SCIENTIFIC ABSTRACT RYSINA, N.S. - RYSKIN, A.I.

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• Collection: Scientific Abstracts
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• Release Decision: RIF
• Original Classification: S
• Document Page Count: 99
• Document Creation Date: November 2, 2016
• Document Release Date: September 26, 2002
• Sequence Number: 5
• Publication Date: December 31, 1967
• Content Type: SCIENTIFIC ABSTRACT

Problems of Physical Metallurgy- 983
Card 7/8
17 .

Problems of Physical Metallurgy 9193

S,

~/Eng ee-Ang'-,--Modu'bIb-`6f nidri
Ai bolii~co V
Pub 22
N.
Rysifia

~-irig~;adirdj pera ur"--'d
Effect'.of.bdlb t e---~ epen ence-o
-
o6n diepli~6 nt~,
od
. ..........
Per odlicai.;

i er ~the-
f ng~.~a
Experiiu Atempietature.,-,- eIff e* diii
oy -dc-sc-
on them hardpess s, i Hb

rith 'the-'hel
-co t -,wit on.a oys-t ,4~vacuum'furnace:ii
'
~

.--~ eml hte
iiAi~~e-,regxi o or
torsional~ a anee And-
elictron 6
b 1
,
a p;-,-~~grap
tii
Ineti ti6n
of'Mit 2:the': Ceht*r
#C66~,Of
6
illurg
,
cie C: s u e ~~o ei-r6lis:~ Met'
hun . RO, 6ii6fi
s
Presented;~by Acdd~~i6ian-.d.- ~,-V-.'~:Kur-dylm'ov',t-IU~--:4-:'--19'54

1~064
'AJ)
'742/62/000/690/006/021
~-IO15/I215,

AUTTIORS
:Rysina, T,.N.,~lsevelevap
,

TITLE: ~Offs
The transmission of plutonium to the
Pizing

~ :SOURCE: Plutoniy-7239; rasprodeleniye, bio'lbgicheskoye

at.
d
ey viyd

uckoreniye vyvedeniya 'Ed. by A.V..,.
Lebedinski Yu.I Moskalev., Moscow Medgi
y and z
1962,:'41-44
' '
TEXT:
. the
The problem of the: transmission of plutonium from
inlaternal o)-onnism to tho-offopring.during pregfiancy as well a's during
1~LctaUon nsufficiently studied, xperiments,were carried
has.been i
out on 17 I
puppies of varyinj!~. agesp "which-were boni at'different t i6e, a k
after the -administration of. plutonium to do s.- Plutonium nitra~te
was.adrain istered i.v. fo r times -at intervals of one month*,,,,- The. t6talL
u
Pu 'The liver and, the.bones were~ examinedfor:
done of was 0 2p(4kg b.w. ,,',

-Card'1/2
-6.
4

k--.T

28242
S/581/61/000/000/013/920
The distributibn'and ~excretion. D299/D304
,.animal's~weight Plutonium distribut ion -was' studied . 3 '6 - and 11
months, ..,and 3, 3.5,,and 4 years. after,its lntroduc'tion.~_ Bothlexpon-
escriptio
ential and:Power mo'dels:'were usedlor the .mathematical d n
um n the body~, tissites and excreta, ,,but,
o " Ethe behavior of plutoni i
the,exponential - method was.'f ound- Ito conform best with thc.experi-
melntal:'findings. ~: MathematicA calculdtion.of the-.ekpressions--was
accomplished by the method-of,l stributi'l
e ast, squares.; The' di 01 of
Pluto elbody is shown in tabular and, orni, broken'..,"
nium in'th graphic f
down into,skeleton, liver,sple idneys'and'
en, muscles, lungsi k other
t,?j ~,organs,',at the various stages of investigation. . The distzibution,'
.tai ''Yas , as follows: 'skeleton,40% .,,:liver .307*, muscles 12.476, spleen 2--3%1,
.Z,-,tI Irugs 0.450N0, kidneys 0.36%. -In all organs radioactivity decreased:
'with'time.~ In~the spleenit dropped to 0.4976 by the:600th day and,
in the kidneys,to 0.1276 by the.1000th day. :.Subsequently the~pluto-',
nium content in these organs remained c'nstant.,,.The data from the.
0
excretion :0f.plutonium is broken down into 2.lperiods:.'I) 2nd-23rd
day, 2) from the 23rd.day on,7ards.-For the first.3 weeks plutonium
--reti-on-with the stools was higher,~than excretion with,the urine.j

