3/078/63/008/004/003/013
Density, viscosity, and surface tension of .... A059/A126
Figure 1: Pyanometer for the determination of the den-
sity of chlorides: 1 - pyanometer; 2 - constant tem-
perature jacket; 3 - marks; 4 - place of opening of
the pyonometer; 5 Hoeppler thermostat.-
AA
card 4/5
S/078/63/008/004/003/013
Density, viscosity, and surface tension of .... A059/A126
Figure 3: Improved gas setupfor the determination of the
surface tension: 1 - gas cylinder; 2 - electric furnaces
3 - tube of the apparatus for liquid and gas filling; 4,
8, 10 - connecting pipe, '5 - container for tube calibra-
tion; 6 - calibrated t~4; 7 - intermediate cylinder;
9 pressure-gauge cylinder; 11 cushioning cylinder,
12 trap.
- --------------
Card 5/5
~VANOV-EMIN B.N,; ITISEL'SON L.A.; SOKOLOVA T.D.
p .0 -
Reactions of scandium chloride with ethylenediamine. Zhur.
neorg. khim. 8 no.6:1381-1383 Je 163. (MIRA :L6:6)
(Scandium chloride)
(Ethylenediamine)
ACCESSICK Nit: AP4036963 B/0078/&/009/005/1049/.1052
AVZHOR:. Nisellson,, L. A.; Pustil"nik., A.
TITIZ: Orthobaric density and critical parameters of njobium and tantalum
pentaeblorldese
SOLMCE: Zburnal neorganicbeakoy 'rbJ-Ji,, v. 9, no. 5., 1964, 3D49-2052
TOPIC TAGS: niobium pentachloride., tantalum peatacbloride, ortbobaric density,
critical parameter, critical density, critical pressure, critical teWmture,,
niobixn tantalum analysis,, density temperature relationship,, Bertbelot equation,,
Uquid vapor phase equilibrium, crystal liquid phase equilibrium
-ABMM=: The orthobaric density of NbCl and TaCl throughout the 31 uid state
ritic2 parameteL were dete d fig. 1).
and in the vapor state,.and their c nmine r
The densities of the liquid TaC15 and NbCl and of their mixtures were measured
11 precisely from their melting tez*eratures ?216.2 and 204.2 C, respectively) to
300-320 C. The critical Rarameters for NbCl were: critical twperature 534 C.,
density rit 0#68 gm/cm.), pressure p T~9 atmospheres; for TaC2,% vere: 49~ C,,:
0-89 in/=S and 43 atmospheres. Sinceagle liquid-vapor phase and the crystea-
ACCESSION NRi AP4036963 ENCLOSURE z 01
Fig. 1. Data for orthobarie density
of NbC3.5 and TaCl f. 4r
5*
1. --NbClc; (vapor); 2--UbCl5 (liquid).,
data obtLned in a small pienometer;
3--NbCl (liquid), debe. `.-tained in 44
large pkenemeter- 4--Ta-'! (vapor);
5--TaM.5 (liquid5,, data ~b":~ in
SM66U Pl==Oter; 6--TaC15 (liquid).,
data obtained in large picnameter.
tki critical temperature
Tact$
tn4 melting temperature
%C11
AAF1441
zwp-
V
dens Ity gm CM3
Card
141SELISGHI, L.A.; SOKOLOVA, T.D.
'rthobar-ic densities and the criti-cal uarameter- of the viobium
and tantalun, Fentabrormides. Zhur. neorg. kh-irl.. 9 no.9:2066 2067
S (III Pi A 17: 11)
Gosudarstvernvy
proyektnyy
~u 6
-~3 "' T. 'SON,
L. A 1, TJZ~ 7. 1 T
densttles -:-,d crjt~cal parar-,-~--tera cf nfobium
7hur, noorg. kh-m, 9 no.5e
and tanta,urr rentachlor-(,
IC-49-1052 My 164. 04T-F-A 1,7z9)
t
C
#
Pg/Cm t C
tP
ewcqL
g/m _t$ C
.
~
'71 0
1:
9
0 00495
:
204 0*
-
2 1799
: .
327,0
0,00444
'
2st,so
ab 1e 1. D
ensity
D
3-
0
3170 0
00510
012
0 2M:5
O'
24t 2
1358
951
2 BWO 0103 321,0* 2,6338 of U(Traid
molyb
1:3'
0
,
,0188
e
0
08
,
5s
261,
0
,0
,0W
2,0
0103
0 OW
:
353.0
382,V
*
2,5811
2 5071
-
:
:
achlorkb
denimn
pe
2
.
351.
282,5
and tungsten hexa-~
2,010t 400.0 0
,
0182 4tO,O
2
4Aot
1mo
3%,0
40816-
459.9
474,5
47810
4884
50?:0
5105
0
j5f 2:
.1 533,0
&%,0
563,0
567,5
511,0
574.0
$770
578:0
-6786
-&id
.0,03m
I W3,00 1
9687
406,0 0,0212-
2-
436,
2,1119 dbloride
and of
0,0396 32t,O* t:9354 443.0' 0399 478,0** :
2,280
0,044 -
353,00
1 9651
446.0 0
0356
484,5**
-240 their cELtumted
2,
O'm 331,70 1:8031 480,0. 0598 .52615*0 2,080..
vapors
0,1064 397 0* t,7661 00793 565 5.00 1gj()
OT
0,1 414 01* 1,724 .50
:0. mg
0: 540
583:
17w
0 134 422 1,700: '555,0 0, 15T - 599,5** i, Weasurement results,
0:164
457:5-
1 fm
557,0~
0,177
65010#0 Ob-,
tIOM j of' high accuracy
0 166
0 IV 49750*
574000 1:470
0
774 562,0
577
5 O'lig
0,2f5 /650.w*
000
650 0066.
tedned with large
0 m
0,23 , ,
.-592,6 0,269 , Mr=ometer.
