SCIENTIFIC ABSTRACT SHAFIYEV, A. I. - SHAFRAN, I. G.

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SCIENTIFIC ABSTRACT
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ACCESSION NR: AP4018393 S/0120164/0001001/0.109/0200 AUTHOR; Karaoik, A. S.; Shafiyev. A.,-I..*. TITLE: Counting -rate characteri is tics of CO sub, 2 counters -199 SOURCE: Pribory* i tekhnika eksperimenta, no. 1, 1964, -200 TOPIC TAGS: carbon dioxide counter, counter. particle counter. counting ratep counting rate, characteristic, isotope study ABSTRACT, Results of an investigation of counting -rate 7vs. -voltage chaIracteris- tics are -reported of these Soviet-make counters: SBS-S with an external graphite cathode, MS-6 with a copper cathode, and SBM-7 witha stainless-steel cathode. The counters were filled with COZ at 50-660 torr with a.quenching adn-jxture of ethyl-alcohol vapor at 15 torr. With no external quenching. satisfactory counting-rate characteristics were obtained at the end of~the proportional', region 1~ and in the limited -proportional region up to the beginning of t1k4 Geiser region. CQ: 1/2 ACCESSION NR: AP4018393 (table aupplied) The plateau was found to extend within 10.0-150, v with a 3 or 5%' slope per 100 v. The SBS-5 counter exhibited a better plateau, longer for higher pressures. The plateau of the SBM-7 counter disappears at pressures over 360 -torr. In the Geiger region, the plateau vanishes because of a sharp increase in the multiple tube counts. A few experiments with an external quenching circuir are also reported. Orig. art. has: 2 figures and I table. ASSOCIATION; Pernwkiy gasudarstvenny*y universitet (Perm' State University) SUBMITTED: Z5Jan63 DATE ACQ: ISMar64 ENCL: 00 SUB CODE: NS NO REF SOY.. 003 04 OTHER: 0 Card Z/Z ; I - , ;!~!.IJ 1, 111; , 1 I~ i~i.- i F. 111,'! . . '. ~; ~* s I z I ; I . I ; I I' Ili, 1:11111; 11111 1~1~i ., ~ . . , . . I ACC NR: AP7012430 SOURCE CODE: UR/0075/661'0211009/1107/1112 AUTHOR: Gabov, N. I.; ShafiYev, A. 1. Shafiev, A. I. ORG: Perm' State University Im. A. M. Gorlkiy- (Permskly Cosudarstvennyy universitet) TITLE: Chromatographic separation on paper of alkylphosphates and alkylphosphites. SOURCE: Zhurnal analiticheskoy khtnit, v. 21, ho. 9, 1966: 1107-1112 TOPIC TAGS., paper chromatography, phosphoric acid, phosphorous*acid SUB CODE: 07 ABSTRACT: The author's investigated solveai-with-the best sepiratbry capac- ity for paper chromatography of a mixture of alkyl esters'of phoIsphoric and 2~07' R0FO3H21 phosphorous acids, of the composition ROPOgH2) (RO) H and (R0 In each individual case, one of.t.he following radt- (ROVC~ffl )3PO' cals served as alkyl groups: CH n-C and n-C4~9. Instead of 32 C2ff5 31H71 and dialkylphosphoric acids and mnoalkylphosphorous4cids, the monoalkyl thin, ",Mt acid chloride were used., Vnich hydrolysed..w.ith er,~present in the solvent, into the correspop~Jm4..a,~idse Crig. a'rt. has:,,'3tabies. jJPRSr.- 40 42 Card UDC: 543.544 -0937- /376 ~V.i ~!4 - ~ ., s ... . .. .......... *""-' - I I . . I i I ~ I : It I 1 .1 ! IR 1 ME IN 1, 1 IT- I i .1 ; ! T' F." -171, mr PIT . AID F, 2094 Subject USSR/Mining Card 1/1 Pub. 78 T/24 -Authors Askerov, M. G., Shafiyev, B. N., Makushkin, A. G. and Popova, N. V. Title Ways of improving well cementing in~major~overhauls Periodical: Neft. khoz., v-33, no.4, 35-39, AP 1955 Abstract Dependent upon the condition of the:well whose walls have bden damaged and require tightening'and.sealing~of the damaged places, different amounts of cement are necessary. The coefficient