SCIENTIFIC ABSTRACT STEPIN, V.I. - STEPINA, V.

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SCIENTIFIC ABSTRACT
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I I/ - " , 'f",I., ,- GR,ttS1iCiU;11KOV, 11.1.; STi!,'PIN, V.I. PathophyRiological analysis of patients with periodic attackn of prolonged sloop. Zhur.nevr.i psikh. 54 no.1:48-51 Ja 154. (XLRA 7:1) (Sleep) 7 f NIKONOVA, O.S.; STEPIN, V.I. Unilateral lesion of the cranial nerves in tumors of the cranial base. Zhur. nevr. i psikh. 54 no.8:653-658 Ag 154. (MIRA 7:9) 1. Ner7noye otdaleniye bollnitsy imeni S.P.Botkina. M VES. CRANIAL, diseases, unilateral lesions caused by tumors of cranial base) (CRANIUM. neoplasms. tumors of cranial base causing unilateral lesions of cranial nerves) ST'"JIN) V.P.. 1 7 ~~ Drill for dril.'A= I-- -, Ful- I i nut.khc -_. 7 no.,,-3 163. (MIRA 16:10) 1. lf~irhnllnik - .1 1 ti "Itilaugoll", g. Tula. SITEPIN, V.M. (Nla) Reconditioninr of tie2 on aFl;roact, tracks. Put' i put. kho:~. 9 no.D.:10 161~. % (M!iL-' 19: 1) STEPS, V.S,,,, dotaont Ettopathogeneoia of mLlIct poiaoning of Wimp. Veterinarila 42 no.9t6l-63 5 t65. (mw iilin) 2. smipalaU=kiy cootekbniaboDko-voterinarayy iwtltuTo L 38262-66 E'~IIT (I )/T JK ACC NR: AP6028649 XUT'01i: StoDin V. S., (Docont) 0;', G :Sordpalatinsk Zootochnical-Ifetorinary Institt~:t',o (3onipaa"Uns;-dy voterinarn,yy institut) TITL~: Localization of antibodioPin vaccinate-. aiLinals and in aniz-als viti, bracollosis SOU.,",G:,-;-. Votorinariya, no- 5, 1966, 13-15 TOPIC TAGS: antibody, brucellosis. blood, eirculatol-3r tiysten, aninal, vaccine ABST2,ACT: Vaccinated animals differ from animals with brucallosis V:IAL"h respect to the antibody content of various lymphoid organs, Vacoinatedanimals have a high titer of antibodies during the first 3 weeks only in the regional lymph nodes, after which all the lymph :nodes'oontain antibodies in a low titer (1:20) or none at all. .They can be found only in the superficial cervical nodes. Siok animals with a hiZh antibody titer In the blood have large quan- titios of antibodies in several lymph nodes, generally in the superficial 1riguinal and pelvic nodes. A Zather high antibody titer Is occasionally found in the mesenteric and other lvnph iqq4es, spleen, and In udder tissue. Card 1/2 uDc: 619:616-981-55-097.2_17:636.3 L38262-66 ACC NR, .The nature of the serological reaotion in the lymphoid organs'Is helpful in evaluating the degree of their involvement In the vac- einal process. The presence of iantibodies In the ingu'=3 and pel- -vic nodes of sick anina"s can be used as a supplementary method of .differentiating bruaellosis in animals scheduled for slaughtor. OAg- art. has: 1 table. Dh S: 36,9327 SUB CODE: 06 / SUBM DATE: none Card 2/2h,ie,,-,~ ~X_CC _WR1*-iP602ql86 SOURCE CODE: u~/6016/6~/O-oc)/00-5/C-6j/6(*81 AUTHOR: Stepin, V. S. ORG: _~jMpalatinsk Zooveterinary Institute (Semipalatinskiy zooveterinarnyy institut TITIZ: Significance of the regional Ipph mcd9o in immunogonesis in rabbits vaccinated with dried live brucellosis\Vvaccine~q