SCIENTIFIC ABSTRACT CHEMERIS, N. A. - CHEPULIS, G. K.
Document Type:
Collection:
Document Number (FOIA) /ESDN (CREST):
CIA-RDP86-00513R002200520019-0
Release Decision:
RIF
Original Classification:
S
Document Page Count:
100
Document Creation Date:
November 2, 2016
Document Release Date:
August 9, 2001
Sequence Number:
19
Case Number:
Publication Date:
December 31, 1967
Content Type:
SCIENTIFIC ABSTRACT
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CIA-RDP86-00513R002200520019-0.pdf | 3.65 MB |
Body:
USSR
1MG 576-314,576.8
FIM40, B. A., and CHEMORIS, N. A., Institute of the Biochemistry and
Physiology of IlicroargME-ss, -Kc-gre-my of Sciences USSR, Pusbchino on t~e Oka
WThe Mechanical Properties of Cell Val-Is of Microorganisms"
Moscow, Mikrobiologiya, Vol 40, Ito 6, Nov/Dee 71, pp 1060-1063
Abstracti The rheological properties of living cells of nicroorganisms can
be determined on inclusion of these cells into macrofilms irith known elastic
properties, In the procedure applied, the elasticity modulus E of gelatin-
glycerol films containing calls of microorganisms was determined by stretching
the films in one direction. If addition of cells did not change E of a
film with a definite composition, E of the cells could be assumed to be
equal to that of the film. The relation E - kc9 applied to gelatin-glycerol
films, where c is the concentration of gelatin. On the basis of experimental
results, the 0.1-600 kg.=?- range of B, which could be obtained by varying
c, included the values of E corresponding to thoce of microorganisna, E
for E. coli (0.26 kg/mm2) corresponded to a gelatin concentration of 66.Y.,
At high values of c, stretching of the filn was best carried out, at a low
rate (0.5 rin/sec). The properties of cells were not affected sienificantly
by inclusion into the films and stretching of the latter. Experiments with
1/2
4 FIM4AN9 B. A., and CMERIS, N. A., Mikrobiologiya, Vol 40, No 6, Nov/Dec
71, pp 1060-1063
'Schizosacch. pombee incorporated into the films indicated that the mIls could
be readily observed under a microscope in the course of rheological studies.
They retained their capacity for normal growth and division.
2/2
-'3
3- -
USSR
CHEMERIS, N. N.
"Transformational Grammar for a Fragment of the Russian Language"
Lingvist. Probl. Avtomatiz. Inform. Poiska [Linguistic Problems of the
Automation of Information Retrieval -- Collection of Works], Kiev, 1972, pp
22-33 (Translated from Referativnyy Zhurnal Kibernetika, No 9, 1973,
Abstract No 9VS22).
Translation: The fragment of the Russian language described does not include
single-unit sentences (impersonal, incomplete, etc.), sentences with intro-
ductory words and phrases, sentences containing quantitative numbers, etc.,
as well as sentences with separated components. The grammar describing this
fragment consi3ts of three parts. 'lhe first part is a context-free control
grammar, a generalization of the domination grammar: the right portion of a
rule not only notes the controlling element, but also indicates the type of
control. The terminal symbols are not word forms, but rather characteristics
of entire classes of word. forms. This grammar generates nucleus statements.
The second portion -- the transformational grammar -- processes the marker of
the components marked for control and the characteristics of the nucleus
statement, converting them to transform statements, The third portion, onl,Y
1/2
- 79 -
USSR
Chemeris, N. N., Lingvist. Probl. Avtomatiz. Inform. Poiska, Kiev, 1972,
pp 34-47.
briefly described in the article, includes supplementary transforms of state-
ments in place of certain characteristics in the independent transforms and
constructs the final chains of characteristics which are replaced by Russian-
language word forms. Ye. Burgina
f -
2/2
USSR
BOYKO, YU.V-, CHWERIS, V.T.
