SCIENTIFIC ABSTRACT LURYE, YU.YU. - LURYE, YU.YU.
Document Type:
Collection:
Document Number (FOIA) /ESDN (CREST):
CIA-RDP86-00513R001030920006-0
Release Decision:
RIF
Original Classification:
S
Document Page Count:
100
Document Creation Date:
November 2, 2016
Document Release Date:
March 13, 2001
Sequence Number:
6
Case Number:
Publication Date:
December 31, 1967
Content Type:
SCIENTIFIC ABSTRACT
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CIA-RDP86-00513R001030920006-0.pdf | 4.21 MB |
Body:
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f C. A. 26. 42#3) giv" inconsistent results, depending on
themint. of CU impurifictiand the conditions o(operatiori,
4z
R"tills accurate to OJO)l It. Za for 0.102 g. Zu in V) If.
00 3 Cd are obtained by pptg. of flit- availatile Of
with metallic At and defg. Zn in the filtrate. Diualve 110
411100 9. Cd in 120 cc. of 2.511 ItCl with 2 adrins. of 2-3 cc. of
00 3 coned. TIN01. Introduce into the solo. 4, 1 and I x.
At sits vings at intervals of 111 -20 imin. Filter tfirouxh cot-
*0 Itin and wash the AJ-Cd with 2r; 110. MI. Zn in the
so R 1111fale as Z110 toy flit, J1,.S or anv tither intthtid. C. If.
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copper In metallic nickel. VII. vc,
1,111'r and St. I. I'ttwitsksya. Zaroirkap, Loib. 0 -.IV; *r
(IM7, 1; cf. C. A. 31, Ol". -- I'lie meth,xi )I j~trrnal
di~etr,,Ilyrii, i. u-wd fin wPa. C,- Irms, Ni %ith the aid ,f a
14, lif-alt, Full details are given fin vitityinig nut the Inti-
-titur anti the rvsift* in detig. w(KA; 11.24% Cu were ext-t-l-
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00 cQuirstel and their products. %'it. moll I.. it. i-00
Ginsburg. Arodikap bill, 6, !.141 Vjilr..).. it) livat !-00
64 A-1.0 g. 0( "Hipli. Willi fit nit. of coned. UCI and with i
00 5 MI. ul Imird. 11NO.. Dif. tile lf-~Ulfinx X411. will) .10 -00
list of water &nil 3 fill. MI. Nil. fiber and allow to cool,
itipo 4 ro'llic cold A411. &d.1 11 N 1.0 a. till IAl I,- avid. a 'fight vuv-
4 N11.011 and S fill. of A,:Oll. till. to limo od And I-pt
00 4
PbCf(h with III nil. of .*)4;'v KvCtM. Fill" Mail waA Ill
94 9 PI)Crill, With dil. Ac4)II. Di%,olve the pill. in a ruht. of
00 1 X. Nat'l. NMCI fulln., 14 fill. water stiff Ifil) nd. of contd.
IlCI, Pit, life fillistr *nil dri. life Cr iodomelticaily.
00 -3 i t2) Tu the %oln, pirlkl. a% In (1) add a Alight vu-mol NIll
And di%N0IVt! 411Y Pill. Of FV(011)j fly Adding Ill till. 1113 N
[f%'Lh. Dil. to 2W ml. and lipt. PbCro. by invans c4 -;zoo
0 11) nil. of (1101#):CrOs. Filter, wasit &nil dj&-~Jfe as in
it). To ihi-tsoln. add water to make2fl!) fill., add 2 fill. ~o 0
00 Tiltatetlic
0 0 v exerm Ve Willi Standard K.Crt(h skills. Willi diplu-110
ainine Its internal itifficitor. (:It I)ix.,Ivc lite sumple 1A
00 z
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if ) t with the onfission of tile rinal 11C1 treatment.
zoo
4 Pitt. the 111) as Micro. by Illeans 1)( 14 111mlialicd Vol. o(
IlA N K,Ct,Ot, filter slid take an Aliquot pull of file fit. 1,00
I! ji if ate for lite drin. I)( the cxrmt K,Cr,( h, fitti.hing the ansly - so*
4is as In (2). Chas. Plarw
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Z! Detenal"flais of small minouts of cobalt to of". cola-
costrat" aad Wisp. %'u..Yu-,Luv.%t-&nd It. St. Tat. .00
7,RW,bdy$ Lab. 8, 3K"4 109).- A mrpatativv study of -60
vaskm wetholits indicates that the nitrite Inctilod frilloutood
by grzovinurtric dtin jim hilther rrsulto suit ratinat I*
rate method I* the nitrite promitur
";,;Inb )rJuietric deln. The nIvIllod In. howrvri, -00
long. The method of prellininary wpn. -4 Ni anti C-- .00
xj! 1byttergrolysistorithout A"C"Itsidecuffent istiotastorcursor '00
so but it is satisfactory for routine aludY414. Direct Moot-
00 Metric test may alvit results miffk*ntly sovisrate for 09
0; ordinary needs but It requires the adda. of entough pyto.
*0 pho4phate to bind the Fe as NaFePA. This, i4 the son-
plest and mven rapid method. In rAse the ratio of Fe/Co a**
is 4(M or more the nitrite-colorinictric triethod is recom.
nieudrd. It, Z. "nich
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8b
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clinnot bound Miod..torujina.
tion of Mb by the Blum#nthid method Imd, Ab,. (j. 10W. Md4b), 19-2m, 40
0 & .
513 1) gives good results if the imisioquout precipitaicin of Bb Is carried out on
0
1 Cu foil and Da with 11.4. "Is best mettiod for determining small amounts
-
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b
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-
I litrv of the 1.1mrol best to W-03' C
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Add N 0
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to
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ve all do Sti and deters
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(irimetricaliv.
