orgaric acids. Example.
Solutions of equimolar quantities of II and thiourea hydrochloride in
butanol which are saturated at 60-90*C are heated at 80-90*C for I hour,
cooled, and filtered, giving I with a yield of 85-96%. Evaporation of
the mother liquor gives an additional quantity of 1. The overall yield of
I is 95-100%. The following compounds of type I (A = Cl) are synthesized
(given are R and the melting point in 'C): Ph, 165-6; 4-ClC6H4 (Ia),
1/2
471

USSR
BLIZNYUKx N. K. . et al. v USSR Author's Certificate No 337381, f iled I Aug 63,
published 1 Jun 72
144-6'- 3-CIC H,, 168-70; 2,4-C1 2C6H3, 157-9; 2,4,5-Cl3C6H , 178-80; 2,4,6-
-C13C6H,, 18~ '(decomp.); 4-NO 2 C6H42 155-8; 3-MeC6H 16M Saturated
aqueous solutions of equimolar quantities of Ia anA,2,4--Cl*c H
2 6 30CH2COONa
are mixed at 90-100'C,, cooled, and filtered, giving compound I (A =
2,4-Cl2C6H30C[12COQ-, R = 4-ClC6H4)I melting point 134-5*C, yield 99.5%.
in concentrations of 3 .1-25 mg per liter compound I suppresses the growth
of the mycelium Botritis cinerea and Piricularia orysae by 50-100%; in
concentrations of 0.25-1 mg per liter, compound I suppresses the growth
of spores of Botritis cinerea and Piricularia orysae by 8-100%, and in a
concentration of 0.1% the chemical suppresses rust of the wheat strain
Puccinia graminis f. tritici by 42-58%.
2/2

USSR UDC 632.95
,~LIZNYUK PROTASOVA, L. D., KVASHA, Z. N., KLIMOVA, T. A., and
KLOPKOVA, R. S., All-Union Institute of Pbytopathology
"Synthesis of Thiophosphocyclopentenyl Chlorides"
USSR Author's Certificate No 327208, filed 16 Jun 70, published 28 Mar 72
(from Referativnvy Zhurnal -- Khimiya, Svodnyy Tom, (I, L-5), No l(II),
1973, Abstract No LN457P by T. A. Belyayeva)
Translation: The intermediate products for the synthesis of pesticides, the
alk-.ylthiophosphocyclopentenyl chlorides, were prepared during the reaction
of diene hydrocarbon with alkyldichlorophosphite and PSC13 at 100-150%.
Example. One mole BuOR is added to 3 moles FC13 at 15-200C with constant
stirring, the mixture is heated at 60-650C for 2-3 hr; the reaction mixture
is cooled to 0-5'C, then 1 mole of colled Cf12=CHCH=C112 and 3 moles PSCI
are added, the mixture is heated in a stainless autoclave at 110-1200C ior
3 hr. The mixture is distilled and the mixture of acid chloride isomers of
thiophosphocyclopentenic (2 and 3) acid is separated from the reaction
mixture. The yield was 81%, b.p. 120-1400C/14, n20D 1,5840, d~,O 1,3225.
The acid chloride of 3--.iethylthiophosphocyclopentenic-3 acid was also ob-
tained, b.p. 137-140OC/12, n20D 1,5895, m.p. 43-45*C, as well as mixture
1/2

USSR
BLIZNYUK, N. K., et al., USSR Author's Certificate No 327208, filed 16 Jun 70,
published 28 Mar 72
of isomers of acid chloride of 3-methylthiophosphocyclopentenic (2 and 3)
acid, b.p. 125-1350C/12, n2OD 1,5845. Example of the reaction with
piperylene.
2/2
- 17 -

