SCIENTIFIC ABSTRACT ZILBERMAN, V.M. - ZILBERMAN, YE.N.

• Document Type: CREST
• Collection: Scientific Abstracts
• Document Number (FOIA) /ESDN (CREST): CIA-RDP86-00513R002065120017-7
• Release Decision: RIF
• Original Classification: S
• Document Page Count: 100
• Document Creation Date: November 2, 2016
• Document Release Date: September 19, 2001
• Sequence Number: 17
• Publication Date: December 31, 1967
• Content Type: SCIENTIFIC ABSTRACT

USSR/Electricity Apr 1948~
Heating, Electric
Electrical,Equipment
"Unification of High-Frequency Installations," D. B. Mondrusj S. M. Margolin, V~ M.';
Zillbarman, Engineers, ElektroPech 'Trust, Ministry of Electrical Industries, U$SR,.8 pp
"Elektric lies t" No 4
Soviet industry is sorely in need of invention of a series of apparatus for use;in high-
frequency heating technology. Mentions work done by SevZapPromElektro-Pech in~this:field
of research and successes achieved. Some machines and equipment have already been placed
in various industries and authors ask that work6rs operating equipment send in testimonials
or criticisms.
.PA 69T27

. - . !1A1,11,11511 Til MAL:
]IF 1 ; 1 11 :! I' I , 111 ill 1:1111:"

ACCESSION NR: AP4035099 s/olgi/641000/005/0013,/0015,
AUMOR: Smirnovaj 0. Vo; Losev,, 1. Po (Deceased); Yerofeyeve., 5, Bo;
Zil'berman, Ye. Go
TITM. Ftfect of emulsifiers on the courseof the inter
phase polycondensation
ireaction in preparing polycarbonates based on dichloro"Pheviolprop=60
SOURCE: Plasticheskiye massy*., no. 5., 1964p 13-15
i TOPIC TAGS: emulsifier, interphase polycondensationj, poly6arbonate,
dichlorodiphanylolpropane,, dichlorodiphenylobroyade polparbonate, Trilon B)
leveling agent A. OP 7. Nekal, Avirol) molecular weight, yield,, specific
polyether., solvent effect
viscosity.
ABSMCT: The effect of certain emulsifiers on the molecular weight and the
yield of polycarbonates based on a chlorinated dihydroxyftPhenylaMane were
investigated. The following emulsifiers were studied: Trilon. B., leveling.aseat
'i A (quaternary -ammoniun salt of diethyloinomethyl derivatives of polyethylene
o~ctyj
glycol esters of isooctylphenols),v OP-7 (polyetbyleaa gVeol ester of Is
phenol),, Nekal,, and AvLrol (mixtuiv of neutral esters of butsnol,, sulfuria
i Card

i'ACCESSICH NR: AP4035M
oleic acids). CC14 tdCH 12 were selected for the organic phase., P_(Pe-
it
run at optUmd con ons as-described by 1. P. losev., S. B. Yerofeyeva",
f were 0
0. V. Smirnova, L. L. Dlyachenko (Plast. massy*., no* Up 1�63). The enclosed;
figures 1-5 summarize the effects of the emulsifiers on the specific viscosity
and yields of the polymer. The process of preparing polycaxbonatis based,,
2,2-(3.,,'j 1 -aichioro-4.,4 I -dihydro3Qrphenyl) -propane and phosgene dapeinds oa'tbe,
nature of the organic pbase and on the amount. and nature of the emulsifier,
used. All the e=xIsifiers except TrIlm B lower the specific viscosity of tb,6
polymer when the reaction was rtm In CC~4"Ia which the polymer is lnsolkbiee~
TrIlon. B and the leveling agent A lead to an increase in molecular Veight aZd
Aeld of the polycarbonate w2um reaction Is run IA~ C%012 vhich dissolves the
po34,etlierroxmed. Orig. figures.
ASSOCLMCU: None
DATE A00 ENCLe. 7
SUMMED: 00 1: 2&41* .03
SLT13 CODE: OC NO MW SOV:
~,OTW: .001
7
Card 2/5