0,303
~622 0
0,430
VVeasurement re-
0,35
389 622:0
023,0 0425
0:539
th
-cults 6atainedin
0:516 ~624 4 01376
0386 645:0 0.590,
O:Gf4
059 647,0 0.722
0:62~ M 0, 0:71s
0 w?
L 29547-65
. 'ACCM-ION Im: AP5002796 EM
WSURE:
Table 3- Viscosity of liquid
molybdenum pentachloride and tungsten hexachloride
KOCII WGI. HOCI, WC10
I
i. can-
rataise cen-
210,5 0, M 285 5 1',193 276,0 0 564 342,3 0,882.'
221 0- 0.700 290:5 JiM 289.5 0:525 351,5 0,8M
0 732 308#1 1 i042 m,5 0,479 370,7. 0 742
240,5 0:681 309,8 1,051 - 385.7 0693
252 5
0,621
MiS
972
0
00,5 00(w
0
264: 0,599 333,0 0:908
Card
-15/5
0~4j~ Ot (m)/r-AP b) /EWP (t) IJP(c) JD
-ACCESSION-TM:- AP5oo848o--- SAW/65/010/003/65 95
AUMIOR: Nisellson,, L. A.; Mogucheva, V. V.; Sokolova, T. D.
T'.-"LE: Critical parameters of phosphorus, axsenic., and antimony trichlorides
Z;DM,CE: Zhurnal neorganicheskoy khimii, v4 10 no. 3, 1965, 592-595
IMPIC TAGS: antimony trichloride,--arsenic trichloride, jpjj2sphoru~ trichlori
critical critical~!~s!-Ey---ZAhdbaric density
ABSTRACT: This study has been carried out because the available data,on the sub-
ject are disconnected and Incomplete. Orthobaric density curves for SbC'31 ASC13-) 1,
are plotted, and the critical-temperatures and densities of the chlorides
-a PC 13
are deteimined f"rom the density data. The experimental data are processed by the 1
method of least squares and presented in the farm of interpolated equations. Den-
sities of the SbCl liquid from melting Point to 320C and of the AsC13 and Wl
3
Itz,aids from 0 toLhO-140C are measured with great accuracy. The results are given't
in Table 1 of the Enclosure. The experimental density results areV as a rule, in
very good agreement with available data in the technical literature.- The criticdl
data
temperatures for SbC13 and PC13 are also in good agreement with the available
Carcl 1/4
'4375o-6.5
L
ASCESSION NR: AP50081180-- MWSURE:'- of
Table 1. Orthobaric densities of antimony,, arsenic, and phosphorus trichlorideso-,
abuts AsCle
v U4uirl VaVDr TLA Uid Vanor MmAA
Dmi
ty,
ty,
,,. S, C an
)3 613 - wM PIP A
Mj4 0,00420 03,3* 2,7032 166,5 O,OM 8,0*2,1878 08,0 0105 -9,54 1 GM
237,6 0,0093 78,4 * 2,6653 195,9 0,0238 32,50 2,1344 121,6 0159 0,001:6102
247,5 0,0115 944 * 2,6325 M,3 0,0352 34 8 2,1288 125,5 MO 15.84 1 5821
0
249.2 0.0103 123 is 2 2663 243.0 0,0503 73:0# 2,(972 126,8 :O(qf 27i5* 1:5597
0
259,3 O.ORO 153:5 2:4975 255 4 0,06M 75,5' 2,0413 t46,1 .0260 40,561 5339
0
2887 0 0225_ 182 7 2,4281 275:5 O,QM 7810* 2,0356 159,3 0337 54 G* t,5wi
0
0 0242 207 ?s 2,3703 296,30 'M
296:3 : "" 84,54 2,ozt5 t6t.0 0,0350 6697- to 14
0 00326 239 3 2,2949 3M,3 0-122 I(M.70 t,9743 193,60, 79.3$ i.46M
30 0596
316:7 0:0327 270:0 2,2199 332,3 0,169 126 80 1 9M 05,7 0,062 90,4* 1,4377
W1,5 0,0301 207,5 2,1468 353.,2 0,272 128:50 1:9185 236.t 0.12t 102.5s 1.404 - 0'
Card 3
If 43?50-65
A--MS:EON*hR: AP50ON180 ENCIa
(Table I cont.)
325,5 0,0354, 322,5.. 2,08 378,6 OAU 146,74 8771 252;7 0;156 113,94 C38a
338,7 00419 346,9 2,04. 3785 0484 Mj8l 87H 266,0 0,203
MO.O t:34
344,5 0:0406, 374,7 1,94 381:2 0:560 02.5 84. 271.8 0,215 160,0 1,29
353,9 0,057 418,0' 1,84. 0,0' t,83 278 3 0,256 f79,O t,24
402.7 0, tO4, 437,0 1,70. 186,2 1,79 237:2 0,021 194,5 'M
415 5 Of 121 454 5 Im. -
204 ' 8 1 73
~ 290,9 0.4 01 206f2 116--
425:6 141 469:7 58
, 223,0 69 290,0 0,4 57 218,5 t: f 3
430,9 0,154 619 5 of 237,5 t,65 20t,2 0,4 57 226.2 1 to
444,5 0, 08. 521 1
00, 251 5
' 61-
3 t:07
459,0
0 2095
522,8
10 264
0 1,57 . 241,0 t IDS -
471,3 236
0: 296"a t,46 t 021,
"
247 '
512,9 0,444 319,5 38 251
5
1,00 y:
'
515 '7 0 441 33795 f:29, 254 0.99
'0
' M 3 0:555 348,0. 1,23 290
D 55
'0
521:5
,k 0,705 353.0 t 20 289
5 O:Gq
8
5
22
7
92
31 2
:80 ,
521:0 O:M 382:5 0,88
519,3 0,856 -
The accurate density measurements were obtained in a pycnometer of large volume.!
