SCIENTIFIC ABSTRACT SOLOVYEVA, G.S. - SOLOVYEVA, L.D.

• Document Type: CREST
• Collection: Scientific Abstracts
• Document Number (FOIA) /ESDN (CREST): CIA-RDP86-00513R001652320020-0
• Release Decision: RIF
• Original Classification: S
• Document Page Count: 100
• Document Creation Date: November 2, 2016
• Document Release Date: August 25, 2000
• Sequence Number: 20
• Publication Date: December 31, 1967
• Content Type: SCIENTIFIC ABSTRACT

L 10438-a EWT(m)/EWP(b) JW/RX
ACC, NR. AP6000281 SOURCE cow; uR/oo78/65/oiO/009/1971/1975,/.-/
AU'T'11r_Q,,, Gorbution A. 1, ; S010VIZ!va, G. S.; Antonoy 1 8 Kharson, M. S
IV,/. t 5 YYZ5
ORG, no7h
T ULF:! Solubility of d1boradin diethylene glycol dimethyl other A
'I
SOURCE- Zhurralrlaorganicheskoy khiniip v. 10,, no. 9p 1965, 1971-1975
"')PIC TAGR,, ether. sdJubility,, heat of vaporization,, diborano,, dieWlene glycol~4
pre,;~rir-_, ta7perat~r-,~ dop^ndence,, high temperature effect,, low temperature effect
A13SMCTL Th,~t %cl-Lbility of diborazw Li diathylene glytol dimethyl other (DGDE)
Va.'s aetem:U.'ett At tan;*ratrave of -50, -20s~ 0. +20p +40, and +60C and partiAl
prt,3warse ~,f diborane frc= 11L, tu 695m Hgp' a~td also at -20., 0,0 and 420C at
pressures frzmr, I tv 1.0' at!". The solutions were foiuvi to obey Henryto law under
these conditions. kn empirical equation is given for the temperature d$Dpnjgnco
of the Henry coeffitients for pressures &t0 1 atmes log I a 16.86- -7U9
for presiures up to 10 atm, log X - 6.66- 02 0 The.calculAted heat ory
vaporization of d1borane from its solutionST9 DEDE is 3 - 3.4 keal/mols. It
was found -that the reaction of diborane with ME is autocatalytte &M forus
methane, the reaction rate being accelerated with rising pressure and texperaturse
Card 1/2 UM 546.271

L io438-M
AW. NR. AP6=281
The vapor preasure-of DODS was dstftmiusd in t~hO ranga of 40 - 90C* M. to
ga=mlova kindly supplied the DODS mwiplese Orig. aft. hits: 4 figures, T GMK#
aW 3 form,las.
SUB CODES 07,,20/ SUBM DATES Umar64
ja
2/2
Card

ACC NR- A P7006226 SOURCE CODE: UR/0,678/67/012/001/0003/0007
AUTHOR: Gorbunov, A. I.; Solovlyeva, G. S.
ORG: none
TITLE: Preparation of d1borane by hydrogenation of alkyldlchloroboraneal
Murnal neorganIcheakoy Idilmil, v. 12, no. 1, 1967, 3-7
~TOPIC TAG3: d1borane, chemical syntheuls, boron compound 3 INOvIe,16FLIA4045
Ar~;TRACT: Diborane ha3 been prepared by a new method involvinc, hydro-
of all.-yIdLehloroboranes at titmo3pheric or high prealureu,
Identification of the reaction product3 by IR 3pectro3cripy Indicated
that the hydroF-,enatlon probably proceeds vin the B-C bond
+
ectitir. the B-Cl bond to form dichloroborane: r(BC12 + 112 if:' 112
,Dlborane Is probably formed as a re:31.ilt of the disproportionation of
H-3C 12 The results of experiments conducted at atmo3pheric prreosurc
and 250-5110C In a flow apparatus griven In Table I indicated that the
~alkyldlchloroboranes are hydrogenated only In the presence of OOKLT-D
I or AR-3 carbona. Lower degrees of conver3lon based on 1=12, "AS Com-
jp%red with those based on 1111, Indicated that the diborane formed under-
,IgoQ3 pyroly313 on the catalyst. Experiments at 300-340C and hydrogen
lpreasure3 of 100-200 atm (Table 2) yielded d1borane in the absence
[card l/ UDC: 546.271-05
- I --