NNEWIM&
UDC[621.362:5:",8.41-16:5~5.9.083
'movement Of Electrical Arc In Transverse Magnetic Field"
V eb. 'Teplotekhn.probl.pryamogo Preobrszov.energi (Ileat-Engineering Problems
Of Direct Energy Conversion--Collection Of Works), Issue 2, hiev, "Nsuk.dumks,"
1971, pp 95-102 (from RZh--Elektrotekhnika i energetika, No 12, Dee 1971,
Abstract No 12A186)
Translation: The paper presents a scheme, a description of the arrangement of
an experimental installation, the peculiarities of a system of Drobe measure-
ments, and the results of a study of the movement of an electrical arc in a
magnetohydrodynamical channel with argon and argon with an additive Of DOt8BSiUm,
in a transverse magnetic field. A diagram is presented of the distribution of
the speeds of motion of the arc with respect to the length of the channel as well
as the scheme of movement of the are with respect to the electrodes. 4 ill. 4
ref. [In-t el-dinamiki AN USSR, Kiyov--Institute Of Electrodynamice AS UkrSSR,
Kiev]
1/1
USSR uDc 669.243.87
GUDIMA, N. V., IE~--V. A., BYKOVA, T. D., and ZOOKOV, 0. M.
"Effect of Current Density on Production Cost in Electrolytic Nickel Refining"
Moscov, Tsvetnyye Metally, No 3. Mar 70., pp 29-33
Abstract: The production of nickel in electrolytic shops may be raised by increa8-
ing the number of electrolyzers, raising the current density., and simultaneously
adjusting the principal operational parameters, such as nickel concentration,
electrolyte salt composition, and the circulation rate. The optimum current
density must be determined for each individual plant taking into consideration
the specific process technology and changes in various items of expenditures as
a function of current density. With the shop expenditures being a major portion
No-45t,) of the total conversion cost, it vas the objective of this paper to
determine the correlation of current density and shop expenditures on the basis
of report data of an electrolytic shop. It was also essential to establish the
factors, other than current density, affecting changes in the absolute shop
expenditures, eliminate these affects, and arrive at 11net" (cleaned) expenditures.
Depending on production volume, the items subject to changes are: vithin-plant
transport, maintenance of basic facilities, current repairs, and depreciation,
1/2
41-
USSR
GUM%, X. V... et al., Tsvetnyye Metally, NO 3, Mar 70, pp 29-33
Within the period of analysis, the production volume at this specific shop was
affected by the number of electrolyzers, current density, cathode surface, current
yield, and extensive utilization of electrolyzers. Formulas are cited for deter-
mining shop expenditures as a function of current density. Calculation shows that
an increase in current density -from 241-3 amp/mP to 388.9 amp/m2 and the resultant
higher production volume made it possible to reduce the shop costs of 1 ton of
cathodic nickel by 45-4-
2/2
USSR
MARKOVA, Ye. V., CHEMLEVA, T. A.
"The Composition Principle of Investigation of Multicomponent Mixtures"
VopTosy Kibernetiki. Nekotoryye Voprosy Planirovaniya Eksperimenta [Problen's
of Cybernetics. Certain Problems of Experimental Planning], Moscow,, 1972,
pp 73-86 (Translated from Rcfcratixnyy Zhurnal Kibernotika, No 6, 1973,
Abstract No 6V294, by the authors).
Trans lat i oil: MICII COMj)()SjtiOIl-j)rOj)CrtY diagrams aro studied, it is necessary
to develop sequential experimentation plans. The sequence of plans should be
constructed so that all or part of the experiments of the initial plans are
included in subsequent plans, i.e., planning should include the composition
principle. This article presents a classification of typical situations
arising in planning in diagrams with qualitative factors which are us'eful
for the development of the composition principle of planning,
34 -
USSR
CHEMLEVA, T. A., ADLER, Yu. P.