,
Curd
ILIA .0
L 59240-65 EWT(m)/WP(t)/EWP(b) IJP(c) JD
ACCESSION NR: AP5015012 UR/0078/65/010/006/1297/1299
546.2841131 + 646.271131
AUTHOR: Nisellson, L.A.; Pugachevich, P. P. Sokolova, T. D. ; Bederdinov, R.A.
TITLE: Density, viscosity, and surfacetension of silicon tetrachloride and trichloro-
silane
SOURCE: Zhurnal neorganicheskoy khimil, v. 10, no. 6, 1965, 1297-1299
TOPIC TAGS: silicon tetrachloride, trichlorosilane, chloride density, chloride viscosity,
chloride surface tension
ABSTRACT: The article continues a series of studien on the thermophysical properties of
halides. Silicon tetrachloride and trichlorosilane are important source materials for the
preparation of high-purity silicon, Data on their properties as reported in the literature
are contradictory. In this report, the authors present the results of measurements of the
density, viscosity, and surfa6e tension of SiC14 and SiHCI~ between zero C and a tempera-
ture slightly above their normal boiling points. The chlorides studied were thorou ly
gh
purified by chemical means and by distillaqon. Density was measured in quartz pycno-
meters, viscosity in a capillary viscometer, and surface tension by the method of maximum,-..
pressure in a bubble. All the measurements were carried out in sealed devices in order
[Card 1/2
L 6a 589=62 BWT(M)/EWP(b)/EWP(t) Ps-4 IJP(c-)- JD/1JG
ACCESSION NR: AP5018241 UR/0078/65/010/007/1516/1519
546'.6231131+546.681.31131
AUTHOR: Nisel'son, L. A.; Sokolova., T.'D&-
TITLE: Density, viscosity, and surface tension of aluminum and gal lium trichlorida
SOURCE: Zburnal neorganicbeskoy kbimii, v. 10, no. 7, 1965, 1516-1519
TOPIC TAGS.- aluminum chloride,_&4~,.llium chloride, density, viscosity, surface ten-
sion
ABSTRACT: Pycnometric measurements of density yielded the followin equations:
fAl 2Cl- =1 2841-2.32 x 10-3 at - 2 36 x 110-61 At2 dcm~ from tfus
to 256.0C, here ~t t - 192.5C (mean square error46?sq 0 0006) and
2 0546-1.985 x 10,3,6t - 1.44 x 10-6 At2 g/ci;~ from
ra2C' tfus
78.0 to 240.'OC, w9ere b*t = t - 78.,OC (mean,square error bP, ='0.0013).
sq
From the peaks of orthobaric curves,, the critical temperatures (t
cd were found;
the critical densities were also determined. From viscometric data, the followin'!
9
equations were derived:
Card 1/2
UNKOVSKIY, B.V., MALINA, Yu.F.-, SOKOLOVA, T.D.
Stereochemisti-i of acetylene synthesis, Part 4: Synthesia
I
and spatial configuration of ,he geam-Aric isomers of 1,-2-
dimethyl-4-ethynyl-4-piper4-do'l~ an.. -eir derivatives. Zih-ur,
org. khim. 1 no.47699-?06 Ap '65. (MIRA
1. Moskovskiy in8titut tonkoy klimicheskoy tekhnologil imen~'
Lomonosova.
N-!.'A;,''-QONF L.A.; C-OK01,I)VA -r.D.
Orthobaric densities, criti-al para-meters and viscosl-y of
kc0l, and "'C16 khlm. 10 no.1318-21 Ja 165.
Zhur. nearg.
1 (MIRA 181,1111
1. Gosudarstvennyy nauchno-issledovatuellskly 1 prwfektnyy
instLl,ut TedkoLetallic-heskoy promyshlennosti "ONJITMET";
Moakm.. Submit'ved ~ug. 3, 19656
7
L Y;85-0-66 7,T(ri)/7-7,~T (t) /.,TI
ACC NRt AP6ol4898 (N
IJP(c) '.--T,-I/JD/JG
SOURCE CODE: UR/0076/65/039/012/3025/3032
AUTHOR: Nisellson, L. A_~_; Stolyerov, V. I.; Sokolova, T. D.
ORG: Moscow State Scientific and Desi n Institiite for the Rare 1-letol
Industry (Moscovskiy gosudarstvennyy nou6-hn-o-issi~-3o-vfife-Yf-6-ki:y--f-
proyektnyy institut redkometallicheskoy promyshlennosti)
TITLE: Properties of liquid zirconium tetrachloride
SOURCE: Zhurnal fizicheskoy khimii, V. 39, no- 12, 1965, 3025-3032
TOPIC TAGS:.- zirconium compound, chloride, heat of vaporization, -TUMMer.
ABSTRACT: The zirconium tetrachloride used was the purest fraction,
purified by rectification in a metallic packed column. The content of
hafnium and other metallic impurities in the chloride was less than a,
hundredth of a percent. The temperature mes.surements were calibrated on
zinc (M-P- 419 500) and were mode with a Chromel-Alumel thermocouple
using a type R~/l semiautomatic potentiometer. Determination was first
made of the temperature of the triple point; this was done from the
cooling curve. Next, measurements were made of the pressure of the
saturated vapors. Results are exhibited in tabular form. Measurements
of the viscosity were made with a special viscometer (illustrated in the
UDG: 54-1.