30352
S/205J61/001/004/011/032
The excretion of... D298/D3031
and xanthine (average of 007 mg) was found.in the urine of normal rabbits
Irradiation of the. rabbits led to anAficrease in the. excretion of these,
substances with the urine., The effect depended on the radiation dose in:
a range of 50 to 300 r, The,maxi- level of,oxypurine excretion was
reached on the first,dAy:after irradiation at 50 300 r and on the
second day after irradiation in a dose of,1,000 re The increase 'in the
excretion of xanthine and hypoxanthine at eairly,states after irradiation
was'obviously,a consequence of the disintegration.of,nucleic acids and
further oxidation of the purin* nucleotides which formed, with their mini-
Mum u s e fo rthe synthesis of high-polymer compounds. These results are
gs of Western and Soviet researchers. The,
compared with the, findin
heightened xanthine and.hypoxanthine levell.in the urine on the second day
was probably due to intensive,lesions and late.restoration of nucleic
acid synthesis, especially the synthesis:of deoxyribonucleicacid,-under
the. effect of lethal and , sublethal. doses -of radiation. .:R. Ye . Libenzon.
helped with scientific direction of, the research, while N. M. Nilmlina
and.R. N. Zakharova helped in the:experiments. There are I table and 19
a
rd,2/3 J(

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REF
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ACCESSION NRt AP4038932 Z/0017/64,/053/006/026.5/0267,
AUTHOR: Ryska, Zdenek (Docent, Doctor in engineering)
TITIXs Highly ref raotozy ceramic materials used in electrAhermics%
SOURCE% Elaktrotoohnio ky obzor, v. 63, no. 6, 1064, 265-267
TOPIC TAGS:. alurainum oxide, magneeiumoxide, silicon dioxide, thorium dioxide,
zirconium dioxide, beryllium oxide,' metal oxide, ceramics, ceramiomaterial,'heat-
resistant ceramic materials refractory onramio material, electrothermics, electrical,
hoat production
:ABSTRACT: The present article is a continuation of a.previouastudy (Slaktrotech-
.nicky Obzor, no. 5 (1963) page 247) and . pertains - to highly refraoLtory ceramic
materials which are usedin elootrothermias and'which have been recently finding an!,
nver-increasing application in rocket and,atomio engineering. The primaa7-indices,
of these, materials, which are. used, in.equipment. operating at high vaouums, suoh as
that in oil diffusion pumps, i.e. Ix 10-9 mm Rg, 11 ~ 10711 mm Hg in mass
and 10-14 ma Eg in measuring equipment,with photomultipliers. ~The.new areas of
application of,these'materialelpermit.a,wider,use of-elootrio heatsouroes with
high temperature gradient (eegeeleatria.,aro, plasma, eleatronio heating)e The
Card 1/2

oil@) (Raman. effect)

Al . . . . . . . .
is 11 11 11 W n 16 it
1-4 _"imliji 'In' is it V a M n U U W a H U U al U it
[it tNp..l.~G 1.0 'kV al. Elul.,
00 .6"issal
Mixed 4aolital 61 u; and their "molecular
00 A Compounds. W. - The .17:110f certain ketones on
a
btyl *Wum Iodide In other solution. V. M.
u"
t a'0'
To'
T.I." atov and A 'chuk.- J. GeR Chrm.
S. R.) 9. 1 cf. C. A. 29. 4'p4R'.-
_ hm
Th reaction of BuOhIgf (1) wilh p-.%IcC.H.COI'h (11)
rS;, R
Th (n
0renone (111) and dibenzalacetone (IV) in ether wa;
00
rr at b,
rried out by the metbod prr7iously dc%cribed. Of tile
/it, only
00 jri,:~ ketones only 11 gave s mall. compd. with Nig1j. III anti
IV avacteat in the same manner aa,; ahlehyd" anti benril
to give mol. Cmilptis. with 1. 1 (0.1 H1411r) with 11 (41.15
Os mole) gave 24% yield of 311AKIS. _ III anti IV -with I
under the same condit ions maire 111.1. oranite-brown (80%
yield) and IV.I. yellow-brown (88% yield). rrsp. -The go 0
00 bitter, decompd. with dil. H.SO., gave BuOll and 9A 51'
IV_ John Li.~
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Practical Work in Organic Synthesis 614
Part I. General Procedures,
1. Distillation
~7
2. Extraction 27
3. Crystallization 30,'
4. Determination of the melting,poiht 36