of absorbing capacity,, the coefficient of,permeability, the kind and size of, fissures and the amount and pressure of'the water Iflow into the well will determine the am 'ount:of cement,mixture, to be pumped, the pressures to be applied, and also the cementing methods to be used. Charts, diagrams. Institution: None Submitted No date AK011OV, R.Ya., knnd. ekon. nauk, dots.; BASYUK, T.L., d.oktor- ekon. nauk, prof.; BIRMAN, A.M., doktor ekon.nauk, prof.; GRIGORIYEVY A.Ye.,, doktor ekon. nauk, prof.; DOKUKIN, V.I., prof.; IKONNIKOV, V.V., prof.; KONDRASHEV, D.D., doktor ekon. nauk; KURSKIY, A.D., doktor ekon. nauk,- LOKSHIN, E.Yu., doktor ekon. nauk, prof.; MALYY, I.G., kand. ekon. nauk, dots.; PERVUSHIN, S.P., kand. ekon. nauk; PLOTNIKOV, K,N,, TYAPKIN, N.K., kand. ekon. nauk; FILIMONOV, M.P., kand. ekon. nauk;_~~ ~doktor ekon. nauki prof.; BAKOVETSKIY,O., red.; KOKOSHKINA, I., mladshiy red.; MOSKVINA,,R., tekhn. red. (Economics; communist means of production]Politicheakaia ekono-. rn~ia; kommunisticheskii sposob proizvodstva. Uchebnik 2., pe- rer. i dop. izd. Moskva, Sotsekgiz, 1963. 599 p. (MIRA 16.5) 1. Chlen-korrespondent Akademii nauk SSSR (for Plotnikov). (Economics) (Communism) i . !i I ; I . I z I I 1 1 -- ---7 , ~ . , , iqt" I . . m . - 1 ~ i , . , i I I . , . v . . : . . i . I il: . " - . I' I '. , ; I I:I i 1: 1 !- I ; Ili ~~Ij Jill lo".! .~ . ', ... , -, .. I ... i-CM-I.S.SIGN Nil: AP4012007 S/0208/64/004/001/0139/0143~ rLUTHOR. Shafiyev R. A. (Baku) 1"ITLE: Iterative processes SOLTRU: . Zilurnal vy*chisl. matem.imatem- fizap V* 4j, noe I 1964,~139-143 TOPIC TAGS: iterative process, nonlinear op6rator,, Banach_space,,~tangent hyperbola,- convergences approy-imation, recursion relation ABSTRACT: The author studies P(X) 0 where PW is a nonlinear operator acting,from the sphere D(xoxR) of the Banach space X into the Banach space Y. Other authors have obtained conditions for con-, vergence of iterative schemes for.the solution of (1) under the 533umption" amone others, that there is a constant bounding the nom of the second derivative in some neighborhood of the initial approximation x0. -In the present work the author. replaces this constant by a number which estimates the nom of Fll(x~). He refines the bo4rds of applicability of the given processes, Orig. art. has: 19 formulas. Card 1/2 a it .1iii, i I'll )k . 3/058 61/t)00/009/027p5o A001YA701 AUTHORSS. Efendiyev, G.A., Shafi-zade, R.B. TITIS# Application of1kinematic electron-diffraction examination to in- -vestlgations of phase formation-in Bi-Se double layers PERIODICAL: Referativnyy zhurnal, Fizika, no. 9, 1961, 191: abstract 9H6 P - _3 ("Dokl. AN AzerbSSR, 1960, v. i6, no.-g. 833-8-36, AzPerb. summary) TEU; The authors developed a method of taking electron-diffraction-photo- graphs on a moving f ilm in the electron-dif fraction analyzer a r. (EG), for study- ing phase transformations proceedift when the.spectmen is heated.:,A bi-Se.alloy was investigated. It is shown that in this,allo the p~ha4p:Bi _y 2S63 is formed .during settling anda further annealing does not change the;ph&se composition, [Abstracter's note: Complete translation] Card 1~1 28075 S/181/61/0o/009/007/030 It, B102/B104_ ~AUTHORS: Efendiyev, G. A., and Shafizade, ROB. TITLE. Electron-diffraction study of phase formation in Bi-Sedouble layers pEHIODICAL: Fizika tverdogo tela, v. 3, no. 9, 1061,:2564 2566 TEXT: The method of kinematic electron diffraction (A. Boettcher, Thun. Optik~ 111, 22, 1954) was applied to study Bi-Se double