ACC
P700 22
Table 1. Hydrogenation of alkyldichloroboranes
at atmospheric preasure

Catalyst

13C2,j;Hj
ratio
-
C Conversion
based on
I HB019, Conver

ion
based on
RH, %

ontact
time,
see
Ethy ldich2orob orane
Without catalyst 114 475 slight 60
10 ml SKLT-D carbon 1.5.26 370 - - -
10 ml SKLT-D carbon it5.a 475 3.72 56 3
N
10 MI 0.44% Pt on 1:5.3 450 -
graphite
10 Ml 0.44% Pt on 135.3 500 - slight -
graphite
10 mi 0.44% Pt on 1:5.3 540 0.98 28.3 3.5
graphite
10 ml 0.2% Ft on 137 411 4.69 76.2 3.4
SKLT-D
3 ml 0 .2% Pt an Is7.5 475 3.93 34 2.2
SXLT-D
10 ml AR-3 carbon
is6a
400
2.5
36
3.6
Pro 6ldichlor tborane
10 ml NI on Cr*OS lo6 250 - 3.5
10 ml 0.6% Pt on Is6 300 slight -
3XLT-D
10 01 0.6% Pt on l16 420 40
SKLT-D
Card- __

*CC NR- AP7006226
Table 2. Hydrogenation of alky1dichlorobaranes
at hlgh pressures
1 2 1 3
I 6
Ethyldlchloroborane
I
A
I -. Ig! r-'l

'(W .
,
1
1.1
2-1

41.5 1.6
.16.3 - 22

)v S1.1
U, 37
5
2 1.97 V3
11
s
; ril, ,
2:1 2
41:6 '
17
v)
311 77 1 1 7
'
'
,
, 41 9
5
A
2
I'l 1
!.
; 51 1
9.
319 2,Y) 9-~ 2j -
,n
S '01
1
2 3'

7.2
141 M
170 :
'1
1 31%2
1 : 0. r )

37.2

1.1
Propyldlchla rorborane
3.1
31Y3
110 1-.3,4
S

1
;
4

3
2. :30 :3 4
2 7
: 4
LCord----3/~
Ethyldlchloro- I
borano charp
,el g;
2 - Temperature of
the autoclavol 0c.
3 Pressure, atm;
4 RDG12012 ratios;
5 Contact t1m,
aec; 6 - Converajon
baaed an G21% Or
7 - Yield
In diborane, %,-
8 - Diborane content
In the mJLxturot %
by woleht; 9 - Par-
Win content, % by
voluma.

ACC NR. Ap7oo6226
,of catalysts. Study of the pyrolysis of neat diborane and of its
'mixtures with hydrogen and boron chloride indicated that pyrolysis of
1diborane sharply decreases in the presence of BC130 probably because of
the formation of the stable B2115C1 and BHC12 compounds. Orig art. has:
3 tables. A. T7j
1 NO
SUB CODE: 21p 07/ SUBM DATE: 20Feb65/ ORIG REP: 007/ OTH REF:

AUTHOR:
,Iovlyeva, I.A., Engineer 117-5-7/28
TITLE- HDdemization of the "W-110" Machine 2bol Hule by "Billetor-KIms" Co
(Modernizatsiya stanka. firmy "Billeter-klunts" modeli "TH-110)
PERIODICAL: Mashinostroitell, 1958, # 3, p 16-18 (USSR)
ABSTRACT: The article describes in detail how the face grinding
machine "TH-110" of the firm Billeter-Klunz has been modernized
by mechanizing the manual movements of the crosshead boom and
of the small grinding heads slides. The modernization project
has been worked out at the Central Designing Bureau (TOKB) of
Remmashtrest and put into practice at the Moscow Grinding
Machine Plant (Yookov'skiy zavod shlifovnllnykh stankov).
Other Billeter-Klunz face grinders - "TT-50" and "TT-80" -
can be modernized in the same way.
There are 3 drawings and 1 photograph.
AVAILABLEi Library of Congress
Card 1/1

SOLOVIYEVA# I.A.; OURkRIY,, G.Z.
Cryttal structure based on seismic and gravinstrio data. Blul.
MDIP.Otd.geol. 37 no.5sl69-170 S-0 962. (KM 15 $12)
(Earth-Zurface)