ACCESSION NR: AP403M UNCLOSURZ i 01~

M V
01 4
0 4W
?A
412
.
P

0 q5 I 1A I 4F
45 1 1A
amount % amount %

Fig. 1. Relationship between specifio viscosity,.. Fig. 2. Relationship between
-~olyetherand amount of Trilon B. ~~;
an& yield of specific viscosity and V.eU of
W".4pecific viscosity,; 1 and 2- polyether and amount of level-
in carbon tetrachloride 3 and 4 in metbylena,.:. ' Ing agwit A,:.. Symbols same
chloride

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to the TIVA.Wh + Valmh +
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and NaHSO. and their mists. wm treated with a HiS .00
current at 20400"' until the reaction was cotripleted. eels
Thcrc=imwulolimrtdby-mmorinciampicistdtfinite
intervah and analyzins KSAQ.. NAIISO.. N&AA
N&40~ and polythlocates In the mist. by [be method of
Rurtrnacker and C&%ach (C. A. 22. 362). The an.
J reacted 112.1; was absorbed in 2 flub cmtg. KOII and as*
analyzed. Contrary to the litmture data, the reaction LO 0
fams abe, KaISPo, Siam It Is not oxidized by Br In a
neutral sola., it was Altid. la the filtrate front the fla$" age
by the imbod of Bassett and Henry (C. d, 29,7210). 0g
At ilat optimum ratio of NaqPOs and NOMA - 1; 1. no
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..a and decratsinp ratio of the reactants the ykMs
Xrdv=sc and become x"o with NavS(h iind Ks-
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acklitylsollsojottivemists.
use
ahwre3O`jhq ykidol N&A00rcreatesawl that of N%.N:
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it hypothesis for the Nwh4sians ;1 the v~sctW betwe"
1115 and HOSOs W iiinn, Ile$ nacts with 11160~ to sit
sq. tola. to the "latusupbasel MIA+
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IIISA + _HIO whkb accesstpeusled by the re*ctioia'
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creased tem - the f NOMMS take Pla": Ilsoll goo'
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HaSO4 HIS
3 .200
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T RIO + tim of HISA is the result of
a secondary reartim.- which proceeds in the pnwnce of 409
Ill8s% as follows. HSOH + 3114A - H IN +
Tho + Ulf*. RA04 Is forand as fullows-'. 1&I +
Fee
211ACN - IlAOs + 110 + 11A asul this prucru pro.
cmh through an intermediate formation of thlornowthio-,
nate lost, the ciftnerization of which forms HsSA: Tte
Stamm and Goebring theory (d. C. A. J4, 12W) for
the same pmcen does not preamt a clear teArcelon of
thtir g%ptl. data, but their data support the above pre.
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04.111110 and S4.41Nvaim.
0 i. 11=t prepd. A"djA
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can be k* In the dry state for mmtb* without ifeempa.;
they aft threwt hunittliately d4cot pd. vim *An. In
40
sibid. water. -714 key I* the A*h1c Iwepov. is-tbe r*pWlty
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Ji =0 0
lkpwn and moisture. 11. Calclum mats. 1W. I lV44t. " I I 1~1
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the ertins. rt-whinic ft-m hittracqIon of C%A^ w*1M Ag,-:
CCIM anti ACN'O.. rrV. rbe formur malt Is Ish ly st,61ile Its, '00
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too a ml. 1,00 7&-M* Is added. with alcrifix. an 'o o
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0 The act *. fibemd. wbAW uUt bot. lkxigh a Fvo
itkhw futiod, The filtnite h axint witla
The dmibk ~k;~pu. is thus efected with lk inistim"M of
WAICT (04&4 SbAmt entimly *s watm d rrymn. 411 Ill'* so
"Itriab). It The 1cm , firmbi *)*. Nit-Wh.
muti 0
r1w y1chl Amen"Is W
61130 eoxnvpws vrith 14-pn. 44.Q. A
The pffulurt wittsful
XsCl O'~4%. By rwrYstn. the e(mtvnt of X&Cl ints be to 0
4 to QjQ4"jMi;%. 1-he find prothict tumnip
rawaitiLd inidang"I in storisge durins
00 A. A. lkwhtfinsk r0
0o
L WfALLUKICAL L1TtR*TWM CLA $06CAk?"
ti) cm.
- I a I."- ,94
I11A -1
U I AV 10 11?4
d It R K In ~ I'll all 0
0 o 0 010 6 a a a0 0 go 64 so 0 of 09 0 0 0 a 0 0 9
)ZOISO 000*140 o0 60000 09 000 666440i0o Goo 6490* 0#0 6:1~:

