SCIENTIFIC ABSTRACT FR:PLATE, N.A. TO:PLATE, A.F.

• Document Type: CREST
• Collection: Scientific Abstracts
• Document Number (FOIA) /ESDN (CREST): CIA-RDP86-00513R001341200037-6
• Release Decision: RIF
• Original Classification: U
• Document Page Count: 99
• Document Creation Date: November 2, 2016
• Sequence Number: 37
• Publication Date: December 31, 1967
• Content Type: SCIENTIFIC ABSTR

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Kc~~ssro~a tit; u~5o22595 . , .
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Fi Q ~lc.x
g 1� Elongation curves for gutta-
percha and chloragutta_percha films at
20C� l- gotta-percha 2
percha contain, 3 - 5� chlorogutta~
of Cl reepectivel '+$'wlb.~' 26.0, 52.0
(5.8 Cl) after artneali.ag~tta�-p~ch~ film
Cord 3~3
~4 ,~

A r,~i .~~
i
t
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,,
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~� G
I~
{

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f
Fig. 2. Elongation curves far
gotta-percha at 20C,
1- gotta-percha 2 - 5.. broma��
gutta..percha containing 1,3.3,
16.5, 20.2, 27.2 of Br
respeatively~

EP~IASURE t Ol
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~~ N1~t~AP~22595)/~'(3) ~ UR/4180/65 007 009 1 26 1 2$
678.41:53+b78.76 ~ 5 ~!5-_`'
AU.~HORSs Tran iC~`x-yeu; Plate, N. A.; Shibayevs V. P.; targira, V. A. . ,
` TT:~LE: Effect of the chemical irregul.ar~.ty cif trans..ls(~ po]yisopren~ an its ~,.
structural and mechanical propertiQS `..~""~`"`�~'~�__ _ ~_.
SOURCE: Vysokomolekulyarnyye soyedineniya, v. 7, no. 9, 1965, 1526-1528
'TOPIC TAMS: polyisoprene, polymer, resin rubber ~yc stalling of er
-- , ry' p ym
ABSTRACT4 This investigation is an extension of tha work on gotta-parcha reported
previously by the authors (Vysakomolek. soyed. 6, 231, 196l~. Mechanical
praperti�s and electron m. ragraphs of the following chlorinated And brominated
specimens of utta- srchal'~ontaining ~".$, a1~.8~ 2bs and ,~2$ of 0~. and 13.3 1~i.
5,
'20.2, and 27.2 of Br respectively were determined. The mechanical ;iroperties
were studied by means of a Polyani dynamometer. The experimental results are
shown in Figures l and 2 on the Enclosure. xt was found that the transition from
the regular to irregular structure leads to degQneration of spherulite structure
and to formation of a ribbon-like structure typical of rubbery polymers. Orig.
art. hasp 2 graphs and 11 photographs.
Card l~3
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Z llt,.a-bb
ACCESSION NRs Ap5p22594
~ ~s
s
I U
i
SaCL09UAgs Ol
~ ~;
_._~~ I
t

1 ~ �i ~~~~~ u,ru 0,29 X~
-____1._.` ~
~ Dependence of melting point of Etta ~
' the number of chlorinated linkages (%) for he~tero and homo`-n
i geneou9 chlorination of epecimens(aN H mole fraction of ehlorin-
j aced linkages in gotta-peraha). 1, 2 - Tmp and Tsm~r ~- of hetero~-
geneot~ly ahlarinated apecimena, determined, before and after the
..,. melting of oC � Etta-peroha res dive
Card 3/3~~ ~ ~ aalated after Flo .. ~ l3''~ ,~ theosrotioal curtre cal�
I`Tt 4 experimental ourve
- �
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L 11t1o-66
ACCESSION NRt AP5G2~5g4
chlorine or 3-,~. atoms of brom;tne por x,00 ata~ of carte
the meltin ~ _'`'.
An increase nithe Cl~ra~ ciof ~ttaMpercha in agreementevit Fl lovaring of
amorphization of guts t ntenty up to 30 or 4Q,~ respeati~rolg o~- s theory.
the ~( to ~percha� The introd~tation of ,causes complate~
Z e ~ trn~itiot~ ~ 8~tta~-peraha. Orig. ark, he ~~ C1 .~aa~x~.t,~tes
quatioue. ass 2 tables I
I - B'x'apt~, and
ASSOCIATIONt ~ekoTelt~,q gogadaretve
S_.. ~e Un3tire.~~~ ~Y univerei~t ~ i
~ ~~ vs LO19Onot9o'~ ~AbepOp ~
9UBMYTTED ~.~
= t~Octtf~ ENCLt p1 ~ i
~ ' sO~/t 006 " SOH ~L1Et ~
OTAERY p01~ r
i
i
y
{
coed z/3 ~ ~
t ~
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ACCESSION IdR s AP5022591~
~/oi9v165/oo~r/oo9~i~zo/z~2~ ;_
678.01s53+678,/~81
r'
~' +~ '
AUTHORS t Plate, N, A~ ~ ~.1- ` `~ ~ `" '~
~f Iran Kh yen; Sh~,beyev~ V. pe = K~urgin~ Y, A '~ ~
1~..,~::~ n _
TxTLg: Structural trattsformation in t -~"-'~ fM .
ical re .~ ta-.~er~ha due to disturbance of the c~�m-
gularitq of the chain
SOURCES Vgs~okomolekul ar
q nq~re sogedineniya, v. ~, no. 9, 1965, 1520-1528
TOPIC TAGS: rubber, resin, po~.gmer, gotta peroha~ chlorinated ~
prene, ch~.orine, brom9,ne polymer, palyiso-
ADSTRAC'!'s Tha influence of the degree of irra u
! cx'ystallization, structure formation, and certain phgsi o-cp�ham~icr chains on tl~e
i
Polgmars Was studied. The substance investigated ~s trans_ al properties of
~~tta-percha). Irregularity of the chain way rea~.3zad ~''~`-po~'yfsoprans ~
a1d brominati,on. E~logenatioxa was aacompliehed under honio ~rtial chlprination
geneous conditions. X-ray analysi~- of halogenated t~_ g nexus and hetero-
carried out, and - resu],ta are given in tabular foxxm. T~re~feotea~ns Was !
on the melting point hoe been invgeti8ated arad the reau~,ts are inn ~logenation
in Fig� ~. aan tho ~nolasars. It was found that 3ntrnduatio~q of 8 ~`ePhi�
Card 1/3 5"'6 atop of I
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AC+C NR~ b
~�,~"`~ :t~URCE CQDE; UR/0286/65/000/022/0459/Q05
~ ~, a ail, ~ ~
INVIENTORs Plate, N. ,: Mal'tse~,~~~,; y ~'~, `~
~~:,~:~,~~~ olesnikc~v~G'. ~. ; ~av+ dc~va S. ~"~~ t
ORG: none
TITLE: Prepargtion of organotiri and arga,no ermenium of ~f',
._......~.., ..~......~~.,....,_ p ymers. Class 39, No. 176408
~.w~.