1, 8~0-66
ACC NR- AP6014698
rticle). Finally, the surface tension was measured, and the results
-Ivan in a table. Calculations were made'of the critical pressure, the
.ussinormal boiling point, and the dependence of the beat of
'aporization on the temperature.. Orig. art. b9s.* 10 formulas,, 4 -figur
nd 3 tables.
CODE: SUBM DATE: 28Nov64/ ORIG REF: 009/ OTH REF: 010
ftASE I BOOK EXPLIDITATION SOV/4726
Kly:v. Gosudaratvann;i7 nauchno-lsolcdovatollo~cly I proycktnyy In-
titut ugol-noy rudnoy, nertyanoy I gazovoy promyshlennosti
Nauchnyyo zaptaki, ~JP- Is Dobycha i porerabotka nefti (3cl-
entific RLports of the State Scientific R~soarch and Project
Institute for the Coal~ Mining, 011, and Gas Industries, No.
1: Extraction and Processing of Petrolewn) Kiyev, 1960. 91
p. 1,000 copies printed.
Sponsoring Agencies: trkrSSR Go3udarstvennaya planoviya komicalyn
Soveta Minlatrov; Gosudarstvennyy nauchno-13sladovatellskiy I
proycktnrl Ins.11,ut ugollnoy, rudnoy, neftyanoy, I gazovoy
promyshlannos ti *Ukrnilproyekt."
Editorial Council: V. P. Ak5enov, S. Ye. Anushin, S. I. Balinakly,
V. Y&. Volchanakly, D. 1. Gal-tacV, V. S. Grin ant eyn (Reop.
Secretary), B. V. Dzbanovokly, M. M, Zherbin (Chaim n),
A F. Kotov, M. 1. Logvinov, Yu. M. Catrovokly, L. M. Orzhekbov-
sLya, 0. V. Prisedskly, V. T. Sklyar'(Deputy Chai'man), 11. Yu.
3tasivi and V. V. Tsarltsyn, Reap. Ed. for this Collect.1,on:
V. T. Skylar. Candidate of Chemical Sciences; Ed. : A. Novik.
Card 1/5
11j1:_'_C0_j1_ec tIon of ~ticles is Intenaed for petroleum
F, researcher engineers, and refiners,
COVERAazs The collection or articles deals with the production
and refining of patrols=. Individual articles discuon the
effect of bound water on the depletion or pctrole= deposits
u conditions t the
nder dIdsolVed 943 1 the affect of presnure on
viscosity or dega.81fied petrels=, the strui:turo of hieh-molo-
jar patrols= hydroolLrbons, the asphalteno and tar co=po-
ou
ments of Carpathian crudes and menillte shale asphalts, slid the
liphatic composition of a1cchol3 produced by aelective hYdro-
:enation Of the CO and H2 product or synthesi3. Other articlc3
describ the carba=Ide dowaxing method for filtrates or wax dig-
of flotation agents with he use of
t stg:, the pcduct;lon -men
oxidized pat ro latu=, and the Inveattgation or six bered WO
.tic and naph'.1enic hydrocarbons by means of infrared aboorption
spectra. The remsl=ng articles are on the relations of pressure-
voluuge-tenperature-ethylone and on the phase equilibrium In
:thylene-n-heXane. - th7lene -aye lohaxano, and ethylene-bonzone
ystogs. specific vol=es and compression coefficients at
Card 2/5
PETROLEXX W21NXNa
Serglyonko, S-OR 'P Te. V. Lebed-v, and A. A. nkhnovskaya. On 13
the Structure r i&*i Molecular F4drocarbon5 of Petrolmm
Card 3/ 5
P. Lizogub, A. F. millnev, and 0. A. Puchkov-
Sklyar, V. T., A. Cale Hy-
ska7a. Study or Si4x-Membcred Aromatic and Z;nphth 25
drocarbono by Infrared Absorption Spectra
and N. V. ArCVYI~.
M. S&Mt30Vl, T Q SOk0IOv3
Sklyar, V. T.p L.
me
Asphalteno and Tar Ccmponents of So a;~a~ -an Petrolena and 30
Asphalts or Menillte Shilen
~abirova, 0. V., G. M. Shapova 10 V' and V. H. Kara3eva. - Pro-
ductiOn Of an Frfective Plot"tion AF, ent Based on Oxidized PC 56
trolat=
Zhurba, A. S., and T. P. ZhuzC- CoapArison of the EthYlene-n-
Hexane, Ethylene-CYclohexane, and Ethylene-Ben=ene Symte.= by
the P-v-t-N [pre 3 s,re -0 lune - tempe riture-nolar facttan Of
ethylene In the mixture] Rol3tions and Phase Equilibrium 68
Zh.ze, T. P., and A. S. Zhurbl. Specific Volunc3 and Com-
pression coefficients of the n-Hexane-EthylCne System In the
Interval of Pressure to 150 atr and Temperature of 30-150'C 78
USSR/Opt.i-cs Optical Engineering. K-4
Abs Jour Referat Zhur - Fizika, No 3., 1957, 7649
Author Sokolova, T.I.
Inst
Title ODtics of Russian Microscoi3es and its Develooment.
Orig Pub Vopr mili-roskys-Ii. M.-L., Mash-.ez, 1956, 4371
Abstract Survey of the optical characteristics of microscope
objectives in ocullars, produced by the Russian industry.
A large number of tables is given.
Card 1/1 - 16 -
SOKOLOVA, T.I.; PLATONOV, M.P.
Biolouical microscopes in 1961. TSitologiia 3 no.3:345-357 My-,
0
je I&l. (MIRA 14:6)
1. Gosudarstvennyy opticheskiy institut, Leningrad.
(KICROSCOPE)
SOKOLOW., T.I.; TIUNOV, L.A.