i 04- ~ ! ;:
.. 9:1111
out v a it 10 11 a%P )A 11 1~ r a a 4; dA a w41,100
LA-40-AL-1) -1-ju- lux, P-4*11-111-14-TZ-A 1 '" aI` z
00 A
.00
.00
.00
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latsulficatim al tM pnpustWo of N&AO, by Ow w41.,. -00
Ademethod.
*0 ('"Um. latol. (U. 3. $. RJ lilk. No,
-00
Cbio. Zagr. IOU, U, MX.,q.-%'hgn a,
*4 mit NmaLth la panni down a towrr to attvt a
fiWUS ItrumAn of 80j. tho Nat8t0a ykki depeads, 4ma Lim, 410 IN
di rafJoals" vvwty 4114 mte of 1111vt of the A"al' llwtm.
ivWt trfimOAUtaO.lTm./i*L.fa6estbarkld'
'30 0
W"51 w 6y DM'O"nl The Mte of 4Uid ftW froM
00 r0 CIO*
It the lowtf Is k4b knamA, a tu coola. 7% Sol ivqj
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w NasAand "Mcalle. 0.6% SON cimp 79-84
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SO.-

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wo

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Ittit". (of Ali--- by Illicit in the C1,I& 1*., the Willi
~tovlo, okhve tostatownt itit, ..tj lot sill. .4
,
Ackil I and 3 loal. of 4t%11 lilt., yollil lipl
with Ir,6 luct, W", TU UvIlrary L4 the (IC131, (IrIvitils
to 111 bit* "Upt on the CM(litivnit Of tile Stila. of ,
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-
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-
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fly this viellbod TV Stood .. Its. Add 0.5 t.1 -Anipit
r
to Ill td.tol 401ro
wootalin end Pop
If
, . to ont, .,I fly(vtol,
twooker I.M of 10 mi. of 20% Av(
twhtg t A. to 3CO-400 mi.. rpt. sAk- - with I i It.Cl
,
in the mlot- Set st&M #01' 1-2 hrio.. filtell. wath with wstrot,
1pite, and w0th. Four rtfavoices. W. R. Iftn"
tie 0
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t4t*$. Lu 0 m a4t. Va. 1. 211,1girlisaitt
t .00

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Afftentatts firtivin all. .41l.; the Mg N4 ~ltl Wal "Ylilhe-
9,ucd: SIMI thu anslylival Promfilfir 1-6 W01 ox"11g.11. It'"

drvejolvd. AgCl (Irutit 100 list. AgNoi vAilu. (im micit.
xims)) WaS added jot 40' 10 a -Ili, 4 4.1 g. AlgVX In P, a
fill. water; attff (he jurtick-i A AgCl hail dituol"ItItl.
fit., suixt. *;k4 djhl. %fill PrOII-Mt0l mixt. (1:1) all'I
"04 solkewril III .(.Itltl 40%rollight to jivhl 14"I'lett .114,111 ago

Nu. th" I-1-fuct% wulLkim,tl all.4 Itia, MI it, tit,
6wits c4 Ilse 1IMSW "It.