USSR
UDC 632.95
BLIMVM, N. K., LEVSKAYA, 0. S., KVASHA, Z. N., IIATYUKIIINTA, Ye. N.
"Procedure for Obtaining Bis-thiolphosphonates"
USSR Author's Certificate No 319605, filed 16 Mar 70, published 17 Jan 72
(from RZh-Khimiya, No 2 (11), Feb 73, Abstract No 2N530)
Translation: Fungicides with the formula AICH2SP(O) (OR')R]2 (1) (R = alkyl,
aryl, aralkyl; R' = alkyl or aryl, A = arylene) are obtained by the reaction
RP(O)(OR')SR" (II) (R" = alkyl) with xylylendihalogenide at a temperature of
140-200' in an organic solvent. As an example, a mixture of 0.05 moles of
II (R = r-CIC6114, R' = R" = Me) and 0.025 grams of 1.4-(BrCR2)2-C6H4 in 5 UIR
of xylol is boiled to completion of precipitation of MeBr, it is evaporated
and the I (A = 1,4-C6H4, R = 4-ClC04, R' = Me) is separated. The yield is
67.3%, the melting point 167-8'. The I is synthesized analogously (R, R',
yield in %, n20D or melting point in "C are presented) A = 1~4-C04: Et, 'Me,
96, 1.5580; Me, Et, 97.4, 1.5330; 4-1-IeC04, Me, 88, 160-2 (acetone) ; PhCH2,
Me, 95.7, 1.6075; A = 4-HeC6H3-1,3: 4-CIC6H4, Ife, 92.4, 152-4 (acetone).
I/l

USSR
UDC 632.95
BLIZNiYUK, N. K _, KHOKHLOV, P. S., KVASHA, Z. N., KARKOVA, L. I., LEVSKAYA,
G. S., PROTASOVA, L. D., SOLNTSEVA, L. M., NMATYUKHINA, Ye. N., VARSHAVSKIY,
S. A., BARANOV,Yu. I., LIBMAN, B. Ya., ZHEMCHUZHIN, S. G.
"Method of Production of Dichlorides or Dibromides of Thiophosphonic Acids
or Their Bis Analog"
USSR Author's Certificate No 332095, filed 19/08/69, published 17/04/72
(Translated from Referativnyy Zhurnal Khilmiya, No 24(11), 1972, Abstract No
24N591, by T. A. Belyayeva)
Translation: Compounds of the formula IZP(X)X2 (I) (R=alkyl, aryl, aralkyl;
X=Cl or Br) and X2P(S)A(S)PX2 (II) (A-bivalent hydrocarbon radical) were pro-
duced by the reaction of mono- or dihalo hydrocarbons with S, P-and PX3 with
heating to 250-400' in an autoclave of stainless steel or nickel in the
presence of catalytic quantities of 19 or its compounds. Example. A mix-
ture of 0.24 mole PhCl, 0.24 g-atom S, 0.16 g-atom white P, 35 ml PC13 and
0'05 9 12 is heated at 290-330' for seven hours in an autoclave of stainless
steel, the PC13 is distilled, then vacuum distillation is used to separate
I (R=Ph, X=Cl), yield 60%, B. T. 109-1120/3, n20D 1.6241. Similarly, I
were produced (given R, X, yield in %, B. P. in 'C/mm, n20D): 4-Clc6114,
1/2

USSR
BLIZNYUK, N. K., et al., USSR Author's Certificate No 332095, filed 10/08/69,
published 17/04/72
Cl, 53.5; 124-3/1.5-2, 1.6229; p-MeC H4 Cl, 54.5, 125-7/1, 1.6120; 4FC6H4,
Cl, 72.2, 95-7/0.5, 1.6028; Ph, Br, 9l,'127-130/2, 1.6850; 4-FC6H4, Br, 55,
135-8/1, 1.6758; PhCH2, Cl, 76.4, 120-3/2, 1.6150; 3-FC6H4, C1, 108-110/1.5,
1.5908; 4-11,IeC04CH9, Cl, 53.3, 126-9/2, 1.6035; 4-ClC6H4CII2, Cl, 61.6, 129-
133.2, m. p. 74-6', --; 2-FC04CH2. C1, 61.6, 129-133.2, m. p. 48-9', --;
2.4-~'e2CO302, Cl, 47.5, 140-1.6045; 2.4-C12C03CH2% Cl, 43.4, 147-9/2,
m. p. 100-1", --. Also produced were II (X=Cl, A=CH2CU2), yield 61.5%,
m. p. 92-3*. 1 and II are intermediate products for the production of
insecticides, acarocides, fungicides-'and herbicides.
2/2