layers. An "electronograph" of the type 3r(EG) made it possible:to take pictures also at hi6her temperatures, and, thus, to record phase formation and phase transitions on the photographic plate, Bi-Se layers were decided upon as test specimens because of their particular interest in semi-. conductor engineering. The purpose of the investigation was to determine the succession of phese fo--mations between the two layers,jn addition to determining the nature of the phases and the conditions for phase ormation and phase transition. The specimens were prepared by sputtering the two components onto each other in.vacuum (10-5mm 11g).- The total thickness ranged between 100 and 400 A. Three specimens were prepared., Card 1/3 23075 S1118116110031009100.71039 Electron-diffraction study... B102/B104 (1) Bi on Se, (2) Se on Bi, and (3) Bi + Se simultaneously. The following results were obtained; (1) Bi on amorphous selenium.- The electron diifraction picture displays four diffuse lines,(4-480:3.05, 2.08, and 1-72 190, all of whichR except for the first one9 derive from Bi Se if 2 3 0 the specimens are heated for 1 min at 200 C the lines:becomeisharply defined, and the one mentioned first vanishes,,which means:that- re- crystallization takes place without phase change. If'Bi condenses on crystalline Se, Bi Se will likewise result, but not all of,the Bi and Se 2 3 under6oea ruaction.. (2) If Se condenses on Bi, no Bi 2Se 3 7w i 11 form ,-ithout -min.ileating at 0' v. ~ h e a t i r It will form, however on a 15 100 C.- The fact that the phase formation depends on the succession in which the' components are sputtered is explained by the circumstance'that Bi atoms reach tne,layer with a higher kinetic energy than Se,atoms,and thus have the energy required for the Bi Se formation. .(3) The simultaneous 2 3 sputtering of Bi + Se by Vekshinskiy is method gave ri se to Bi 2 Se3 only, and the BiSe phase would not arise even if tiie concentration bf,components Card 2/3 2.1975 5/181/61/00/609/007/039 Eleetton-diffraction sLudy... B102/B104 Corresponded to tiiis phase. This selectivity in phase:formation was observed in all the experiments. To establish the phase transitions, kinematic electron-diffraction pictures were examined'for 1.5 hr under heating from room temperature to 400 0C. Only Bi Se4 was found to form 0 2 at first, and 20-min heating at 400 C was not accompanied by a phase change. BiSe lines are not allowed to appear until a:further 40-min: heating at about 400 0C- 1.5-hr heating at 4000C is ro6quir;ed for Bi-to arise as the th -ird phase, so.that Bi.Se 3Y BiSe, and IBIi are, present simultaneously. The following values were obtained,for the shortest interatomic distances in the layer structure (D5 - R3m group): 3d Se-Se = 5.30 kX, Bi-SeI= 5.07 kX, Bi-SeII =,2.99 kX. There are 3 figures and 6 references: 7 Soviet und.1 non-Soviet. ASSOCIATION: Institut fiziki AN AzSSR Baku (Institute of-Physics-of the AS Azerbaydzhanskaya SSR, Baku) SUB1,1ITTED: March 6, 1961 card 3/3 . ~ , - ~ ~ - - I -- - - ---.I- "I W~~- -MT , . .1. -~ 40 MM (Krivoy Rog Basin--Iron mines and mining) 11: H 111T 111-fl;,; .. ;:. . I"; 1~ . z , -.-:11; 1.I-., . . - , -.- I' I I~ "I I it I I III] I[: I I . I f I tliffF,71pil", 11,11 T 1 111- H 1; FIF4 L 3593-66 ACCESSION NR: APS024566 ribbon 6 ~cm long aie.