JIM 6=111. litrital with i0fifir. Vw ats I-Vov .12M.
fee
'
in the matc, w bile sulits. in vi-att: r (Imynij-" i if tati-l-

inc,
jv:tll~ mt ItcAtfitc. At WAV 11CIII. It)- 1
)pffl. 4'
110

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-111. q 1111, ~11 1.4
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frAm
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At I I I L A
414TALLAWCCa MUST4414 CtAWINKAMN
mwtl,/- total') it 04. 46C $)Jill in Q%T ii-1-
a a IF a Fit 0 4 0 1 v W 9 All 0, 3 0 9;
1, to al" to, a', K 't
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0 0 0 0 0 0 0 4 6040004 O:im 0 000 0 16 0 a .6:0 0 0

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1 ?!!,off 9 10 11 .1.110010#10t
P'--jL
-j_jL_P--9 :J111iff A-AL.,
-00
Psecolst I ANO plop$* m ~66
sig Itut. Applied Chem.
swaylk and Ya, 1. ZUlxmmn (St
0 0 grad). J. C-a- CAM. (U.SSR.) 13. 718-23
C.A. 40. Wffi-QZ;=1w4vrd In a .00
Na. and
h. (-I
sol". of 1611-V not
00-3 L's "IC41, The ratio
am RtOll (1:2) 1
An
oil ppts. and It is w0. and mIIwWvvdIn MeOll. AWn.
0( twice the vol. of Stoll ppts. cryu. MgsA&(SA)#.-
91(go. U= the rsik" of solvents amend. an iminarr
O&W Wt is "bie in the edd but Is
product Is obtained. The
0% 4 pd. by sulfide%. Cl. bollint 11,0. and bom. If It is
alkmvd to stand In MeOll moin., It 4CCOCIPOM to lu#4-
MgAj,1P4O#)l.311vO. which Is Im stoW and d#rmp~%
to &q aft statmong. tkKh %aitt ~w jID W cryam, over
logo
SO 0
If No*
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L
ilir;ii4-- 7-
so
q a K a a It Vt r, AN I Vw 0 P
d44
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W 11, W1
A.,j _ I.-
-AJIM
Jj LU
!-Igo
a "doam bttwated hy&vA4n mulfide gild sulates- IV.
99 ji M= .1 the felactlaam umnq F.1"S In the Propitiation 1~111 0
aful V. M.
041 JL of S"Um twataffmo. TO. 1. %
17thfiltati. Or". 10. 441,21
-00
00 MO), 01, C.A. 43, (W. -Tbe noram Ajf 148 HIjilt
so solos. wail sttulk-d (it 4 sutall %tivivil mu, -00
-Lion vvvwl lita, that %alutithlit mul I'miselkilent, vrf(W% wetv
Igo crtint"ted. viiih vach clarre ccmUtuting a &I, vilot. -09
The Ov"VA ressictka of His with 6 tv Igo
;P.!,e iv I by
lee 4 t CIA - 3NAiSA + 2NaII3 1 411. N
go it with Naillgis%2 ways- .00
111411 115 - 2NA~SA + IIjS and 4Xm#.%Ot + ONWIS m:
SA + IOU 1 A which cmill ion the lomintlott of 11,3 to 0
of j ataid 8 at t aid of Interaction of 11.14 with __O9
00 voins, the (mmatiors 0(thlo-mllate b6 a two-step
2N's.S(h + 211*3 is 2NORSOI + 2Xaligmul Milr-SO, 4-
00 2XIIIIS - 3N&*SA + 311,0: tho Istitrai pnirmli. tali to
the 1xvint of di4mI=ance of WSUMIC and 6 Otafacletilt-it
Oe'r
thAtIM-401111 orination a( trithkinAtt. the 2nd Ist-
=Matter disApticarance IA b6ullite mIII is CII4tIWkfiZ"I
by slow dkmppce~rzuce aftrithlottale. .0. X Ktwslapoff
INS 0
is
1110.1tai ATALLOGICAL 1.171010440111 CL&tSIPiCATMA
$I ~Jay-
1,110114 Hit 04V Gas O&W IW4.~
At 011 1 1 1 1 1 1 1 1 4, j v T;
u . as 0 at 'a K I m * it it it a a A i N, All L I I fW 0 1 it 24 0 a
00 . L . 0 4
ore 0 0 0: 0 006 966 see 60 6,000.000 0
1* 000 a 0 IS 0 0 64 so 0 0 0-4 0 0 1111 111to 0 000 00 Co 0 4 0.00 0 0 W to