I M_
LTc 6 2.95
BqZRYUK, 11. K., PROTASOVA, L. D., and KVASHA, Z. N., VEII (All-Union
c-`~- fi-c'Rd_&e-&rch Institute) of Phytopathology
S en 4
"Preparation Method of Anhydrides of PhosphacycloTenteric Acid"
USSR Author's Certificate Ho 314?54, filed 4 Feb 70, published 26 Jan 72
(from Referatinvyy Zhurnal -- Khimiya, Svodnyy Tom, No 19 (11), 1972,
Abstract No 1914458 F by 1. A. Mlel'nikova)
Translations Anhydrides of phosphacyclopentenic acids which are intermediate
products in the synthesis of organophosphorous compourds are preF-ared duriln.-
the reaction of corresponding acids with their acid chlorides (AC) by heating
the mixture in the absence of solvent and fiC1 acceptor. A m1xtU-.C0 Of 0-05
moles of phozphacyclopentenic acid (I) and 0.05 Moles OfE' AC of i Is heated
at 1500c for 30 jain, to I hr followed b~,3 romoval of the AC of T (TI). The
yield of product was 9~,.J, with n.p. 4)- 1 C, boiling point 215-2-20"C/1, AcIU
chlorides of other acids are aynthasized similarly (aaid involycd, 11o' yield,
boiling point in 0C/mm are given in that orde--)t 2-FlethYl-l, 93, 190-195/0-5,
n'L 114 r
'D I-qWZ65, 20 1-25121 3-methYl-I, 93, 230-235/1, A rzixturu Of 0-0.~ ;:Ole
~L
of II and 0.25 mole of absolute 1-1e0lf is heated at- 20 0C for 10-1-9 hr 1 d 11); F,
(methyl eater) of I is separated. The yield 76%, 1,olling point b0-82 C;/2,
1/2

USSR
BLIVIYUK, N. K., et al,, MSR Author's Certificate No .314754, filea 4 Feb 70,
published 26 Jan 72
n 20D 1.4860, d211 1.1913. To the remaining avount of 1 0.06 mole of AC I
~ 4
Is added# the mixture is heated0at 100-1500C until evolution of HC1 stoppa
(gas), and evoporate at 130-150 C115. The residue contains, 11 to which
0.25 mole MeOH is added without a preliminary purification. After separating
the methyl ester of I by the aboye methods tho yield was C14% (on conversion
to startin- II). To t~e remaining residue (whitc cryotals) AC of I Is added
again and the whole process is repeated again. The yield of a ready pro-
duct is 86%. The methyl esters of acids (constant, % yield, boiling point
in 0C/mz, n2OD, d20 a--- given in this order) are prepared in ana-logoud
Wayi 2-methyl-I, 80-90, 100-105/2, -/1.4830, --,-1.1343; 3-methyl-I,
63-87o 100-105/2, 1.4~6o, la4?6.
2/2

UDC 632.95
BIJ7,N7UK,_P. K.,-PROTA30VA, L. D., and k-VASHA, Z. N., VTJI (All-Union
SCientific, Research institute) of Phytopathology
"Preparation Mlethod of Anhydrides of Pho3phacyclopentcnic Acid"
USSR Author's Certificate No .3114754, filed 4 Feb -to, published 26 Jan 72
(from Referatinvyy Zhurnal -- Kbiniya, Svodnyy Tor., No 19 (11), 1972,
Abstract No 19N458 P by 1. A. Mel'nikova)
Txanslationt Anhydrides of -nhosphacyclopenterlic acids which aree intermediate
products in the synthesis of organophosphorous compounds are prepared dur~n i-
the reaction of corresponding acids with their acid chlorides (AC) by heating
the mixture in the absence of solvent and HC1 acceptor. A mixture of 0.05
moles of phosphacyclopentenLe acid (1) and 0.05 moles of AC of 1 is heated
xl
at 1500c for 30 121.11, to I h-tiollowed by 8 removal of the AC of 1 (11). The
yield of product wa5 97;2, wi h m.p. 43-441 G, boiling point 2-11'-2200C/1. Acid
chlorides of other acids are synthesized similarly (acid in-~olved, 1% yield,
boiling point in OC/.= are Eiven in that order)t 2-methyl-I, 93, 190-195/0-5,
20 11C 20
n D I.r2o d 1.2512., 230-235/1- ~ nixtur2 of 0,05 nole
4 3-r~ethYl-I, 93
of II and 0.25 mole of absolute ReOff is heated at- ?.Oc)C I-or 10-12 hr ar.1 ?2
.f
kmethyl eater) of I is separated. The yield 76%, boiling point
1/2