SOURCE: Byulleten' izobreteniy i tovarnykh 2nakov, no. 22, 1865, 59
TOPIC TAGS: organotin compound or an ~~ ~~
merizatian, lithium compound ~ g ogerinanium compound, polymer, catalytic poly-
ABSTRACT: An Author Certificate has been issued for a preparative method for organo~
tin or organogermanium polymers With er~banced heat resistance. The method involves '~
polymeriz�tion of tin,or germanium vinyl derivatives aver a1ky11ithtum cgt$l.yst. BO
~ ~
8UH CObE: 07/ BUBM DATE: 18Sep63/ ATD PREBSs ~~ ~~(J
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ACCESSION NR: AP4017633
orinated polyethylene compounds obtained at 1lolublelfraction contain-
that the chl
homogeneous in their composition~h~8 thedch orobenzeneeinsoluble fraction ofalaOC~
ing l,j,~,0 and 17.9 of chlorine, O,~,y at a reaction temperature ~ ~
ed 8.2 and 7.0~ of chlorine, respectively. of eth lene, did the
onds to the malting point of trs crystalline polyethylene containing
which corresp soluble. The samples of p Y
Chlorinated product become fu~-lY to er stallize and to form spherul.ites and
up to 8~ chlorine possessed the ~~bi].ity Y
the samples tiri+.h a higher chlorine content rntethedpolyethylene
monocrystals, wh~.le At a ~0~ chlorine Conte g electron-
indicating agaseous-crystalline sow ~ art. has: 1 chart, 2 tables,
acquired an amtupresusan ~L x~ray picture.
microscope pic :
� ki osudarstven~Y universitet im. M. V. yomonosova {Moscow
ASSOCTATTON: Moskavs Y g
State University) ENCLs DD
~ DATE AOQ s 23Mar61~
~ SUBriITTED: O1Novb2 OTHERs 010
~:; NO RbF SOV s 008 ,
~~ SUB CODES a~ .
cps 2/Z
a
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oN t~tR: AP1~o17633
a
s/ol9o/b~:/o~1002/x231/x236
ACCE55~
V. P.j Plate, K. A.; Grushina, R. K.; Kargin, V� A.
AUTKOF3: 5hibayev, ,_ , .,.
� ucturation in ch].orir~at'-ed polyethylene and its � solutions
TITLE: Str �
ul am ye soyedinoniya, v. b, no. 2, 19b1~, 231 236
SOURCE: yy~sokomolek Y ~ of eth lens,
of etr lens, chlorinated p Y Y
polymer, Polymer structure, P Y ~ talline structure, gaseous
TOPIC TAGS: c~orob,~nzene solution, arts rimarY morphological form,
supermolec~~7.ar structure, amor hous state, p
crystalline state, spheruli~te, bundle, p
ordered morphological forth
ins fraction cf nolyethylen� was usedUctionsuby boelgi~
ABSTRACT: A high -erystall removing the low-molecular .~r
The samples
of 2d0 000) which was obtained by stallixation in chlorobenxene�i~5~
in carbon tetrachloride and dous~turated solution of chlarine at i1~, or partlyOC,
were chlorinated by means �f a The resultin; products were eimethanol precipitation
under incandescent lamplight. art was purified by
t'ri lone samples with a chlorine conteic of 3 to 50
soluble in chlorobenxena ('tho insoluble p studies in
from toluene solutions). Polye Y
fined: these were sub~ec;ted to x'rt esdobtained therefrom. It was found
were o~ta ta~.line struc
m.,xylene solutions and in cry's
Card 1~2 .
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CHTCHIBABIN, Aleksey Yevgen'yevich. Prinimali uchastiye: I~UTi?V,
O.A.; KITAYC~ORODSKIY, A.I., prof.; LIBENMAN, A.L., doktor
khim. nauk; BAGDASAR' YA?~, Kh. S. , doktor khim. nauk; ~_.,F?`E,
N. A, , kand , khir~. nauk; KOLC>Sii',1, ~.'~. , icarci, k.r,S. ~, n:-.:~.k;
~TvINIK, M.M. , doktor khim. nauk; STEPAIJGV, V.M. , kand.
khim. nauk; MEL'NIKOV, N.N., prof.; DENEVITSKAYA, V. A.,
doktor khim. nauk; LIHEAMAN, A.L., red.; SERGEYEV, P,G.
[deceased]; ROMM, R.S., red.; SHPAK, Ya.G., tekhn. red.
[Basic principles of organic chemistr~r] Osnovnye nachala
organicheskoi khimi.i. Izd.7. l'od red. P.G.Sei�geeva i A.I,.
Libermana. Moakva, Goskhimizdat. Vol.l. 1963. 910 p.
(MI RA 16:10)
1. Chlen-korrespondent AN SSSft (for Reutov).
(Chemistry, Organic)
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,~ - -
~; ,- ._
~~Yo-}i.in:w.vY::.

~C~4~I s A~'~I1169
~polyestex w~~ sub~eated t;o a po~.y~er~.~at3.an reaction faith methacr3-3.ic acid, yie~.d-.
~~ ~ 3~g the d~sirad cc~pa~ae~~ of 1;~. ratio. `The latter ragas stud~.ed by electron micro-
. *_ t sae- axed ~-rays, follQw~;ng ae~:l at 60.�1~OC and ~~ fasted to be a~marphaus,
~~` ~ ~'~} ~~~, tbe- a~aea~ing tae~-tux~e way ra~,sed to 14,~..1~~C, tt~era appeared in
.' ' the aide, cba~ ~ ~~ the ~lc~palle~` f~.brf~,~r ~trs~btttl~es ~� ~~.ament~ of 100
-j An~etx~n ~~in da~mete~. TYuus, the- ex~,~ta~nce a~ a ,ohdaa3;c~1 hand between the two
` pc~ly~n-ers s�ems to in~erfe-re w~.tr. the c~ry~t~llitiatio~i of palyhydxoa~gpelargvnate.