5 ublimation
S
39,
6. orderof completion of experimental work by students.
Instructions for keeping records
, 40
7. ,
Instructions for laboratory~work 41:
8. special precautionary measures for certain cases 41
9. ;chat to do in case of fire. First aid in case of
ac,d-idents
Part IT,' Synthesis, of Organic Compounds
1. Halogenation reaction 44.~
Ethyl bromide 51
Ethyl. iodide, 52
n.-.Butyl bromide
2
1.2-Dibromoethane 53
Bromobenzene
54
Card 3/8

--------------------
'Practical Work In Organic Synthesis 614
2. D6hydration reaction 65
Ethylene-
'Cyclohexane 58
Isobutylene
58
Isoamyl ester 6o,

3.
Introduction of nitro- and nitroso group 6o
NItromethane .66:
Nttrobenzene ~67
Dinitrobenzene
o- and p-Nitrobenzene 68~1
P-Nitroace
tanilide and g-nitroanilide -69'.1
,
4-Nitrosodime,thyl aniline 70
4-Nitrosophenol 71
4. sulfonation reaction 71
Benzenesulfonic acid 74
Benzenesulfonic chloride' 75

Sulfanilic acid 75
Naphthionic acid. Sodium naphthionate 76
5. Synthesis through organo-magnesium compound 76_,-,_
Dimethylethyllcarbinol 83
Methyldiphenyl.carbinol (from magnesium bromylphenyl
and acetophen.one)'..
Card 4
V8

Practical Work in Organic Synthesis 614:
Methyldiphenyl carbinol (from m,agnesium:bromylphenyl and
ethyliacetate) 86
Benzhydrol 86.
Triphenylearbinol. 88
6. Oxidation 89
Formaldehyde .94".
Propionic aldehyde 97
n.-Butyraldehyde, 9T.
Benzophenone from benzhydrol .991,
Benzaldehyde from benzyl chloride 99
n.-.Butyric ester-of butyric acids .99,
Quinone (bentoquirione) 100
Oxidation-reduction reaction '101
Benzoic acid and*benzyl alcohol from benzaldehyde .102~
Benzyl alcohol 103
Butylbutyrate from butyraldehyde 103
8. .
Reduction 104
Ethyl benzene 108.
Benzhydrol*
109
Card 5/8

.Practical Work in Organic..Synthesis 614
Aniline 109
Azoxybenzene
Acylation.reaction
Ethyl,acetate
Isoamyl Acetate 115-
Ethyl ether.-of benzoic:acid 1i6
g-Pentaacetyl glucose 11T
Tribenzoyl glycerin
Acetanilide 118
10. Alkylation reaction 118.
sec-Butyl benzene
Benzophenone ( from.b,enzoyl,chloride and bf_.mzene) 123
om benzene.and
Benzophenone carbon tetrachloride) .124~
Acetophenone frombenzene,and,
E acetic anhydride)
Acetophenone from.benzene and acetyl chloride)
Triphenylchloromethane (from.benzene and carbon.
tetrachloride) 127
Ethyl benzene (according to the Radzivanovskiy
reaction) ~128"
Ethyl benzehe.(according-to the Fittig reaction) 129,
Card 6/8

Practical Work In Organic Synthesis 614
~11. !Condensation:
(ethyl acetoacetate)
Acetoacetic,,ester,,
,
Clnnamic.acid*'(according,to, Perkin)
Ethyl ether~of'cinnamic acid 139
Benzalacetone i4o
Benzalacetophenone
Benzylaniline
142
Fluorescein
Eosin ':~l42:
Malachite ~green 143
12. Ref ormatskiy ~ reaction

I 'phenyl-,p.;-4ydroxypropionic:aeidI
Ethyl ester. of
..