"Decision Making in Informalized Stages of Planning of Experiments in
Studies of Composition-Property Diagrams"
Voprosy Kibernetiki. Nekotoryye Voprosy Planirovaniya Ekspcrimcnta [Problems,
of Cybernetics. Certaiii Problems of Experimental Planning], Moscov.,, 1972-
pp 97-103 (Translated from Referativnyy Zhurnal Kibernetika, No 6, 1973,
Abstract No 6V297, by the authors).
Translation: Methods of experimental planning are ever more widely included
in the practice of studies of composition-property dinprams. In the past
10 years, large numbers (if plans have beeii suggested -for various tasks.
In developing each new specific assignment, a decision must be made con-
cerning the selection of some definite, most suitable and efficient plan for
realization of the task at hand as an experiment. This work Studies problems
related to making thi.5 selection.
1/1
USSR IMC 669-2951292'71
T. A., Moscow
yELYLrrIN, 0. P.j KALININ, G. P., SOBOIKV, N. N., and
"Optimum Planning of the Eyperiment in the Investigation of the Proparties
of Ti-V-Al Alloys"
Moscow, Izvestiya Akademii Nauk USSR, m6tally, No 4, jul/Augg 72, pp 234-238
Abstracti Mathematical methods of planning were used to establish diagrams
of chemical composition and specific electric resistance for titanium-rich
alloys of the Ti-V-Al syztem in the form of an iMDroper simplex with the
vertices x, (109% Ti), x2 (60,1Z Ti, 40% V), and x3(90% Ti, 10% Al). The
use of D- and G-optimum. plans made it possible to construct an adequate
mathematical model of the investigated diagram by means of which the value of
the specific electric resistance at any point of the system can be
calculated. In applying mathematical methods to the investigation of com-
position and properties of multicomponent systems, computer technology can
be effectively applied for processing experimental data, plotting and
statisticaily analyzing the model of the investigated dependence, analytical
calculations of" the studied propertyp and for diagi-damatic representation of
modeling resultz. Three illustiations, one table, five formulas, seven
bibliographic references.
i/I
112 022 UNCLASSIFIED PROCESSING DATE--30ocr7O
TITLE--RADIOCHEMICAL STUDY OF PLATINUM DISSOLul[ON IN ACID ELECTRDLYTES AT
VARYING POLARIZATIONS. 1. EXPERIMENTAL PROCL-DURES AND SOME RESULTS -U-
AUTHOR-103)-CHEMODANOV9 A*N., KOLOTYRKINt YA.M., DEMBROVSKlYt P.A.
CGUNIRY OF INFO--USSR
SOURCE--ELECTROKHIMIYA 1970v 6(4)9 460-6
-DATE PUBLISHED ------- 70
SUBJECT AREAS--CHEMISTRY
wTOPIC TAGS"RADIO CHEMISTRY, PLATINUMv ELECTROLYTEr SOLUBILITY, NITRIC
ACIOv HYDROCHLORIC ACID9 PERCHLORIC ACIDv SULFUkIC ACID
CONTROL MARKING--NO RESTRICTIONS
OCCUMENT CLASS--UNCLASSIFIED
PROXY REEL/FRAME--1998/1149 STEP t4(J--UR/0364/7i)/006/00-t/0460/0468
CIRC ACCESSION NU--AP0121708
UNCL!"SSIFIED
2/2 022 UNCLASSIFIED PROCESSING DATE--30OCT70
,CIRC ACCESSION NO--AP01121708
ABSTRACT/EXTRACT--(U) GP-0- ABSTRACT. THE DISSOLN. OF PT IN H SUB2 SO
SUB41 HCL, HCLO SUB4r HNO SUB3, AND THEIR MIXTS. wAS INVESTIGATED OVER A
BROAD RANGE OF POTENTIALS INCLUDING THE REGION OF H EVOLUTION.