Th~a:nks axe given to p~. S. Kolesnikan far supply~.ng ~e graft copolym+~rs. Orig. art,
'has: ~ f~.g~urea and 3 fozmula~.
,a
~SSQ(~AT~QNs Mosl~evsk~,y gosudarstven~yr*y univexs~,tet ita. M. V. Lomanosova (M�sco~t
.~,..~,.
State Uz~.v+er~itY)
k
SU~CTT~D: o6Jan62 I~ATE~aCQs : n~.a~.6~ rNGLs o0
SUH CDD~a 00 NO ' S~Vs Q10 OT~iERs QOQ
a
.,,.
..}
.., ...,,
- Card 2~2
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S.~'.w.-ei~4.~,.....r .....w.~ +.:,ti..._~.-w,~........:--r,...M.,.. .......:,........:.r. ,..,,......w .r ~.+,-~r-..ti�,v-.w .,,...:.,.-.�.w. tit. r, it-~.Y~~ r -~r.r .w..r ro < r.. ~. ,- wr..s~+~-~w---�.... . ~~ -.. .. w
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A~T~~s ~h~.~a~ Ya P,~ ~ Plat, ~, A4 - ~ez~.na, ~. A. ; Ka~'g~ - V. A.
,.,w
~~~# P#~~~~~ ~~~ ~tru~tv~xe ~�rmati.on l~ a graftc~1~ on
or~~ta~l.~~,la~g p~~.~re r
7~2
the basis of a
5t)URC~~ Wr~sekamvlekul~raxny*~e s+~yed~.neniya, v. 5, nc4 ~, 1~3~ 9~~~937
T4~C ~S~t ~:att~.c~er f~~~~aza, g~a~~ ~pc~~yme~t pa~l~r~~ter4 pa~.Y'd~�r~~-pel.~rgcz~-te,
maarc~~~v~.ecialee, pc~.yYa~tl~a~rylic goid
` , ABST~A.GT~ Sn ~~rlier p~ablicatiQns the authflrs investigated copr~lymer~.c systems
..r;. _ . , whew- the laaef,c~ c~~~~s~.sted c~ ~ ~ryst~l~.~i~g hca~tApcl~nttsz'~ wJ~~.e the side
_ ~ g~a~'k~- wed off' 'tie ~~~nc;t~st~1.~,~.~ing typek they de~;onst~a#:~d that the crys-~.1i~a~
~` tion~ ~:~ the :~~n~palymdr' way pr~vebted, hav~ang s~cppad ~t the fibrll~.ar type stage.
' Tha pui~pc~se of the presl~nt in~rest~.gaticn was to f~.nd vut whether in a copol.ymeric
;; sgstem cans3.st~g of a ~oxystall3.zing and an amorphous polymeric components,
grafted, 3.n the reverse garde , a s3a~.l.ar inhibitory e~feet would take places
this aase m~ethacrsrlis a~ci.d~olymer foamed tha basic ~hain9 while crystalline poly-
� a i ~~+rri i it
o~pela~rgo~te c~nstitu~ted the grafted s3.de chains. Macromolecules of polyoxy-
pel~rganate were treated with methacxylch~.ox'ide, and the xe~ulting unsatu~ted
t
' Card Y/2

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L 1$,12-63 EPR/l~P(j)/EPF(c)/~rT(m)/BDS AFFI'C/ASD Ps-l-/Pc-!s/Pr-!c
.RM/1nCW/lr,fl/MAY - -- -. _ -- - _ _ ._.. _..._ _ .. _
AccESSZON NR: Ar3ool805 ~/0030/63/0o0/o0b/0o5b/oobo
AUTHOR: Plate, N~ A.-(Candidate off' Chemical Sciences)
(-
~~ ~ JJ
,TITLE: Synthetic optically active polymers ~ ~f/
' ~3
'. SOURCE: AN SSSR. Vestnik, no ~r~b, 19b~, 5b-60
(TOPIC TAGS: optical rotation, synthetic polymer!,, asymmetry, macromolecule ,
stereospecific polymerization., polymeric chain , cocatalyst ,functional group
`ABSTRACTS This paper presents a brief review of the chemistry of optically active
synthetic high polymers, which several Soviet institutions of the Academy of
:Sciences have begun to study ~I~nly since 19b1. The importance of this field is
''~ especially stressed in connection with the synthesis of macromolecules, where the
~, presence of asymmetric atoms permits an insight into the mechanism of synthesis
,by optical means and its strict control. The author discusses how optically
activo polymers can be synthas:ized, such as by polymerization and polycondonsation
of monomers containing an Asymmetric atom or by copolymerization o.f' an optically
active monomer with a di-substituted one. 'Phe list of other methods includes
polymerization of substituted dienes in thn l,lt position, the use of a catalyst
,Card 1/2
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t~.U i b,~ ~ lE'd r~;f a:1tT'U~iuC]n~; arl am..n (., ~
�rras rynthes~ ~ then{~~~ - , "~
elastomers ~ to Increase tYLc r ,(:::~~ :; i
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Vlit~i Co11,~11;;~.. r)OCl~1S l1;1C~ E'.Jr'Ci;t?ta.Cii~ic.l
ymers. Polymers
Curd 3/~
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ttara~. G}'I:I,il;i',S. 1 I;ic '1 r.cl ' ,
t ,;~ ' r ,"�r~(:~~lii'1:5 ~.ri LrlB o'1 v ~.r.~� ;-+ ,,!
GpB, t~ls~' F,'Llll};1 i x,;17+ rt i:',~! .~ ) I''i:tlu ;J;,iT'cl l .LC)I; ,.f ~.1.:~1+ !',. _ ,
~p ... yt~ rr;:n~ CA) P.~.ti~~i'. r .;>t,.,,., t1,y mE,~lu., ~f t1, 0. ~,.