13. ,
.
~~~Diazo:compound reaction with
Diazotization
reaction.
-
,
I separation of nitrogen., Nitrogencompounds 146
Phenol
155
Iodobenzene
Diazoaminobenzene 156
p-Aminoazobenzene
157
Helianthin -157
Card 7/8

GHUKIIN, T.S.; ASAKEM, D.Zh.; RYSKELDIYEV, A , otv.,red.; ISABEKOVA,A.,

ptiKa
IaI i7*,-,fttii- il-e-a- s~"u~,-ii
re o -~z;rti
er
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0 m,e-n-s on a:.

op-ticai:, ti be ro
iiel:.ct ro4op Iti ca
to,~:receive~,-,, he
ar range c1 2.n.-.-

L i9481-63 AFFTC/A5D/1JP(G)/5SSD- JD,
ACCESSION N'I: AT3002230
257/0200-
S/2941/63/Wi/660/0
RS:. -,Tolstqyi-N- A
AUTHO, kr~kin, A.' I,b
4-~
Z
TITLE: Excit ati on nM~~phonhors n
SOU'RCE: Optika i spektroskop ya;"; i~6r
s nik statey.-*. lt Lyuminestsentsiya.
0.
L963 257-~6
1,1103COWS Izd-vo AN S35RP P
T0111C TAGS: excitation ~interaction,;dipole transit ion oranee band, absorption
+
MILCT - The energy transfer.process of,M
0 STE n ions in ZnS-Mn has been studied.
;~The assumntion is made that at low temperatures xcitation energy occurs In
~this e 4L
blue centers (spots) lying on t1m periphery of interaction with the Mn2+ ions.
The radius of this interaction, Rk, is designated as. th e ratio of orange band.in-*'
ccd by Yin2+
tensity (produ ions) to the integrated light intensity. Values of R
are tabulated for.various annealed phOSD
hor specimens. It is shown that dl ole
-ers exists
sitions between -blue cent
dipole energy trans only in: a region of A.
Apart from dipole-dipole energy transitions, probability of interchange transi-
'tions depends on the extent of blue centers; large magnitudes of the latter.beini
cormpensated for by small magnitude, overlapping, integrated spectra of radiation
-calculation is made of the distance R between blue centers a
and absorption. A nd
Card 1/2

Problems of Physical Metallurgy- 983
Card 7/8
17 .

Problems of Physical Metallurgy 9193

S,

~/Eng ee-Ang'-,--Modu'bIb-`6f nidri
Ai bolii~co V
Pub 22
N.
Rysifia

~-irig~;adirdj pera ur"--'d
Effect'.of.bdlb t e---~ epen ence-o
-
o6n diepli~6 nt~,
od
. ..........
Per odlicai.;

i er ~the-
f ng~.~a
Experiiu Atempietature.,-,- eIff e* diii
oy -dc-sc-
on them hardpess s, i Hb

rith 'the-'hel
-co t -,wit on.a oys-t ,4~vacuum'furnace:ii
'
~

.--~ eml hte
iiAi~~e-,regxi o or
torsional~ a anee And-
elictron 6
b 1
,
a p;-,-~~grap
tii
Ineti ti6n
of'Mit 2:the': Ceht*r
#C66~,Of
6
illurg
,
cie C: s u e ~~o ei-r6lis:~ Met'
hun . RO, 6ii6fi
s
Presented;~by Acdd~~i6ian-.d.- ~,-V-.'~:Kur-dylm'ov',t-IU~--:4-:'--19'54

1~064
'AJ)
'742/62/000/690/006/021
~-IO15/I215,

AUTTIORS
:Rysina, T,.N.,~lsevelevap
,

TITLE: ~Offs
The transmission of plutonium to the
Pizing

~ :SOURCE: Plutoniy-7239; rasprodeleniye, bio'lbgicheskoye

at.
d
ey viyd

uckoreniye vyvedeniya 'Ed. by A.V..,.
Lebedinski Yu.I Moskalev., Moscow Medgi
y and z
1962,:'41-44
' '
TEXT:
. the
The problem of the: transmission of plutonium from
inlaternal o)-onnism to tho-offopring.during pregfiancy as well a's during
1~LctaUon nsufficiently studied, xperiments,were carried
has.been i
out on 17 I
puppies of varyinj!~. agesp "which-were boni at'different t i6e, a k
after the -administration of. plutonium to do s.- Plutonium nitra~te
was.adrain istered i.v. fo r times -at intervals of one month*,,,,- The. t6talL
u
Pu 'The liver and, the.bones were~ examinedfor:
done of was 0 2p(4kg b.w. ,,',

-Card'1/2
-6.
4

k--.T

28242
S/581/61/000/000/013/920
The distributibn'and ~excretion. D299/D304
,.animal's~weight Plutonium distribut ion -was' studied . 3 '6 - and 11
months, ..,and 3, 3.5,,and 4 years. after,its lntroduc'tion.~_ Bothlexpon-
escriptio
ential and:Power mo'dels:'were usedlor the .mathematical d n
um n the body~, tissites and excreta, ,,but,
o " Ethe behavior of plutoni i
the,exponential - method was.'f ound- Ito conform best with thc.experi-
melntal:'findings. ~: MathematicA calculdtion.of the-.ekpressions--was
accomplished by the method-of,l stributi'l