8/02OJ62/146/004/014/015
B142/BW
AUTHORS: Gurariyj 0. Z.,
TITLE; Preliminary data on the density of the earth's mantle
PERIODICAL: Akademiya nauk 333R. Doklady, v#'146, no. 49 1962p 677-880.
TEXT: Attempts were made to elucidate horizontal variations of density in
the upper parts of the earth's crust. GloVal seismic and gravimstric
data were compiled by the laboratory for structural geophysics of the
Geologicheakiy inatitut AN SSSR (Institute of Geology As USSR)# headed by
P. N. Kropotkin. 365 velocity columns were set up for all points with
precisely determined gravity anomalies and sajamically well determined
structural characteristics, down to the Mohorovici6 (Moho) boundary, and
the mean velocity of longitudinal waves in the earth's crust was
calculated. Columns of equal deithe (1) and of equal gravity anomalies#
,u reduced to the Bougier values, were compared* For (1), the difference in
41 Bouguer anomalies reached 200-250 mgal. This fact was assumed to be
di explicable only by density variations, in a horizontal directiont
occasioned in the upper parts of the earth's mantle by the fact that
Ca, bard 1/3
12 Of t e 00
a at

3/020/62/146/004/014/015
Preliminary data on the density ... B142/Ble6
probable densities for individual pointal is advocated., There are
I figure and 2 tables.
ASSOCIATION: Goologiohookiy institut Akademit nauk SSSR (Institute of
Geology of the Academy of Saienced USSR)
PRESENTED: April 20, 1962, by N. M. Strakhoy, Acadeaician
SUBMITTED; April 16, 1962
bard 3/3

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SOLOVIYEVAj T. A.
USSR/Memistry - Color Photogmpby Apr-51
",~ctlon of Chlorosulfonic Acid on 2-Cyanoacetyl-
coumarone," I. A. Solov'yeva,.G. I. Arbuzov (de-
ceased), Synthetics Lab, All-Union Sci Res Cine-
Photo Inot
"Zhur Gbshch Khim" Vol XXI, No 4, PP 765-767
Investigated components of purple dyestuffs for
multilayer color photo emulel ono. When 2-cyano-
ace,~Ylcoumarone reacted with HSO Cl SO Cl group
took 5-position on coumarone nucleusp. ~;timux
reaction conditions gave 7% yield of 2-cyano-
acetylcoumarone-5-oulfonic acid chloride. Analide
and p-toluide of latter synthesized.
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mar* -5, 1954 imwwr, M. how IOD' I to 156* In on open
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fink 40 wha. Nils CY4000
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dw. With I Q; .1k. $go$. at.
pead
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Ai..

Pu n of
of P-'*' ~'L 'yn
June 1953. Unclassified-
t or Russian Accessions, LibrarY Of Congress,
9. Monthly List

5ot-ov ycvtl
USSR
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ture, n~-ld ii & ,oMjjM3tjCn GXJ4
n-Hydroxyvaphtfick Blues Lre Me kast w1sWe dy" wwd.
New clultweil cumpds, ve fAvuted during the (=~rg, awl
theit furtuation ntc is di'Yertnt for clifftmt dy". Th-,sv
I c-traed ci),mptis. nze G-rincd c%,tn %hen (he frAing is itighi.
The c~ikw during UvItIng I-ccotn,~s divphrtd towwds the rcd
end of the swtru-n It-- R,:w coL-Xtj com'At. cjUA bc
((,ftvrd by Itr. ol tile tires, of &ny rtsidull dr-

1-(CALtboq- Md Ak9dwsy-l-bliu
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1. A SOW*gvs- )A- V- Kt-l- L"Wr.
PAP, I:Uajm cifte-Pbao Re%mcb Ind., .
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td_s, and "kilfcotim with 11191 1 1.000. 5-
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f'oll. thea with 13.e ml. 19% N $414 Nd 14444..
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50)
AUTHORS: Solovlyeva' 1. A.9 Guseva, A. G. 20V/79-29-6-63/72
. . . . ............................ ...... .........-
TITLE: On Several Benzothiazole Derivatives (0 nekotorykh proizvod-
nykh benztiazola). VI. On a New Method of Synthesis of
2-Hydrazine Benzothiazole Mono- and Dicarboxylic Acids (VI.
0 novom metode sinteza 2-gidrazinbenztiazol-mona- i dikarbo-
novykh kislot)
PERIODICAL: Zhurnal obahchey khimil, 1959, Vol 29, Nr 6, pp 2068--2073 (USSR)
ABSTRACT: The methods of synthesis of heterocyclic hydrazines, recorded
in references 1-11, are not convenient for the synthesis of
several benzothiazole derivatives, especially of benzothiazole
mono- and dicarboxylic acids. According to Th. Curtius and
E. Schmidt it had to be aesumed, that the 2-aminobenzothiazole,
in which the nitrogen atom of the amino group showB an apparent-
ly amidine character, could react with hydrazine hydrate just
in the same way. The authors studied therefore the effect of
hydrazine hydrate upon 2-aminobenzothiazole and its deriva-
tives. '4hen 2-aminobenzothiazole is heated with hydrazine
hydrate dissolved in water at 1200, a vigorous formation of
ammonia takes place. After precipitation of the product by
Card 1/3 cooling, it easily formed with the ailvernitrate dissolved