1
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the cloctrolvols prorvmla slowly eind In determining Ali
In metallic Zn Is Is mvvItastry III mitt I ing. As (as P41t) Ill-fivre the rhwtn-l)~im.
S ~ 96
90
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C Detitentination of lead In mounts IICI and 60 nil. wairt and lival 10 I"dilIll- CQW to FIx"ll
Zapod. troll).. 41141 111 :!11 sill. of Y" cittic or tartaric arid and
of Wax. %'I6. Yu. Lur,C .00
skayu lAb. 9. 1U.' 7(19440.- In delit. Ph in the presence of ricuttakee will# Nil, to laimlj*- Add -*, Ful. eviol-d- IJOAc
large amt. I Ila the tivistultilt with Illso, followed Ivy bqpt to Willing. add Ps ml. (If III)% KrCft(h. Im'd for noi
0 a u*r5mW.antIfilIvtandw4,h- thtfli't-in the
eviralin. to ~411r" 6 not perini-ible. In anallylins sulfide
:0 ories the cvaim. to dryness with ordy IINO, or filter, dill, to 150 nit.. alit[ 1 1.5 KI &lilt liltAtc will'
I I ot lie tarried out because lltR)4 Is squaresla ti~ktwulfate. Ili the electrolytic triethtd. di-Itivc 11.5 it.
tH n It , formed. In
both the IWW. is devitroyrd and ratc or of tire in 15 mi. IIN(h. a4hi III mi III goo
00 Mst. lattice of ut,
04 4 wime of the Ila loris to into ia)in. 01 subkvcltt dila. "I'll, 114"J"ll. of Ju(NOOt rorr-ix,riditis to I x. Cit and
j with water the &tar costabi ate spin covered with layrn clectrulirw with ItWirr clivircitic*. In the raw 14 otillised
of H&W4 with the tcsultant Occlusion of PID, which camult otes arid (Quills, treat 2 K. and.1, N'. tetil.. fir-t with It) nil,
00 a he extd. by liolvvrots. Accordingly, two mediods of detS. IICI and thcn with 10 mi. IINOs, eval). GIS list.. add 2 K.
Mita-mbirrisdevrioswil. Inthrehlorlde-chromaternethod %H.N0,jLndevap.todrynm. Tothedrytirsulucadd.5
diwilivir 0.3 it. of the concentrate (2 jr. of ore at 6 S. of till. IINOlt evap. to drytims, add 3 nil. LO mL bot
0 1 fallings) in 10:-4) sill. JiCl. hear for 15) inin.. add 5 nil. itrat". Ilod A min.. dil. with hot water to 1114) mi.. add ncts-
*41111 1 IINO, and 3 g. Nat'l. evap. it) dryrims. coul. add .5 nil. trad VWNW). and rIcvtr.jvxe. It. Z. Kmkh ties
coo
All
lir
tre 0
-;L t:0 0
141,01i; -71 14114.1 .0 1111, too
U AV 00 Is
Ant Isado 119111 142',
a nit 001 *11 Wq K(ttt ag 4 1 94
foo ~194 M41
0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 01
Is 0 0 :* 0 0 0 a 0 0 0 0 0 0 0 0 0 0 0 0 0 : 0000
1*0000000000000000001
gal V
A f V V 0 0 4p a 40 41 0 a 0 0 0 0 40 Ole - k7 4b " . ,
11? 0 In E W_W_
r r to 1111ILF-EMIF-17- To 11 a
T
irl.1.1
L Tal. 2ldrodfiop J.;h. 9.
dein. of the equiv, [*,I'll IlY
041, inwtry hag varkxis advantaces over the visual'Ictil. 11,
-
ti
f
I
A
A
ftf
le
A
11W S
A
M
1,rtna"anal-nuctry lb,, pink t
oint 14 reached Incrvaw.-I in intell'itY -ith the 41141".
nd
p
g~ajc in acruirdarice with the Landwrt-liccr
rman
skes it Ixtuible to reduce the titration it) 3
ti
Tj
av
nwa-urrilients of tile tutyrnt 'A tile phollwkr. cell: oric
so at life r(july. 1X1011 APAI 1W.) aflort, it, Tillatioll of Collard
~ 14 Callird Willt ShO W1114' Valle 411111 8-1114,-Y a*vi)tlr -
%s utlnc Avidimetric (lifittiono with a pikilix-lec. cill
1,
were aW) studied. The natute u( the titration corvto
indimtes that theindicattwo Ill ujhr may be divided Into two
W V0111A. Tile fint limp (v. S, plurnolph-halvin) Ila, all
'
,
10
* 11telit-t"Ill gFIA111 a
life advottiagrof tit rwirkninprukurtry.