e ast, squares.; The' di 01 of
Pluto elbody is shown in tabular and, orni, broken'..,"
nium in'th graphic f
down into,skeleton, liver,sple idneys'and'
en, muscles, lungsi k other
t,?j ~,organs,',at the various stages of investigation. . The distzibution,'
.tai ''Yas , as follows: 'skeleton,40% .,,:liver .307*, muscles 12.476, spleen 2--3%1,
.Z,-,tI Irugs 0.450N0, kidneys 0.36%. -In all organs radioactivity decreased:
'with'time.~ In~the spleenit dropped to 0.4976 by the:600th day and,
in the kidneys,to 0.1276 by the.1000th day. :.Subsequently the~pluto-',
nium content in these organs remained c'nstant.,,.The data from the.
0
excretion :0f.plutonium is broken down into 2.lperiods:.'I) 2nd-23rd
day, 2) from the 23rd.day on,7ards.-For the first.3 weeks plutonium
--reti-on-with the stools was higher,~than excretion with,the urine.j

30352
S/205J61/001/004/011/032
The excretion of... D298/D3031
and xanthine (average of 007 mg) was found.in the urine of normal rabbits
Irradiation of the. rabbits led to anAficrease in the. excretion of these,
substances with the urine., The effect depended on the radiation dose in:
a range of 50 to 300 r, The,maxi- level of,oxypurine excretion was
reached on the first,dAy:after irradiation at 50 300 r and on the
second day after irradiation in a dose of,1,000 re The increase 'in the
excretion of xanthine and hypoxanthine at eairly,states after irradiation
was'obviously,a consequence of the disintegration.of,nucleic acids and
further oxidation of the purin* nucleotides which formed, with their mini-
Mum u s e fo rthe synthesis of high-polymer compounds. These results are
gs of Western and Soviet researchers. The,
compared with the, findin
heightened xanthine and.hypoxanthine levell.in the urine on the second day
was probably due to intensive,lesions and late.restoration of nucleic
acid synthesis, especially the synthesis:of deoxyribonucleicacid,-under
the. effect of lethal and , sublethal. doses -of radiation. .:R. Ye . Libenzon.
helped with scientific direction of, the research, while N. M. Nilmlina
and.R. N. Zakharova helped in the:experiments. There are I table and 19
a
rd,2/3 J(

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REF
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ACCESSION NRt AP4038932 Z/0017/64,/053/006/026.5/0267,
AUTHOR: Ryska, Zdenek (Docent, Doctor in engineering)
TITIXs Highly ref raotozy ceramic materials used in electrAhermics%
SOURCE% Elaktrotoohnio ky obzor, v. 63, no. 6, 1064, 265-267
TOPIC TAGS:. alurainum oxide, magneeiumoxide, silicon dioxide, thorium dioxide,
zirconium dioxide, beryllium oxide,' metal oxide, ceramics, ceramiomaterial,'heat-
resistant ceramic materials refractory onramio material, electrothermics, electrical,
hoat production
:ABSTRACT: The present article is a continuation of a.previouastudy (Slaktrotech-
.nicky Obzor, no. 5 (1963) page 247) and . pertains - to highly refraoLtory ceramic
materials which are usedin elootrothermias and'which have been recently finding an!,
nver-increasing application in rocket and,atomio engineering. The primaa7-indices,
of these, materials, which are. used, in.equipment. operating at high vaouums, suoh as
that in oil diffusion pumps, i.e. Ix 10-9 mm Rg, 11 ~ 10711 mm Hg in mass
and 10-14 ma Eg in measuring equipment,with photomultipliers. ~The.new areas of
application of,these'materialelpermit.a,wider,use of-elootrio heatsouroes with
high temperature gradient (eegeeleatria.,aro, plasma, eleatronio heating)e The
Card 1/2

oil@) (Raman. effect)

Al . . . . . . . .
is 11 11 11 W n 16 it
1-4 _"imliji 'In' is it V a M n U U W a H U U al U it
[it tNp..l.~G 1.0 'kV al. Elul.,
00 .6"issal
Mixed 4aolital 61 u; and their "molecular
00 A Compounds. W. - The .17:110f certain ketones on
a
btyl *Wum Iodide In other solution. V. M.
u"
t a'0'
To'
T.I." atov and A 'chuk.- J. GeR Chrm.
S. R.) 9. 1 cf. C. A. 29. 4'p4R'.-