-gr OW Transparent yellow-orange acicular and -filament crystalA*2,- are 3 hours. Since reacti6n-products:are on the sides of the crucible in 2 removed- the surface of the charge by the argon stream the're'is no chin!6e' of i 'a", tioush sur-~ face crust of gallium phosphide preventing the evaporation of the gallium suboxide.' Chemical and spectral analysis show that the impurity contentAh the'non-doped crystals is no greater than the impurity concentration in the:ipitial r'e& nts. go K Sulfur, zinc and tellurium were used as dopants. Sulfur changes-theis4ape of the crystals as well as the electrical and physical parameters. When 76:~mk Of sulfur is added to 5 g of phosphorus, 100% formation of ribbon filament is 'result s. . zinc was introduced by adding zinc oxide to the gallium cnarge in the,crucible,:since',ad-j dition of zinc to the phosphorus resulted in growth impairment 'and change in crystal et .color to grayish-orange. A third heating zone was added to th lfurna6ei for dopi; t e~ with tellurium. This doping method is more convenient than thel~6ther.two since impurity content qan be controlled over a wide range. This mthbd,was~used for ducing ti-type crystals-of gallium phosphide with * carrier concetit rationg from 10, to; J 1 17 cm73 -in the-crystal 0 Howqver, the dopant-content s is_not'a~ ~s nglti-~:valued~funcii4fi~L of'the tellurium vapor pretsure corTesponding.to the. temperatures in thetelluritui heating zone.: An increase'in the temperature in the phosphoruillione reduces them charge-carrier concentrationAn the crystals. The~temperature-in tha~r-eaction z6ne 'also has a definite effect-on the imp urity,concantratioh..~ High! apanti,concentr'- a l Card 2/3 A "Is 8593-66 CESSION NR: AP5024566 A C amike th tions cause imperfections in the crystals'which em useless' 'for applkatio;ns, finished c t 1 Ithough they:make tikal;for duel: ed-,- as good starting mia pro ' V h : i phosphite with the.use of taxial 1ayers3 ;J gas tr port-r eactioned Orls art. has: 3 figures, 21formul as ASSOCIATION: Gosudarstvennyy nauchno-issledoviaiteltak4y i stitut r*&!~ 1iq*ektnyy in tate Deal kometallicbeskoy promysbiennosti on and p1imnii4:SCli, btif ic M2.0drch Institute of the Rare Metals Ind SUBMITTED: 30Dec64 ENCLv 00 :SUB CODE: ~,,OTHER:',' 001 NO IREF SOV: 002 -:~~;.,ATD 'Pass q P Card 3/3, . . I I I 1 11 11 . 1 11 11 1 1 . '. I' I I 1 1 - . ; ~~ 11' - Illf,111, :; 'K i, I 'I l' I T " L A- "b DIr k 1) /T JK ACC NR: AP6014018 SOURCE CODE: UR/0220/65/034/001/0073/0078 AUTHOR: Iye usalimskiy, N. D.--Ierusalimsky,.N. D.; Shaf orostova~ L. D., Balaphov,.V. I. ORG: Institute of Microbiology, AN SSSR (Institut mikrobiologii'AN SSSR) TITLE: New principle for regulating the composition of medild:.used in continuous culturing of microorganisms SOURCE: Mikrobiologiya, v. 34,- no. 1.0 19651 73-78 TOPIC TAGS: microbiology, cell physiology ABSTRACT: In flow-iype, apparatuses based on the chemostat'~p~~rl~inc.ipl~e, :sooner or later dynamic equilibrium is established:between the multiplication of n~and growth cells and loss thereof in the liquid flowing out. The po Aati,;~` P4 .rate of the cells, their morphophysiological properties, and composition of the culture fluid become.stabilized at some constant levle'~l. i,ny 'change in the flow rate entails a change in the composition of thellmedim, Yet for precise physiological investigations it is important tojIbe able to vary, only individual.external factors, leaving the~others unchanged. To achieve. this purpose, the authors proposed a new device (here desdribed i'n idetail ~7 and illustrated) permitting independent regulation ot the amount Ofseveral. tinui i solutions making up the medium. It worked efficiently'in~con ous cultur ng of Bac. megatherium for 21 monthe in a medlum~consisting ofl,glucoae, XaCi Ngso sodium citrate, ammonium succingte NH41~1 601 knSO and. 4'- K211P041 4 Car 1/2 UDC: :576.8.093.1 i I % ;I r :1 i IJIF : . . I -- .f-: .! 