WO 3 R
BLIZ11YUK, 11. K., et al., USSR Author's Certificate 110 314754, filed 4 Feb 70,
published 26 ja-n 72
20D - .4p
n 1 '60, 20 1.1913~ To the remaining amount of 1 0.06 mole of AC I
d4
is added, the mixture Is heated0at 100-1500C until evolution of HU stopp3
(gas), and evoporato at 130-150 C115. The residue contains II to which
0.25 mole keOH is ad-ded without a preliminary purification, After separating
ti
the methyl ester of I by the above method# the yield was 84% (on convex-sion
to starting II). To the remaining residue (white cxystals) AC of I is added
again and the whole process is repeated again. The yield of a ready pro-
duct is 8610, The rinethyl esters of acids (constant, % yield, boiling point
m, n20D, d2o are given in this order) are prelx-tred in analogoud
in OcIn I "
wayt 2-m?-iethyl-I, 8-0-90, 100-105/2t --1.4830, ;-1,1343, 3-niethyl-Ip
63-87, 100-10512, 1.486o, 1.1476.
2/2

US~R Ui)C 632.95
K.- II.-K. I KALUTSKIY, I., A. , ZIMICHUZI 111' , S. G.
"Procedure for ObLaining O-Chloralkyl Amidothiolphosphates"
13SSR Author's Certificate ~Io 296773, filed 28 Nov 69, published 15 Jun 71 (fror,
RZh-Khii-.iva, No 6 (11), Jun 72, Abstract No 6N610)
Translation: Substances with the general formula ha
2
high fungicidal activity (1; R = alkylene; Rl = alkyl, aryl, arqlkyl; R and
R3 alk--,rl or R2R N = a rinu radical) - are ob tain'ed by the react .ion of cyclic
v 17
alkyleneC-I,-;LnI chlorophosplDites t;ith sulfenar.-,ider, with hlE~.-:Ltin- of an eqvii-olar
U
mixture of rengents to 60-1.00'. A solution of 0.025 moles of ethyleneglycol.-
chlorophosphite in 10 ri~. of C 6116is added to a solution of 0.025 rioles of phenyl-
sulphenmorpholite in 5 m' of C 6H6 (reaction temperatur.2 of the mass 3000-
Analogously obt ad are the following.1 (enumerated are Rp yield
112

TiSSR
BLIZNv--UK, N. K., et al, USSR Author's Certificate No 251576, C1.
12oo 26/01, (C 07 f), filed 6 Apr 66, published 20 Feb 70 (from
I
RM-Khimiya, No 19 (11), 10 Oct 70, Abstract No 19 N578F by
G. V. KUzNk;rS0VA)
in percent, d422 and n22-23D): Ett 94.6p 1.5669, 1.5360; and Pr,
84.5, 1.5436, 1-5350. 1 are intermediatos of the synthesis of
biologically active su stances.
2/2

Olt UNCLASSIFIED PKOCESS ING LA"I'E-27NOV70
TITLE--ANflMALOUS REACTION OF ARYLTHIOETHANOLS WITH PHORPHO;~US TRICHLORIDE
_U_
1%UTHOR-(O5)-KHOKHLOV, P.S.v KALUTSKIY, L.A.t NAZAROV, T.A.9 MOCHALKIN7
A,I.t BLIV11YUKo N.K.
=1NITRY
SOURCE--ZH. OBSHCH. KHIM. 1970, 40(411 795 1
DATE PUBLISHED ------- 70
SUBJECT AREAS--CHEMISTRY
OPIC TAGS--ETHANOL, PHOSPHORUS CHLORIDE, ORGANIC SULFUR COMPOUND, ARYL
RADICAL, ORGANIC SYNTHES15
XNTROL MARKING--NO RESTRICTIONS
KICUMENT CLASS--UNCLASSIFIED
IROXY RFEL/FRAME--3006/1502 STEP NO--UR/0079/70/0'to/004/07')5/0797
IRC ACCESSIO.'.1 ',1O--APrj135163
UNCLASSIFIED