_ hm
Th reaction of BuOhIgf (1) wilh p-.%IcC.H.COI'h (11)
rS;, R
Th (n
0renone (111) and dibenzalacetone (IV) in ether wa;
00
rr at b,
rried out by the metbod prr7iously dc%cribed. Of tile
/it, only
00 jri,:~ ketones only 11 gave s mall. compd. with Nig1j. III anti
IV avacteat in the same manner aa,; ahlehyd" anti benril
to give mol. Cmilptis. with 1. 1 (0.1 H1411r) with 11 (41.15
Os mole) gave 24% yield of 311AKIS. _ III anti IV -with I
under the same condit ions maire 111.1. oranite-brown (80%
yield) and IV.I. yellow-brown (88% yield). rrsp. -The go 0
00 bitter, decompd. with dil. H.SO., gave BuOll and 9A 51'
IV_ John Li.~
00
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a I a. SL A 41TALLUR6K.L LITFQATL;
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Practical Work in Organic Synthesis 614
Part I. General Procedures,
1. Distillation
~7
2. Extraction 27
3. Crystallization 30,'
4. Determination of the melting,poiht 36

5 ublimation
S
39,
6. orderof completion of experimental work by students.
Instructions for keeping records
, 40
7. ,
Instructions for laboratory~work 41:
8. special precautionary measures for certain cases 41
9. ;chat to do in case of fire. First aid in case of
ac,d-idents
Part IT,' Synthesis, of Organic Compounds
1. Halogenation reaction 44.~
Ethyl bromide 51
Ethyl. iodide, 52
n.-.Butyl bromide
2
1.2-Dibromoethane 53
Bromobenzene
54
Card 3/8

--------------------
'Practical Work In Organic Synthesis 614
2. D6hydration reaction 65
Ethylene-
'Cyclohexane 58
Isobutylene
58
Isoamyl ester 6o,

3.
Introduction of nitro- and nitroso group 6o
NItromethane .66:
Nttrobenzene ~67
Dinitrobenzene
o- and p-Nitrobenzene 68~1
P-Nitroace
tanilide and g-nitroanilide -69'.1
,
4-Nitrosodime,thyl aniline 70
4-Nitrosophenol 71
4. sulfonation reaction 71
Benzenesulfonic acid 74
Benzenesulfonic chloride' 75

Sulfanilic acid 75
Naphthionic acid. Sodium naphthionate 76
5. Synthesis through organo-magnesium compound 76_,-,_
Dimethylethyllcarbinol 83
Methyldiphenyl.carbinol (from magnesium bromylphenyl
and acetophen.one)'..
Card 4
V8

Practical Work in Organic Synthesis 614:
Methyldiphenyl carbinol (from m,agnesium:bromylphenyl and
ethyliacetate) 86
Benzhydrol 86.
Triphenylearbinol. 88
6. Oxidation 89
Formaldehyde .94".
Propionic aldehyde 97
n.-Butyraldehyde, 9T.
Benzophenone from benzhydrol .991,
Benzaldehyde from benzyl chloride 99
n.-.Butyric ester-of butyric acids .99,
Quinone (bentoquirione) 100
Oxidation-reduction reaction '101
Benzoic acid and*benzyl alcohol from benzaldehyde .102~
Benzyl alcohol 103
Butylbutyrate from butyraldehyde 103
8. .
Reduction 104
Ethyl benzene 108.
Benzhydrol*
109
Card 5/8

.Practical Work in Organic..Synthesis 614
Aniline 109
Azoxybenzene
Acylation.reaction
Ethyl,acetate
Isoamyl Acetate 115-
Ethyl ether.-of benzoic:acid 1i6
g-Pentaacetyl glucose 11T
Tribenzoyl glycerin
Acetanilide 118
10. Alkylation reaction 118.
sec-Butyl benzene
Benzophenone ( from.b,enzoyl,chloride and bf_.mzene) 123
om benzene.and
Benzophenone carbon tetrachloride) .124~
Acetophenone frombenzene,and,
E acetic anhydride)
Acetophenone from.benzene and acetyl chloride)
Triphenylchloromethane (from.benzene and carbon.
tetrachloride) 127
Ethyl benzene (according to the Radzivanovskiy
reaction) ~128"
Ethyl benzehe.(according-to the Fittig reaction) 129,
Card 6/8

Practical Work In Organic Synthesis 614
~11. !Condensation:
(ethyl acetoacetate)
Acetoacetic,,ester,,
,
Clnnamic.acid*'(according,to, Perkin)
Ethyl ether~of'cinnamic acid 139
Benzalacetone i4o
Benzalacetophenone
Benzylaniline
142
Fluorescein
Eosin ':~l42:
Malachite ~green 143
12. Ref ormatskiy ~ reaction

I 'phenyl-,p.;-4ydroxypropionic:aeidI
Ethyl ester. of
..

13. ,
.
~~~Diazo:compound reaction with
Diazotization
reaction.
-
,
I separation of nitrogen., Nitrogencompounds 146
Phenol
155
Iodobenzene
Diazoaminobenzene 156
p-Aminoazobenzene
157
Helianthin -157
Card 7/8