ELECTRODES WERE MADE OF PT PRETREATED IN A STREAM OF NEUTRONS AND THE
QUANTITY OF PT IN THE ELECTROLYTE 4AS FOLLOWED BY RADIOMETRY. THE RATE
OF DISSOLN. OF PT WAS GOVERNED BY THE COMFN. AND CHARACTER OF THE
SURFACE OXIDE FILMS IN BOTH THE ANODIC AND CATHODIC REGIONS. THE KIND
AND CONCN. OF THE ELECTRULYTE WERE OF MINOR IMPORTANCE ONLY.
FACILITY: FIZ. KHIM. INST. IM. KARPOVA, MOSCOW* USSR.
UNCLASSIFIGO
A H6017116-
AUTHOR-- "IAN
'CHEMODANOV'g. fl, DEPUTY CHAIRZ SIBERIAN BRANC4 OF
THE ACADEMY OF SCIENCES, U.S.S.h.-
TITLE-- A BRIDGE LEADING TO THE SHORES OF APPLICATION
NEWSPAPER- SOTSIALISTICHESKAYA INDUSTRIYA, JANUARY 21, 1970,
P 22 COLS 1-5
ABSTRACT-- THE ARTICLE DISCUSSES THE Pa08LEM OF 2RIDGIN^j THT'
RETICAL AND APPLIED SCIENCES. THE AUT14OR CLA IMS THAI MORE 'IHAN HALF
OF THE ASSOCIATES OF MANY INSTITUTES OF THE SIBERIAN BRANCH 01' TPIE
ACADEMY ARE WORKING ON PROJECTS DIRECTLY RELATED TO 1NDUSTRY OQ
AGRICULTURE. THE NETWORK OF RESEARCH INSTITUTES, DESIGN BUR---Ai-ic- AND
PILOT PLANTS WHICH IS BEING DEVELOPED BY THE NOVOSIBIRSK RESEARrH
CENTER OPERATES ON THE PRINCIPLE OF DOUBLE SUBORDINATION., WXICH MEANS
THAT THESE ORGANIZAl*IONS ARE ADMINISTERED BY MINISTRIES, BUT THEIR
RESEARCH ACTIVITIES ARE GUIDED BY THE ACADEMY, THE' CMDRE FOR THE
1/!o
1-7
19600324 ~9-41
AZI0017116
ACADEMY INSTITUTES ARE TRAINED AT THE UNIVERSITY 'WXICH IS PAR7
L
THE-NOVOSIBIRSK RESEARCH CENTER SYSTEM. T14E SAME. PROCEDURE VI
BE APPLIED TO THE TRAININC OF CADRE FOR RESEARCH INSTITUTES AND DE'S411,31M
BUREAUS UNDER DOUBLE JURISDICTION. SOME WILL AMLSO BE TRAINED IN A
NEWLY FOUNDED POLYTECHNICAL INSTITUTE.
THE FIRST ORGANIZATION THAT WAS PLACED UNDER DOUBLE'SUBORDINATION 1S
THE SCIENTIFIC-RESEARCH INSTITUTE FOR AUTOMATED PLANNING AND CONTROL
SYSTEMS /NIISISTEM/ OF THE MINISTRY OF INSTRUMENT CONSTRUCTIONY AUTO-
MATION AND CONTROL SYSTEMS U,S,S,R, TODAY ITS RESEARCH ACTIVITIES
ARE GUIDED BY THE INSTITUH OF ECONOMICS AND ORGAN12ATION OF 1NDUS-
TRIAL PRODUCTION OF THE SIBERIAN BRANCH OF THE ACADEMY.