I
tA. all
forthyl Ifff, Isn"1101111clicil Illur)
r .1,'l
toorat Advallfaseq liver Ilk, vinkil 111VIII44 III 11114101A
2
dko Iv-% .411114. Its 1111111ing Mill'VII MAIM With A 1111411104111dIr-
flurtcr and lk(tulophrflol Illue it io [),.4blo Io lict. a6lily
It "I f4, It, .111(All, "I Ni atlJ c". file wi.filv .I ch-vilmlyll,
Will, 'I'llig l1a.. '111'. Wild fill, mufilv 'd m.- .11,0,
I L A 411AIL(UNISKAI. J11,111ttilf ... IS'NWAtkial
u a A, is,
#1 09
0 set* 0 so o so,
0000 0 a so 0 so,
M
u
0
-so
-00
-00
-00
r
.90
nor
Its
-A
go
4
13
*0
f
J, - - '
11
6 4'
Is I
I I
Dlits"Wasdoo Olf Isfid"Iss and scrattlifil in W wage
WOVI'll fit 911141190110410i'll N'll I'll I HF'v -4611-4 14t-
III, fit '011111 1 1 ~111 W. Ill 04-il, *4111 4,14 A
fill. of It'luellp Unit IiIIJ, 44 Ijulft-t w4n. 0 1. 111 IWAn smi
Ahet radi ilif-In-
44 [tic bufIrt %Ali. %lLike thtwoulthly. Allim tile IjquuI* Ill
ilep.. tli%mtIl in-1 It( tile WW" IJY". 41111 TT411-fef tile I-I
N*c-l,r yinuirr. Add 'dl ull. I( tile bulhir .4u. 1,,
another INC-ler CY111111cf. slid :1 nil. of tolintic, and tormic
drupwise with a standard zanthate"n. (I ml. - "A MK-
of xanthate) and Julke th(proughly Rfirr each arldn. of tile
reagent until the color of tile ttguene Wyers in [with cyl-
inders is the "me. The 4cusitivily of lilt rinfliml k re-
illiml fly utiliff pho4pliale buffet IV 10 Af lartaric acid fix
deconalwising flit zanthate. Arrofloat Ill
ROPO(S.SWO L* detd. similarly. The deconspia. of the
aer"floal Wn. mramipli.heIl fly melicAtevinte bulTur still
fee a buffer Illixt. -If K;fIPO.- It I. III
dri. OAN15 ills, .4 IlAnthal" m Awroll"at ill tit, "Inple.
If. Z. KA111i"ll
ftl~_A
u Ill At 03 It
44 0 0 46006 000_00_0
If
ivi E"'f ill too
fill 0 it I I ill a 9 a a 1-i 9
0*0000000000040000
0 000-00 0 0 0 e 0 * 6 0 0 0 0 0 Z~
;~;~ *.O.fp
* 4 0
W a is ! ! a a ill
J. I I I, . . . I-
110 0
-0*
see
b
boo
0o
051A5 1
0* 1
*0 &I
00 11
so
SO it
00 4z
0
v
00
S
a a It a A lot 9. is
1 st 11 U ALL"t J
. -
PWIS1111 ..0 retAt"'Ut LIP
Deternalcustion of thlocyamtes In waim waten ow owr
d9grits Solations. Yu. Vu. 1jeLrv
_Cj;~J,Zavvhkdyg; Lak. if.
-'ri-80945).-Th had e (or Om deta. of
"I = rawast'l wNters and
svtAba.U. pittituittary septi. of CNS-
and Ca- by AsNO., purifimition of the
together with C1
rcsidue Frout impuritim of arc. subtItsam. decamps. of
'Ax salts. and colorimetric deta. of CNS- In the furnt of
~hc complex "It with Cuznd Pyridine. The method is
Tcry amwate. Add scm drops of Ic'e' N&CI 90a. &W
tlanobb s) igloo* %it GMv 449
-1
U 9 &W 00 U It
Se.SLA MAKULLIAGIC11,16 LIT2111ATtAtt CLASSIVOCALIM
M union *Ujip*ilooo 4
~R_JL_
C-g~$41
III I.') nil. of I N Ag.No~, to 5W ml. at the sample, filter
after 4 firs., wash the ppt. on the filter ouccrssivvly with
small Portions of water, sk., toluene, &k.. and at",
transfer the ppt. and filter to a 100-m]. flask, add 20 nil. a
water utd. with 14S, let static! on a boiling water hath (,,r
30 mlu- with cOnst- mixing, filter off the A&S. wa-.b it
with water. and evap. the filtrzte tu,',I() ml. T,,L,,%(,-t
the win- to an Eggettit test tubr, add 3 mt. of 67,.Njf,.N0,,
0.4-1-of yridikov, 0.5 tnI. of 10~~ CUS04, and 3 mt, of
ClICI., and ah. e vigorously. Add B-lo mt. of pure
water and the same quantities of all the reagmts used (,,r
the sample to a shuilAr test tube and tittlite with a stud.
ard XCINS soln. until the CQUXS of the ClIcIl layers
matels. W. R. liens
9-9,7
an I I 'M 0 1 Mr at 5 a a
I %A
.00
ago
190
0
400
g
0
too
100
4111111111
so*
41
Joe
400
ISO
too
too
tie a
ZI Me 14 1:1 be j 111
Is -w-m i 11 .11 - I'-- , -~
j.t- L -L -A - a. 0, 4_ 0. ..
A-A-A-
&"Estes
Egli -4 p1!
DiEttiffellnottiOn Of N-. A --I~-
A Willi*
I's of '41111'
I.1111 til.
is it till
loemilklit 1, Ill" I,,,- o.vrf "Llil.
00
"toli'llic till,
I.V
400 -06
t .11
clict, lulw to", 0 1 -00
96 a "11111111 alld es,julot-"
lite W13110" I'llo MAIL
111 lot I lie t
00 if IL -
t1lit I ,III ~31AV!lv
thrilmilrollose'll, 11-00
t 1. -At- to fell, (If tile 1,111h
jilt- Ill 111111'r, tiralls I Allot fill th"
11111,01 1" of wilit
00 till, dtl. ,, till-All"
low
to A'I'miAl.,
a
All
00
00 Allot of the,. Alld ,e
;J7 till. I.-Ild I loses "I
III SIC- All' - ,"j,01 Ile
e", p-lold. 11 -Ill
..... Ile 100-1 ,, the .4,111 0
,4,ioml ill 11" it
"phit'l .,1,% 00
A lite 11001 slit. ~11,
I., tile tit,, III It
to I . I (I)f tile
'11111"tcl Vy is I tit
he 4. walrt
11, I)IMillt's, Opffli live 0
wool "What I(Ywrt I"" lott'ji'llivol mItIv '"olliev
ate 1J.'t
it, till' 111'e, 1, .1
the It'll'taltv loll.1.10" E%t
a W-k C... 0 0
0, moo
di I CLAIIOPICATIO.