1 ,~ . z 71.I,-,- . I I . I _i ,I i I I Card' 2/5 =jjj. UCLJ-..LCL.L -LMy:--.L ~ ;_ ~ I -L - . ;ic i'16ha]~d of'! r6s Qlut-ion~bf ireabihq g aij of i-the, rate:' f; T e~;.t 0 :4n.,; ;4n me 4 , friil!lml6-9111 Iml I ply. Ittle M."MMMS-2 H N Card 3/5 AL ye t-ny,, ; ~C4 I �tryl i!!. . 02 3 A: - I . : I ! : 1 11 11 1 11 .1 1 .. . I - I 5ROINMENMAREEME - --- ;, ! ; j..! I , j . I I ~ l'i ! 13 .. I;;! I ~ I ~ : I I ~: flillill qll 11- iiiii'l"i 1-1111- I i !h ! 1 : ~ i . 1 1, I V !, ~i - " lifli,41 M I , I ~~ !:. ; I' I I 'j; ; I T'.. It. .!i i I , rm ~= F~l -I- ~-,- - -, FrT -- . I I . f~ Iff ., IT )III, RF ii FT, Il! 117~ 1 *7 I 1 :1 , i 05299 211(7) SOV/170-59-8-lo/,18 AUTHORS-, Ovechkin, G.V., Ustinovich, A.B., Shaforostova V.D.: TITLE; The Effect of Sodium on the Relative Intensity:!of an,Analytical Pair of Lines of Magnesium and Copper PERIODICAL. Inzhenermo-fizicheskiy zhurnal, 1959, Nr 8, pp:78 83 (USSR) ABSTRACT., One of the authors, Ovechkin, expounded LRef 1-7, amethod of theoretical determination of graph shifts following achange in the concentration.of a third component in an alloy. The present paper contains the results of' an experimental Investigation undertaken to check theoretical conclusions deduced. As a sample was taken a solution of magnesium and copper, and sodium served as a third component. An alternating current arcTed from a PS-39 generator at a current, intensity of 5 A served asa source of emission and the substance to be investigated was introduced into the Interelectrode gap by two methods. Fllectrodes~emplojjred were nickel and carbon ones. The spectral lines of the samples were~studied by,two: different methods with two spectrographs of the ISP-22 type. It was con-, firmed that the rate of magnesium evaporation relative to that- of copper Card 1/2 increased with an increase in sodium concentration, L,e. with a decrease- 11 ;j 05299 30V/170-59-8-lo/18 The Effect of Sodium on the Relative Intensity of an Analytical Pair of Lines of Magnesium and Copper of plasma temperatijre. Using the --,xperlmental :data obtained the authors constructed a graph showLng the dependence of rela tive rate of magnesium and copper evaporation on plasma temperature or'the sodium.concentration in the sample, Figrur~' 3. There ar,~~ 3 graphs and 8 Soviet references, ASSOCIATION- E--Iorusskiv gosudazr~:t-rernyy univer,sitet !m. VJ. Lenina (Belorussian Stat,:- Univers-1-w I'me-zi V-1. Lenin), Minsk. Card 2/2 I I ! I if - I , ~TIT.VIPI'.!Jll , !11:.;. .41 i.D-. TIF, rFj . i , 1: . . 111 1 PI f !IQ 11 1 . I'! ~! . I i I ; III It, I- ; 11 11 1 '1 1 11 11, 1!!~;! "! ! " I - 1:1 '. I- pf'~ :.! I .. 1, i I i; I 1 -1 ~'. I I . :;.~ -- - . 1~ I' I'llill '1111: PfliTtil lil'! I I : !,1 .1 : i . i I ; ;,; I I 1 11 111 1 1 If I I. " :, . - I .- - !"T-] -*:-F-[7j[Tl,'-,F IFT., I` ~ I, , 1. T PANGHMKO. Aleksandr Mironovich; -SHAFRAN, A.A., otv.red.; MIROSMICfMMO, Tj 1.13i J!Iglp 4 . 11=4 1 11, .1 .- .. 1. . - 1 111 : 2 1 11 11 - - . dim U . .1~: I Til ~11 11 .. ......... - -- -- . 1 1 1 , :1 11 .1 1 , I- . . . F Fff 015m, I ! ~! - ~ -I I [:.I.: I'd IMI . ;H 1 11 '1 1 ll Itill MUM11111111! p I pall-lu I't 1 11 171, M r-flT T I M 711, ~1111! I - ~T.. " . ! : I ~!; . . III : 11;11. 1 !t, I I I Ill'i ; Ii 1:1 ~. - im2. 14. 