ComDosition of diesel engine exhaust. Gig. i san. no.10:48
0 155. (MLELA 9: 1)
(DIESEL ENGINES)
T
27 no,~;2~-32
60*11116,00,1111000:::
A A r. A I I L 2 A It L
GNVI .1
410 A
c4talytic decomposition and 111JACIOD of O"Julonid 'Alth Wculifol cataf)AID. I I
1
.
f-111111 A-41,
1
1 1'44%411A~16A Zhhl, P,ithpf-f KAP-~ 4. lial L~4kjjql~
00
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da 'a., It 00
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.CCIIIIIS AND 020PENT-IS Dt A
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con,
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PSOCIMS AND POCOINIIII M004 -00
An 60 00WASM Pro-
0. X T. L
R. owa. bd. Rem., iny, %, ml-iw) ~~-IU
- 1, ofeaw"balk at V cataly~4 at 470' is "00
cc 69 rw
109 .00
4-6-40%. 2%9 nwv of &din-
tion, is sale. to bi 23.000 S.-a&L The optimum ISOJ zoo
Tarim Wilk do (0j, Mw " W" the Mkw of the
ow4m of Oas for Ovdiriary.pyrf" VW Man. too
ollislatkni im obiahwd with 70' fiw ~btualfenvue
ma with 3-60,qa. amording 9'0* C amtent, atul
=
8 with 8-2% 8%. Higbw conwa. of 80, can
be vasd proMed that the ps mixture is enriched
with 0, R. T.
JL OfIALL~AL LITIIIIATMI CLASSAPICATION
loom 11.1519W.
.11 GOV Got a A a S i T -4w -(;A -.1 S I
U an a 9 a rid 0 it 4 1 Is 61 -j a 3 aI
46 *10 0 0 0 0 0 0 0 0 0 0 0 0 0- is 0 -0 0 0 0 0 0 0 0 0 00009
Mee
464
0049
Coo
coo
too
0-6-Ar-O -W- W--W - I - ..
0 0 9 9 0 0 0 0 A
if 14 IS 16
v It 12 1,
11 Wis um S&P U0041 dium
A
W1 A I~Q 4"
PROCISSIS AWD ~RV*tAlItS ;%VC1
i
he
of Con't"t olddatiml of Ulf&tr dioxide In
'
r. 1.
P1 firric axide. C_ K. t%dxt,L,.v ;Vtoi
X
(A J. phys. ('heti, (U.S.s.k.) 18.147, - 101(1044);
k
s
Any
-
,
W SA I
1
l (
API
4
l
l
Got .
ma
t
y'
. FO). I, 'k Koo,
it 13
-
40,
C
l
'
r
is
f
11
;
let, It
v
ll. I Vill 11. o
; I lie lo
y
l /' (), - SO, UIX)VC 1411 71)
d
I
sc
low when it 6 re&chctl by cooling still high when tv"
gem by heating. Above OW the cataly't Alow, in sill %-ray
Go Clolloln. only the spaciript of hematite; Wow (17j)* it coil-
WHI 111) 10 41% Of SO, Mind shom, Adiful. -vachiss. The
sulfated catalpt is probably a mixt. of JI'VAh and irel-
*
go 'ji
~li (.SO,).. At (W
the rate r of SO. fortuation deptuds on
the conert. of 9%(x), SO~(y), and 0~(z) according to.& m
go j k, I - (I1Kj(y1x)'-'I. Thc app&ent energy of
Goa activation of the SOs fornuation is 39 ka.-W. It is su;-
it-ted that SOt Ill oxidlud by the surface &turn of 0 in
FV.0, which then 6 reolidited by Or. B.A.
0 0 :1
g
Fl
o
SLA ETAL UR41CAL. Lill MAT 64 1 CLAISIFICAY100
90.111v
to luol) I. om, '.C SULSI(Pff lll[Lill OW OWW Ill
-i-- a L S a rm 0 a If I N 01 5 d3 4 3 0 9
if It OF a a a a, 1*9 elf 1 13 W. An
0
=00
too
moo
Wo
uo
*too* **.*so*** W-V-
I v 10 11 if of 14 it % I? U .11M, nmn J*17&m oil Lin Jim U U a*#) 41 n8l 4411110
A 4"-& m *-(X-MLU~A --- L 4-11 .-~L
A- i;F 0 Tt's 0
0110CM11% AND OftPlklitt IND94
Prolimaralloo of moNdes of phoqhorus froln fe"hom-
'Bag. mead. Jci rJ
1943, M-101RIWAsummary)-ifeating 5.2S parts P
with 41.38 parts S (as pyrite) under
W-11
~~!.rvv 7.2% recovery of P as mixt4i sulfliffs
sea C f-t h
n, P,7~-
at 700 azmt 877, at 1070*. The most ft~momkaf pm~
ceduselowtobeat 31irs. atowl, niea~ure p ill the residue,
add p3iifti stoichlotmetrically to the reqldue according to
15Fc$1 + 4FelP ~ 23FeS + P~&, and repeat the heating.
This gives 90.3% overall recovery of P as mixed sulfides,
whow compn. can he adjusted by adding P or S. For
conversion ill I kg. P to PA. when pyrite is uqvf,.111
ego' 177 kg. when 5 Is used, aft - -1004 kg Up
to 15M*, the action with 8 H practically irreversible.
00 -3i
Cyrus Feldman
V
A 8.1LA ASTALLU0160CAL LITERATUNI CLASSAPOCATIOM
slow 1711mit'.