SOURCE: Zhurnal mikrobiologii, epidemiologii i imunobiologii, no- 5, 1966, 93-98 TOPIC TAGS: rabbit, vaccine, immunization, brucellosis, circulatory system, blood,, antibody ABSTRACT: Initial and repeated vaccinations with brucellosis vaccine from strain 19 caused a simultaneous increase in the plasma cells and antibodies in the lymph nodes. The cytological and serological changes reached a peak about the 6th day and disappeared about the 30th day after vaccination and bout the 90th day after revaccination. These changes were more pronounced in the regional lymph nodes than in the remote nodes. Resection of the regional lymph nodes 24 and 72 hours after vaccination or revaccination markedly inhibited antibody formation in the blood and remote nodes. The significance of the regional lymph nodes in immunogenesis is greater after revaccination, perhaps because of intensification of their barrier-fixing function. Orig. art. has: 4 tables. (JPRS: 36,9321 SUB CODE: 06 / SUBM DATE: O2Mar65 / ORIG REF: Oll Cord OQm son or GOP 00 100000000000 A 0000900000! 000 ::: 0000000000000 0000 0 00000000 to P. V 42 a .4 , 011`401 0 0 CPU as Tw""Al 4. It 0 AT lot eel Ife) 'UK 'jj 'LL Iffy 'A p of "wow OW-N! p "up Iq P-On Im (1) -,,own ic "W40 r am" p ipmaw a[ )~MA (n SMAMM WMq WW" JWO" V jMjqXIP YOM n1m oil I VILOA 96 + 10 ro"O"m "to"" Im"I C, 'I-iw/)'Xwu# *A 6A Ptm INK"walm -0 -,% AND A M IM " 'J"w4ral XDW 9 Im "M WRINIV I 118 00 0 0 : 00. 0 0. 0 41" 00. 00 so t I Is ts ft It IS 4 4 S I I I aANALAA-MLA" . . . . . . . . . . . . . . . . . . ~ . . W . . 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O ation with KA COO 0 s , do* see **9 goo too boo A S 4 1 L A M(TALLURGICAL UTINATWI CLASWKATION 1111041 it OWv Ott 418111 *0 Oftv M a A U 16, 4 ; " 0 A , 0 d 0 1 : o 1 d" 04:4 Me o 0 a 0 0 0 0 0 o 0 0 0 0 0 9 9 * 0 0 9 e 0 0 a a 0 0 0 0 a 0 0 s 0 0 'a 0 0 * 0 0 0 0 go 0 0 0 0 0 0 0 0 0 a 0 0 0 0 & 0 0 0 o 0 0 a a 4 If 0 0 0 0 a 0 0 6 ~6 a 0 4 A . 1 1. 1 1. ~ .' 14 . A; 1; - ZI It L A 77 A I A I Ah 04 X it I 1 it t L t St IS I t 0 so 00 00 - -00 -00 00 , ," Date Lion of chrocalum in the presence of vatuadium r2 in li m r awetite ores. V. S hVIA~Hnlkll AIM V. V, 00 Sic it,. I-sh 6, GV6 91(VkI, ~ Ignit, 'I 1C S e 4 , ;r V 4%, .%Ili S x N~.ki, ths, iiiiii 1 1 It 1) 0,v 1,111.41. t hili I I J 00 *1.. *111, if,,( h-11 416% 1 't- I " 9 1 AhOllh. NVIKIA111t. tile 6111 'it %, 11 , ditntus a4l,l 2 vv. A'MI, 1,1)t Ilw Cf and % %illl Ac0),PI.. hOll 1111' 2 111111. Ond \VA'lI lite -th ' waym If,(.) and do-iolve it on lite filtri with 1-t it" , HN(h. To remcive IIIL intfIX111', 11) re. .11 . so UpSt)o, LVZt). t0 111111ing And dil. fAilh .1k, cc. If:(#. o* It the pipt. is ccilitred vsUnw, add 3 4 cc. I(SO, and v%Ap. jXain in fuming. Filter frotis PliSA)j, wj%h it with , c 00 Ak-. ituit CV81). tile filtrate it) X) 41'. vo)l. InAt Ihv .,Is j 00 fnmyg. Cr and V) ith 2Lc~ Nil,(M 1,. 04,- 1-1 f-:1wUns ,J J-rtn~ht tu'hwity 41141 then with;.'C' AOM And I C NILCL 1141(fMIU, 4.- quickly P. '-", c- J Nil, at,- -In. and I-d Kently for 20 Intil. W4-h Ow Iflit. 