1 ;, 4, If I ol: , I.;I-i r FILIPPOV,A. M.; PARFENOV,Yu.A.; ?,'LOWZOVA,A. D.; TOMCRIN, B. Z.; UA212"-A T otv. red.; CHSNOKOVA, T.V., red.; SLUTOKIN, A.A.,.tekhn. red. [Handbook on electric measurements in municipal telephohe lines] Rakovodstvo po,elektricheskim izmereniiam~linii go- rodskikh telefonnykh setei. Moskva, Sviazlizdat~ 1962. 120 P. (MIRA'16:6) -1. Russia (1923- U.S.S.R.) Upravleniye mestnoy ~elefonnoy svyazi i radiofikatsii. 2. Sotrudniki lineyno-kabellnoy labo- ratorii-Nauchno-issledovatellskogo instituta gor*odskoy i sellskay. telefonno.y svyazi Ministerstva avyazi SSSR (for Parfenov, Morozova, Filippov). (Tel6p*Mi lines) -(Electric meadurements-_H~h6~11.,' Mhuals): etc.) I il , I]; i :;1,!1l ~ .. I ~ I !: " ! i I I I I I I - - ~ w - ri f .. 7111 Is"'ll FIT F FRI .1 -i ~l I 1 1. , - - I 1 .1 1 1 . 'I If 11 1 11 of I ! .1 . . I I.. . I . -- '' I . . : , i;,::1 i 11 ~i . 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MOOD Of 6$6,%LA 61TALLUPGICALLIMATUNI CLASUPICATION .3c S a )a,. oa.in, I.A0.9 .&1 0- C.( CK C.-Its u ; A---- 4 1 1 , a 61 0 0 0ego !o 0 go o 0 0 000009 0 : e :: 0 : o 0 "o 0 00 00000 0 0 ~ 0 o 0 o 00 0 0 0 000 0 e, o ego OJ 0 0 -1 ___ ___.___.- J i 9, - f - fi k I ff - r RV 0 0 a 11 4 1 4 1 a I Is 11111JU011, Ills "I alf is If a it As m is is is 1) Is Ill a -1 Ap A& a so A,_j. j 0 so j; ptsifying ticron cublde. 1,AL_$LW1'AU- .00 :IV-.;,J. Tile INX00 carb 1e Is bralcil at it mull. Wow Issulteli caustic, until SIts i4tic; lorivreval-I 2 The inelt is then will'ilittl to remove the eliusm-, 6)11~ na, and dried. so 06 so goo 00 X*e 00 00 600 409 tr off Lt~ss - L A OWTALLURGICAL LfTERAT(stiftCLAISWKATION o. I to fit It I t -1. a--, qeC 034711 *0 qmv Ask U 0 AV , . j so As . . - ' . NA 1A 0; Is n a 2 9 0 d A 00 0 . . 0 000 0 0 0 of Oslo & & 0 0 * : Ol I 41 40 00000 0o4 0 of so is a 0 e a 0 0 a AD at w It 4 It x 21 a a v a 26 v 36 j0 if J2 U M is k U is It 0) a z j 41 itif!* -it A A. W XK Sr ii .Deft JL~ If 0& ..v "!! -O!ds . - I- _ , 1 ow~ 47 .4r,(ISS11 A.0 P-611-1-ft --6i ~ 00 00 00 Determination of carbon in borom carbide by the com- bustion meftod. L C, Shafran Anil It, It . %UJirr.4,L;%vA.: A, i, k v I b I Lan LK- drtd. in B.C: -C IMCy it) I fit Ut)jk, y igniting a &%inplv undvr a ruver tit I g. of 0o Ph, filings in a porcelain bout in a cornbmtion tuffe and an z 0 current at for 1(1-21) fitin. CtLwl. l4kno 000. 00 ' 4 0 is is ~ 00 !:zoo , ZOO off A 0. 1 & A AtTALLuncicAL LITERAT01 CLA~J$FtCATICM woo - - - - U is AV W3 Is; P ll Itoll IF 11 Tinvi 1 tw a a a .1 Ir IM 9 a a i S A I No Wk Ji t? rto Op* its v[;I [O 0 0 to . 4 0 0 0 0 * 0 IN 0 a 0 0 04~* & 0 0 0 0 0 a 6 0 !, 1.1 11 11 16 It to it X. I; J2 13 1. Is 16 77 Al )v x it 12 M Id 11 k 11 m 11 1; it 040 3 L L -f -f. 9 1- 1- 1. 1 R, r A V -A-Y --Z- cc W tf. 4- t Diptemination af boron in boron c*fbides. i, G, - I ;IIjIAjj j411.1 %I %,. pavii,vi. Zat,.lttava L.,'i 7. 1- 00 0 t)jj.Ijje Il.c wt IIN, 1, tit if"- p--Isve if III- ItV.1fraill'. A.14 " 'ilight t,., ,.I IICI. 11,41 1.06 1 111 "Ilia "it 00 I tlv tA.1 A "litt. toc%swl 0 h. firlitrA I FV III mel It VI $,,I .,11,1 littAtt- I'IV 11,110, .011 NAOII 31 11-11-91, 1111411" -00 00 00 Ae 00 :09 of 00 00 zoo go ago 00 ZOO 71 80 00 j ~ .60 41 g Oe " 00 of s 00 it Oq ai *9 It Cc[ it m t it rw 0 4 1 9 0 1 fl. a -to I I 0 l 0 p 0 00 0000 0 0 0 0 4, 0 g 0 o & o o o 4 0 o0 - 0 si~ 0:1- : 0 0 0 0 0 0 00 00 0 s 0 0 0 0 o 00 ele 0 0010 0 00 0 0 o 0:0 0; *Goes* G*eooQ*oooQO 4 0 0' so go PPOCISIts 6he plavastill moll go ..so of -00 .00 J. A i-Am. (U. 8. Go wd w .00 ,-B.C mmid W.C Ime alklim J%t imo. to t1w pe'-we of N'Som (to larreaff ombmt woo Go a id IINI),) in m Wftjany d-W-1 smi. (diagmns is all- 00 'i Ivnilrd), Nim A. A, Putilportly ASO* so* *0 00. 