11 la'a .1p C., Oil 41A 31 OW GOV Ill
A A - 1-- 1 1 1 - I An A S is emo-O WIN USAIG 3 9 IF
to a to ill of K it 11 N K it 11
a 0 0 0 : : 0 0 0 0 * 0 0 0 0 0 0 0 0 0 0
00 0 0 0 6 41 *is 000 0 0 0 0
roe
roe
g*0
see
rise
04110
1110011
IT-TARIONOV, V.V.; SOKOWVA, T.I.
Study of the decomposition of solid solutions of the system phosphorus -
sulfur. 1--v.Sek-t.fiz.-khim.anal. 21:153-158 '52. (mT.RA 6:8)
1. Nauchnyy institut po udobreniyam i insektofungisidam imeni Ya.V.Samoy-
lova. (Solutions, Solid) (Phosphorus) (Sulfur)
eo Id
The 1C4+3Ag;::t3AjCl+Bl. 14JQ4R1ov5
-
C 'I-,
.-
y Tn~; ey Tno
(N. sZEFWM - I I -
t-Seklora Pt Anal.
kad , Naak S.S.S.R. 21, IW71
'(1952).-This system Was studied by thermal analysis and'
'Microstructureanalvis. The diagonal cuts AgCI-Bi and Ill.
-s
CIAg of the trapezoid part of the diagram show reaction'
product-son both these line.-;; thisindicates that the system Is
at least partly reversible. There was less interaction along th6-
line ASCI-Bi; this fact indicates that this Is the more stable
diagonal..". The diagrarns show the presence of 2 eutectles.,
one in th ,esystern, BiCI,BiC[-AgC! and the other in BICI-
Aj:CI-Bi. Tile location of still another eutectic in BiC!#-
BiCl-Aj was hard to ascertain. On tile diagram there is a
large n-a of layer sepn. and 2 one-phase areas. Within
the latter are ' he fields where 33i, BICI, AC, AgCI, and
In the are of layer scim. the following phases
BiC13 -5!P a
crystd. Aghl the lowerlayerand AgClla thcupper,(2)
a etitec e alloy of 13i and BiCHu the lower and MCI In the.
upper layer, and (3) a. eutectic of Ili and Ag in the lower
layer and AgC1 in the upper. 'With a virw of. removal of-
Ph refining it is pointed ouC that the chlorides and the
metals formed in this reaction combine very little Ili tile
molten state. The best yield of Di is obtained with all
exec--~s of MCI, near the diagonal AgCI-Bi. Theinax.purity
ofBiis95at.%- In the system BiCI,Bi was found an'un-
stable compd., RiCl, which decompoics into Ili and BiC4.*
N~
2
H20
USSR/Chemistry - Pharmceuticals SeP 52
"Synthesis and Study of the Gamma-diethylamino-
propyl EtUher of 24L-thoxy-6-allylphenol,'~ A. M.
Khaletskly, T. I. Sokolova, Leningrad Chem-Phar
Inst.
"Zhur Obshch Khim" Vol 22, No 9, pp 1648-1650
The garwa-dietbylaminopropyl ether of 2-methoxy-
6-allylpherol, as well as its hydrochloride
were prepd from 2-methoxy-6-allylphenol and I-
diethylamino-3-chloropropane. A salt was -Drepd
from the above ether and 1,5-disulfonic acid
of naphthalene.
232T28
USSR/Cbemistry - Phosphorus Jun 52
CoMpounds
"Separat ion of a Mixture Of Pocl3 and PC13 T. 1.
Sokolove, V. V. IllarionovY S. I. Vol fkovich
"Zhur Prik Khim!' Vol XXVY No 6, pp 652-657
It in sbawn that values expressing the dependence
of partial pressures on the compn of the PCI KPOC13
mixt, an derived for the purpose of plotting the
isotherm of partial pressures of the system, satisfy
the Duheme 7 eq and allow calen of the Duheme-
Margulis const. On the basis of the data obtained,
USSR/Chemistry - Phosphorus (Contd) Jun 52
the dependence of the compn of the vapor phase on
the compn of the liquid phase can be plotted. It
can be considered, with sufficient accuracy, as an
isobaric function.
218T37
t4
9
10
,to
SC1KCj7'0VtA1' T.
L)
Th%1ajWM of-the r
inremandformaidebyd ..Ivnff=~an
Fdm-akol. i TO(-M"4o . 10, No. 4, 45-7(IUMI. Beat-
instilatingf,,la3tic'(I)Prtfd.froinHCHORndureit(asstar)!s
Isprepd.1up ates (sp. gr. 0.03) and crumbs, which
1p.rWisisily but do not burn. At 180-2000, 1 Is carbonized
and decompd. to form gases. A complete decompn. takez~
place at 400--500*. On an open flame the decNo * uIck
d Complete. Among the formed gases HC Tn. N,the
an foun
presence of which was detectid by absorbing the gas" with-
a dil. alkali with the formation of Prussian blue. When I
Irg. of the plastic Is burned 4,738 g. HCN Is formed. Burn-!
ing 0.15 g.'plas Ic causes the death of voice after 1-2 min.
(0.71 mg. HC'N
is produced). L. Goldenberx
ANIRMV, V.V.-, SOKOLOVA.. T.-I.
Toxicity of heat-iasulating plastic with a formaldehyde and urvea base.
Farm.1 toks. 16 no.4:45-47 Jl-Ag '54. (KLRLA 7:5)
(Hydrogen cyanide-toxicology) (Plastic materials)
T IUNOV, L.A. SOKOLOVA, T.I.; PARIBOK, V.P.