IN 1966 THE REQUEST OF THE SIBERIAN BRANCH AND CERTAIN MINISTRIES
FOR PERAISSION TO BUILD FOUR NEW DESIGN BUREAUS OF DOUBLE SUBORDINA-
TION WAS GRANTED BY THE GOVERNMENT. RECENTLY PERMITS HAVE BEEN
19G00325
A-NO017116
GRANTED FOR THE CONSTRUCTION OF THREE MORE RESEARCH INSTITUTFS AND
DESIGN BUREAUS OF THIS TYPE, THE INSTITUTE OF CATALYSIS OF THE
CHEMT
SIBERIAN' BRANCH AND THE MINISTRY OF ICAL INDUSTRY HAVE DEVELOPED
PLANS FOR A DESIGN-TECHINOLOGICAL BUREAU WITH A PILOT PLANT. T~4F
MINISTRY OF GEOLOGY S.S.R., AND THE INSTITUTE OF GEOLOGY AND
S T
GEOPHYSICS ARE DISC6SU-j.NG A PROPOSAL TO ESTABLISH A DESIGN SU,~EA[` FOR
DESIGNING GEOPHYSICAL INSTRUMENTS ON THE BASIS OF THEORETICAL "%Nr)
EXPERIMENTAL RESEARCH CONDUCTED BY THE INSTITUTE.
-3/3
19600326
USSR
Cq A
UDC 547.241-)
RAZUIOV, A. I., LIORBER, B. G., SOKOLOV, M. P., MOSKVA, V. NAZVXNOVA,
G. F., ZYKOVA, T. V., CHEMODANOVA, L. A., and SALAKIIUTDINO.V, R. A.,
Kazan' Chemical-Techno~-lo-g,-i--c-a-l-,--I-n-s--t--i-t-u-t-e imeni S. M. Kirov
"Reactivity and Structures of Phosphorylated Carbonyl Compounds. XI. Study
of the Aldol-Enol Equilibrium of Phosphorylated Aldehydes as a Function of
Temperature"
Leningrad, Zhurnal Obshchey Khimii, Vol 43 (105), No 3, Mar 73, pp 568-572
Abstract: The aldol-enol equilibrium of a series of alkyl substituted and
non-substituted phosphorylated aldehydes has been investigated is a function
of temperature using IR, NIMR-111 and NMR-31p spectroscopical analyses. With
increasing temperature the nozisubstituted compounds go from the trans-enol
form through the aldol form into the cis-enol form. In case of the alkyl.
substituted phosphorylated aldehyde only the conversion from trans-enol
form into th~ aldol form has been observed. Quantitative determination of
the ratios of aldol to trans-enol form has been made.
1/i
UDC
,k'CZ-':VA, V V. N-AZ-VU-U1' G F'. "nOVA, T. V. and
I
A. Kazan' in-s'.-J"u-te of Chc-r-dcal Tec'=-oj-c)-~ S. N- ydrcv
Raw
" - alkoxy-
"Subztituted V-Inylp,--c-sphonin Acid Derivatives. X -
v3nylphosph,onic AC-ld D~~rivativcz"
J
j,cnjn,--,d, Zhua:~~l Ot:~hc~,ay Vol i~j, ?o ?J, pr,
Abs- :-:,.c t, t of P- ;;-or-c co'-an'letle studv of
C d 0, 4 i yr- c~ Lj i I
by reaction, Of 1-
thc!--e acir-- c r~,o
in the
Id ItA., I o 7i z~ - (7
1 p h c. 3 ~:Crcc-nt
of onic
-z' t
1. 17 -'re
c
Ide
P-na s 7-, c c!-a well as in
fro.-,
tb~ form Of Cs,
th
1/2 032 U, "CLASSIFIED PROCESSING DATE--13MOV70
T I TLE--fi I GH CHROMIUA DIFFlislu-N COATIING ON CH-`,0MIWi NICKEL AUSTENITIC
STEELS -u-
AUTHGk-(j3j-SmIRNu,v, A.V. i CHEMPUKOVA, E.N., NACHINKOV, A.D.
ccjtjNrRY OF INFO--USSR
SGUACF---=ILIKC-Kiilt'~ICH;-:SKAIA MEKHANIKA MATER[ALOV, VOL. 61 NO, Z, 1970, P.