"I CTALLURGKIL L17141"'99
-A
1;04, SIVI#p,V-
CK ~Aa 111 1 !IE1
Wit 099 Kate
u AT 90 Is to P It of 00 0 0 0 0
too 'q
11 U 11 0 b 11 1
A S J A m ft-M-W JIL j A-1-1-1 1,
90
=Jaks &A4 cow-
It medwilssin
11. AM 1MVIAs' of c f Al. I0 fl~ ain't..
.film tlllml~fl
Call P,"Ist tithtf bY tilt API�tWAIkV tOl fill like %IIMIIIWA.
IMKV A 1111111kitlY Mail- Ill 4 litrAti't 46'11141~V 1114R it. 14--
41
'wi*"lly. T1W isic'mar In lilt lulbillity *lilt tilt
f titt
tial (w th
, I
Wil
t
t
4 ti
1161it
d
J
"
o
a
e
et
rav 4
lt
"1
y
lip
4
11
1
4
l
1k
1
1
L
i
l
h
1
it fth
6
"t 40
,4114
W11,
ret
1%11"1
l
I
ItA
)OPYS O
IM, 1
l
st"t I... 14t 11,011 the 4qlliv. pporst am If# 'mh
11ir rquiv. Im4tit eau I~ 'let'l. 11121.1mally .61 #Ike
00 tutcc.~ftkgs .4 j trAtglll Ollie. 1114wit 1111,41ills J I-clic.
'1 h
4
1
i
d
t too
. U_ '
eut 1. ..
lt ri'
"
1111416~"s
l
(Itill)(UllifftfidiffK-OriC tiltat*M) (J`Al0GK1t1% Ill,- %'0116PAIA-
zo
irm-mraft meth-A of DruiS& atid I'Askes mto all :
iviviall, nitshi"I suitable 1w IWOVi.- AllAtylics. The
i
tswth-ki was uwd to det. chWides by tilliditill %Itfl
-
with AlON0,
lix(N(h)j its acid mAn.. f4w fillation id CN
.
C.A. JOS. 4NMI). wid bw flor drill, of ell
(Ammiding to pasims). W. R. 11cust 9
id
gee
v
I o4T ALLI 44GKAL 1.11 111141411111CWIVICS1100
u a Lik ID Ls s 8 fw a a I vr IN a dj
alvill, wags plan Illamoll 1116 4 4AM
mw
0 n
)000000 * 0 0 0 * 0 0
0
WWW
WII"
0
# WWWWWWWWW IF 111111 0 W a W W
0 0 0 0 a ol 0 0 ; ; ; We
It to is 16 W V W Wf"L
d'Go
004
00 -00
.00
god AVtioa of the phatocolodmeter In volumaftk &easy 4 lee
*of SIB. . Titration to msxbu= tarbidity. -00
_~.Ua.aud H. N1. Tal. ZaWytaya lAb. 11, 71118-1m1
01145), cf. C-A - 40. 24MI.-NA, hen a pliolocolorittitter is .00
u-I in cletnts. of the end point of titration of Ph with age$
00.3 Nli.)t%[oO. by max. turbidity, the max. may appear
!
Itht.r I;eforr or after the equiv. point. A coincidenct of
max. turbidily with thr equir. ImAnt con Iw ributined by
ki
i
l
d
e in
tnt
r
la
ng A unip
r
, III lip IM-111. r111141 10.11.11~
In 411P III inAlip for t4juirld of 11
, 00
:
A.0 lilt. Vistler Ilifte C"11,111111ill It
it 11
CI I fulloarvarale 0 0
and Iv applicabir for large-f-cale atutly%1% of ort% and of
004 thrir cnrichivirnt products. Mototurbittimetric tictn. of Cloo
Zn by K.Pc(CN 4 rtquires no addig. at stabilizer to the 0 0
"n. Owing to the slostmem of the reaction in the col-I.
the method con he used only if the titrated Wig. can be 0 0
brated (luring the tilralion. W. R. Ilenn
-S
goo
goo
woo
41?ALtUnKAt Lfftl&ti*l CLAIWCATION 0 0
woo
claw 11"4111116 ago., 410.00 tie 0
A 140101111) .&P GMT all
0 U In A, 00 as
t It 0 4 0 a if 9 1111 a Aft I t a no 0 0 a I III N 2 a a 3 a
it 414 A I KA
t
1 1 1
4 00 0000000000000000000000000*00004000001
4
- - - -
0 0 4 a e 0 0 0 0 4 0 0 0 ei 0 0 0 0 *
* 0 0-0 0 0 a 0 0 0 0 * 0 a 0 0 0 0 0
12 It 11 It t? Is n it' a' a At a311 V ail 12 v N
owe'1*110t -1.
MMaNMOK OF WALL OONUMUTIOXS OF MMM. AXAMS
2090.