Rate of carbon monoxide excretion from the body [with summary in
English]. farm. i toks. 20 no.4:76-78 Jl-Ig 157. (MM 10-:11)
(GARBON MONOXIDE, metabolism.
excretion rate (Rus))
VOLIFXOVICH. S.I.; SOKOLOViL, T.I.; KULA GI M-S I'AIRNOVA, Z.G.; KDYAZEVA, K.P.
Carbonizatinn procoa-; for production of cryolite from fluoroaili-
cate gases. Zhur. prikl.kbim. 31 no.7:969-976 ii l58. (mm 11:9)
(Gr7ollt") (Fluorosilicate)
40-111' 4p
a it v JF
2 IQ it 13 u W u
f a k _L__
_JL
.'~&
00 A J.D No 41. votes
c
17 ..a J-D act#$ --- --- -
Away MMPQUU&L VU11nation of chlolosuftonle Wove
0 ~A T N
hydrosynso compounda by the "16m of cAjagoaWfoole
awsycof"Pouncts.
Comow. few, dfaLd. lei. U.N.S.S.
In it little CC4. golaed
'
with A tvat'Jil excess of CL%hll below -8
, stirml I hr.
at -P. aim) thrown onto ke, YiWs' After let., a. frM
004 abs. AcOll, 70!'a p4jWr#zy&wbmvxe cAkr#jq2vW~k
-00
oranse-yrilow cryows, to. sluidetly.
'
'
di
-
3.3
nvelbyUsusybenzew yieMi J,J
4jxk4AjW_ .00
t
:0 '
i
0 ,e uns, in. 46-7.5
pr
(from ligroin) , 3 WAichlormiczybens-
ene yiekis M% W
00 '3 ora-
lldfo-k (111), Grange-yelk- er"tals, m. 56.4-6.2' 200
G
0.3
(frons anhyd. AcOll); antl the a- and fi-isorners of 4- oo
bromosaoxybenzwe ykM 80% #-broav.-4'_hjeIrvxysu_
-
00,3 brx3me chlorassifonate (TV), m. 106-7*. 1. U. M.
and
goo
00. IV are sapond. by boding 4-5 bra. with 2-31~ aq. or air.
0 a KOII to the corresponding hydrolynso camp&.; that from
'
It Tn
114-15* (from li
i
h
f
0 -
gro
n); t
at
rom III un. 124.6-5.8
(froinaq. McOlf); and that from IV m. 157-81, ClsoH COO
n-Acts slowly with P-hydroxyambenjeue (from sapon. of '400
1) to yield 4-(4-hytfroxyphcnyfaw)benwn~utfonyt chlo-
*
i 900,
tle, m. 131-2
r
. Robert W. Shortridge
1
I ISO*
L9 CL
ti
&ETALLU"ICAL L"INATLIMIR tLASSORKATION
sanoso -4 % ldo L' aw. car a3"21 met
a . - 4 W -I- & v ZA a I a a a 2 a v
?p IP I ; a it 9 of It 11 tt 0 No A I a
4
1 1
0 0
: : : 00 Oes 0 0 0 0 0 0 0 0 00000 0 0 0 a
0
0 *
0 4
~ 0
0
a 0 0 0 0 * 0 0 0 0 0 0 0 0 0
0
0 0 0
0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0
0 0
10
0
0 .
SOKOLuVA, T.N., dotsent
Clinical aspects and diagnosis of odontogenic inflammatory
processes in the facial vein system. Stomatologila 38 no.3:
50-54 14y-Je '59. (MIRA 12:8)
1. 1% stomatologicheskoy kliniki (zav. - prof.I.M.Starobinakiy)
I Mosicovskogo meditsinskogo instituts, imeni I.M.Sechenova.
(FACIAL VEIN--DISEASES) (TEETH--DISEASES)
GORBUNOVA~ Z.V.; SOKOLOVA~ T.N.
Syphilitic aneurym of the aor-ta with external nipturs. Klina
0
med. 38 no.'s2-47-149 Je 160. (MIRA 13.-12)
(AORTIC MWRYSN3) (SYPHILIS)
/V
PHASE I BOOK EXPLOITATION SOV/6333
Bochkarev, V. V., ed.
Tekhnika izmereniye radioaktivnykh preparatov; sbornik statey (Tech-
niques for the Measurement of Radioactive Preparations; Collection
of Articles) Moscow, Gosatomizdat, 1962. 4600 copies printed.
Eds.: A. M. Smirnova and M. A. Smirnov; Tech. Ed.: S. M. Popova.
PURPOSE: This book Is intended for specialists In nuclear instru-
mentation.
COVERAGE: The book is a i3ollection of articles on recent developments
in 1) measurement of the activity and 2) analysis of the composl-
tion of emissions of radioactive preparations. The methodology and
apparatus used in these studies'are described in detail. References
are given at the end of each article.
TABLE OF CONTENTS:
Card I/P /
Techniques for the Measurement (Cont.) SOV/6333
Pigoreva, N. S., Ye. 0. Solodovnikova, and V. V. Fokin. Prepara-
tion of Samples for Measurement of the Activity of Certain Com-
pounds Labeled With CI4 and H3 Isotopes 67
Golutvina, M. M., and M. A. LIvova. Preparation of Specimens
for Measurement of the Activity From O-Emission ' 72
Levochkin. F. K. Measurement of the Activity of Thick P-
Sources 83
Kononenko, A. M., V*. A. Petrov, and V. Ye. Yakhontova. Dose
Distribution Along the Axis of a O-Emitting Plane Disk 100
Bazhenov, V.. A.j V. V. Bochkoxev,.and T R._�9kolov Measure-
ment of the~Activity of Gaseous Prep~At"ions by Means of a
Gas-Filled Counter 115
Turkin, A. D. Radlometry of 13-Emitting OF-ses by Means of End-
Window Counters 124
Card 3/5
BOCHKAREV, V.V.; KRONIGAUZ,A.N.; SOKOLOVA,T.N.; TIMOFEYEV,L.V
Determination of the dose of radiation from 8-applicators.
