SCIENTIFIC ABSTRACT BRODSKIY, A. I. - BRODSKIY, A. M.

• Document Type: CREST
• Collection: Scientific Abstracts
• Document Number (FOIA) /ESDN (CREST): CIA-RDP86-00513R000306930013-6
• Release Decision: RIF
• Original Classification: S
• Document Page Count: 100
• Document Creation Date: November 2, 2016
• Document Release Date: June 9, 2000
• Sequence Number: 13
• Publication Date: December 31, 1967
• Content Type: SCIENCEAB

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BROTMIY, A. I.
"The Concentration of the Aeavy Isotope of Oxygen
with the Distillation of Water L an Isotopic Anal-
Ysis of the Water"; 11, No. 4, 1939; Cherlico-Tech.
Insti. Lab. of Physical Chem., Insti. of Physical
Chem. imeni. L. V. Pizharevskiy, Acad. of Sci.
Ukrain-
ian SSR, DAv. of the Chem. of Isotopes,
Dnepropetrovsk;
RcH I JulY 1938.
Report U-1613, 3 J2n. 1952
C.t)- 33, 14Li~-

BRODSKIY4A818 6oo
1. BPODSKIY, A. I.: RADCHENKO, N. P.; SMTOLENSKAYA, B. L.
2. U.--!SR (6oo)
"The Isotopic Composition of Arctic Waters and Ices," Zhur. Fix.
Khim, 13, No. 10, 1939.
Dnepropetrovsk, Institute of Physical Chemistry, Academy of
Sciences Ukrainian SSR
imeni L. V. Pisarzhevskiy, Department of the Chemistry of
Isotopes. Received 15 June 1939.
9. 4WReport U-1615, 3 4an. 1952.

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ad. U.&S.S. 53, 437-80m)(18 ISAAHAW.-In order to
det. whether or not toluene 11) forms a tautomef of
type (H), the method of hiotop" was used. If such
CUr-Of
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If
(U)
watomerim could take place in the presence of a D
dasar (13i0. RtOD. etc.) adda. of D wom be expmed.
and a partial loterdsonp of It arA D from tbe doom
should be ohwvW In the Me voup as wil at In the ortho
*W pers pooltions of tht nucleus. I was beetell with 37,o
heavy water 00 Ins. at IW-70' to a walal tube. After
from the water and careful 4ryidX and clombustlon.
content of the water foolued was detd. Under then
cootditions no entrance of D into I either In the absence or.
can of catalysts (3% 1 IvSO, or 2% NaOH) was rmted.
."Int"chngr of 1) and It took place when sivollar mixts.
ff
tit I &W the catalysts we" expoml loultra"t light 40'
/0
hmst4o". Whit" heavy 14011 (omit. A% D littlorIV)
trilop) vu used. no interchativ wat i*ftk tvftpt in the
OINAOllorlito. . teven rm mort t n
% of the H atoms in the Me group of were replisced by
D within 00 hm at 170*. Very unWar results a e ob.
tained when analogous readions w= attempted with
nualtykne(W).
the Its to the nucleus is excluded the revolts obtabol,
voint to the absence of tautanocrissA6 in the ease of I awl I
G ..logesoation of I or III Presumably cannot be ascribed
to suMn. of halogens at a double bond. 71w slight later.
change of D and I I In I and III may be due to lanizatiou
of It In the Me grotip. In preliminary rapts. It was she
aluvorn that certain subethutins voupt In the aromalic,
nucleus decreased The stability of the C-if bond is the
M p. Time nitrotolveras exch" It Wod D fairly
=d ry Then expts. am no, d...= L. IL Wine
loom 60411%V
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ol"n, "I. hall'. 1*10 le"24,11iteaku, 1. 11. Grairs WW-u 1.
SH.U.S.ViX.Moscow). PPkkdyAkad.A'awkS.S.S.M.
37, 40-6(111,47); Citm. Zesir. (Rum4itu 7one Vd.) 1%6.
U. M-9; C4. CA. 43, 501le.-A satuir wa- made of the
tnechantim of the reaclionti of afouutw compl, repre-
w,n1rd by the formulas PhXY, D-VC411,1XII. 41A p.
YWI.Xii. In which X - Oreltilland V - Off.,%(h, Me,
f 50sit. orally]. For this purpotc. the special rate in
which
X - 0 and Y - It was Invntizated. S4urr thiii would
make the 3 farmul" identical. the Investigations wrtel
"oried out with be-Avy phenols. Phenol with a known
content of 0 in the OR group and In the nucleus was
prcpd , from ordinary phenol by trteatusent with heavy
water in the cold and in the absence of catalysts. Bythik
treatment, D displaces the H of the Oil rapidly W1 enter%
the nucleus akwly. Wbru the phenol sopr;e66u hCAled
in a closed tube at 2001 the reaction V - o- or
p~DC*HjOHwwabwrved. Equil.wazestablisbedintess
tima 50 Jars. with the Dequally distributed in the OR
group.
the ortho, and thepara position. No exchange occurred in
-themetaposition. In order todet. whether the migration-
al the 1) occurs within the unit mol. or involves 2 inoli..
MOD and anisole were heated In a closed tube. at 20V.
hfigratiou of (be 1) tim both the pheuol and the auitiole
nuclei occurred. The saw result was obwsvW with
pheactak. At fWst migration of the D from MOD into
the phenol nucleus was more rapid than migration into the
anisole nucleus. The cossclusiam of In". Raisin. and
Wilion (cf. C.A. 31. 6661) served to explain the meCh_L
anism or this reaction. M%ca anisok was heated with
J.S44kakn*hnsd at 200' for 20-100 hrs., no D wa.,
tran4erred. to the anisole. M. G. Moore