~ ~'i trl, i ~ rl f t, ~') t ; I- .l '!1 , I 1 ~ ~~~ ~r ~
. I i E., :J i
$tta.dl~tn. W1?i.. .4i.~j'f.r~�' Il~c.-.~;,; I(i�-iil,: :y11:1tF', iLtir''~.."IIiM''i.t.' brttl'. L~ Hr+
and 9c~mp (~r~~n:.., ., t;.. ! ii,~,,._'., i GhE~ I~,~r~ ~ .. 7. c.llti+l! VJta,. 1." '~ /
dispersl.''~ti cif r~1C:_ - ;(..,1!';i . t':`:~l%' i`Ci;:3E-Z11`E�, G't' C i'~rlyriE) t' ;flf' ~ (' 'IIt. t 17
c,r ~ a ~ _ �! ~~ rap. a }, ;, I!:
~ Chang Yrei-kan~', L~ S~ Jal'-
V~ A~ Derevi.tskaya; Sun T ung, ~~
Z� A� Rogovin, 1, N� Yermolenko, F. l;s
braykh (USSR}: synthesis oi.' cellulose ethers` I Ivar:ov
s thesi~~ of phosphorated celluloses~ V~ ~ '
KaputskiY (USSR} ' Yn influence of the Structure of
Tvar~ova (U5SR)
~~ ya. Lenshinay V. S.
of lucoside chains on thl~ oxidative tranVedeva(USSR}f reducedsrates of
P yg ~ 5. a� Med
V. M. Yur yev, A� N � Prave~9r~kov,
tion of hydrocarbons 'in the presence of formic acid or formates.
oxide vin 1 chloride under the acLinri of various
Thermal deetruc tion of pn1~Y y y an ovskiy (USSR}
compounds had been studied by Z~efelPnp(~SR~ndepQr~ted on she destruction
0~ Wichterle9 E~ Sch:~ttler, P� deetruc
ca rolactam, M~ Ku~eray J� Lanikova, M� Jelinek (CSR):
of poly p Thilo, 'jl. `~Jicker (Eastern sermany} :
dimethyl siloxane. ~� I Gemer , 0� Mle~nek, L. ~timel
ti on of poly ho ~pht~t e ~. n ~'
destruction of inorganic polyp esters. M. S.Neyman, B~ Pyf� Kovarskay~~,
(CSR} : thermal destruction of poly I� 1� I,evantovskaye., hi� S.. Akutin
L~ I� Golubenkova, A� S. Strizhkova9 L A Angerty A. Se
(USSR}: on thermal destruction of epoxy resins� ~ the oxidation
Kuz~minskiy (USSR} : initiating effect of seconda~SRamiaein�r`of chioro-
V Mat sek, J� Polacek ( }' g g
of rubber I� Kessler, y k�ang(USSR): protective effect of
prene� A� N~. Pravednikov, Yinq Sh..ng-
1
,~ Card 9/ 10
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The International Sya-poslum� �
i31G1~B21 j
M~ Kustanovich, L~ S� Polak, A.. V�
B� E� Bavydov, B~ A� Kx�entsel�, I�
Topchiyev, R� bt~ Voyterako (USSR): on semiconductor polymers J~, hgikes,
L� Kovacs (Hungary): on bipolar ion exchange r.es.ins� Ko Ma SapdaLasev
(USSR) reported on the sam�: subject; Ye� Au Trost,yanskaya, I� 9
Nefedova liu Iisien-.~ao (USSR) on
Ao S� Tevlinay 5~ B~ Makarova, G� Ze ~
the chloromethylation of copolymers of styrene and. da.vinyl benzene..
Kho U� Usmanov, U� N� Musa;yev, R� S� Till.ayeY (USSR): on radiation
gr~'ting of acrylonitril on polystyrene aAdkhodzharev,oU~~AZizoV (U55R)nto,
K� Gal (Hungary), Kh~ Un Usmanov, B� acr lonitrilyon cellulose)� I~1~Lazarq
also reported on rad.i,a~ion grafting ( y
R� Rado, Jo pavlinec (G~SR), Go Sd Kolesnikov, 1'sln~Sm~1^mzrlgy(USSR~ystro~r
on grafting by initiators., I, Ao Tutorskiyj Z� ~yy
(USSR):on copolymers of butadiene styrene rubber with ~~caprolactama
A� A~ Berlin, Ye� A� Penskaya, G� I~ Volkova (USSR.): on the formation
of sttzrch mrzcrorriclic~~ls in fr.eezi.n~; and rr-~;lting of aqueous nolutions~
V, A� Kargl n~ N � A., ~?late: (USaR} r~: poY'tt;d can a ni. ti r:~ti n~; vinyl };olyrn~.~ri �r.f.t-
Rado- T~1� Lazar (~sR) ; palyrnf~ri-
tion by disperse ino:cganic; substances; R~ y
zation of polyethylene by peroxides I, Mladenov, Iq A, Tutorskiv,
B~ A~ Dogadkin (USSR} : action of '~ -rays on butadien styrene rubber,
Card S~ ~ G
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1 f n, < ~
5~~1 yO/ c1;'~OO;~~G~, 0't; ,; ~
The International Sympos~.um^ ~ ^ 81018215
thods c?f determining stereo-characteristics ationcofminsolubie, malecu-
me of mer~z
Kargin, V� A� Kabanov (USSR): on the p y
D� Abkin, A� P� Sheynker, M� K� Yakavieva,
lar, disperse substances� A� erdiation in li uid phase� The
{USSR) on radiation palym 9
~,� P � M�zhi nova,
ird Section dealt �with problems of chemical transformations in po ymer
Th
chainse T� Rabek, Z� Kosmider (Poland) repridea oA�tYa�cYakubovichn To Yae
I�
phenol-formaldehyde resins by sulfuryl chlo
ordon L� I� Maslennikova, Ye� b4� Grobman, K� T~ Tret'yakava, N�
G , 01 carbonates G� I�
Kokoreva (USSR): on the transformation of P 5�.Mazel� (USSR): on the
Kudryavtsev, Ye� A� 11asi1'yeva-Sokolov a, I� z Valkaber,
interaction of poly-a-chloro-methyl ~einteractionbofasubstituted aromatic /
Holl y G� Turczo (Hungary): on th J
T Y A^ F,~ Vo rob ~ ;;~ eva, G ^
amines b,y polyvinyl c;hloricte.. I� M� r,uifuri nation of the poll mer
Shirokovas M� P~. Doktzchayeva (USSR)
01 vi.n 1 acetate� B� A�. Dogadkin, Pd� S.. Fel'dshteyn,
during alcoholysis o:f p y y
E� N, Belyayeva (USSR) reported an vulcani~etWithaconiugaterbonds� t�
Berlin (USSR) gave a survey on the polyme
USSR reported on poly-
y� I~ Liogon~kiy, Vo P� Parini
Ao A� Berlins
'u ate olymers on the basis of aromatic bisdiazonineso M^ A�Geyderik ,
conk g P
Card 7~ 10
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The International Symposium...