GHUKIIN, T.S.; ASAKEM, D.Zh.; RYSKELDIYEV, A , otv.,red.; ISABEKOVA,A.,

ptiKa
IaI i7*,-,fttii- il-e-a- s~"u~,-ii
re o -~z;rti
er
di-s--trAbistii
0 m,e-n-s on a:.

op-ticai:, ti be ro
iiel:.ct ro4op Iti ca
to,~:receive~,-,, he
ar range c1 2.n.-.-

L i9481-63 AFFTC/A5D/1JP(G)/5SSD- JD,
ACCESSION N'I: AT3002230
257/0200-
S/2941/63/Wi/660/0
RS:. -,Tolstqyi-N- A
AUTHO, kr~kin, A.' I,b
4-~
Z
TITLE: Excit ati on nM~~phonhors n
SOU'RCE: Optika i spektroskop ya;"; i~6r
s nik statey.-*. lt Lyuminestsentsiya.
0.
L963 257-~6
1,1103COWS Izd-vo AN S35RP P
T0111C TAGS: excitation ~interaction,;dipole transit ion oranee band, absorption
+
MILCT - The energy transfer.process of,M
0 STE n ions in ZnS-Mn has been studied.
;~The assumntion is made that at low temperatures xcitation energy occurs In
~this e 4L
blue centers (spots) lying on t1m periphery of interaction with the Mn2+ ions.
The radius of this interaction, Rk, is designated as. th e ratio of orange band.in-*'
ccd by Yin2+
tensity (produ ions) to the integrated light intensity. Values of R
are tabulated for.various annealed phOSD
hor specimens. It is shown that dl ole
-ers exists
sitions between -blue cent
dipole energy trans only in: a region of A.
Apart from dipole-dipole energy transitions, probability of interchange transi-
'tions depends on the extent of blue centers; large magnitudes of the latter.beini
cormpensated for by small magnitude, overlapping, integrated spectra of radiation
-calculation is made of the distance R between blue centers a
and absorption. A nd
Card 1/2