14-18
DATE PUBLISHED ------- 70
SUBJECT AREAS"MATER14(_S, MECH., IND.t CIVIL AND MARINE ENGR
TOPIC TAGS--CHROMIUM NICKEL STEEL, ALLOY DESIGNATION, METAL DIFFUSION,
14ETAL COATING, CHROMIZING, METAL POWDER, STAINLESS STEEL, 4USTENITIC
STEEL, ALUMINA, IRON ALLJY/(UlE1612 STAINLESS STEEL, (lJ)lKHL8N9
STAINLESS STEEL, (U)lKH18N9T STAINLESS STEEL
CC"TROL MAM ING--NO RESTRICTIONS
DOCUMENT CLASS--UNCLASSIFIED
PROXY REEL/iRAME--2000/1574 STEP 140--UR/0369/70/~)06/002/OCJ14/0018
Clll(. ACCESS(ON NO-AP01~5?00
L I I- I F D
2/2 032 UMCLASSIFIED PROCESSING DATE--13NOV70
CIRC ACCESSION NO-AP0125200
ABSTRACT/EXTRACT--(U) GP-0- ABSTRACT. STUDY OF THE FORIMATION OF A HARD
COATING DURING C011JACT CH.-,OkllZlt%G OF AUSTENITIC STEELS IKH18N9,
IKHISN9T, AND EI-612 I-N A :-41XTURE OF POWDERS CO~,qSISTING OF: 40PERCENT CR,
30PERCEt--IT FECR, 28PERCEINT tLUMINA, ANO 2PERCENT NH41. IT IS SHO'ri:l [HAT
THE TOTAL DEPTH OF DIFFUSION OF CR INTO THE IKH18f49 STEEL IS TWICE THAT
OF THE tI-612 STEEL. IT IS FOUND THAT THE COATING CONSISTS OF AN
OVERGRO41"I AND A PRJPER DIFFUSION LAYER. THE STRUCTUREE AND CHEMICAL
COMPOSITION OF THE COATI;NG AKE EXAMINED. FACILITY:
LENINGRAUSKII INSTITUT AVIATSIONNOGG PRIBGROSTRGENIfA, LENINGRAD, USSR.
UT A S S I i. I t-. 0
In
USSR LJDC: '0 . 7 4
0 C H ME 1" ) V C ~FIIEMIYAIKI- I N." Q._'M
"Calculation of I~otential Functions"
Tr. Zap.-Sjib. n.-i. geolocoran-ed. neft. in-t (11,Corks Of the I "'o
Siberinn Scieit-_:,f-,c Pescarch Institute of Geolo-qical
PYOSPCCtilli~' VI~P. 55, 1)1-, 215-219 (from
NO 10) Oct 72, !I)~;tract Nlo 1.0117065 [authors' abstract])
Translation: A standard rrcnram in Mins'11-22 codes. The proi~r-
is designed for computip(l the potontial function oil objects
Z, -
havina numb--r -Da-.-ameters of m distinctive features. I t c.-I n b -2
C, I
used to deirclop a pattm-n recognition program.
USSR UDC 621-371-029.6
A MWOV, S - KOLAR-P., V - V - , CIE 1,T, 13. B., 1MY1ZOV, I., and
RADMULOVA, K.
"Statistical Characteristics of UHF Signal Distribution Over Open
Land and Nountain Waterways"
Moscow, V sb. X Vses. konf. po rasprostr. radiovoin.. Te,-,is-V dolft.
Sekts. 2 (Tenth All-Union Conference on the' Propagation of Radio
Waves; Report Theses; Section 2--collection of works) "NaWk.a," 1972
W - - - I
Pp 13-17 (from RZh--Radiotehhnika, No 10, 1972, Abstract No
IOA352)
Translation: 3"Xperimental integral functions are given for the
dist-ribution of average-time values of the siewil attenuation D-tc-
tor, togethcr with results of an investigation into the daily
course of the fadine range during the various months for land and
mountain waterways in the rayon of Lake lssyk-Kul'. Two illustra-
tions, bibliography of ?two. A. L.