Med.rad. 8 no.2.,66-73 F163 (MIRA 1611l)
S/115/63/000/002/008/008
E194/E155
AUTHORS-. Bazhenov, V.A., Bochkarev, V.V., and S-okolova, T.N.
TITLE: Sorption effects in measuring the radioactivity of
gases
PFRIODICAL; Izmeritel,naya tekhnika, no.2, 1963, 57-59
4r.,XT: In measuring the radioactivity of gases with gas-filled,!
.Y:adiation counters, the absorption of P-radiation by the walls and
end-effects cause errors which have both been thoroughly discussed,:
particularly in the non-Soviet literature. However, there are also~
two sorption effects. some of the material becomes firmly attached'
to the walls and remains there after the chamber has been nominally~
.swept free; and some becomes temporarily attached to the walls
during measurements, so disturbing them, but is afterwards released~
and swept out, so that the effect cannot be directly observed.
Tests were made to determine the relative importances of these
effects. A chamber, filled with a gas tagged with a source of
P-radiation, has a thin mica window in one end over which is placedl
an end counter. The chamber also contains a layer of material of
such a thickness as to absorb p-particles of maximum energy.
Card l/ 3
Sorption effects in measuring the ... S/115/63/000/002/008/008
E194/E155
Then if this layer is plAced next to the window without breaking
vacuum, the counter records only p-particles from substances
attached to the inner surface of the mica and to the surface of the
layer. It can be confirmed that radiation originating in the gas
filling of the chamber is not being counted by withdrawing the
layer and inserting an analogous layer between the mica window and
the counter. This gives the background level. After sweeping the
chamber, the background contamination due to irreversible sorption
can be determined. The actual experimental chamber, made of
duralumin, was 178 mm long and 50 mm diameter with a window of
1 cm2. A disk with 12 positions could be placed at various
distances in front of the window so that the material of the layer
could be altered without breaking vacuum or changing the gas. The
gas used was CS2 tagged with s35 with a specific activity of
25 milliCurie per gram of liquid carbon disulphide. Surface
sorption was studied on the following materiitls: teflon, mica,
special lubricant for CS2, brass, aluminium, methylmethacrylate,
olished and unpolished ebonite, rubber mastic and sheet vacuum- p
p
rubber. The experimental procedures are described in some detail.
The materials were found to fall into two groups: the firs'
Card 2/ 3
Sorption effects in measuring the ... S/115/63/000/002/008/008
E194/E155
instantaneously acquire a certain surface activity which then
increases exponentially with time (PVC, ebonite, methylmethacrylate).
The other group includes the remaining materials except the rubber
mastic, in which surface activity instantaneously reaches a certain
value which then remains constant. The relative sorptions of
samples of the different sub.9tances, i.e. the percentage of the
radioactivity picked up by 1 cM2 of the given surface to the
activity of 1 cm3 of the chamber was: teflon 5; mica 5;
brass 6.5; aluminium foil 6.5; methylmethacrylate 13; PVC 28;
polished ebonite 30; rubber mastic 39; rubber 45; unpolished
ebonite 65. For materials of the first group the calculation is
made for an exposure time of 26 hours. From these data it is
in particular experimental
possible to assess the sorption of CS2
equipment. Thus the activity Of C52 sorbed on the walls of the
measuring chamber filled with radioactive carbon disulphide was
.directly measured. A large proportion of the sorption was
.reversible and so is not revealed by background measurements after
cleaning. The sorption effects are very considerable, and differ
for different materials. There.are 4 figures.
:Card 3/3
BOTVINKINA, L.N.; SELIVERSTOV, V.A., SOKOLOVA, T.N.; YABLOKOV, V.S.
Some genetic types of Tatarian red beds in the Ural Mountain region
of Orenburg Province. Izv. AN SSSR.Ser.geol. 28 no.5:47-66 My
163. (KRA 17:4)
1. Geologicheskiy institut AN SSSR, Moskva.
SOKOLOVA, TX.; SAKOVA, T.V.; KONSTANTRIOV, N.N., doktor biol.
- I nauk, red.[deceased]
[Photoperl:odism of plants; bibliography of the literature
for 1940-1963] Fotoperiodizm rastenii; bibliograficheskii
ukazatell literatury 191,0-1963 gg. Moskva, Nauka, 1965.
364 P. (1,URA 18:10)
1. Moscow. Glavnyy botanicheskiy sad. Nauchnaya biblioteka.
Sf,IKOIffVA-f T.N.
Phlebitis &s a complication in purulent processes of' the
maxillofacial region. Trudy 1-go WI 44:119-126 165.
(MIRA 18:12)
T, CM11;4-67 x; i
ACk- Nwi A,17002769 '07Li',ZC': C6j).--. Ult/0039/66/021/602./01411
AUT60'.~: i1nvhonov, V. A.; ilochicnrov, V. V.; Golubev, Yu. M.; LGv1n, 1. V.;
"o,
1~olovn, T. N.; Turkin, A. D.
OXG: nonc
TIMZ: r',casurements of activity of radioactive gases by means of spherical
Ionization chainber -i
SOURCZ: Atomnaya onorglya, v. 21, no. 2, 1966, 141-142
MIPIC TAGS: ionization chamber, radioactivity measurement
ABS T, copper barrier, filled with
RACT: A spherical, 24-cm ionization chamber with a
air under atmosphcric pressure and operatin,-, in the -spectnim energy ran-e (0.15 to
2.20 Ncv) vas used fmnicas~5ing the ~as activity In experiments wich 13~;