212 OIL UNCLASSIFIED PROCESSING DATE--27NOV70
IRC A:CCESSIOIN NO--AP0135163
BSTRACT/P-XTRACT--(U) GP-0- ABSTRACT. ADDING 0.01 MOLE PCL SUB3 TO 0.03
MOLE PHSCH SUB2 CH SUB2 OH AND 0.05 MOLE ETHYLE,',JE OXIDE 'IN, MEPH AT
a-50EGREESt HOLDliNG AT 10-150EGREES UNTIL REACTIVE CL HAD 8EEN CONSU'iED?
AND EVACIJATING THE MIXT. SEVeRAL HR AT 100DEGREES GAVE AFTER ADD.N. OF
0.01 MOLE .4 SUB2 0 AND HEATIiNG TO 100DEGREES, A LITTLE PHSCH SUB2 CH
SUB2 OH, B SUB2 110-17DEGREES, AND 80.9PERCENT (PHSCH SU,32) SU32, M.
61-20EGREES. Slj'-,ILA7'LY WEr%F PPEPD. THE ANALOGS WITH ARYL GROUPS SHOWN:
P-MEOC SUB6 H SUB4 (1) M. 102-30EGREES; O,CLC SU86 H SU84, M.
75-60EGREES; AND P,CLC SU36 H SUB41 M. 87-80EGREES. IF PCL SUB3 IS
REPLACED BY PHCH SUB2 PCL SUR2 THE IST REACTIONGAVE THE SAIME PRODUCT BUT
IN 61PERCENT YIELD; REPLACING ETHYLENE OXIDE BY ET SUB3 N GAVE A
68PERCENT YIELD OF THE SAME PkODUCT; IF HCL ACCEPTOR fS OMfTTEOt THE
REACTIWI WITH PCL SUB3 GIVES MAIINLY CLCH SUB2 CH SU82 SPH. HEATLNG 3
MOLES PHSCH SUBZ CH SUB2 OH WITH I MOLE (ET -SUB2 N) SUB3 P AT
120-30DEGREES WITH DISTN. OF ET SUB2 NI-1 GAVE AFTER FINIAL TREATMENT WITH
I MOLE H SUB2 0 AT 90-100DEGREES 2 HR, 77PERCENT (PHSCH SUB2) SU32.
HEATING 0.06 MOLE PHSCH SUB2 CH SU82 OH WITH 0.03 MOLE H SUB3 PO SUB3
AND A TRACE H SUB2 50 SUB4 IN XYLENE 3 HR WITH SEPN. OF H SUB2 0 GAVE
68PERCENT (PHSCH SU32) SUB2. REACTION OF P,MEOC SU36 H SUB4 SK 141TH
(BRCH SU32) SU82 IN ETOH GAVE 33PERCENT 1; ANALOGS riERE PREPO. SIMILARLY
,FOR STRUCTURE PROFF. FACILfTY: VSES. NAUCH.-ISSLED. INST.
-FITOPATOL.t USSR.

USSR
UDC 632.95
ELjZ'4Y6jjj Z. N., VAI,.ShAIVSi~IY, S. L., and !.:kD3KLiL, G. A.,
All-Unim, a`cientific Research Institute of Phytopathoilog~-r, Xoscmr, ---'rdstry
of Agricul-uure USSR
"A liethod of Preraring 1-Uxed Esters of Dithiophosphonic Acids"
USS-14 Authors; Certificabalio 222384.. filed 20' oct 66, publislied 20 J;-n "C'
(fro!,,i Referativnyy Zhurnal Fhirrdya, !-'0 17, 10 Sept 70, Abstract ;.o 17 1~5-' P)
Iranslation: A vdxture of 0.03 g-mole of acid chloride of 3-0thyl -.ethy--,-thio-
phosphante, 0.12 g-mole alcohol, 1 nolli P2~ and 2 mold pyridine is for-
4 hours at 90-1000C, and 0 S-diethyldithio~~osrlionatep C 5", 0,65 2 i
isolated vith a 2rield of 8Z~ and a boiling point of 78-89C/2f n2~0_~
1-5310. 0-i-,etliyl-S-I)heYV2.dithip;riethylr~nosphonate C8 11110P52 is also
irith a yield of 10C~, melting point of 46-70C, 1,i20D = 1.6125-
T. k. '-Eelyayova