004 **'I 00 coo coo woo ttee LOGICAL UYIN&TURS CLASSWK&TIN lee ASO-ILA OFIAL see "I =1411zrl 4m, a.. ill 00 go **I,*, goo 0 0 40 Ole 0 0 0 0 0 0 0 0 0 0 Goo 0 G;O I 44' 0 0 0 0 0 a 0 0 ke 0 Wo 6 0 0 0 0 0 e 0 0 0 0 let? 104 Ousu is 14 11 111 a id 13 JJVB ju it Sill MIS lilt birv &.1 4144 off 41'r 0 RfIL ) I ..t, I !~ 6 Il -1 A - AL _r, A A S-111 F Q : -71 0 A I A"IYOW of btwm ftiftirif, Shafranlawl R; A. Le"I"I"On. 1,PPIW C". 3- I x~l ~*, , 1; 0 in Frevirb. I , ('.)).-Grind an av. %inipir of JUN 00 n an apte Inorlar to (hpwder, I'll"v the wrighell Kround sample (About 0.2 K.) its a KIA" tutm, fA( whi%if .00 the tantfum and wWb are covered with a thick wycr, ,( (w%etl and solidified NaOlf. Addanachint.0.5g.41.1wd 00 X*011, mix writ with the ON an4i %-o)vrf with a lAyer 41 1"A mm. NeOlf. Pour 50 ail. tri W I Y 16~4), intomi , I, tneM fiask and add 2-3 drops of a 1% suln. of pliviltwi- plitholein. fleat the US + NaUlt num. in a test tuba to 300' and abmwb the evolveJ NH, in the jklmvr 11,SO. "n. =00 0: 13 The prefeffed app. i- shown and its operation is described in derail. A. A. HoelithuSk 00 13: 06,5~ 00, soo g coo Neill Do no 9 00 WOO 0*' 1, all _9 J4. Lie* A V no a Iw IJ a 0 5-: 9 v 0 1) U it v Is) K it It P00000!909069609009046~1`1 0 0 64 0 0 0 0000 000 * 0 0 0 sores 0-0': 0 0 0 W:070 0 0.6 0 0 0 :10 *1 go 0 0 C Flu P19- I t T *-tr-o 0 6 4 -- - - 0 0 0 0 41 0 0 0 * IN ease Go 0 O I I t j WW w- # e a 0 0 * 9 0 1 11 1; 11 14 ti W IY 4 If JO ~ I 0 0 1$ A V 3911 IIIJ 149MV N b -0 Al 0 41 43'a 00 4j go Boron carbitti. I.G.Shaimmandn.F.Ormont. Rum. 06 it ! W,444. March 31.1941. A chars. of altern"'te layers of d b go - out to a 11,0t and C is beste Q I 1 11 1 00 6 log, coo moo- 00 va most Is A I L A ETALLUACKAL ILITIEN&TUOIE CLAWFIChTION a it a.. Qat j4nOv7 -j - U St AV 00 L% at K it it it 9 K INILA)IO-t ! NJILL111 CK a4r lit M L S I A 0 is 0 N so 5 a a V 0 0 0 0 0 0 0 0 0 IS 0 0 0 0 0 0 41) 0 a 0 10 0 41 0-0 0 0 0.0 0, 0 0. 0,0 0 0 0 0 tg;*~* :1 T: 'I ...... MV IV' 4~ 11 I'll L ? 2. V,~ F V2207. Daterminadt)IJ o1 ffma &=U4 -4- A 14*7rm. i ~j ShIJEUB and' it Rif. ZA t datermble CO %) 40- cminjeftV teagon 0, 61(lation 'Wlth ']M041! COO., ubtlklndd~~ C-G-PPtd. with MIA, tba PPI. Is dirAved W I mi of'. aidif 04 rfll of And the conc. HC1 conw SOIA. is ev-.1ponated to drynem jhp !mldtm~ i dis;solved: in water, 0~5 mi of 0-16/4 nitio3o-R Wt- soln. and I nd 45f satu;ated Ma aretate s61n.-,'Whfch has been neutrallsect,to PH ~t! 8-5, i am ddd 2 friin., I Jhl:of djL Solu. is boiled for i Oll (1'+ 1) is added and the sollb it &n evaporated to aivol. of a to 1 -L, Thq mh'~r is c6mpacd: %~th that of standards prepared sinulaily. The iiror of Co'. A p-z 77~ '17 J. SUBJECT: USSR/Luminescence AUTHORs Shafran I.G. TITLE: New Chemical Methods for Determination of Small Quantities'of Admixtures-(Novyye khimicheakiye metody'opredeleniya malykh kolichestv primeoey) PERIODICAL: Izvestiya Akademii Nauk SSSR, Seriya F,izicheskaya, 1957, Vol 21, #5, p 661 (USSR) ABSTRACT: Methods for determination of small quantities of admixtures were developed in the All-Union Institu ,te of~Chemical Reagents for use in the manufacture of luminophores. These methods de- tect following quantities of impurities.s - -6 _5% of Cul- -5% 10-5% of Co;- 0 10 to 10 10 of Fe; 1 _5% of Ni and, some other elements. There are 3 proposed methods: 1. Separation of iron admixture in;the form of settled hydroxides or other difficultly soluble compounds by means of passing solutions through a column with glass wool used as Card 1/2 an adsorbent; 60782 S/137/60/000/01/01/009 T-rans I a tion from-, ReferativnTj zhurnal, Metallurgiya.. 