Author: Brodaki:6 Aleksandr, Illich
title: The rwthod ae'using rarked atoms fok choinjogI A atenogr*hIc
record -if a public lecture delivered in Moscow. (140tod mechenykh.
atomov v khimii.) 29 p.
War: ;403eow
Vubi.ishers
Pra*qda
Date: 1948
Availablei Library of Congress
Sources Y*nthly List of 'Hussi4n Accessions, v. 3, im. 8, page 522

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1k4d. Nank N.S.S. R.. OkIll. Khim. N`a`l'#M�, 3-12.-. rtchansvil
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114 ~ III
laolunKril lleillog Willi 11,0 Lit I-.0' vvvii lit the I'TrWlkV
FILChallte 10,A) ao~j I '-%P; .)Ill. ,I 1111,CC1,11-
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alkali, IX5-CIl,Nfrj does cwhange 11 in tile \It group Ability
of tile o- And t-11 atollis ill I'll.c. (21 Thv o1j.
f "if ITC-Atil(K Willi CJ),111)(otheexteut of IYV of Ilse
equil.. ~,tvitiotl that in ifir l1rcliamoll m4mmat,111"It
')#.,C:,;
, ;4 It
!it A) lim tit INI"; till% vxchaugr vNidrotly ImAct-rd. fly
Mill fit thr larm-n- .4 PCI. mil 1101 l-i ich, I It
Willbiliou of tile Me group. calal.vyed by the C,I),O-
AlIthrOolthe NOll gi.nipi-i Ach.tug,d (tit =lgo
ion, '11M lolloWills 41ALI refer to tile temp. of 17.11". I'lle
ilitt,tillol. lov0ml,ii,k, mi'l I, e~.llm,lvllf "ith tile
stiftlitt.
DiO attaim 30% rt ill. (C.A. 8, 37-S.',; 16. :M'_N'0, "lilt
ti,chatige Ill-tWeen p-N(1iC.II,Me And
13 of the equil. in (I% firs. in alk. soln.. but does not take
I'll Cos
W I-L-ter lit Acid Aoln.; lit the cse of 121.4-OXIDJAIIAle.
tile th,- intermediate mage fi-rululated -4, C _. N Cl
%auir drKree tit rXChAn&r 1% attaiu~l fit the samle time fit
[I'll> ~;q 0
neutral Volu., and riLics to fill% lit alk, soln. Hitt
atolm arv not uxeli-inged. Ill the 3 isomeric NII,Cti III
the 2 11 atonly of the Nil, group arrexchanged mrY ruPidlY
exchaugr it( ring It ill PhMv vulud- .-Sly iti'vIts- IS
fur D; in alk. %oln. exchange goo no farther but in and nisin
tu I oil a tautoolerivitioll CIII < .~ Cit.: