SCIENTIFIC ABSTRACT LURYE, YU.YU. - LURYE, YU.YU.

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CIA-RDP86-00513R001030920006-0
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S
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March 13, 2001
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December 31, 1967
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SCIENTIFIC ABSTRACT
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Oa it Is If 10 It A a a J? A mail Bill Ida low 01"441 11 I I III r a a I i 11 a "Po v I v 2 ti 0 9c (a a l I 00 60 41: \j*sp14 dootOMID1111013 01 lisic 'a COPPir as"fe "d siffoucts' ' fill NAh III Ism. V s * 14jlic 0 61 copper ismilffing, YAJ - ' 1W ill 14 " " d O I . r W J. 1l l1 1-b. 4. 11;4 1 "1 Vishi, it'.. I,$, 111-i 11. J I . 'lFg. 411 o 6~j /if its Ills lot. to lof f A-20, All) NO ' l i vi.. q l, Nvoliw I width all's if,$ III'. IM111,11 lot I Inmi, OIA1114. thAll flow I v fAfIIAfr 4t.fl.1.1cf, 11%. It-Ing it if NAU if *1111-111,I)SIV Off's a fulad and 4-milpli-Ir ppill .4 Illill. SMA.- 01V ppt. i4 Away. / ON" Ill --mv sa,Alk, life dim, smile vo i t.4 I'll-ted I'l 11.11m, Man.. a so so goo SOO Joe j ties 'S ILA OfThILIJI14MAL 1.111111,1601 it nelf as t , - 9 wee 010 0 ;, ;t on 4 4 is W it or 160 AA 0-; of It 9 i --) I 1 i 0 00 0 a 0 0 0 0 0 00 00 0 0 a a 4 : F 0 00 0 so 4100,9e99900,000 0*0 *00siosedoosoosoogooo : 000 00000 foe 4 006004 0: V !A,~ II 1 4 % 41 it0it it If W it $6 11 1# it All jif b 14 0 A )0 . 1; Vv 11 1& a to It is IN G 11i AA-I-A-A-" ~". I- U-C 1-1 A.-j- T X-M if a QVU44 III I i,.# - I a% A s - - 0 -C%I.P A 4 1C 4 C ' 8 T' Det"MinatiOU Of dAC iWPUhd*S in CAdsWum N'ij 1- ' d V F*N' 'MYUtina i ZdVVdS*13 U 1 IW W 5 ' . A . , , Y i V d... of Zn in Cd by the methm] of 1,1wil f C. A. 26. 42#3) giv" inconsistent results, depending on themint. of CU impurifictiand the conditions o(operatiori, 4z R"tills accurate to OJO)l It. Za for 0.102 g. Zu in V) If. 00 3 Cd are obtained by pptg. of flit- availatile Of with metallic At and defg. Zn in the filtrate. Diualve 110 411100 9. Cd in 120 cc. of 2.511 ItCl with 2 adrins. of 2-3 cc. of 00 3 coned. TIN01. Introduce into the solo. 4, 1 and I x. At sits vings at intervals of 111 -20 imin. Filter tfirouxh cot- *0 Itin and wash the AJ-Cd with 2r; 110. MI. Zn in the so R 1111fale as Z110 toy flit, J1,.S or anv tither intthtid. C. If. 1 1-1 -00 -00 -00 .00 -4110 gee 0 0 i~~ roe goo see woo be 0 till*ATVAI C1,ASSIP)MION 1:100, G-V ',At r it, 0 4014: U *"4c wit YIN platt It it 1 AS 000 4 0 0 00 0 0 esee o 0 0100 00 0 0 0600 000 0 * 00i 0 11 m I, m I," Itail'i a XVXM.Joll I:Ujdb JIM*** 41 40 4U 4f ~ 0010*00 A -T~ v I -A-A-j.AA N 0: W Et b 00 1 40 00 1 00 tin 0 :*,I od, for We I study of Me T,tittic"Y"' 0 0 Cato off$ r slid 0 IM 00 lock, o;o 000 a 0 0 0 0 0 111 0 0 0 M., ..l. 1 1. s a Ow o ad Is 0 0 00 0 6 -41 0 0 0 goo ::::::Ooood Woof sees**141111411111 goo 6 0 I j, 1 4 a 6 1 1 0 1$ to u It w Is 16 if 0 of --Aa K I a L a a Vol 410 oot a 0 x 00 a.1 a 00 of 00 It 00-A 0 0 X~ v a or a it 4 4) 40 ano A- t-A-1-A-MALM AD 11+9--k- s_A.,j_ 1_11 Ji. j 0 0 ;:o0 -00 -0411 moo =00 a a 0 zoo roo :z o* moo ties ts9O A t a I L A mETALLUMUKAIL Lillsoituill CLAWFKATIC" IV* '00 k 0.1 u It is loompsoi; Nis 999 "MIll 11"Kwn I 'o 0 0 a 0 0 a 0 0 a 0 0 O's 000.00 Ole 0 06 0 06 log so Ole 00 100 0 00 Ole 0 0 0 0 0 0 0 0 0 00 1 JI a Ut .,W? copper In metallic nickel. VII. vc, 1,111'r and St. I. I'ttwitsksya. Zaroirkap, Loib. 0 -.IV; *r (IM7, 1; cf. C. A. 31, Ol". -- I'lie meth,xi )I j~trrnal di~etr,,Ilyrii, i. u-wd fin wPa. C,- Irms, Ni %ith the aid ,f a 14, lif-alt, Full details are given fin vitityinig nut the Inti- -titur anti the rvsift* in detig. w(KA; 11.24% Cu were ext-t-l- Via. Ch... 141.6tit, '0 O'oo-4-6 0 0 a 0 0 a 0 0 0 , tits& is ''OlItzl3mll" it w it A . I a it n I. 4T itsoll'soll u1) 3415 lip Jolla at u it a Be A 0o A A-11-1--'J' -v- kii'- - - 0 1 ad I I L P-2 9-1.1 11-- ix__w tar ..r. I 0 0 -0 0 00 0 g 1.00 040 t -00 00 tk. tdy .Ow. too, is- c d -00 00 a - I oor V,4 zaw YU. i On , 1 11 C -40 , . - T . 4M4 t. -00 0 .00 00 so 0 --0 0 000 ago 00 '3 so -.00 00 -00 04 1 .00 tie LO 11 L too". so 49 'mool f4joe") -hp oftv (W I a I r ----- - 144JI ~arf .7.1 aft ' - - ~ I I u : AV to of it 11 K Is it 4 19 of cg is it ' AMA A V 'd o vw (31 79 KA 0 so 6 66 0 a 6906 ID !0 : g : : u i 0 0 0 0 0 0 0 0 0 p : : : : : : 0 0 0 0 0 & 0 0000 6000 o ' 0 0 00 v a 0 0 0 9 q * 0 0 0 4 1 '00000000 0 0 * 9 0 00 0 0 a 0 0 0 4111 0 6 0 0 a 0 0 0 04 4 1 1 a I is it 11 is 14 it is it m alai a a A b- .4 2? at u If m 0 Ip 0 A 41 #1 if a it 1! 0 2 L-a a 1--r- Af I. -1-1-m 00 q Ll M it, .!v J-D COOtIll 1-00 0 7 ~-00 0: ~~w~Raftiiol dotersminstion of Itsd in lesd-zinc Ms. can. 00 cQuirstel and their products. %'it. moll I.. it. i-00 Ginsburg. Arodikap bill, 6, !.141 Vjilr..).. it) livat !-00 64 A-1.0 g. 0( "Hipli. Willi fit nit. of coned. UCI and with i 00 5 MI. ul Imird. 11NO.. Dif. tile lf-~Ulfinx X411. will) .10 -00 list of water &nil 3 fill. MI. Nil. fiber and allow to cool, itipo 4 ro'llic cold A411. &d.1 11 N 1.0 a. till IAl I,- avid. a 'fight vuv- 4 N11.011 and S fill. of A,:Oll. till. to limo od And I-pt 00 4 PbCf(h with III nil. of .*)4;'v KvCtM. Fill" Mail waA Ill 94 9 PI)Crill, With dil. Ac4)II. Di%,olve the pill. in a ruht. of 00 1 X. Nat'l. NMCI fulln., 14 fill. water stiff Ifil) nd. of contd. IlCI, Pit, life fillistr *nil dri. life Cr iodomelticaily. 00 -3 i t2) Tu the %oln, pirlkl. a% In (1) add a Alight vu-mol NIll And di%N0IVt! 411Y Pill. Of FV(011)j fly Adding Ill till. 1113 N [f%'Lh. Dil. to 2W ml. and lipt. PbCro. by invans c4 -;zoo 0 11) nil. of (1101#):CrOs. Filter, wasit &nil dj&-~Jfe as in it). To ihi-tsoln. add water to make2fl!) fill., add 2 fill. ~o 0 00 Tiltatetlic 0 0 v exerm Ve Willi Standard K.Crt(h skills. Willi diplu-110 ainine Its internal itifficitor. (:It I)ix.,Ivc lite sumple 1A 00 z I (I till if ) t with the onfission of tile rinal 11C1 treatment. zoo 4 Pitt. the 111) as Micro. by Illeans 1)( 14 111mlialicd Vol. o( IlA N K,Ct,Ot, filter slid take an Aliquot pull of file fit. 1,00 I! ji if ate for lite drin. I)( the cxrmt K,Cr,( h, fitti.hing the ansly - so* 4is as In (2). Chas. Plarw J tro 0 ALL UOISKA L 1.171 1111&1 URI' C, -AS-SWICAVICk !too L bog 0 3 T ZA AA L I V Od 0 9 1 v 94 -j - - - I it 'no; -; 0 ml. A. to to or KLO n I 9600000009000000400 640100000#6600404060000 0000000000000000000::Ooooolooosoogooooooo00*0*i~ 0 0 0 0 0 1 6 v It ti 11 m is m I! to If X; i 0 n .4,1011 UU six Mir X J 1 n AS J& 15 A V At A L-A 1-4- lt- A.- L.-V- Y . J. - - --t . 4 k. 'g- I --L AA 0 (Z d--JL I 00 cadmium by intemal electroly~iv. 00 00 Xu .u - and ?*1. 1. TrrAtskaym. 74mlikaya 1.3h. t 00 rf I W 7 1, In the Ivits. III Cil Isy a previttt, meth-.1 00 1 -00 (C. A. 31. 61 ). a little'4 the plild. Cd i% "Nitliml hy Cl 00 and dissolved fit water oblidned by dism. t4 chlivinatIA -00 11 water. The difficulty can t* uvrrv~omv It adding 410 f 3 1 .00 1 1w i unis cc. 4 0.1 N Na'%flt, to lite efemolyte and it 00 it) the Irs'll vvmt~r. Ch4q. Plant: to 'V* 0 '00 of ill so j of so 00 of ."Ise 00 .09 00 00 00 00 C3 00 A .11ALLUNI.Kkt (ITIN41%,KC CCASUPKAIM- U00 WIN 0 U 0 W 4 00 0 0 0 00 0 00 0 0 0 0 0 0 IT a 0 0 0 0 0 0 0 q 0 0 0 0 0 0 0 0 0 * 0 0 An I a It 4 A4 0 4p 0 Ill 0 49 0 0 a 0 0 0 of 0 00 0 010 0 0 0 0 0 0 a 0 0 0 0 0 o 0 IF 0 0 0 0 it is #4 " " 11 7 a 0 1$ ) p A tt a ))4 a a ) V~y MAX A 1. ~kl) ~.v ~Sulql- A fK! oil um ids mu N064, AhtenW"doo of cadmIum by Loilomid oleclMyWA. N's, V%%. Lut'r. tLireis"m I.A. 6. 104OVIXIM, d. V. A. 11 AuAwrr 1-*t4rrhk%i Awl Kalmi,kovs. c. A. 32'. 1114M. 60 tol I jai ji 5 1. A 04TALLU041CAL UNNATM CLAIIWKATPD* It a, ;a, . ; , - U 0 0 9 0 0 4 0 0 4 0 a 0 0 0 0 0 0 0 0 0 0 0 0 0 Od 0 V I KA , ; - :4 ; , I- - a 0 0 0 : * : 0 00 so* 00 -00 off so* got 00 1.* 9*6 0 0 0 *00* 00 0: 0 9 :000*000#00*000 0 "One -polo ~16100 -.101, ~11104: 10 ~111114__Itm_u MMOA, a. MCIS"Uski, 00 OOA 60A Oet sea *A 0 : 0 04 of _j ii-i-I1.1 1In 604. 18, .0141,11, -00 -00 1 Qd#m methods of inorganic analysis. 1. V. 001 I'Sh WA ill% uWUH., Ch4q Walk. 111 :0 0: 0 0 ~z I g, d If L A 41111ALLURGICAL 1,179111ATUNI! CLAStIFIC&TWild 4 L---,- age., f1w,;mJ&- it Gjoasti -A 1 114114112 .11 (14. C!" U 6 AV 10 Ill; ; ; ; I, ; j j I - j - j 'i .11 pooooolooooooooooo*ooodoo:iooooooooooo*oooeoo IOT44000*0,006090000*00000400 q Ell"I 11RAM& IN ado It a I w a s a a 3 0 V 111,00000*000040009-0* :4 0 -00 -00 -00 000 goo 000 goo X0 NO it woo J1401 0 0 0 0 4V6 0 0 0 0-6--f- 1-111144 :- : : : : 0 6 0 0 0 0 0 0 a 0 9 0 1 4 11 0 " 4 4 L111 I v a N1111, gull, 1 11 1 It tA Ze, bumove 'I mumose k of broad analysis 7 Imm still L. I ~,, 00 lil air Trtu'll", .1MIrsw 21131VAil 14 ill 0., ""Imm IttAlle "let 1kx ~:~l A S N - S t A 1 look, Sivoliv. 144041 01TALLUNWAL LITCNATUNN CLASSIPICATOGN not 000 ZOO Gies 400 go* zoo we 94- In. too .11 04. a I I I I I ca a.. it. 40 0 If 4 0 OGG o1@ 0 "s OOOGSOOGOOOOOO.O 0 OIJA U M 36 11 U a It V 36 * 410 41 0 4 'A 41 6 C D IFIF 9 98 X L & It 0 ft _%T uv a b 40 Il I h -P 6 1 -1 jAy 00 01111 ys*T* son on ot IF or of -11, 64 IK"Ij till W W '%' Imajul pq polilm V go go llsic" "t 0-1 At-#,- q OF wa I 111I ItA 111 0, a a it a a I I I I I I Ipo gI ,'A! 000 0 0 0 00 0 * 0 0 000 0 * 0 0.0 MW_ ft MLWAD~0 4 ~*i 06 ~90 0 ~00 0 ~09 *~* 0 I I IN 11 u is w IS 1? 10 It a isv"'NRXII 99 big ABU spool ou go 0 A f- a & I 111~ a 44 is Oak L to , , " " ~ " ~? At #s$ .0-1ilit ..a 1-00 CV7 .00 Z! Detenal"flais of small minouts of cobalt to of". cola- costrat" aad Wisp. %'u..Yu-,Luv.%t-&nd It. St. Tat. .00 7,RW,bdy$ Lab. 8, 3K"4 109).- A mrpatativv study of -60 vaskm wetholits indicates that the nitrite Inctilod frilloutood by grzovinurtric dtin jim hilther rrsulto suit ratinat I* rate method I* the nitrite promitur ";,;Inb )rJuietric deln. The nIvIllod In. howrvri, -00 long. The method of prellininary wpn. -4 Ni anti C-- .00 xj! 1byttergrolysistorithout A"C"Itsidecuffent istiotastorcursor '00 so but it is satisfactory for routine aludY414. Direct Moot- 00 Metric test may alvit results miffk*ntly sovisrate for 09 0; ordinary needs but It requires the adda. of entough pyto. *0 pho4phate to bind the Fe as NaFePA. This, i4 the son- plest and mven rapid method. In rAse the ratio of Fe/Co a** is 4(M or more the nitrite-colorinictric triethod is recom. nieudrd. It, Z. "nich 000 00 0 g:00 logo '00 go A I A. I L A 11411FALLUJI&ICAL 1,11111ATIAll CLASUPIC41100 milt, It U V AV 00 At V S a ad 0 0 0 1 Mr 0 9 0* 0 0 a ft ila -- I ;~14 [4 00000 * 0 0 19 :::0640090009 0~6_ __ : i see w 0 ~"* & P Of ei 004 00 00 micluchfullul J010IM111400" of 1111C in offil by this mer 0o cury twocyouste method. I1,11. Xtt 1.111 't- will N. A I till- : l viii. I'mighAr,ossl Lot.. A. N.;, lorn fill; Al.'t likii), kR 00 I i ""Khrill 'Irtis A Zoo III Ili- In M, Ill. J I.... A 1. 1r.. I'v 00 of I'villiv.41, 11111AIIIIII lot II 4 .11t.1 I., "Ifillhig"I "till %,I ph-pbal. pfil- If, so 1 1, Ow I'll J."'Afild '.1 0 -111 -lK III- It" "Ild "fla-Itl Iq lit ttliAlifillig 11.111. %$Ih %41 M Nimple. mutg 11 4 j /it 11.2N, 1) Alld to L!hl I" ' J ahrr atid Kia.d'.bthiLiiv isivili.-I bw I,tg /it will) osli'llill. 11111., %.111411. .01.1 to ppin toillf A 111.1imt of l #ljI1fIIll11r~ Ohl , I"N't Il'till. III Ill.. 1-1. all.1, ol Ve 41111 Al,,inillo; It. Ille .-IV. 14 lit It-kil 4, 1.1 A411'. dold 1'. list- I... lit MI. tallidw 11"'Ilti'll. Sug rickorcmv.. W U. fic'm !.t I L *fjAjLueGKAL Lit 1. 15. r K a It u n it off n 9 to i00 -00 100 *00 goo too* gas Co 0 00 No 0 too IFO 0 WX11 s a 1w a or too to dola: It , m Am 0 0 0 004 006,00 0 0 0 0 0 000040 0. V o o is 0 0 0 0 0 0 V A XJA 0.49 10.0 U -.1 1- 0 - so A .~-"-Olt.flts Wt- 00 'LMWMWGUM d Val 204 Aumb of AsUmmy is Zkdmbao BjM -as 10 j: ad In Ksbft rhm Yo. Yo.. E. M. Tal, and L. R. Floei'man (Zatod. ' LAbj Lab rk W Ign (Y S %LIM Ab o s . ( . , ; e., 190, 14 3778).-lin , . R-M ) Moctrol0le Zn bmW contain &MOI m 8b 30 " y - . g. . o. mg. clinnot bound Miod..torujina. tion of Mb by the Blum#nthid method Imd, Ab,. (j. 10W. Md4b), 19-2m, 40 0 & . 513 1) gives good results if the imisioquout precipitaicin of Bb Is carried out on 0 1 Cu foil and Da with 11.4. "Is best mettiod for determining small amounts - (ShL b t i l h l oo : n e n *ma c %Aro tiort4kmrdbyt"winictritit-amWim4i. AdJ y ) z 0 13 nil. concentrated IM and 0-5 griu. hydrazino (chlorldo or sulk"te) io - I litrv of the 1.1mrol best to W-03' C i i C l 00 . ant mmerst a u wire spira Cathode joined to ant-or Ph anode e th s K l ti t C f zoo 0 0 o . e e u on a . or p 1 hr., remove the electrodes, discontriftt. and wash rapi In 5% 110 and in Add N 0 di l 2 i go* 0 0 water. to sso ve all do Sti and deters le co (irimetricaliv. 1 11 III tile bwnco . the cloctrolvols prorvmla slowly eind In determining Ali In metallic Zn Is Is mvvItastry III mitt I ing. As (as P41t) Ill-fivre the rhwtn-l)~im. S ~ 96 90 Id $L A WALLV(KAL to[OATLOC CLAWSIFICATION WOO 1 09 ' ; 4 A at W) It t 9 It 11 t1 it x a T I TIL AA 0 tw o IN of 5 it 4 A I itl wip 31 j 1 4 one U Is If 0 0 IS 0 6 00 0 0 0 0 0 4 1 : 0 0 0 6 0 0 0 0 1 6! 90009960946: - W 4 0 0 0 0 0 0 a at 0 9 4 It 4 It W is III I? 111 11 a 36 V a lot a It a 13 Do a is I? offs &I UUMOVO I a IF a R ir a , III , I J1111- cc- 'k =~SISUS .S -SOOW-11 -"I it k 00 A C Detitentination of lead In mounts IICI and 60 nil. wairt and lival 10 I"dilIll- CQW to FIx"ll Zapod. troll).. 41141 111 :!11 sill. of Y" cittic or tartaric arid and of Wax. %'I6. Yu. Lur,C .00 skayu lAb. 9. 1U.' 7(19440.- In delit. Ph in the presence of ricuttakee will# Nil, to laimlj*- Add -*, Ful. eviol-d- IJOAc large amt. I Ila the tivistultilt with Illso, followed Ivy bqpt to Willing. add Ps ml. (If III)% KrCft(h. Im'd for noi 0 a u*r5mW.antIfilIvtandw4,h- thtfli't-in the eviralin. to ~411r" 6 not perini-ible. In anallylins sulfide :0 ories the cvaim. to dryness with ordy IINO, or filter, dill, to 150 nit.. alit[ 1 1.5 KI &lilt liltAtc will' I I ot lie tarried out because lltR)4 Is squaresla ti~ktwulfate. Ili the electrolytic triethtd. di-Itivc 11.5 it. tH n It , formed. In both the IWW. is devitroyrd and ratc or of tire in 15 mi. IIN(h. a4hi III mi III goo 00 Mst. lattice of ut, 04 4 wime of the Ila loris to into ia)in. 01 subkvcltt dila. "I'll, 114"J"ll. of Ju(NOOt rorr-ix,riditis to I x. Cit and j with water the &tar costabi ate spin covered with layrn clectrulirw with ItWirr clivircitic*. In the raw 14 otillised of H&W4 with the tcsultant Occlusion of PID, which camult otes arid (Quills, treat 2 K. and.1, N'. tetil.. fir-t with It) nil, 00 a he extd. by liolvvrots. Accordingly, two mediods of detS. IICI and thcn with 10 mi. IINOs, eval). GIS list.. add 2 K. Mita-mbirrisdevrioswil. Inthrehlorlde-chromaternethod %H.N0,jLndevap.todrynm. Tothedrytirsulucadd.5 diwilivir 0.3 it. of the concentrate (2 jr. of ore at 6 S. of till. IINOlt evap. to drytims, add 3 nil. LO mL bot 0 1 fallings) in 10:-4) sill. JiCl. hear for 15) inin.. add 5 nil. itrat". Ilod A min.. dil. with hot water to 1114) mi.. add ncts- *41111 1 IINO, and 3 g. Nat'l. evap. it) dryrims. coul. add .5 nil. trad VWNW). and rIcvtr.jvxe. It. Z. Kmkh ties coo All lir tre 0 -;L t:0 0 141,01i; -71 14114.1 .0 1111, too U AV 00 Is Ant Isado 119111 142', a nit 001 *11 Wq K(ttt ag 4 1 94 foo ~194 M41 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 01 Is 0 0 :* 0 0 0 a 0 0 0 0 0 0 0 0 0 0 0 0 0 : 0000 1*0000000000000000001 gal V A f V V 0 0 4p a 40 41 0 a 0 0 0 0 40 Ole - k7 4b " . , 11? 0 In E W_W_ r r to 1111ILF-EMIF-17- To 11 a T irl.1.1 L Tal. 2ldrodfiop J.;h. 9. dein. of the equiv, [*,I'll IlY 041, inwtry hag varkxis advantaces over the visual'Ictil. 11, - ti f I A A ftf le A 11W S A M 1,rtna"anal-nuctry lb,, pink t oint 14 reached Incrvaw.-I in intell'itY -ith the 41141". nd p g~ajc in acruirdarice with the Landwrt-liccr rman skes it Ixtuible to reduce the titration it) 3 ti Tj av nwa-urrilients of tile tutyrnt 'A tile phollwkr. cell: oric so at life r(july. 1X1011 APAI 1W.) aflort, it, Tillatioll of Collard ~ 14 Callird Willt ShO W1114' Valle 411111 8-1114,-Y a*vi)tlr - %s utlnc Avidimetric (lifittiono with a pikilix-lec. cill 1, were aW) studied. The natute u( the titration corvto indimtes that theindicattwo Ill ujhr may be divided Into two W V0111A. Tile fint limp (v. S, plurnolph-halvin) Ila, all ' , 10 * 11telit-t"Ill gFIA111 a life advottiagrof tit rwirkninprukurtry. I tA. all forthyl Ifff, Isn"1101111clicil Illur) r .1,'l toorat Advallfaseq liver Ilk, vinkil 111VIII44 III 11114101A 2 dko Iv-% .411114. Its 1111111ing Mill'VII MAIM With A 1111411104111dIr- flurtcr and lk(tulophrflol Illue it io [),.4blo Io lict. a6lily It "I f4, It, .111(All, "I Ni atlJ c". file wi.filv .I ch-vilmlyll, Will, 'I'llig l1a.. '111'. Wild fill, mufilv 'd m.- .11,0, I L A 411AIL(UNISKAI. J11,111ttilf ... IS'NWAtkial u a A, is, #1 09 0 set* 0 so o so, 0000 0 a so 0 so, M u 0 -so -00 -00 -00 r .90 nor Its -A go 4 13 *0 f J, - - ' 11 6 4' Is I I I Dlits"Wasdoo Olf Isfid"Iss and scrattlifil in W wage WOVI'll fit 911141190110410i'll N'll I'll I HF'v -4611-4 14t- III, fit '011111 1 1 ~111 W. Ill 04-il, *4111 4,14 A fill. of It'luellp Unit IiIIJ, 44 Ijulft-t w4n. 0 1. 111 IWAn smi Ahet radi ilif-In- 44 [tic bufIrt %Ali. %lLike thtwoulthly. Allim tile IjquuI* Ill ilep.. tli%mtIl in-1 It( tile WW" IJY". 41111 TT411-fef tile I-I N*c-l,r yinuirr. Add 'dl ull. I( tile bulhir .4u. 1,, another INC-ler CY111111cf. slid :1 nil. of tolintic, and tormic drupwise with a standard zanthate"n. (I ml. - "A MK- of xanthate) and Julke th(proughly Rfirr each arldn. of tile reagent until the color of tile ttguene Wyers in [with cyl- inders is the "me. The 4cusitivily of lilt rinfliml k re- illiml fly utiliff pho4pliale buffet IV 10 Af lartaric acid fix deconalwising flit zanthate. Arrofloat Ill ROPO(S.SWO L* detd. similarly. The deconspia. of the aer"floal Wn. mramipli.heIl fly melicAtevinte bulTur still fee a buffer Illixt. -If K;fIPO.- It I. III dri. OAN15 ills, .4 IlAnthal" m Awroll"at ill tit, "Inple. If. Z. KA111i"ll ftl~_A u Ill At 03 It 44 0 0 46006 000_00_0 If ivi E"'f ill too fill 0 it I I ill a 9 a a 1-i 9 0*0000000000040000 0 000-00 0 0 0 e 0 * 6 0 0 0 0 0 Z~ ;~;~ *.O.fp * 4 0 W a is ! ! a a ill J. I I I, . . . I- 110 0 -0* see b boo 0o 051A5 1 0* 1 *0 &I 00 11 so SO it 00 4z 0 v 00 S a a It a A lot 9. is 1 st 11 U ALL"t J . - PWIS1111 ..0 retAt"'Ut LIP Deternalcustion of thlocyamtes In waim waten ow owr d9grits Solations. Yu. Vu. 1jeLrv _Cj;~J,Zavvhkdyg; Lak. if. -'ri-80945).-Th had e (or Om deta. of "I = rawast'l wNters and svtAba.U. pittituittary septi. of CNS- and Ca- by AsNO., purifimition of the together with C1 rcsidue Frout impuritim of arc. subtItsam. decamps. of 'Ax salts. and colorimetric deta. of CNS- In the furnt of ~hc complex "It with Cuznd Pyridine. The method is Tcry amwate. Add scm drops of Ic'e' N&CI 90a. &W tlanobb s) igloo* %it GMv 449 -1 U 9 &W 00 U It Se.SLA MAKULLIAGIC11,16 LIT2111ATtAtt CLASSIVOCALIM M union *Ujip*ilooo 4 ~R_JL_ C-g~$41 III I.') nil. of I N Ag.No~, to 5W ml. at the sample, filter after 4 firs., wash the ppt. on the filter ouccrssivvly with small Portions of water, sk., toluene, &k.. and at", transfer the ppt. and filter to a 100-m]. flask, add 20 nil. a water utd. with 14S, let static! on a boiling water hath (,,r 30 mlu- with cOnst- mixing, filter off the A&S. wa-.b it with water. and evap. the filtrzte tu,',I() ml. T,,L,,%(,-t the win- to an Eggettit test tubr, add 3 mt. of 67,.Njf,.N0,, 0.4-1-of yridikov, 0.5 tnI. of 10~~ CUS04, and 3 mt, of ClICI., and ah. e vigorously. Add B-lo mt. of pure water and the same quantities of all the reagmts used (,,r the sample to a shuilAr test tube and tittlite with a stud. ard XCINS soln. until the CQUXS of the ClIcIl layers matels. W. R. liens 9-9,7 an I I 'M 0 1 Mr at 5 a a I %A .00 ago 190 0 400 g 0 too 100 4111111111 so* 41 Joe 400 ISO too too tie a ZI Me 14 1:1 be j 111 Is -w-m i 11 .11 - I'-- , -~ j.t- L -L -A - a. 0, 4_ 0. .. A-A-A- &"Estes Egli -4 p1! DiEttiffellnottiOn Of N-. A --I~- A Willi* I's of '41111' I.1111 til. is it till loemilklit 1, Ill" I,,,- o.vrf "Llil. 00 "toli'llic till, I.V 400 -06 t .11 clict, lulw to", 0 1 -00 96 a "11111111 alld es,julot-" lite W13110" I'llo MAIL 111 lot I lie t 00 if IL - t1lit I ,III ~31AV!lv thrilmilrollose'll, 11-00 t 1. -At- to fell, (If tile 1,111h jilt- Ill 111111'r, tiralls I Allot fill th" 11111,01 1" of wilit 00 till, dtl. ,, till-All" low to A'I'miAl., a All 00 00 Allot of the,. Alld ,e ;J7 till. I.-Ild I loses "I III SIC- All' - ,"j,01 Ile e", p-lold. 11 -Ill ..... Ile 100-1 ,, the .4,111 0 ,4,ioml ill 11" it "phit'l .,1,% 00 A lite 11001 slit. ~11, I., tile tit,, III It to I . I (I)f tile '11111"tcl Vy is I tit he 4. walrt 11, I)IMillt's, Opffli live 0 wool "What I(Ywrt I"" lott'ji'llivol mItIv '"olliev ate 1J.'t it, till' 111'e, 1, .1 the It'll'taltv loll.1.10" E%t a W-k C... 0 0 0, moo di I CLAIIOPICATIO. "I CTALLURGKIL L17141"'99 -A 1;04, SIVI#p,V- CK ~Aa 111 1 !IE1 Wit 099 Kate u AT 90 Is to P It of 00 0 0 0 0 too 'q 11 U 11 0 b 11 1 A S J A m ft-M-W JIL j A-1-1-1 1, 90 =Jaks &A4 cow- It medwilssin 11. AM 1MVIAs' of c f Al. I0 fl~ ain't.. .film tlllml~fl Call P,"Ist tithtf bY tilt API�tWAIkV tOl fill like %IIMIIIWA. IMKV A 1111111kitlY Mail- Ill 4 litrAti't 46'11141~V 1114R it. 14-- 41 'wi*"lly. T1W isic'mar In lilt lulbillity *lilt tilt f titt tial (w th , I Wil t t 4 ti 1161it d J " o a e et rav 4 lt "1 y lip 4 11 1 4 l 1k 1 1 L i l h 1 it fth 6 "t 40 ,4114 W11, ret 1%11"1 l I ItA )OPYS O IM, 1 l st"t I... 14t 11,011 the 4qlliv. pporst am If# 'mh 11ir rquiv. Im4tit eau I~ 'let'l. 11121.1mally .61 #Ike 00 tutcc.~ftkgs .4 j trAtglll Ollie. 1114wit 1111,41ills J I-clic. '1 h 4 1 i d t too . U_ ' eut 1. .. lt ri' " 1111416~"s l (Itill)(UllifftfidiffK-OriC tiltat*M) (J`Al0GK1t1% Ill,- %'0116PAIA- zo irm-mraft meth-A of DruiS& atid I'Askes mto all : iviviall, nitshi"I suitable 1w IWOVi.- AllAtylics. The i tswth-ki was uwd to det. chWides by tilliditill %Itfl - with AlON0, lix(N(h)j its acid mAn.. f4w fillation id CN . C.A. JOS. 4NMI). wid bw flor drill, of ell (Ammiding to pasims). W. R. 11cust 9 id gee v I o4T ALLI 44GKAL 1.11 111141411111CWIVICS1100 u a Lik ID Ls s 8 fw a a I vr IN a dj alvill, wags plan Illamoll 1116 4 4AM mw 0 n )000000 * 0 0 0 * 0 0 0 WWW WII" 0 # WWWWWWWWW IF 111111 0 W a W W 0 0 0 0 a ol 0 0 ; ; ; We It to is 16 W V W Wf"L d'Go 004 00 -00 .00 god AVtioa of the phatocolodmeter In volumaftk &easy 4 lee *of SIB. . Titration to msxbu= tarbidity. -00 _~.Ua.aud H. N1. Tal. ZaWytaya lAb. 11, 71118-1m1 01145), cf. C-A - 40. 24MI.-NA, hen a pliolocolorittitter is .00 u-I in cletnts. of the end point of titration of Ph with age$ 00.3 Nli.)t%[oO. by max. turbidity, the max. may appear ! Itht.r I;eforr or after the equiv. point. A coincidenct of max. turbidily with thr equir. ImAnt con Iw ributined by ki i l d e in tnt r la ng A unip r , III lip IM-111. r111141 10.11.11~ In 411P III inAlip for t4juirld of 11 , 00 : A.0 lilt. Vistler Ilifte C"11,111111ill It it 11 CI I fulloarvarale 0 0 and Iv applicabir for large-f-cale atutly%1% of ort% and of 004 thrir cnrichivirnt products. Mototurbittimetric tictn. of Cloo Zn by K.Pc(CN 4 rtquires no addig. at stabilizer to the 0 0 "n. Owing to the slostmem of the reaction in the col-I. the method con he used only if the titrated Wig. can be 0 0 brated (luring the tilralion. W. R. Ilenn -S goo goo woo 41?ALtUnKAt Lfftl&ti*l CLAIWCATION 0 0 woo claw 11"4111116 ago., 410.00 tie 0 A 140101111) .&P GMT all 0 U In A, 00 as t It 0 4 0 a if 9 1111 a Aft I t a no 0 0 a I III N 2 a a 3 a it 414 A I KA t 1 1 1 4 00 0000000000000000000000000*00004000001 4 - - - - 0 0 4 a e 0 0 0 0 4 0 0 0 ei 0 0 0 0 * * 0 0-0 0 0 a 0 0 0 0 * 0 a 0 0 0 0 0 12 It 11 It t? Is n it' a' a At a311 V ail 12 v N owe'1*110t -1. MMaNMOK OF WALL OONUMUTIOXS OF MMM. AXAMS 2090. OF FUD VATZR FOR RMIN #IBM DOWWA. LUr-'0#,TL-aAd NUMIGG'm ibetr.p 191 Z.T. (ZSVW$kap lab. p 1946# a# 161-70i Aj, *0 b.: A colorliestric method for v=7 snall coneentrations of Cl- Is based *0 St,;~~ on the suppression of Cl- in the reactions between ft** and d1phany1o, as, xlt earbasIde. The colows obtained *bed the lambert-beer law w1thift the Halte of concentrations studied. The determination can be **,3~ ; : either by th* coloar seals method or by the equilibrium nothod. The 0 0 .3; oolotw is 6teblo for $-)0 aft. and to not affected by walI ocneentra- Sov f a that my be present in the water. The ivolutlon abotild tious a so v be pre"042 lly aftutrallsed If tb-9 content of a exceeds 12 mg.Ae a io tive. Tbg ulnt~34steot&bje omega- Ah* method Is aeomge and sawd tratlon of al- to 0,025 ng./I* go colourm were obtaln9d In strongly sold solutions. Best results were obtained at yK 4, Ohs contmt of up to 0.5 mg* of F* per I# does not interfere with the deteralastles, .11 Aiwtber oolorlastrio method studied for the doteralastion vr Cloo is based an the reaction WrOj, 2 Cl- Ov04-. be Cr%7 -A 1 41 1 It. A al, AWOROKAL LITERATURE CLAW06C ATOGN t 90404111 -tit Q"V got LW 0.. 114 U is AV 00 is 1; -1-# . . , r 4 W I-# -R, a Ct Ly it W A a A 19 9 W 0 0 Is 0 0 0 0 9 0 0 0 Is 41 -*4 -00 10 S, -00 -400 00 6 =00 As* -coo see 000 -0 41001 -040 see too .46 0 : 00000000000000000000000*00 0 0 00 0 roawd in the solutlon can bo dotendmod eolow6istrioally. The Crq47 : 0 #0 diphoWlearbasiMe mothod Is as accurato as the sethad ~-lth Ndp" 00 04 but Is wro embersomso 00 10* 00 40 00 !so 00 00 00 00 0* g :l o 00 0* 00 00 of, 00 00 00 90 00 00 00 00 00 *0 010 00 00 0* *0 00 hL*&*-000000*0*ooooooo00000000000*000000000*0*00 40 Ms-t-o*OOOOOOOOOOOOOO00000000000000*0000000 It -1i i i A --- I-L -I.- M.A. 9;-A.U-4~A-A -t A so Al &Y Orgiudc esch-- 9 m4sm Tbak me; in Lur*e ZmWjkdya Lab. a"AW ch*mlWy Va Yp 00 . . . ... -JS '3M -13ttags mv IS b32--9(1947) cf iven C A 0 . . . ~ ; , ; g f ll 4h f i l ti it b W w or su aremirc ao ca on e prem. o to S m *P 00 was usbi as * culkmite mind wAs found to =1=113 b f Wt f h M a rom t a#nt watm y wt. o e * % of a Pb dnmWng pLant. -h 11. Z. XAMiL :41 410 00 CCAMP&C ATION L 491003 oit aw v4( vj$ir ;i -r-T Y -6" is M3 0 Lt 0 0 0 It OF 44 1 a it ;WA ali10C a.. Lt, 71 S4 AM I 1 0 rw 0 4 4 1 w Is 5 a a I v 9660640*66900040000 -00 so '00 .00 00 -so 'so .00 900 "0e *0 .700 so 100 goo 0 0 0 0 0 0 0 9 j , IT ill of f 111 f ffifflil. 11 A r -1 It -1- ON W U. _W LT 6 A 1- 1, i_ B_ 4 j it -1 A 0 _A_1_ 0041 eil A I!; use 01-0-Cpa4ul Yu. Lur I N, A, MIOWWA. Z,;=,; Lbl-U- MW47t14Ar-Fxp1*, st" show IhA a dil of m CO: 00 . . , l d b kW b f "I b 00 an Cu ma ts can e cnr y tuems o ra tts y 'about 40 titnes or umm. The io" of metal in the total cycle of abiwints AM ftig"Mation awounts to 1-2"'. It h prvisible to uqe catiostit" for quAnt. Repo. of dimpho- ittis- raef4is frora Anims 4rvi nitrissinphOrrk catkins by 01 a"whirig theta with rationite and then fttg. with allkall %atill. In thi's minner it 6 possible to iwp. Sit, Mo. W. 00.9 Zu, and Al from all the ekarienti whkb fom bask by- h h ich temAlms wit the dmakles (Fe. Cv) sisr! (mas As w 0 This ifiethas] hu the ad- 1,11111tap when campand with the um of stka hydroside for the Repa. bftwm it eiiinintes c"pla. and sn.,kes possible a qtjxnt. salm of thir amphoteriv mrfatA. 4111- It Z, Kamis-h 411 NAAA ------ - - Asst.* SITALLMICAL WISFAUM CLASSIFICATION 9 1.10 -d Islas, .10 04, 0.4 ills 51-5._~F- *14411 ag GNP All U 41 ,bit :::n4ite m an it Nan T!Tr 01-0 -0 0 0 0 0 0 0 0 0 61 0 0 0 0.0 0 0 0 0 0 0 0 0 0 0 : : : 0 0 6 0 0 0 0 *Jae _, TI-00 N, 00 00 00 100 ve 0 ago t!9 0 too . M NONN 9-: 0 0.0 :17r;Tz~" 0 000 4l tit A yet 0,111111unk trio" g 010 A ogs *0 A Ir o 00 :*0 sew sew Z A.G -Acpllv.t~ u a Ad IN Al 0 2 -A tree of Wv&mlj%:-4 Im titif maylls of mto. Yo-yo. Lar,,t and S. N. Steknovick. Zffadsbeys Lab. 13. 8W-3 1=116= ); d. C. A. 42, 448U---Ca,,v.7= ,k AWnste Ca and Mg in lewtr wattr, Ead. Ca and Mg are f by a"m LOWIlLesta. 190 dw Altrate with 0, FN"94201 (methyl Omage bm~mtc~k- Gemv A. LAwidn a is 4141 N-4-6 W A-A.-Ask- -;p 0 ~ee ILA AITALLUNGK&L LOYFRATUME CLASSIMATMON J .1113113.9 alkill CA out tit =4-0- U 95 AV X:' 43 V ZA 1A I I a rw 0 ;g Of t7 It If (v 49 K a x 91 it ty el It OT"Some *goo!* 0 0 00 0 0 0 0 0 0 * 0 0 0 040,4e, q!oo o o e so o 0 0 *0 sees so* *000 *Cs 00000010009*0 0000 Gooo* 0000*00 goo coo c:4 a too* Fie 0 lw*ol BABKO. Anatoliy Kirillovich; PYATNITSKIY, Igor' Vladimirovich; ALIKARIN, I.P., reclaktor; DYMOY, A.M., professor, reciaktor; LUR1YH.-M&Ajq-... professo , JAM I redaktor; FILIPPOYA, N.A., redaktor; Whal I S.. tekhnicheskiy redalctor [Quantitative analysis] Kolichestvannyi analiz. Moskva, Gos. naqc1tao- tekha. izd-vo khim. lit-ry, 1956. 736 p. (HIMA 9:11) 1. Chlea-korrespondent AN SSSR (for Alimarin) (Chemistry, Analytical-quantitative) LUR I YE 9 YU. x YU Prq~. USSR/Chadstry - Awaysis Chemistry - History PAW 1947 asoviet Analytical Chemistry for Thirty Years rof %j Ai Klyachko, FTef 1-1. L. Capele- vetddy, Prof &U# rw Lurlyep 91 pp *Uvodakaya Laboratorlyaw Vol X1119 Do 12 Analytical chemistry developed foom the science of applied chemistry Ww served will In the development of the indu tries and agriculture of Via Soviet Union.6 Article presents general,jacts concerning the development of national econmy and analytical'ahemstry In the SZiiet Unlong, and names saw of the people most responsible for the remarkable development during the Soviet regime,, Last part of the article consists of a general discussion of the futuro of Soviet analytical ChemIstry with respect to further indus- trial achieveaents* Greater development of now fields such as nolecular physics, elec- trcn opticag radio chandstry, geocIi=jsU7p etcpq J~- fecommuWa PA 36710 01W V V 9 1 ;;;;j;;OwwqqO9'**OOe 1 : 1 9 1 d I # 6 1 4 A's.jL-A M -I-A-.L - A- 04? A 4- A oil 0* 0 e 00 me V~ i 00 of oil a k; ti. 4"F_w_w_1(w A Now Vark" of OW CYMSIC Uedwd of t1w DOW- maywka=,L (in RMIM) L B. Gwburt and U. U. Lus ' zovodskuva Woratoliva (Fac- m -545. tory LaboratdFy v. 13, July 1948, V. SU Discusaft a new variation of the cyanic metliod of phatocolorimetric determination of molybde- num, with applications as a reducing agent for potassium Iodide- This dam not differ from the old method in application to stannous chloride, in respect to degree of sensitivity and ran e colorimetry. but does differ In having a r period of coloration and in degree of stability. AIM-SLA OCYALLURCKAL UTFRATUR2 CLASSWICATION lee lee see Zoe goo go* got too too U AW;10 As 4 4 ; ; is I't tc ILI-FA a 3.6 1 *1*; 0 0 0 0 0 0 0 0 4 0 0 0 0 0 0 'S 0 49 0 6 0 0 0 0 a 0 0 0 0 0 0 0 :1: 0 0 0 0 0*0 0 0 0 0 0 0 0_0 0 e 41 0 0 0 0 0 0 * a 0 0 0 0 0 a LURIYE, Ya. Yu PA 3/49T21 UM/ChemisU7 -,CyAnideso Determination of Aug 48 Chemistry Analysis 'Teternination of Small Concentrations of Cyanides In the Presenee of hibibiting Substances#" Ya. .Yu. Lurlye, Z. V. Nikolayeva, Inet Vodgeo, pp 'Zavod Iab" Vol X:LVj, No &istIng methods of analysis cannot be applied ,,to determine cyanides in dilute solutions .containIng slWle and complex cyanideep thio cyanides, sulfides, organic conpounds, ate. Authors describe their cnin method. 01*-:NNN:::4111*111110111101111 -'a . I"- - , k 4. - %. -A'. t 1 4 1 11 1 7 It 11111044 fill, liMSTIP-11-Sau W-0 I,_v is" I J .ptmt--,-. 015"#$I1$ Also I'llef-for'll -.09 As is wt4lytk,4 tAirmi 00 A Vu. I N. A. Fill~mlvia ifilli'le lost- -Ndn-I'mt- -114 "R.). 14o; shira, 1.4, 14, IfW71)(INJI); re Sol- s 0: armspla. wrle rim- clutford with phrocalic "tilittile Widmit 11). The hallow- Wit me x. mm t* mlialle t (I ~ Zn %,%I At (total Pas Ity wkvik%v e%tn, Willi NAUIl film tho Nlf4'-ftatld. anAll-mille. 12) Mi ati.1 Pki I"mil As Ity pa"ing thIrvilu. limpulth It'- -00 001.1, 14III-ills, 1.) itivemb q4 0114 %% .4111 &tilt Moral 002, "Oh d& 110 W) Ito liml 01 to 1% tilt 1&4-A1%4 11% wsha, th""Ish k VASIMIllis I'S #411-41) lo..111 that) 00 eaq. lit with I q K I mAtt. 144611fivol with flaM), I's give 0. 1 X cimmi.) viat-I tfrtg. ruhmirlottirkally. (4) lit froon Wit as thialcyatittles by mOmill it( ej(iAxkht laroville4l tilt thiij;l VYAIIAtf MIMI. Is VIL.WtIV 11"v; it Bill Ill lot 140 IVIIIAIII It 'iflifirdill Allil, 14 rjl 11 111161WAIII0, the 411111, 4#111 410 11191 Ce 0 0 1111 j "Ifirlt. $11(millf lor it have 11,411 .14114 Ito to- $4141. 01111 :1 0 0 Mile fit I, partmisottale, (tit omen. shoulif lit- hatlow fllv'~ Anion-raichmille elptit. weft Cosailucttit with austatithur 0 its late, Ill Atilt torlIll, N 0,- 1'% frifilml to 11,110 C-111 ISO VXtIl- "%Ill NA(Ill .11.1 a I Insolvil inlav the filtrat is iieutral tior Alk. IKIIII. litivo, lit thV .4 M I, '11W.1cl,mily it ... 0-1 "Iltv lit ml -trld t,1111 h folUtINI Ill 11,111f), Whis'll J111I.I. IN) file Allklifile Aftilill, (folll WhICII if 0,411 Ile CX(,I, 'With it,*).. Cf0,-1t%ALmmtj4.d Ill All .641111t .... I.tv-d ..hl. -ally V"'. 1. f1w k"'1 by CLFIJUnitC (MIS a MAII. U fill 1-12 Mika CAn be extil. With "A" 11 1 ill, 1,11, 2', N~o Ill -N I's flat- pyr.- Pro! 2,-o Na0l I itolit. To Step. CrO4 lit "ni. Ili Oil" -4 01.11tv acid. :i'l 1-11-mrijOr'l it'All IICI -Ill" tbctc -I firtsurt Ni which Ni;Cr Islas hish Isimm the itintsioniocal alotil rl" -1,11. 'it 'S" films' all ~~ ell'I'liti(MIS 11CCA1111' IStairs limmigh 1110. 111i0illir, Will 4 11fl.11) 14 IVV[hytlllli N. ill mle v%f"It, 1*,I ~J, lit (f", CIS all A'v twl'arr the 210 Atill Jail fillf,iliml Iss, anialue assay Co V4111CI& CIS: lit a, .%, 111001 t, im1ple all Cr,'- "ll-I Ott. Calls 'Willi N.14114 III flat lairsvilce Ili I N11011 to,limtav,all Cis Q!~ 4 paime tit IllimrallAir Ili I% %mi-JAC('Wily Lb*XW Wall It voillplet. pA.. 01migh 4111~,Jjllv, I'Al. III from Am."Mr Willi ~Wift Arvi untlaitiorlwal VA". ; the AIWxkjL,mW v acI. all 10 1 L A41ALLUJIGICA1, 1,1710011111 C&ASSIFICA11001 IL V- to 0 to 1 -- - --- - - , , :_ -.'T - too. W.4% VIL,J) ISIS a., I%. L__~ IQ U Is AT LI 9 to it to a of a at IS; a n Ct a it Sol J?AD A' is. Mr me a a ova: 0 0 0 0 0 6 0 0 0 0 0 0 0 0 * 4111, 0 0 0 0 0 0 0 0 6 0 0 0 0 0 * 00000600000 0 0 4 ~ *1 0000 1111, 0 41111 -2 00 *0 0, 0 -0 a w W-W -0 w w W-W w,- oil un us Mv assil Q4104;no 0 Now variadon In the thlocyanate determination of molybilintsca. L, B. Gint-burg and Vu, Yu, 1, ' Z rod lkaya lAb. 14, of .00 sample In 10-111 nil. of aiju.i rrgi,i. To the w)ln. add III mi. of 18N 11,9). and evap, to funte-e. Cf,ol. add 23 mi. 01 water, and hoil (,) olkiolvir all ~tilfatvc DiLtolf)(Iml, ; ::o 0 in a voltimettlic 11A.A. mix. anti ki-vaii.0i;Iwit coti(j. WIN'- mi. of Mik. Tran-I'vir to a gradual,,,I rylindt-r. r* 0 Add in the follo%ing v4pieuve, I11WIIR after Pach mldn., 35 mi. of 3 N IICI + 3 int. of KCNS iln. + I X, zoo KI + Unlof freshly prvIKI. 1% NUSO, "III). Dil. 10 'A itil. -,IIt N IICf anti after 10 min, measure the color at 520-560 mp. Rian a blink un the rragrnts. G. Af. KowbiwifT go* Zoo J NO 0 1--oo AIA-SLA A(TALLURGICAL LITIOIATUME CLASSIPKATIC11 ::O0 too 410 ;00 117 it i -T- r -1 IF I IF 3 1 .71 41 L 1 41 400 ;0 11 it x St K t( It C1 K U If It N KLa It 1 %4 0 0 0 0 4111,00 0 0 0 S., e so 00 0 0004 00 0 40 0 00 0 O~ 0 TO* 00*0!::: :::: 00 000 00 0 0 00 ooo~oo 0 0 0 Is sociliti AND '690,999000000io 10 . - I . ~- i~ . -~ :1 - - - 0*00000000000000000 - ------ 4 11 le It it 11 M is 14 V 4 0 It u a ii ha va -16 a 11 32 a M is M V is 0 a a 4 IN Vt. Mu "I M-1. 0 4F 1 00 V *eCIMI AND FROW11411t .bit 06 A ; j)*ta. of saall conene of cynanides in go ' U 6 00 110 1. V. NdwIseva. Zataikayt; Lab. 14. Y' OR tow cyanide content by PPtK. with 09 a -1. 1kxNOi,. and tmtbis the ppt. with witer and so disq. into 1% XaOll. and i1ttIC. the CN content of tile dilt 1l ith t W l a e t er i Innetr" 1y tw, .04~itrtetricauy with thcC%' p4rfivowidsolu Tattet irrocitatk%itti te 00 . . I p I., expel the JICN by COt awl rillett it lit a receiver Mit4. it 111CAUS"d Vol. 4110.01 NI twil. filitowril 11V 4. - 100 he revelyrr nuitjl. a known vol, I)( otandard N;t,,Vh. I ' colilents L4 the 2 receivers are emillwly Iflitril mid OIC 00 CUM" NAISA Is litrat"i with 0.01 'V I IMArt. Ilftmlt tile 00 4) i diffiretrier between the tOtAl CY311141C XMI the simple Cy. 06 4 attide, the cotitent ig complex cynnide i% known. , W 00 st k t f4AUNO .1 1 ~.j At U S 0 00 LAI L S to nd 0 14 0 111 ita At Itax% n(atent Ica 4 1 :14 4M 0 P000001000000*00000*44000*'Oo*OGOO*OOOOOOOOofe I ! 2 ! OTIS@ 0 9 0 0 000000000000.0010000-*oooooeooo*oooo 0 1.00 -00 -00 -00 -00 .00 :Go 0 zoo to 0 40 X0 0 see to 0 tgo 0 LURIYE) YU. YTJ- PA ~~USSR/Chemistry Analysis Feb 48 Chenistry Sorption "Various Methods of Utilizing Chemosorbente for Analytical Purpbses,." Ya. Yu. turlye., 2 pp "Zavod Iabu Vol XIT, No 2 Describes own method, in which liquid tn be analyzed is mixed with sorbent instead of being filtered through it as In Yao M. Kbotrikin's method. FAItors ask laboratories to report on their experience with both methods. 4/49T16 [000900*0*000000000 004 I C 0 fF 6 M A L it 0 fu I to- "ma OOC 0 99: OOK o ON 4-4-0 : - 3, m 39 &D At 4? 41 U AS, 0- Oly I$ n Cl 1101MIdISM) 11-11,41111 00 0o - Poe oen piivlnqwl pug paullp aig w3w(l ul aAoqv -00 C. **--I 04) JOj 11POInaltu 2uflglxa gaz.(Ivuv A3A!jvjlydwOj 'OC-IZ *d lot6l uvr 191 'A '(AJCrl*J 00 1 00 001 1 pug 10,1-1 nA mA (vel-11 tq) ."lWalixual 00. -aa qsnumm la rpqlan ilipwl"a III u9pallsajul 00 9 0. 00 0 300 00- 00 0o go 120 fit 14 if if m fj It 00 0 00000 0 0 0 0 1 i Ve a a 1 0 0 9 0 * * 0 0 A 9 1: 00 * * f1lotilliv I? _W AA I f. A 1. It L. 004 Iiiq COQM PAGM05, A-S PROW11) -A it Materials in AumlYdeid to Application of Ar Chemistry. IV. Determination of Satfar. I'h-Ph-- "s, and Armair in I'lickel and Co P". (In fliumall. j Yu. Yu. L ud N. A. Filipliova. mv0(bk4ya 1whimi- r U&iratory). v. 15, July 1949, p. T 71 - 711! Develms ronditions foralm"tion (if Cumid Ni freim wrakly acidic solutions. thus petimitting determhuttun !go of S, P, and As in these metals by well-known nwth- 0 ods. Two variatiom of the miorimetric detennination 0 (if As and P are descrificti. Tjpical thtj ATC WHIlAt(A. A I N - I L A SITALLURrICAt LITZ44TOC CLAHOKAMPI 0 U 0 'AV 10 is It or K K It It It .304, An L 0 a ---- iii- 14 1 a a 3 a V T;;& dh 0 40 0 Joe too goo Ob --ds d mbrimeriel Modkob of DOWSWAC Slatuth. Yu. Yet, Lur'o and L. H. (.'intburW (Z4md. Lab.. IWO, 14 (1). 21-M).-lin flumianj. A iiDiupwixem in madle of the K 1. fbo&mide. and. thiourea metho& of eolori. metric quantitative determination of IN in the presenoe of 1%, 8b, So. As. Cu. awl Fe. l'be fireel: methott in dencribetlb wo others in detail. A vk4et-light filter with intex. pLnne"ty 1=4=1400470 mg. Corre- a nuling to mi. extinel"i by BI-compkim is used in all throe meth,xis. "n, tC I(otionafetelounA Hi-complexes occurs In 1-2,V.H2N4)&. 1-3-3' Y-If SO &M 0-4-I-2N-H.XO,. respectively. TIw sensitivitka of the three meAZ dercetreseecin the *det x 101 y1cme.l. whom y is the coneentration ~~ thickneem of cielorimetered layer (cm.); the ranges of rerrew