5~19O~61 /r0U3~(iG ~'1u12 j G12
B1G1~B215
rate. K. Vesely (CSR) on. cationic and anionic polymerization. Z. Zlamal,
A. Kazda (ASR) on the effect of non- polar compounds on the cation
polymerization of butyler.~e. R. hlihail, J. GhS~~mon~C1GYxoHeamga~Hungary)
the formation of stereoregulary polymers A. ~
(C H ) el
on the polymerization of ethylene in the presence of~TiCl~y ~ 5 3
or (C H )A1C1. 0. yYichtea�le, M. Marek, I. Trekoval (CSR) on Ziegler
~ 5 V. Topchiyev (USSR)
catalysts for the polymerization of isobutylene. A.
reported on the polymerization on oxide catalysts and experimental
data obtained in the in~'t Nef tekhimicheskogo sinteza AN SSSR (Institute
of Petrochemical Synthesis of AS t1SSR). V. BocThe(~ff)ctnofhorganometal-
polymerization by modified Ziegler catalysts. ~ Vilim,
Vesely, J. Ambroz, R. ~.,
lic ca~alys~,s was also studied by K. Wan F'o-sung, A. P. Kavunenko (USa.~),
0. Gamrik (CSR), B. L. Yerusalimskiy, g
Breeler, M. I. Mosevit:skiy,
T. Szanto, K. Bala (Iiungary), S. Ye. Ua%t re orte~d
1 ~ Dal~~oplosk ( ) A
I. Ya. Foddubnyy, Shih Kuan-~ (L5SF~), n A.
an disturbances in the structure of cha~ik iNotN? BoytaovaeM.zG~~Okunev,
of diene a. V. N. Tsvetkov, S. Ya. Maga ~
'I'. M. $irshteyn, Yu. Ya. Gotlib, U. 13. Ft'itayn (t1SSlZ~ s nn phy.ficochcm~.cal
Card 6~~ 0
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,r, ,.
Os~.uTli� a � J 1 `~V ~ ~ ~.ij~ :: ~`~ ~ .
The International Symp B1 O1~B215
decomposition of peranhydrides and peresters; A. L. Klebe.nakiy, U. A.
Timofeyev (USSR) on reactions of hexafluoro butaDienHea~~y3�KOLidit~ay,r~ov,
S. Ya. Frenkel' reported on Hybrid polymers ,
Kovacs, V. P. Li (Hungar;T) on the kinetics of radical polymerization
of vinyl monomers in the presence of SiCld. T. Krishan, M. F. Mar aritova
1 -merization. A. Ry~anek, D2. iilou~ek (ASR)
(IISSR) talked about emulsion Po,~ article during emulsion poly-
reported on the polymeri~aation rate of a p
merization; F. Hrabek, J. Zahoval (CSR) on the kinetics of emulsion
E Turska, G. ~9isniewski (Poland) on
polymerization of chloroprene; Z Maniasek, A. Jerabek
t~3 e redox potential in emulsion polymerization. �
(CSR) reported on the emulsion polymerizae~ic$ of dispersiondpolymerization.
l,. Selinger (CSR)s on studies on the kin S. Medvedev (USSR)
yu, ~,, Spirin, U. K. pol.yakov, A. R. Gt~ntmc~khe~r, S. A. A. Korot!cov,
on polymerization in the. presence of organoalkali compounds.
S. P. Mitsengendler, V. N. Krasulin (USSR)lo~i~hiumolymMerKuceran M~ Jelinek,
methyl methacr late in t;he presence of bu y
J. Lanikova (~5R) on chain ruptures chacekonJC Mejzlik,zJ�~iPataf(CSR)
octamethyl cyclotetrasi].oxane. Z. Ida ~
reported on the effect of the ratio catalyst water on the polymerization

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The Internationa"1 ~y~npo:~i um., n .
(3t01/H~1~ r
,I ~ on bios nthesis. Ko Ta Poroshin, Yu. I~
M, V. Vol kenshteyn (USSR). Y
Prokhorov, N, B. Noskov (USSR); on
Khurgin, To ~o Kozarer-koy N. Io resents of CO2; Ao Vo
poly condensation of a-aminoacid esters in the p
Mo Skuratov, Ao Ko Bon�tskiy on poly-
Volokhina, G. I. Kudr;ravtsev, S.
amidization in solid phase. J. A. Mikes (Hungary) reported on conderisa-
henol and their derivatives, and
tion resins obtained from furfurole, p 9 No ~~ 2Ylikha,~lov, V~ Ia
formaldehydea Aio S. .P.kutin, L. A. Rodovilova, ' L D, Dascalu
Mayborod, S. 5. Nikolayeva (USSR), and L. A. Alexandra,
(Roumania)~talked about interface polycondeusaension polymerization avid
Hrome~ek (CSR) reported on the process of s p G A. Levkovich,
its physicochemical ~.eseription; Ao A. Blagonravov,
I. A. Pronin (USSR) on the catalytic effect,~kl Zrocesseseofypoly~eriza-
polyurethanes. The Second Section dealt wi p
tion and polycondensa.tion. 5g lectures were given in six sessiansa
M Saminekiy (USSR) reported on
S, Ye. Bresler, E~ N. Kazbekov, Ye. ~ Kh< S� BagdF-sar'yan,
studies on the reactivity of macroradicals by epri
s I. Kends, Mo Azori (Hungary): on
Z. A. Sinitsina (USSR) anti F. Tilde, ,
the inhibition of radical polymerization by aSom~tlisC(USSR)aon the A
Razuvayev, L~ &I~ Ternian, V. R~ Likhterov, Vo
Card 4/10
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~~,jo/6~/~~;/~~;Ic~~/v~~
The International Symposium... 81018115
A. Xe. Kulikova, N. M� Teplyakov (USSR) : ~n~ha~ierafanewtpolyluorsgwi ths~
M� M. Koton (USSR) gave a survey on the sy h1~ G,~
Vansheydt, yea ~cUSSR'niSonthesis and
rings in their chains. A� A� Gladkovskiy ( ) ~ y
Krakovyak, L. V. Kukhareva, G� A< x 1 lane and polyphenyl
properties of crysta7.line polymers tYPe P�IyNP Rostavskiy (USSR) on:
methyl. S. G� MatsoyE~n, I. A� Arbuzova, Ye�
V V Korshak S~ L~ Sosin, Va P~
synthesis of polyviny:L acetals� ~ ' mars con tair.ing
Alekseyeva (USSR on the synthesis of new, linear poly
A Andrianov (USSR) : "Polymers with inorganic chains
aromatic rings. K� ~ Topchiyev, S. G~ Durgar'yan
in the molecules". N� S, Nametkin, A� V.