OF FUD VATZR FOR RMIN #IBM DOWWA. LUr-'0#,TL-aAd NUMIGG'm
ibetr.p 191
Z.T. (ZSVW$kap lab. p 1946# a# 161-70i Aj,
*0 b.: A colorliestric method for v=7 snall coneentrations of Cl- Is based
*0 St,;~~ on the suppression of Cl- in the reactions between ft** and d1phany1o,
as, xlt earbasIde. The colows obtained *bed the lambert-beer law w1thift the
Halte of concentrations studied. The determination can be
**,3~ ; :
either by th* coloar seals method or by the equilibrium nothod. The
0 0 .3; oolotw is 6teblo for $-)0 aft. and to not affected by walI ocneentra-
Sov f a that my be present in the water. The ivolutlon abotild
tious a
so v be pre"042 lly aftutrallsed If tb-9 content of a exceeds 12 mg.Ae
a io tive. Tbg ulnt~34steot&bje omega-
Ah* method Is aeomge and sawd
tratlon of al- to 0,025 ng./I* go colourm were obtaln9d In strongly
sold solutions. Best results were obtained at yK 4, Ohs contmt of
up to 0.5 mg* of F* per I# does not interfere with the deteralastles,
.11 Aiwtber oolorlastrio method studied for the doteralastion vr Cloo is
based an the reaction WrOj, 2 Cl- Ov04-. be Cr%7
-A 1 41 1 It. A al, AWOROKAL LITERATURE CLAW06C ATOGN
t 90404111 -tit Q"V got LW 0.. 114
U is AV 00 is 1; -1-# . . , r 4 W I-# -R,
a
Ct Ly it W A a A 19 9 W
0 0
Is 0 0 0 0 9 0 0 0 Is 41
-*4
-00
10 S,
-00
-400
00 6
=00
As*
-coo
see
000
-0 41001
-040
see
too
.46
0 :
00000000000000000000000*00 0
0
00
0
roawd in the solutlon can bo dotendmod eolow6istrioally. The Crq47 :
0
#0 diphoWlearbasiMe mothod Is as accurato as the sethad ~-lth Ndp" 00
04 but Is wro embersomso 00
10* 00
40 00
!so 00
00
00
00 0*
g
:l
o
00
0* 00
00 of,
00 00
00 90
00 00
00 00
00 *0
010 00
00 0*
*0 00
hL*&*-000000*0*ooooooo00000000000*000000000*0*00 40
Ms-t-o*OOOOOOOOOOOOOO00000000000000*0000000
It -1i i i
A --- I-L -I.- M.A. 9;-A.U-4~A-A -t
A
so Al
&Y Orgiudc esch-- 9 m4sm Tbak me; in
Lur*e
ZmWjkdya Lab.
a"AW ch*mlWy
Va
Yp
00 .
.
.
...
-JS
'3M
-13ttags mv
IS
b32--9(1947)
cf
iven
C
A
0 .
.
.
~
;
,
;
g
f
ll
4h
f
i
l
ti
it
b
W
w
or
su
aremirc
ao
ca
on
e prem. o
to S
m
*P
00 was usbi as * culkmite mind wAs found to
=1=113
b
f Wt f
h
M
a rom t
a#nt watm
y wt. o
e *
%
of a Pb dnmWng pLant. -h
11. Z. XAMiL
:41
410
00
CCAMP&C ATION
L
491003 oit aw v4( vj$ir
;i -r-T Y -6"
is M3
0 Lt 0 0 0 It OF 44 1 a it ;WA
ali10C a.. Lt,
71
S4 AM I 1 0 rw 0 4 4 1 w Is 5 a a I v
9660640*66900040000
-00
so
'00
.00
00
-so
'so
.00
900
"0e
*0
.700
so
100
goo
0
0 0 0 0 0 0
9 j , IT
ill of f 111 f ffifflil. 11
A r -1 It -1- ON W U. _W LT 6 A 1- 1, i_ B_ 4 j it -1 A 0 _A_1_
0041
eil A I!; use 01-0-Cpa4ul
Yu. Lur I N, A, MIOWWA. Z,;=,; Lbl-U-
MW47t14Ar-Fxp1*,
st"
show IhA a dil
of m
CO:
00 .
.
,
l
d
b
kW b
f
"I
b
00 an
Cu ma
ts can
e cnr
y tuems o
ra
tts
y
'about 40 titnes or umm. The io" of metal in the total
cycle of abiwints AM ftig"Mation awounts to 1-2"'.
It h prvisible to uqe catiostit" for quAnt. Repo. of dimpho-
ittis- raef4is frora Anims 4rvi nitrissinphOrrk catkins by
01 a"whirig theta with rationite and then fttg. with allkall
%atill. In thi's minner it 6 possible to iwp. Sit, Mo. W.
00.9 Zu, and Al from all the ekarienti whkb fom bask by-
h
h
ich temAlms wit
the
dmakles (Fe. Cv) sisr! (mas As w
0 This ifiethas] hu the ad-
1,11111tap when campand with the um of stka hydroside
for the Repa. bftwm it eiiinintes c"pla. and sn.,kes
possible a qtjxnt. salm of thir amphoteriv mrfatA.
4111-
It Z, Kamis-h
411
NAAA
------ - -
Asst.* SITALLMICAL WISFAUM CLASSIFICATION 9
1.10 -d Islas, .10 04, 0.4 ills 51-5._~F- *14411 ag GNP All
U
41 ,bit :::n4ite m an it Nan T!Tr
01-0 -0 0 0 0 0 0 0 0 0 61 0
0 0 0.0 0 0 0 0 0 0 0 0 0 0 : : : 0 0 6 0 0 0 0
*Jae
_,
TI-00
N,
00
00
00
100
ve 0
ago
t!9 0
too
. M
NONN 9-: 0 0.0 :17r;Tz~"
0 000
4l tit A yet 0,111111unk trio"
g
010 A
ogs
*0 A
Ir
o
00
:*0
sew
sew
Z
A.G -Acpllv.t~
u a Ad IN Al 0 2
-A
tree of Wv&mlj%:-4 Im titif maylls of mto. Yo-yo.