44 -
USSR
UDC: 550-834
BALASMA11D, M. I., FILIPPOV, N. G., YEFDENKO, M. D., MAYOROV,
V. V., KRASNOPOL-SKIY, A. D., SOLODILOV, L. N., YEVDOKIMOV, G. S., Ramen-
skoye Department of the All-Union Scientific Research Institute of Geo-
physical Methods of Prospecting
"A Device for Emission of a Seismic Signal"
Moscow, Otkyytiya, Izobreteniya, Promyshlennyye Obraztsy, Tovarnyye Znaki,
No 8, Mar 72, Author's Certificate No 330407, Dii-ision G, -filed 20 Jan 70,
published 24 Feb 72, p 142
Trpn lation: This kuthor's Certificate introduces: 1. A device for emis-
sion of a seismic signal. The device contains compressed-air and liquid-fuel
supply systemns and a pneumatic chamber with movable piston which opens and
closen the outlet port of the chamber. As a diatinguif;hing feature of the
patent, the compressed-aIr discharge energy is increused and the heat and
force load on the chamber is reduced by fitting the movable riston with
atomizers which break up the fuel in the compressed air during gas exhaust
and by attaching a device for ignition of the fuel mixture to the chamber
housing. 2. A modification of this device distinguished by the fact that
1/2
1(/14
USSR
BkLASHIUUM, M. I. et al., USSR Author's Certificate No 330407
the movable piston has a channel filled with fuel and communicating with
the atomizer through a check valve, and the cover of the chamber has a rod
which enters the channel of the piston and feeds fuel into it through the
chaek valve. 3. A modification of this device distinguished by the fact
that the attachment for igniting the fuel mixture is made in the form of a
wedge.
2/2
USSR
UDC:547.241
CHENBORISOV, i. Sh., and MR~, V. V.
'Treparation and Properties of Phenylhydrazides of Alkylthioal1kylphosphonous
Acids"
Leningrad, Zhurnal Obshchey Khimii, Vol 40, No 1, Jan 70, pp 43-48
Abstract: Nine title compounds (I) were prepared in 87-93,~ yield by adding
slowly alkylthioallkylphosphonous chloride to a mixture of phenyLaydrazine and
triethylamine in ethyl ether under nitrogen at 00, filtering off the triethy-
In nium chloride precipitate, then distilling the filtrate in a molecular
sti.11. 1-111 1 compounds are liquids which decompose on normal distillation.
Characteristic P-3 bands i..,ere detected in IR spectra of 1. The physical con-
stants of I were tabulated. The I compounds reacted exothermally with sulfur
to form addition compounds - alkylthioalkylphosphonic pheny1hydrazides (II),
viscous undistil.11able oils '(yields 90-94p). Li bands ind-icarive of i~35R group
were present in, the spectra of all II. Predictably I reacted exotnermally
with Schiff bases, e.g., p-benzylidenctoluidine, in petrolem ether under
ni.trogen at 45-50o to give 208-64-?Ao' yields of crystallized addition compounds,
The alkylthioalkyl(p-toluino)benzyl-ii-anilinop~iosphazin-- (=) structure was
1/2
USM
CHMBOKSOV, R. 5h., et al, Zhurnal Obshchey Khimii, Vol 40, No 1, Jan ?0,
pp 43-48
attributed to these compounds, because them,,- did not add 3 even on heatinlo, and
ga-ve phenylhydrazLne hydrochloride on acid. hydrolysis. i easilv reacted,
typically at -0-3co , with aldehy-des and ketones to gjxe oO-9--,j y-Jelds of
C~H Which do not add 3. There are 1? bands indicative
'of xz and, IIIIH groups in 'Lhe spectra of the above compownds.
2/2
56 -
AbStracting bervice: Ker. Lode:
53348- CHEIIIIICAL ABST. it Roi)7