USSR xe orted on or,gano-silicon polymers obtaiene.byGZ1S~1Kolesnikovts
P co of erization with pro pYl
of allyl silanes by A y�� .~. ~+~ Shostakovskiy, S. P. Kalinina9
S, L� Davydova, N� V� Klimentovay y
I. Kuznetsova, L~ Vo La ne, Ao Io
V. N. Kotrelev, D. A. Kochkin, Gaon the synthe.,is9 polymerization ar.d
Borisova, V. Vo Borisenko (USSR):
co of merization of crganogermanium and ors ano ~inSmeFlorinskiys(USSR): on
P Y
dimethacrylates� M,~ M~ Koton, T. M. Kiseleva,
nometallic tin and lead compounds. F. Thilo (~aanian olymers)o
orga
"Essential characteristics of the ch�mistry of ino g
Card 310
J
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The International Sy~',posiumo o a
~ .~.z /vv ~JiL� v~L
s/19a/~~/o~;; ~ ,
B101~B215
Soveta Ministeov SSSR po khimii (Stata CommiVt"~~ Academician9 andtl(~ G~,
Council of Ministers USSR), Ao No Nesmeyano ,
petrovskiy, Academician, Director of the Pdosco'NOfn~Y1~rOr~anizationd the
d$lEgates.. V~ A~ Kargin, Ac;Eid~,mi.cian, ohn,irman m~M~r ~~"~Hftij(3tr~ in Y-i ~r
CommitteF gave a survey on the main prnbleNs N� 5gmenov, Academician:
opening speech, Second.~lenarv sessio
"The collective intere,ction in processes bonds'~.meThea~'~-pstaSectionedealt
peratures and in polymers with con,7ugate
of me~'sry Lectures by 5oviE,t-bloc E3c:tHn-
with problems of synthesizing p y Ao Vo 7.'opchiyev, Be Ao Krentsel'
tists: Yeo An Mushina,, Ao Tn Perelman, of mers of ring-con-
(USSR) talked about synthesizing steregreAulllolgoplosk, To Ga Zhuravleva,
taining a-olefinso Yen Io Tinyr3kova,
Na Kuren-gina (USSR): On t1,1� synthesis of cis-
R� No Kovalevskaya9 To Golubeva No Fo
Vu ~
and transpolymers of liienes on oxide cnthesissof copolymers from styrene,
Usmanova, Ao Ao Vans:heydt (USSR): SY Korolev
a-methyl-styrene, and vinyl naphthaleneo Te, Yao ~:efeli, Gynthesis of th~~e
On polyester ac,rylatE,o The sy
Yuo M4 Fillppovskaya (USSR) : ?~,~
polymers had been developed under the U9gerV1gZvon~.r ~CSR):BCopolymeriza-
Mo Bogdanecky, Io Mleziva, Ao Sternsc$sters~ Yeo No Zil~berman,
tion of ;O yrene with unsaturated poly
Card 2~
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~ /r~. ti n ~
;i~19O/61/O~a~IO~~ ~ ~ ~/ :~' G
b1O1~B21j
AUTHORS:
TITLE:
'~~ FERIObICAL:

Kozlov, l?. V. , Kabanov,
V~. A. , P1ate~ N. Ab
The Inte.rnationa.l Symposium on Macx�omolecular Chemistry in
Moscow
Vysokomolekulyarnyye soyedineniy>:i, vw 3, no ~ 3, 1961 , 3?_8-348
TEXT: This is a report on the 14th Symposium on Macromolecular Chemistry,
held in Moscow on the suggestion of the USSR and decision of the IUPAC
(International Union of Pure and Applied Chemistry), June 14th-18th, 1960.
Subject was: synthesis of macromolecular compounds and chemical trans-
formation in polymer chain moleculeso There were 1136 delegates and
279 gues#sb 846 df the delegates came from the USSRa Altogether 170
leotures and reports were given, 64 of which were attended and discussed
by Soviet resea~ah workers. Two plenary sessions and 16 sessions of the /
three sections took place. 8 sessions were held on one day of free dis- \/
cussion. The symposium was opened by the plenary session held in the VVV
great hall of the Moskovskiy gosudarstvennyy universitet (Moscow State
University). V. S. Fedorov, Chairman of the Gosudarstvennyy Komitet
Card 110
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Ordering processes in syster~s SJiOj~6',~QQ;;~~U~;~GQ7;~Q"~
B101~ 8215
up to 140�Co The mir.'ture of crystalline and grafted copolymers then
showed a variety of intermediate stages between spherulitic and crystal~~
line formations whose thickness was 150-200 A Fibrils (40-50 A~ becaue
visible after heati-~g up 'to 160�C.. With tetralin as solvent, distinct
packet structures occurred (250-400 A)~~ The presence of the copolymer
thus inhibits crystal.lizatior.� and causes a variety of intermediate f'orma-
tionso To study the fine structure of the pure copolymer, crystalline
PS additions were precipitated from tetralin by methanol, and boiled in
heptane for 30 hr~ After this reprecipitation tha products originally
insoluble in methyl-ethyl ketones, has become soluble up to 40~~ Hence,
it was concluded that gra~Pting' only takes place on the surface of the
crystal packages of insoluble isotactic P5 under heterogeneous conditionso
The solubility of the product depends on whether the isotactic main chain
remains i.n direct neighboz~hood of the macromolecules of crystalline PS
which did not enter into ~'eaction., i~'i.~;. 2 shows the r~tidio(rraphs taken
during separation by recr~rsta111zation, The electron-microscopical exam-
ination of the pure, grafi;ed copolymer showed coiled gloruiFS of 40-5G .~~
The authors thank N9 Fo BF-keyev far collciborat:ion ar.d discus:~ion~ There
are 3 figures and 16 references: � Soviet-bloc and 7 nonMSoviet-bloc:
Card 2~ 4
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IS~~6i~ 2209
AUTHORS
TITLE:
Kargin, V~ A~, Shibayev,
5~190~F1~003~OG2~009~012
D101~B215
V, Po, Plater Na A~
Ordenin~~ processes in Systems containing grafted copolymers
on the basis of isotactic Knd atactic polystyrene
PERIODICAL:
Vysokomolekulyarnyye soyedineniya; v~ 3, no~ 2, 1~o1s
299-305
TEXT: It was the purpose of the present work to study the influence of
grafting on the ordeni.ng processes and crystallization in polymer syster~s
by electron microscope~so Grafted copolymers obtained from isotactic and
atactic polystyrene (F'S) wera used for the investigationo The content
of the atactic component Ryas 17~ in one sample and 35a in the other
A JEM-5Y electron microscope V{ith direct, 20y000-70000-fold electron-
optical magnifioation was us�d for the experiments, The crystallization
of polymers dissolved in toluene (concentz~ation of 0~ 01 f) was conducted
at 110 C on colloxyliri fi~,m hardened by quartz or coal The first elec-
tron-microscopical photographs showed no difference between copolymer and
crystalline PSo For finding the differences the film had to be heated
Caxd 1 ~ 4
,~
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89590
s/19o/61/003/0o2/oog/o1~
Synthesis and properties of grafted.. B101/B215
showed that grafting of 170 of the atactic component did not change the
diffraction of isotaci;ic PS. 310 of the atactic component shawed wider
diffraction lines. Ttie examination of capolymere of cryeta].].ine and
amorphous components j~s considered to be an important problej.