On Several Benzothiazole Derivatives. V1. On a New SOV/79-29-6-63/72
Method of Synthesis of 2-Hydrazine Denzothiazole Mono- and Dicarboxylic Acids
In ammonia a layer of silver and condensed together with acetic
acid ester to 1-benzotitiazolyl-(2l)-3-mathylpyrazolene (Ref 7).
Based on these results and alao on the results of the analysis
it could be established, that a splitting off of the amino
group tAken plitce In this reaction and benzothiazole-2-hydra-
zino (1) is formed. At a weak acidification of the solution
and after removal of compound (1),a yellow oil, oasily oolu-
ble in hydrochloric acid and sodium hydroxidul was separAted.
Tn open air it in quickly transformed into ft crystalline
product (171 the structure of which was proved by miscibility
test, Thus a partial disruption of the benzothiazole ring and
formation of the o-aminothiophenole (Ref 14)(Scheme), is ef-
fected by this reaction..By longer heating the yield of
2-hydrazine benzothiazole decreases, whereas the yield of
sulfide (D) increases. The same reaction with substituted
2-aminobenzotliiazole did not succeed. Under the above named
conditions the 2-aminobenzothiazole carboxylic acids react
quite differently. When heating 2-aminobenzothinzole-6-carb-
oxylic acid with hydrazine hydrate dissolved in water at
Card 2/3 120-1300, the for-nation of ammonia ceased after 6-9 hours. The

on Several Denzothiazole Derivatives. VI. On a Ifew SOV/79-29-6-63/72
Method of Synthesis of 2-Hydrazine Benzothiazole Mono- and Dicarboxylic Acids
product precipitated in acidification showed a reaction char-
acteristic of t-he hydrazine group (layer of silver) and led by
conversion with steaoryl acetate tc the corresponding pyrazo-
]one derivative (Ref 16). The mentione4 properties and data of
anglypis of synthesized compounds correspond to the structure
of 2--hydrazinebenzothiazole-6-carboxylic acid (111) (85 '% yield).
Analogously compounds 0V-VI) were obtained (Ref M from the
2-aminobenzothlazolo-5,6-, 5,7-, and 6,7-dicarboxylic acids
with satisfactory yields. There are I table and 20 references,
7 of which are Soviet.
ASSOCIATION- Vses,_~-uznyy nauchno-issledovatel~skiy kinofotoinstitut
(All-Union Scientific Research Institute for Cinematography
SUBMITTED: April 4. 10,50
Card 3/3

-SOIDVIYEVA, I.A.; LEVKDYEV, I.I.; GUSVIA, A.G.
Structure of colored substances forming under the offect of the
oxydation by air oxygen of the color components, derivatives of
pyrazolone(5). Trudy NIKFI no.40195-105 060. (1-71IRA 15:2)
(Pyrazoline)(Color photography-FUrna)

GURARIY, G.Z.; SOLOVIYEVA, I.A.; KHOPOTKIN, P.N., otv.red.; PFYVF, A.V'r.
glnvny~ red.; MARKOV, M.S., red.; MENNER, V.V., red.;
TIMOFEYEV, P.P., red.
(Crustal structure according to geophysical data] Stroenie zemnoi
kory po geotizicheskim dannym. Moskva, 1963. 125 p. (Akadexiia
nauk SSSR. Geologicheakii institut. Trudy, no.98). (MIRA 17W
1. Chlen-Oorrespondent AN SSSR (for Peyve).