Lar,,t and S. N. Steknovick. Zffadsbeys Lab. 13. 8W-3
1=116= ); d. C. A. 42, 448U---Ca,,v.7=
,k AWnste Ca and Mg in
lewtr wattr, Ead. Ca and Mg are f by a"m
LOWIlLesta. 190
dw Altrate with 0, FN"94201
(methyl Omage bm~mtc~k- Gemv A. LAwidn
a is 4141 N-4-6 W
A-A.-Ask-
-;p 0
~ee
ILA AITALLUNGK&L LOYFRATUME CLASSIMATMON
J
.1113113.9 alkill CA out tit
=4-0-
U 95 AV X:' 43 V ZA 1A I I a rw 0
;g Of t7 It If (v 49 K a x 91 it ty el It
OT"Some *goo!* 0 0 00 0 0 0 0 0 0 * 0 0 0 040,4e, q!oo o o e so o 0 0 *0 sees so*
*000 *Cs 00000010009*0 0000 Gooo* 0000*00
goo
coo
c:4 a
too*
Fie 0
lw*ol
BABKO. Anatoliy Kirillovich; PYATNITSKIY, Igor' Vladimirovich; ALIKARIN, I.P.,
reclaktor; DYMOY, A.M., professor, reciaktor; LUR1YH.-M&Ajq-... professo ,
JAM I
redaktor; FILIPPOYA, N.A., redaktor; Whal I S.. tekhnicheskiy
redalctor
[Quantitative analysis] Kolichestvannyi analiz. Moskva, Gos. naqc1tao-
tekha. izd-vo khim. lit-ry, 1956. 736 p. (HIMA 9:11)
1. Chlea-korrespondent AN SSSR (for Alimarin)
(Chemistry, Analytical-quantitative)
LUR I YE 9 YU. x YU Prq~.
USSR/Chadstry - Awaysis
Chemistry - History
PAW 1947
asoviet Analytical Chemistry for Thirty Years rof %j Ai Klyachko, FTef 1-1. L. Capele-
vetddy, Prof &U# rw Lurlyep 91 pp
*Uvodakaya Laboratorlyaw Vol X1119 Do 12
Analytical chemistry developed foom the science of applied chemistry Ww served will In
the development of the indu tries and agriculture of Via Soviet Union.6 Article presents
general,jacts concerning the development of national econmy and analytical'ahemstry
In the SZiiet Unlong, and names saw of the people most responsible for the remarkable
development during the Soviet regime,, Last part of the article consists of a general
discussion of the futuro of Soviet analytical ChemIstry with respect to further indus-
trial achieveaents* Greater development of now fields such as nolecular physics, elec-
trcn opticag radio chandstry, geocIi=jsU7p etcpq J~- fecommuWa
PA 36710
01W V V 9 1
;;;;j;;OwwqqO9'**OOe
1 : 1 9 1 d I # 6 1 4
A's.jL-A M -I-A-.L - A-
04? A
4-
A
oil
0*
0
e
00 me V~ i
00
of
oil a k;
ti.
4"F_w_w_1(w
A Now Vark" of OW CYMSIC Uedwd of t1w DOW-
maywka=,L (in RMIM) L B. Gwburt
and U. U. Lus ' zovodskuva Woratoliva (Fac-
m -545.
tory LaboratdFy v. 13, July 1948, V. SU
Discusaft a new variation of the cyanic metliod
of phatocolorimetric determination of molybde-
num, with applications as a reducing agent for
potassium Iodide- This dam not differ from the
old method in application to stannous chloride, in
respect to degree of sensitivity and ran e
colorimetry. but does differ In having a r
period of coloration and in degree of stability.
AIM-SLA OCYALLURCKAL UTFRATUR2 CLASSWICATION
lee
lee
see
Zoe
goo
go*
got
too
too
U AW;10 As
4 4 ; ; is I't tc ILI-FA a 3.6 1
*1*; 0 0 0 0 0 0 0 0 4 0 0 0 0 0 0 'S 0 49 0 6 0 0 0 0 a 0 0 0 0 0 0
0 :1: 0 0 0 0 0*0 0 0 0 0 0 0 0_0 0 e 41 0 0 0 0 0 0 * a 0 0 0 0 0 a
LURIYE, Ya. Yu
PA 3/49T21
UM/ChemisU7 -,CyAnideso Determination of Aug 48
Chemistry Analysis
'Teternination of Small Concentrations of Cyanides
In the Presenee of hibibiting Substances#" Ya.
.Yu. Lurlye, Z. V. Nikolayeva, Inet Vodgeo, pp
'Zavod Iab" Vol X:LVj, No
&istIng methods of analysis cannot be applied
,,to determine cyanides in dilute solutions
.containIng slWle and complex cyanideep thio
cyanides, sulfides, organic conpounds, ate.
Authors describe their cnin method.
01*-:NNN:::4111*111110111101111 -'a . I"- - , k 4. - %. -A'.
t 1 4 1 11 1 7 It 11111044 fill,
liMSTIP-11-Sau W-0 I,_v is"
I J
.ptmt--,-.
015"#$I1$ Also I'llef-for'll -.09
As
is wt4lytk,4 tAirmi
00 A Vu. I N. A. Fill~mlvia ifilli'le lost- -Ndn-I'mt-
-114 "R.). 14o; shira, 1.4, 14, IfW71)(INJI);
re Sol-
s
0: armspla. wrle rim-
clutford with phrocalic "tilittile Widmit 11). The hallow-
Wit me x. mm t* mlialle t (I ~ Zn %,%I At (total Pas Ity
wkvik%v e%tn, Willi NAUIl film tho Nlf4'-ftatld. anAll-mille.
12) Mi ati.1 Pki I"mil As Ity pa"ing thIrvilu. limpulth It'- -00
001.1, 14III-ills, 1.) itivemb q4 0114 %% .4111 &tilt Moral 002,
"Oh d& 110 W) Ito liml 01 to 1% tilt 1&4-A1%4 11%
wsha, th""Ish k VASIMIllis I'S #411-41) lo..111 that)
00 eaq. lit with I q K I mAtt. 144611fivol with flaM), I's give
0. 1 X cimmi.) viat-I tfrtg. ruhmirlottirkally. (4) lit froon Wit
as thialcyatittles by mOmill it( ej(iAxkht laroville4l tilt thiij;l
VYAIIAtf MIMI. Is VIL.WtIV 11"v; it Bill Ill lot 140 IVIIIAIII It
'iflifirdill Allil, 14 rjl 11 111161WAIII0, the
411111, 4#111 410 11191 Ce 0
0 1111 j "Ifirlt. $11(millf lor it have 11,411 .14114 Ito to- $4141. 01111 :1 0
0 Mile fit I, partmisottale, (tit omen. shoulif lit- hatlow fllv'~
Anion-raichmille elptit. weft Cosailucttit with austatithur
0 its late, Ill Atilt torlIll, N 0,- 1'% frifilml to 11,110
C-111 ISO VXtIl- "%Ill NA(Ill .11.1 a
I Insolvil inlav the filtrat is iieutral tior Alk. IKIIII. litivo, lit thV .4
M I, '11W.1cl,mily it ... 0-1 "Iltv lit ml -trld t,1111
h folUtINI Ill 11,111f), Whis'll J111I.I. IN) file Allklifile Aftilill,
(folll WhICII if 0,411 Ile CX(,I, 'With it,*).. Cf0,-1t%ALmmtj4.d Ill All .641111t .... I.tv-d ..hl. -ally V"'. 1. f1w k"'1
by CLFIJUnitC (MIS a MAII. U fill 1-12 Mika CAn be extil. With "A" 11 1 ill, 1,11, 2', N~o Ill -N I's flat- pyr.-
Pro!
2,-o Na0l I itolit. To Step. CrO4 lit "ni. Ili Oil" -4 01.11tv acid. :i'l 1-11-mrijOr'l it'All IICI -Ill" tbctc
-I firtsurt Ni
which Ni;Cr Islas hish Isimm the itintsioniocal alotil rl" -1,11. 'it 'S" films' all ~~ ell'I'liti(MIS 11CCA1111'
IStairs limmigh 1110. 111i0illir, Will 4 11fl.11) 14 IVV[hytlllli N. ill mle v%f"It, 1*,I ~J, lit (f", CIS all
A'v twl'arr the 210 Atill Jail fillf,iliml Iss, anialue assay Co V4111CI& CIS: lit a, .%, 111001 t, im1ple all
Cr,'- "ll-I Ott. Calls 'Willi N.14114 III flat lairsvilce Ili I N11011 to,limtav,all Cis
Q!~ 4 paime tit IllimrallAir Ili I% %mi-JAC('Wily Lb*XW Wall It voillplet. pA.. 01migh 4111~,Jjllv, I'Al. III from Am."Mr Willi
~Wift Arvi untlaitiorlwal VA". ; the AIWxkjL,mW v acI.
all 10 1 L A41ALLUJIGICA1, 1,1710011111 C&ASSIFICA11001 IL V- to 0
to 1 -- - --- - - , , :_ -.'T -
too.
W.4% VIL,J) ISIS a., I%.
L__~ IQ
U Is AT LI
9 to it to a of a at IS; a n Ct a it Sol J?AD A' is. Mr me a a ova:
0 0 0 0 0 6 0 0 0 0 0 0 0 0 * 4111, 0 0 0 0 0 0 0 0 6 0 0 0 0
0 * 00000600000 0 0 4 ~ *1 0000 1111, 0 41111 -2 00 *0 0,
0
-0 a w W-W -0 w w W-W w,-
oil un us Mv assil Q4104;no
0
Now variadon In the thlocyanate determination of
molybilintsca. L, B. Gint-burg and Vu, Yu, 1, ' Z rod
lkaya lAb. 14, of .00
sample In 10-111 nil. of aiju.i rrgi,i. To the w)ln. add III
mi. of 18N 11,9). and evap, to funte-e. Cf,ol. add 23 mi.
01 water, and hoil (,) olkiolvir all ~tilfatvc DiLtolf)(Iml,
; ::o 0
in a voltimettlic 11A.A. mix. anti ki-vaii.0i;Iwit coti(j. WIN'-
mi. of Mik. Tran-I'vir to a gradual,,,I rylindt-r. r* 0
Add in the follo%ing v4pieuve, I11WIIR after Pach mldn.,
35 mi. of 3 N IICI + 3 int. of KCNS iln. + I X, zoo
KI + Unlof freshly prvIKI. 1% NUSO, "III). Dil. 10
'A itil. -,IIt N IICf anti after 10 min, measure the color
at 520-560 mp. Rian a blink un the rragrnts.
G. Af. KowbiwifT go*
Zoo
J NO 0
1--oo
AIA-SLA A(TALLURGICAL LITIOIATUME CLASSIPKATIC11 ::O0
too
410
;00
117 it i -T- r -1 IF I IF 3 1 .71 41 L 1 41 400
;0 11 it x St K t( It C1 K U If It N KLa It 1 %4
0 0 0 0 4111,00 0 0 0 S., e so 00 0 0004 00 0 40 0 00 0 O~
0
TO* 00*0!::: :::: 00 000 00 0 0 00 ooo~oo 0 0 0
Is
sociliti AND
'690,999000000io 10 . - I . ~- i~ . -~ :1 - - -
0*00000000000000000 - ------
4 11 le It it 11 M is 14 V 4 0 It u a ii ha va -16 a 11 32 a M is M V is 0 a a 4
IN
Vt. Mu "I M-1.