1960,~~No 1j" p -91, 621 15-1 2_2 2 0 A UTH 0 R S Ormont, B. Epeltbaum, V,A- Shafran, I.G, TITLE~ Investigation of the Boron-Carbon-Silicon System and-Prepar-ation of Borundum \6 PERIODICAL-. V sb.- Bor. Tr, Konferentsii Po kh1mii bora i:ye?_o:*soved1neniy, Moscow, Goskhimizdat, 1958, PP 177 181 IT a TF Mo-f-ind ways of economizing- the valuable B-raw material:_in the production of abrasive materialS on B4C base'. the authors investigat-ed the possibility of obtaining preparations containing B - C - Si, which are generally named 'borundum". Preparations were studied which Correspo.nded,to the silicon vertex of -the ternary stinictural -diagram as well as. preparati=- with a low (2 - Y15) Si. content in B carbide. The preparations were produced in Tamman furnaces, B20 was obtained from boric acid, Sio, from grotind 41hite quartz and C, from cQon black. The preparation corresponding to the Si BC formula 2 2 Card 112 - -- -- -- -- . ! 1''. -'. I , , 82223 S/081/60/000/-003/004/095 Translattion from- Referatlvnyy zhurnal, KhImiya, 1960, No~ PP.L 378-379, 10048 AUTHORS- Ormont., B. F., Epeltbaum, V. A., Shaftran, 1. G TITLE- The Experience in Industrial Production of Borimdum FId Testing of 1 'Is Properties Bor. Tr. Kgnferentsli po khimii bora i yego soyedineniN,.- PERIOM-CAL: V sb-., Mo5cow, Goskhimizdat, 1958, pp. 182-183 TM- Experiments on the Improvement of the carboilandum qizality by intro-: duzlng small quant-Itles of boron into the charge U-10% of I + C"content.) confirmed the assumption of the possibility of melting boruiidum i ,n, Acheson- type ,furnaces at. a temperatture somewhat higher than the usual one, the:consumption of elsetric energy in this case does not increase. With the introduction of small boron:addit-ioAs, the carborundum vapor pressure changes noticeably. The sub- limation temperature (and the degree of borundum rec--ystallization)proved to be higher than in carborundum, therefore the borundum ci-ystals had in all melts smaller dimensions on tY~- ~,.-.,erage than the carborundum crystals from analogous temperature zonez. It was estaoli,,~hed that boron enters the composition of 'the carborundum lattice, affecting the decomposition pressure and the pressure of silicon carbide Card 1/3 8 22223 3/081/ 60/000/003/004/005 The Experience In Industrial Production of Borundum and Tes-ting o f Its Properties vapor. The losses of borLe a.~ld with the waste gases during l~ melting of borundum were considerably lower than in the production of boron carbide by -the are method. (the flame on the walls of the furnace and in -the torches was not gMen-colo-red) it was established by ana-lysis of the samples that In case of an Increase in,th-- bor-,)P- content in the borundum cr-jstals their specific gravity decreases. This- agrees with the assumption that substitution structures are formeid in U-is orystale latt-i-ae of borundum. Roen' hi investigations showed that the sizes r.jenograp c with an accuracy of up to 0.001 ) of the crystalline rruclel of the 'torundum and carborundum samples investigated remained unchanged, Fhasemalysis detected ki borundum a :!onatar.' of - I C bhe 3rd mod ific-ation. .5% of the 2nd modift atIon and Q5,19 of", of carboruidum (ccmpaned to 50-100 and