3/000/003/04 -04
3/058/6
A0621AI01
AUTHORS: Portnaya, B. S., Solov'yeva. I. A., Turitsyna, N. P., IAvkoyev,I.I.,
Challtsov, V. S.,"~anhemlnnlkova, M. V., Bobkova, T. P#,, Tkachen-
ko, T. 0.
TITIZ: On the proportion of mabk ing color compononts of arylazo derived
pyrazolones (5) and willidea ol' 1,2-oxynaphtholo said
PDIIODICAL: Referativnyy zhurnal, Fizika, Z10- 3, 1953, 86, abstraot 3D584
("Uspakhi nauchn. foiogr.", 1962, v. 8, 35 - 43)
TEXT: An investigation was made on the dependence of the color photograplila,
properties of some arylazo derived pyrazolories and anilides of 1,2-oxynaphthoic
acid on the nature and position of the substitution agents in the amlazo-group.1
It it established'that the phenyl derivatives of pyrazolones and of 1,2-oxynaph-
thoio acid ara compounds considerably less nusceptible of reaction In the condi-
tions of color developing than the initial purple and pale blue components. The
onti-j of eleotropositive substitution agentu into the phenylazo-group somewhat
increases the reaction capacity of the component3p the most favorable influenoe
Card 1/2

S/058/63/000/003/045/104
properties
On the
of masking color components... Ao62/Alol
then being shown by the oxy-group In the position 4. Electronegative substitu-
tion agents in the phenylazo-group of masking pale blue components cause a sharp
decrease of the activity, and In the case of derivatives of 3-alkylpyrazolone i
they may show also a favorable influence. Some of the obtained compounds may be
employed for preparing negative and contratype masking color notion-piature ma- i
terials. It is shown that arylAzo-derivatives of 3-alkyl- and 3-RcYlamino-
pyrazolone usually absorb the light of the blue-violet range (maximum. of absorp-
tion 40o - 420 mu). The entry of strong electron donor substitution agents into
the phenylazo-group causes an appreciable deepening of their coloration. The
absorption spectra of the masking pale blue components of the derivatives of
1,2-o~vjnaphthoio acid include the blue-vialet and partially the green portion of
the spectrum and in many cases they consist of two bands whose relative intensity ?I
may change strongly according to the nature and position of the substitution
agents in the arylazo-group. A particularly sharp inorease of the absorption in-
tensity In the blue-violet range takes place in the case of 2-methyl- and 2-
-chlorphonylazo derivatives. It is established that the majority of the Inves-
tigated masking purple and pale blue components at PH 5 are, as a rule, stable
enough In respect to solutions containing forrocyanic potassium. In alkaline
leaching s?lutions their stability strongly deoreases.
Abstraoter s note; Complete translationj
t
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J

An4016108 BOOK EXPLOITATION
GurarLy, 0. Z,;
Structure of the earth*e crust by geophysical date (Stroyonlys
zemnoy kory* po geofizicheskim danny*m). Hoscow, Ind-ve AN SSSR,
63, 0125 V, illus., biblio., fold. maps. 2000 copies printed*
Added t.p.t in English.
TOPrC TAGSt geophysics. seismology, gravineCryp isostAfYo crustal
structure
PURPOSE AND COVERACEC This publication is intended for Xeologistsi
geophysicists, and other scientists Interested in the structure,
nature, and methods for studying the earth's crust. Seismic data
from Soviet and Western sources were analyzed and compared with
gravimotric and orographic data to establish a correlation between,
them in, order to gain better understanding of the vature of the earth' 9
nantle, A study was also made of the different densities of the
crust using seismic data which indicate that the density pattern
varies horizontally, especially under oceans# This cLicusetasce
jCarJ 1/4
S/

AM4016108
led to a new interpretation of toostasY, though the available date
still roughly indicate the validity of Airy's origin4l.theoryo
oceanic segments differ from each other in that th*,PacL(Lc floor
contains a continuous layer of basalt, whereas basalt to found In
i the Atlantic only near continents and islands. This,papor pro-
sents an initial eflort to classify the major structures of the
I Earth's crust according to geophysical and orographic character-
istics.
TABLE OF CONTENTSt
Editorial note -- 5
Introduction -- 13
Ch. I., Analysis of data used 15
1. Seismic Data -- 15
2. CrovinstrLe data -- 18
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Z!