USSR
UDC: 547.26'118.07
BLIZILIIIYUK, N.,K., LEVSKAYA, G. S., MATIMHINA, Ye. N., and
VAIi~_kVSKIY, S. L., All-Union Scientific Researcr, In5t;_-itute of
Phytopathology, Moscow, Ministry of Agriculture USSR
"A Method of Synthesizing 1,4-bis-(O-alkyl-0-aryLtli-*Lopliosphoryl)-
benzenes"
Moscow, Otkrytiya, Izobretdniya, Promyshlennyye Obraztsy,Tovarnyye
Znak-i, No 14, 1970, Author's Certificate No 268420, filed 22 May
68, p 23
Abstract: This Author's Certifiz~ate introduces: 1. A method of
synthe.5izing 1,4-bis-(O-alkyl-0-arylttiiophosphoryl)-I)C-nzenes of
the general formula A,O,.
110 0~ 0;1
w~,-.ere Ar is a substituted or unsubstitated phenyl or napthyl, and
R -L7s an alkyl. As a distinguishing feature of Lhe patent, the
appropriate 1,4-bis-(O-~i,-,,-'Lchl.orothiophosphoryl)-benzenes are
P
Jjj4-p['ak,tVrI witti alcoholq :.n a, solvent sach as benzene
- I i organic
;I?Lrh the applicat-ioncf Ooa~ 'In Lhe presence of an organi.c base
such an pyri(line as a ciilinlyn!-, with subsequent isolation of the

USSR
BLIZNYITK, N. K., e'%,., al., Otkrytiya, Izobretneiya, Promyshlennyye
Obraztsy, Tovarnyye Znaki, No 14, 1970,
goal product by conventional methods. 2. The method described
in (1) is distinguished by the fact that the temperature reaches
60-900C.

USSR UDC 547.241.07
BL-IZNLYUKV N. K., PROTASOVA, L. D., WASPIA, Z. N. I aCid
S L., All-Un-on Scientific Research Institute of Phytopathology,
M~scow, Ministry of Agriculture USS11
"A Method of Synthesizing 1,4-Phenylenehe),abenzy'i-dipliospiionium
Chlorides"
Moscow, Otkrytiya, Izobreteniya, Prontyshlennyve Obraztsy, Tovarnyye
Znaki, '-Za 14, 1970, Author's Certificate No 2~8418, filed 7 Jun
68, p 23
Abstract: This Author's Certificate introduces: 1. A method of
synthc-,,--,izing 1,4-phenylenehexabenzyldiphosphon4Lum clilorides- The
distinguishing feature of this procedure is that 1,4-phenylene-
bis-dichlorophosphine is interacted with substituted bensylchloride
and white phosphorus in the presence of heat with subsequent
isolation of the goal product by conventional methods. 2. The
method described in (1) is distinguished by the fact that the
temperature reaches 170-2200C.
1/1

USSR
UDC 547.553.1.261.118.07
BLIZNYITK, N. K., LEVSKAYA, G. S., and VARS_;~VS-K!Y, S. ATI., A11-
Union Scientific Research institute of Phytopathology, Ir.,oscow,
Ministry oi- Agriculture USSR
"A Ilethod of Synthesizing Bis-(arylo:.-ychloroth4Aopliosphoryl)-benzenes'I
I-l'oscow, Otkrytiya, Izobreteniya, Promyshlennyye Obraztsy, Lovarnyye
Znaki, No 14, 1970, Author's Certificate No 268421, filed I Mar
68, pp 23-24
Abstract: This Author's Certificate introduces: 1. A method of
synthesizing bis-(aryloxychlorothiophosphoryl)-ben:~enes of the
general formula A-rO x_Z P_OAr
~ P -C I
CI
where Ar is an unsubstituted phenyl, or a chi-oro- or nittrosub-
stituted phenyl, or an unsubstituted naphtyl. As a distinguish-
ing feature of the patent, 1,4-bis-(dichlorothiopl,.osplioryl)-
benzene is interacted with a substituted phenyl or naphthyl with
heating in the presence of catalytic quantities of salts of esters
of polythiophosphoric or thiophosphoric acidg or semiproducts of
1/2