0 4F
1
00 V *eCIMI AND FROW11411t .bit
06 A ; j)*ta. of saall conene of cynanides in
go '
U
6
00 110 1. V. NdwIseva. Zataikayt; Lab. 14.
Y'
OR tow cyanide content by PPtK. with
09 a -1. 1kxNOi,. and tmtbis the ppt. with witer and
so disq. into 1% XaOll. and i1ttIC. the CN content of tile
dilt
1l
ith
t
W
l
a
e t
er
i
Innetr"
1y tw,
.04~itrtetricauy with
thcC%'
p4rfivowidsolu
Tattet
irrocitatk%itti
te
00 .
.
I
p
I., expel the JICN by COt awl rillett it lit a receiver
Mit4. it 111CAUS"d Vol. 4110.01 NI twil. filitowril 11V 4.
-
100 he
revelyrr nuitjl. a known vol, I)( otandard N;t,,Vh. I
' colilents L4 the 2 receivers are emillwly Iflitril mid OIC
00
CUM" NAISA Is litrat"i with 0.01 'V I IMArt. Ilftmlt tile
00 4) i diffiretrier between the tOtAl CY311141C XMI the simple Cy.
06 4 attide, the cotitent ig complex cynnide i% known.
, W
00 st
k t f4AUNO .1 1 ~.j At
U S 0 00 LAI L S to nd 0 14
0 111 ita At Itax% n(atent Ica 4 1 :14 4M
0
P000001000000*00000*44000*'Oo*OGOO*OOOOOOOOofe
I ! 2 !
OTIS@ 0 9 0 0 000000000000.0010000-*oooooeooo*oooo
0
1.00
-00
-00
-00
-00
.00
:Go
0
zoo
to 0
40
X0 0
see
to 0
tgo 0
LURIYE) YU. YTJ-
PA
~~USSR/Chemistry Analysis Feb 48
Chenistry Sorption
"Various Methods of Utilizing Chemosorbente for
Analytical Purpbses,." Ya. Yu. turlye., 2 pp
"Zavod Iabu Vol XIT, No 2
Describes own method, in which liquid tn be analyzed
is mixed with sorbent instead of being filtered
through it as In Yao M. Kbotrikin's method. FAItors
ask laboratories to report on their experience with
both methods.
4/49T16
[000900*0*000000000 004
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I
to- "ma
OOC
0 99:
OOK
o ON
4-4-0 : -
3, m 39 &D At 4? 41 U AS, 0- Oly I$ n Cl
1101MIdISM) 11-11,41111
00
0o
- Poe
oen piivlnqwl pug paullp aig w3w(l ul aAoqv -00
C.
**--I 04) JOj 11POInaltu 2uflglxa gaz.(Ivuv A3A!jvjlydwOj
'OC-IZ *d lot6l uvr 191 'A '(AJCrl*J 00
1 00
001 1 pug 10,1-1 nA mA (vel-11 tq) ."lWalixual
00. -aa qsnumm la rpqlan ilipwl"a III u9pallsajul
00
9 0. 00
0
300
00- 00
0o
go
120
fit 14 if if m fj It
00 0 00000 0 0
0 0 1
i
Ve
a a
1
0 0 9 0 * * 0 0 A
9 1: 00 * *
f1lotilliv I? _W
AA I f. A 1. It L.
004 Iiiq COQM
PAGM05, A-S PROW11)
-A
it
Materials in AumlYdeid
to Application of
Ar Chemistry. IV. Determination of Satfar. I'h-Ph--
"s, and Armair in I'lickel and Co P". (In fliumall. j
Yu. Yu. L ud N. A. Filipliova. mv0(bk4ya 1whimi- r
U&iratory). v. 15, July 1949, p. T 71 -
711!
Develms ronditions foralm"tion (if Cumid Ni freim
wrakly acidic solutions. thus petimitting determhuttun
!go of S, P, and As in these metals by well-known nwth-
0 ods. Two variatiom of the miorimetric detennination
0 (if As and P are descrificti. Tjpical thtj ATC WHIlAt(A.
A I N - I L A SITALLURrICAt LITZ44TOC CLAHOKAMPI
0 U 0 'AV 10 is
It or K K It It It
.304,
An L 0 a
----
iii-
14 1 a a 3 a V
T;;& dh
0
40 0
Joe
too
goo
Ob --ds d mbrimeriel Modkob of DOWSWAC Slatuth. Yu. Yet,
Lur'o and L. H. (.'intburW (Z4md. Lab.. IWO, 14 (1). 21-M).-lin flumianj.
A iiDiupwixem in madle of the K 1. fbo&mide. and. thiourea metho& of eolori.
metric quantitative determination of IN in the presenoe of 1%, 8b, So. As.
Cu. awl Fe. l'be fireel: methott in dencribetlb wo others in detail.
A vk4et-light filter with intex. pLnne"ty 1=4=1400470 mg. Corre-
a nuling to mi. extinel"i by BI-compkim is used in all throe meth,xis.
"n,
tC I(otionafetelounA Hi-complexes occurs In 1-2,V.H2N4)&. 1-3-3' Y-If SO
&M 0-4-I-2N-H.XO,. respectively. TIw sensitivitka of the three meAZ
dercetreseecin the *det x 101 y1cme.l. whom y is the coneentration
~~ thickneem of cielorimetered layer (cm.); the ranges of rerrew