AM4016108
Ch. 11. Comparison of saismict gravinetric, and topographic
data -- 22
1, Craphic method -- 22
2, method of analyzing velocity in stratigraphic CGIMMINS
Ch. Ill. Differences in crustal structure of oceanic basins
Ch. IV. Types of crustal structure 62
1. Oceanic crust -- 67
2, Continental crust -- 70
Conclusion -- 73
Appendix 1. Summary of data on the structure and thickness of the
earth's crust obtained by highly accurate **ionic methods -- 75
Bibliography 122
Appendix 11so Cravinstric maps of Vestern and Central Burope
Cond 3

AM4016108
Appendix Ilb. Central, East, and South Asia, Africa$ and Australia
Appendix Ile. North. Central,'and South America (t4ith Soiguer and
topographic corrections)
SUB COD31 AS SUBHITTEDt 30Nov63 No Itar 5'~Vl 047
OTHZRv 108 DATE ACQi Miy64
Card 44

L 1913-65 PWT(m)/FXP(j)
- 941)/kSD(t)/RAM(t) JU
ACCESSION NRi AR4039920 9/0058/64/000/004/DI16/DI16
SOURCE: Ref. zh. Piz., Abe. 4D894
AUTHORSs Solov'yeva, 1& &.1 Tkachenkot.T. 0.1 Guseva, As 00
TITLEi Research in the field of azomethine qyex~ V1. Asomethine
dyes derived from 2-acylaminopyrozolones
CITED,SOURCE: Kinotekhnika.- Nauchno-tekbn. ob., vy*p.-4, 1963,.,-,--
7~
103-116
TOPIC TAGS: organic derivative dye, photographic emulsion, color
film, sensitivity increase
TRANSLATION: A large number of azomethine dyes (AD) have been sensi-
tized. These dyes are the color producing components of multilayer
color films, and are of the class of derivatives of 2-acylamino-
pyrazolones (5) with different acyl residues in the amino group. The
Card 1/2

L 6913-65
ACCESSION NR: AR4039920
photographic and optical properties of these azomethine dyes have
been investigated, along with some properties of dyes obtained from
them by color development (absorption spectra and stability). The
introduction of the acyl residue into the amino group of the AD deep-
ens their color, particularly in alcohol solutions. The absorption
of the AD in gelatine emulsion is characterized by a hypsochromic
shift of the absorption maximum compared with the alcohol solutions,
and by a simultaneous broadening of the entire absorption band. Many
investigated AD from the I-aryl-3-acylaminopyrazolone series are
quite active under color development and form highly stable dyes.
The latter pertains also to AD from the series of 3-,N-alkyl (aryl)-
N-acylaminopyrozolones, but unlike the preceding series these AD
have a small reactivity. Bibliography, 21 titleso A. Kartuzhanskiy.
Card 2/2

S9LOVIYEVA, I.A.
-1 . ... .. --- - -
Develoinent of tho afferent Innervation of the esophagus In
chicks. Arkh. anat., gist. i embr. 49 ne.9:64-70 S 165#
(MIRA J&12)
1. lAboratorlya morfologli (sav. - chlen-korrejapondent AN ISUR
N,G,xoiooov) rnatituta flziologii iment 1.1P.Pavlova AN SSSR.
Submitted November 5, 1964,

s 01A) "I, I Y '171 li~ A Ii a A 0
Develumint of the npiratua anf,,, syna;tl-: r!onzecticnm of
the p5ripher-al neurcna in the chick, Lokl. M S:-Lh 158 no.5sJJ93-2196 0
'04. (?'.IRA 17110)
1. lnp*Jt.ut rizivicgi. lmd '..I'.Nv2rva AN SSSP. Prads#Avlana akademikom
V.N.Cherrilgovakim.

wahm*ftit dotermloAdoa of Wei"" to SOW-r. ic
Zil
ALI
~54~16.4
foat. ZAIWT -A mimplified'
method for mobtute iktri CA -ult, 0111,NIV 0 dtmuon~
with Iodine-ppidlue WAD. IMitaltil V.111 1;110 '1k Ori
GOSS&M. 111C049, 1914W 19U) *41hvAt ..'I'lme'llrAll
or blank ttst Is dmxWed. 11 the M(Mtum v-11(ent >ITO,:
&PPrUx. 0.4 ff. tAl the adt is glircctLv juv,I slowly titrated WM
the itAin"yridine &AD. Until the "U. Ovff the ppt. chAnces
from Yellow to re4dish brown. if the ori6lure "te*V