.USSIR
BLIZNYUK, N. K., et al., Otkryt.-*L.Ya, Izobreteniya, PcomyshlenRyye
Obraztsy, Tovarnyye Znaki, No L4, 1970
their synthesis such as a mixture of phosphorus peQtasulfide or
pyridine pentasuLfide in an organic solvent such. as xylene with
subsequent isolation of the goal product by conventional methods.
2. The method desc~-ibed in (1) is distinguished by the fact that
the temperature reaches 100-2000C.
21~

USSR
aXU _N...J~., PROTASOVA, L.
BLT,,Z
9'c'!en_tific' Research Inst.Ltute
of Agriculture USSR
UDC 632.95
D., and KVASW-%, A. NLI. , Ill-Union
of Phytopatholo-y, ~-Iorcow, Ministry
L)J
"Method of Preparing Tin-Containing Dithiophosphonates"
USSR Authors' Certificate No 248673, filed 7 Flay 63, published
22 Jan 70, (from RZh-Khimiya, No 20 M), 25 Oct 70, Abstract No
20 N554P by S. LYUBARSKAYA)
Translation: Compounds of the formula /~~op9s09r0ssn(R2 )7 0 (1-
R = alkyl, aryl, aralkyl; R' = alkyl; Z-= substituted or-uNub-,
stituted aryl) are obtained by the interaction of tt-Le anhydride
of dithiophosphonic acid with bis-(arylhydroxydialkyltin)-oxide
at 50-1000. To a solution of 0.014 mole (MePS)2S2 in 10 ml ClPh
is added 0.007 mole /_2,4,5-_-I 3_C614,,0Sn(Bu2)--720, and on conclusion
of the exothermic re-Ection it is hP-ated for 2 hOUr3 in a boilin-f
-richloro-
water bath; the solvent is distilled off and.bis-(2,.I'5-L.
phenoxymethyld-'LL-hiophosp',iinyldibutyltin)- oxide, n2 D i.6005,
melting point 87-900, is obtained. x1nalogously obtaincd are the
following L W = Bu; given are R, A, melting or softening point,
n20D): Me, alpha-riaphthyl, 47-50, --; Ph, 2,4-CL,?C6IiI, 58-601 --;
Ph, p-N02CO4, 50-2, 1.635; PhCH2, Ph, 52-4, 1.6083; 1hCH 7 2P4-
1/2 2

USSR
BLIZNYUK, N. K., et al., USSR Authors' Certificate No 248673
C1 C H 87 9, 1.6145. I's can be used as physiologically active
sugsQ*
nces and catalysts.
2/2

USSR
UDC 632.95
~"I njJK_tN. K. PROTASOVA, L. 0., AW,tSIIV~, Z. N., VAIts.-LIVS;uY,
S. L.7XIM-M'i-on' Scientific Rescar(:-,~', lnstitLIte Of PhytOpathOlOgy,
Moscow, %,11inistry of Agriculature U~;SII
I'Method of Preparing Quaternary Phosphonlum Chlorides"
USSR Authors' Certificate No 250131-, filed 23 Nar 68, p-libLisho-d
4 Jan 70 (from IRZh-Khimiya, No 20 (11), 25 Oct 70., Abstract ~.Io
20 N553P by I. M. IIIL'SHTEYN)
Translation: Compounds of the general formula
(1) (R and R' = 'I lkyl, Ph, PI CH substituted FLA
(Cff~--) ~'CL
or - 2stituted aryl 7,
hCI12; and X and Y are substituted or unsu L
which may possess physiological activity, are obtained by co-F-
jugated alkylation o~ chloro or dichlorophosphines witii benzyl
chlorides at 170-3200. 12 or Lewsi acids can be used as catalyst.
The process can be initiated by UV irradiatioQ. A mixture of 0.03
mole benzy1dichlorophosphine, 0.04 gram atom white Ph and 0.135
mole PhCH2CI is heated in a stream of Nq until distillation of
PG13 ceases (3-3.5 hours); excess PhCI12CL is distilled off the
residue is dissolved in alcohol, and kept in a crystallizer 19-
20 hours, and I (R = R1 = FhCH2, X = Y = Ph) is separated out,
1/2