I. Yu. Marchenko (Ref.13: Vysakomolek. soyed., 2, 5Q9, 1960 is
mentioned. There are 5 figures, 1 table, and 13 references: 9 SoviQt-
bloc and 4 non-Soviet�-bloc. The reference to English language publica-
tion reads as followscc X. Lar~dler, Materials of the Gordon Scientific
Conference, USA, 1958�
ASSOCIATION: Moskovsk:ly gosudarstvennyy universitet im. Pd. V. Lomonosova
(Moscow State Univ+arsity imeni M. V. Lomonosov)
SUBMITTED: August 1, 1960
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89590
5190 61~003~002~00$~012
H101 8215
Synthesis and properties of grafted...
Fig. 2 shows a diagram
contents of atactic components were obtained.
of turbidimetric titration of atactic polygtftedecomolhmercwitht35~soff un
35~ of atactic plus 650 of iaotact~c PS, gra p Y
solvent: tetralin, precipitants
atactic component, anal isotactic PS
butanal). The solubility of the grafted macromplecul~s,�bet higherhthan
of tha lirlenr i.sotaot.ic PS due to iarger
that of atactic P5 due to the form~atl.on of follo~wingc}reaults:Tllftheetcr-
mination of intrinsic. viscosity showed the
initial isotactic PS had a Huggin's constant k' m oerent contentseo~rsfted
copolymers was 0.40, and k' of copolymers with diff Ref.12:
atactic components, in agreement with J. A. Manson, L. H. Gragg (-�
pngew. Chem. ~, 32~ 1955) showed no remarkable differences. Fig� 4
gives the thermomechc~nical properties of the ication temperaturea(90oC)�
polymers were found 'to have a distinccharacteristic of isotactic PS. This
and a high melting point (220`230oC)
is explained by the :fact that the atructurain theseatwohtemperatures,othe
ponent is preserved in the copolymer. ~lith
copolymers showed this ability of reversible, highAyradiographicoanalysis
which was not accompanied by recrystallization.
Card 3/7
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g9~90
s/19o/61/oo3/oat/aoe,~alz
8101/B215
Synthesis and properties of grafted... `
Ozonization was conducted i,n a glees vesaglaction eNpewaseblowncthrough
After the re + 2
ditions are given in a table.
ratus and ev~aouat~~d at room temperatures ta~sCOnpZQnizationiof
the apps ~ elementary analy
02 in the sample was determined by In
PS films was leas effective due to the Jiff arist1957)usthe ~nfrared�
agreement with P. Lebel (Ref.10: Thesis the absence of hydrogen per-
spectrum showed no Obi bands thus proving
roxide of experiment no. 5 (see tabl�~ eerlatter wastcarried�T
oxide. Pe
the polymerization of atactic styrene monomer. The The
either in argon atmosphere or in high vacuum.
out in phials, o then 2 hr up to
optimum was found to be: 1 hr of h~ah~nu utot75�~,C~Faster increase
65�C, 3 hr up to 70 C, and final~.y P
re led to the formation of network. In sol~ained.(bAtactc
in temperatu raftin were ob
toluene), polymere of 1�war degrees of 6 ~
homo of styrene (side product of the reactions) wThermolecular weight of
p Y
10 - 15 hr treatment with G~aftedecopolymers with 17, 31, end 35~
the product was 2001000.
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~~,~bc~
AUTHORS
~t2.O9
89590
S/19o/61/0O3~OO2/GO$/O12
81018215
Plate, N. A., ghibayev, V. P., Patrikeyeva, T. I.,
Kargin, V.A.
TITLE= Synthesis and properties of grafted copolymers of isotactic
and atactic polystyrene
PERIODICAL: Vysokomolekulyarnyye soyedineniya, v. 3, no. 2, 1961,
292-298
TEXT: Tn previous pE~pers, the authors toglth~101it1959;e~~c1547bo1959~s~
(Ref s.1-4s Vysokomol.ek. soyed. ~ ,114,1959 ~ ~ ' sicall
2, 166, 1960) studied grafted copolymee~ re arteionltheaexamination of
different components.. The present PaP P ual chains which are
grafted copolymers consisting of chemically eq _
different in structu~^e: copolymers with ~cysOllstnreneseidetchainsy
styrene main chains, and amorphous, atact P y Y
The were produced b;~ ozoni2ation of isotactic polystyrene (PS) whose
y
atactic fraction was washed out by boial~iagmOleculartweighttofe80,000.
fraction insoluble i:n this solvent, h
Card 1 ~7

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W ~ Vl W ~ ~ { V ~ N tl s
a re 1ati.~~el;y sparse la�, t ~ ~,e a*ruci,+.a-r~; ,: ~~N~l ;~ :.~''.,
according to `~. Vd Gatovsk.�L~doot~ z-nt change the ~last~~c1.Y;~
cf the xubba:r. malecu-ic,y,~ Rhe:r�eas the sma11 d-~..ffe~ren,.=~ b~tvreen.