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ot got to 0
04 ,- ?-0' 1 1
A A. A- -4 a I !.1o 0
00 DefefIruportition and f0mation of
Inithlonale as d"IffaMillan pradva a thifirta,
-1 L. A. ZAlitittyarvis j*;4Atr Imt.1 ~jlp
VtWM tL"tAJ- J. Geo. Ckirmi. (US-S-RI 10, 1.397-
I 100(l"O(In ku-isn), -041 l"hog A ilf 11115 11141,
KF%Ol, with K011. III it toul vol, of K) fill.. It* 2 hiN. .60
4111 (With tefluIL cAmidtawt). anti mlowing sit Ct"t. fiw IS III,
00
the inmin jvtoiluctlf wirm: with a KAOt: Mill rmti~) of 2:2.
Kv,;Ot, K;,Vh, KALN. atul S. with ratio, 2:3. L; 1, And -Sot
Rh 1i
In 1) v- .00
get K.S.O. anti ReFAN. A smallirt anit, 0.2,471:1 Ist!lj see
a sit inKly VA. cTritalf, wall identified. by movallfil Atilt chcul.
"'I with 110) a.
(14-4t
Ifir 'JilhionAte x.%O" Ill" KA041"
KOMAIlit: with let it"U, 12. 2: 4. 2:,%. And .1; ft. flAill,
99-3
Irmit KosW6 k KiWi, wall vrrifinl fly 2 h(-' 1-411"K 14
RM M49C KtVN ill 0 14114) VVI. 4 20 Mi.. With R,.'k),
The cry4talq ppiti. am clivitilml in juil vnimigh mairr at
NV 410'. and allowrill to cryst. fly unallvqke the ykidi in
froill 13-4 1, nere IA v'25. fl.l. r-p.. I,"
h 1W.-Inct. art
1:11. 1:0. Main Aloe
see
goo
000
AlIx-SLA 41TILL11116KAL kItIAIttt CLA% KAMM Clog
Its." 411,8119. .011411T off 0.
A 1 4. fit
11610411% .40 441 dot got
Z 116L A ~?-Mi oll-, i- WT S 0 no 0 a 9 1 of 14 a as 4
it it 11111 It it 4 it 4 Irv, 11% 'Ilo
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ii 040646 0600
I is it IS It a 0 z a V
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MMIM.11by the hydMen
nuids j,,ZjA'btjw" &ad V. St. Fridmass
-'AOOW CbtmA. J. Attl"
0949 1 U-ningmd State tnt., *04
chm. (U.S.S.R.) 19. 33-ft(IM)(Engtish sumtnvwy).---!
die in tbe rvertion 2.N*.90P + 2.V&llS% + 211,S - 3X&t- die
SA + 311,0, optimum temp. Is 2D400. The ricid 1%
00 kmtrcd by Mom temps. The initial t the
004 napnis must beequlosolar. as tillf Wrellvillaltithtl MWU-
br nwm tban 10% lm& to a wricus dmp of thio"str
008 1wid. Uuxk:r the abne coaditions Me N%,SA *ld is -
95-6%. The motbix Hqwn can be rmlded in the p=-,
of G. U. xowkpa
goo
goo
00
goo
04
r goo
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goo
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84TAILLIOGICA1, UTIRATIAl Ct4ltrlCAI;;; goo
kl- IAO,)Vj oil GNP 041 441111 as Inv 411
U 5 A* 10 U AA A I a W a is I I it Is a 31 0
"Oll post SAWN Plan tgxwfl I X%
0 0

IH~ it -11~1 I 11 1, 1 ]1,, 11 ~,,. I ,
S/I MAY'V,)02 /CC0005/026
AQ-.
,;"1A;29
AlMHORS t Zll'b4rNqui, Ya. I.; Fesh~hflvitskiy$ B4 IQ
TlTLE-. The production, cozpok,".1on iLnd ae.-tain propne.!eq~ of urhnyl
PERIODICAL: Radlokhimiya, v. 2, no. 6, 1960,663 o-567
TEU z The artlele detis with a d5scription Of A MthOd f'-'.)r PrOdUOing
salts of the general i'4*a+ (7J0-C&-.-) , whi~re ',P+
I e 3 n is the oation of alk!!Lline
or Alkallne-earth or and C--%r in ths