Card 2~3 the tRO sorption iso+herma? lines Ys e~piained 1r�y rY,o preaAnae
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"~ "' x 643
AUT~OASa Kargint V� Ao. Plate. I1, b~
TITLEa The Ph~-aic;t~~~.~~~,~~:L :Cnvest;,gat~on oY t}~e Stx ac+uxc: and Pz:oper��
ties of t}ie ~~��Polymer of C}~loroprena (F'iz:Lko�~khimic~heakoye
iaaledovariiya at,t~oy~:nya i nrrc~yaty C~)��p:~limert rr~ :~r; coz/ter;t is ;.,-,
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837:34;97 t 687.183.5 - 1
,Pisil~ Cx., _~aic l+ow~ci J, 7~'t~e Atanatsolnrd of a~'##e#! t'hense t~antstn#n*
,, - ~~i"~`'tit b tKw~tkir tram ~'eekuHecd MI#1K, ~:
�� Wytbb ors tyltyCktego a ~eiwartoeet 4tN/i tlua~ezu w euchej .mnalo
r;-, , x mleks p~-at~cyxowatat6o", {~trac~ zaat, 7+rzetn. M#ec~. Nd,'i), Waraza~va,
~ #9t~l.;VKl~Li~ 7 pp.,;~ 1#8q;-.6 ta#ta.. ~ ~. !
~icpc~rltn eta ware asrried cu! over the mai~utaature pt 't`ttn1~ ahee~e
troriti p~~tou. i~od ~.iri~tic,' ~e para~fat bntchee ware made halm ~adth paet~- '
utlsed epd~nun enieu~rteed mUk:. `The f
-p paateucfeatton wes made ~t 72--
Z3�C ovex ~ p8rlod'ot is aecondaYxh~ but#er;etsrter w~ Wa~1, ttr doaaee ;
deter�hiried, With the .~IseiearJstd mi#k the neceeetlT of tharou~h Crtimb�
' ? itng ax the c#ot aal! ~utla+~.,drs~ing nt.the~oheeae karn~ele rvaa t-6~ecved.''
~pealat-:care must Aid taken ~ prevent the.retnteRttt4n Qt the psateiarieed I
1 hlikt tts#ng''tht* ~afi~avp methcnl _Chseno a! x acid t# ~radn w.aa pbtatt~ad.
_.. � ,
xt~ can~tual~l~ s~ea~hiid wee tit~~ tar cheaas_ ttl8hti#actuxed-troil� the ~s'�;;
etcu~eed mf#kr eipe~ls;l etartsra' typleal to 6pe>! ty'~o o! cheese should b!
� ~ tf
�
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~r'~8A6 837.352
~' Jrtkubo~NSitt J., Piat&' z xite Use at' ~'uirlct Curd for the Protlaetlnn tlf ~'
~,I-Il~fn
�W'ykt~rxystr~ni zgilwlaie,~o twnxa~u do wyrabu trnzetny", tPrace ,
Inat, przcnh. Miec~', No, 2)~ Warazrrwa~ t9ti4, 3:t3 pp� 3 tabs: ~ ,
A,disCUesion t: ci~emlcai ehangelE taktng ~placcs to curd dartn~ ttg pu-
. tridi[y. ~i numbe~ot testa were conducted on a laboratory and technical.
~cate tejnd'!ng tq ~cntdye'prgducts-ot proteks decnmlrasltiot~ by rinetng lr1
. ~ratart in iaclditt~d whey anct a$aln ih water; ax also by ap~lyi~,~ cheml-
`cal >~rgtttre~atlo~t cv-teisting nC di~oivln~ In NaCtH nod precip(tat~a~ with
. rnineiral ai�id: ~iitve reuulia were obtained onty vVhen uatn~ acidified .
.. - - ,~.. ._e.,._ ._. ,.. .. .. - - .
, v~heyy'~uCd eteansed bq thta' method could be' used ~tor the production
- ef' ca~ata for fndusstrial pprpasee.
ti:/
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~ ~ ~ ~ g1e01'~ N~- ~ 106~It IOd itt tiM
ley. A.,_ Y. j'ttte, 1'. N. Shahan,
and M. f, Hawpa+~ (.res. C+le~. U551t, 193t}. lit, 4'r2~-~l%9 (U.5
p~,~,l� !l ~ ita).--.Ikhyd�tirg the acctaoe a( I� or 2-syccto-
lutnitbat vioyle~Ctapaufane, tht! etrncture
~ ~ la ~~ is c behsvlaar aad by the frr~
q ~ ~oI flee tdt#otids~~aad~~l~0 tarnab ich rro l~fextrcyd.
etArsd GN 6.p. 71w�-7d�13~-�.~0 mm., A~~6.9'1Z8,
e~� i.xirori~dt ib tul~r, _C~Nr,s~ � (~� , b.p. 9~�-78�l
!~ tam., 179--i~'J7~ man., Ir 0, +r~ ill, wbrn mi~ccd
eritA aad ~aatu~ trtrted lrlth H,PO� (d i �7~-AcsU
ty at *8B'. thyieae oside aesd I furush R-cyc ~
~ Ct1iuQ (~+~ . ~.p. 9{.-88�J'b{ mna., d~ 091 �
l�/'~'lli, Y ~ iata flee atdate, C i0�, b.p. 91~��
Id0�~S~-~:~6 eam.. iM-�-198�~7ig mm.. /~ ~, +r~' 1�i5g9.
~y ~a~e in t alvw atreatn o! N� over
~oot~e-ed I(n~~ 1[0 tubc betted to 5Q4� ~nvca v+syL
or~gw, ~, h ~> �)" b,p. 91~~~~8�~7780 mm., d~'
Q, ~~� 1 Cis ~ > of 1't~-C to eth ~i~
c~tl~ntaae, p_.p. 1 1 "j'f!!A tam., ap Q�y~N7, s~,� 1~41~1
(}xidataun of II aitA ce~M 1+~ KldnO 8iv~ !i ~CU~11 aaA eydu�
lxntaeeaxarboaylk acid. b.p..lltls---1101, /r 1�~7, x~� 1�~b~a.
�eutrat prodt-ca are nat obained. 1 . H aax
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