11, IIIIK~ With 114-t ItO I CIMIX. '-' kV. ALMI And ~.' cc. i,f iti(,c go Nil. 61171tule %An. ill I"VOP lite l"Itrat, to 'Of 0.01 00 00 .4 .. fillor Miltain it 14'. pin 0. It-- 11 div Ow fill.-t . with flit 1111I.. ithith-vit" it. 11(ifit, .,( 1b.1 I'MINP, f.w ~Ivf 1.00 00 wt-ilth Anti iftt. C'.1 .00 00 - A 0 00 too 0 0 r I IF A I - 6-~-S I I 'JA I IN 64 t it ;X11 1 3 4 I'll KO 'Its" 111-9-11 0 0 0 0 0 0 : 0 0 0 0 & : 10 : : #A4 0 0 & 0 Ill v 0 0 0 0 0 0 0 0 0 0 a 0 0 0 0' 0 . .- - ; W, I u CTII 1111 if u a ilea* ?Lw $ CPO a 41 11060 s n &~C D'FGMSL~m 11- A- L C 3- - , Ov 04 Go, ow 00 It 000 00 0 v 11 so Vgo OOP c, 0 r so l 64F 00 I'l " top q 1 00 l l% t 1ur 0 4r l lixwl~lulj Vilve itrull 1 UIV ~10-i , 1 1 " 00 ' M . 1 14, 11 u o0 00- P, .1irt-Ilf r"j. mjlurjqIUqAtj,)q(l '1 1 U I a l - JrPrUrA 13 11.N V qli" be N, U! -.1 Ali) fit'41,111 00 111 ' 130,11 go; "WO o o , l p mrwapmpu xqa WOPWUVA g 1 00 00-1 00 a or go T it )5 0 W -T-'1 T- A ' AA I I1 5 J if 1 to '630 it 7, . v d if ft q a rl R if 11 , 1 9 '? Of 9Ill n II I at m Imill "IA"(11111 a I I d I I I I 1 0 -4k A 940 9- ~"A o Do ego* lego is o 0 0 0 0 0 a - . - . a a III a v v w - : A_dL_ -4- ~ _11 AL -,t& -A -A A At &A a -1111 11 . 4-10- AA a CL 0 t1,6 t. I A A L IN, L-1 -Q--A J--JL k 00 00 DoWnbatim d MobMmum MA IM so 1AIRWISlawl'i)-il. 111311. No. M. jilo, 71011 WN9.7-rm-Runnian). Molybdenum in mlutN,l Nip llso In-iiinvalent, jitatt, by mervury in hydrochloric arid molution. After filk-ring 14) remove file surmury ;nd Hsi(%. the filtrate in jo-idifirel %ith nul. Phuriv avid to give a 7N concentration of mulphuric avid anil then l t it Weil % it h A it) lilt illiI311% V01101111,1111tV, M)IlktiOll V()"--+ 411- MA).'-+ Vo. :11,41. 0o at 11hen-0 anthranilic acid is Named " indicator. Vitivulintri doe" n,,t COO 00 ititerIt-re with thii determination. Klir determining immall amounts reo of phoilliboms in orm, iron, siml. ferro-alloyo, &I-.. lilt, amprujilt- in 00 a 0 diiisplyipill, the molution id oxidised with llivrmaiwaitate. anti the %0 phomilkhorum in pimmipitated with amnumdum molv6late reagent. Vo After StAll(li[W. the is RUCIMI Off And dimmolvetil in goo VilliffIfIllill. thin molution in aritliflion! with hydrochlorie pit-id anil the mi-10piltinnin in sh-Irrimint-41 INNIN dem-filivil above. 'goo ji too oil too Lorfoari,mg CLASIMPICATION t IF W0 p, I W S. ON 'iIIN a NIP 11 V 4111 glans 9,111119 IN of KWaI 00000 1" 0 0 0 0 0 0 0 0 000 0 a 0 0 0 0 go 00,000 see000Ole **go goo o00 60 00 *Zile ?1P ~111ft I I I I "a 4: ,;;-o 0 R. I T 4 -T!CL 0 pit .0 1 1 L-S k A A L I k A j I a ft _11~11U-19-!~L 2EFIVI.J. 011f -00 -00 so go VANADOMITRIC EMOD OF MK=UNING 11011 19 FlUO-VAUDIUM& 066 T. V. Stson and N.V. muso ya. (Zaveddop lamberatorlys, ~06 OSC-Noa, P. 861). (in Russian). iron In ferro-wsma4lum -00 00 can be determined without first seWating Uw vanadium, by '00 0 titrating with &~monium vansdato using phenyl anthrantlic 0 sold us an indicator. The iron is previously reduced to the =00 : divalont state by treating the solution with hydrogen -00 sulphide. nee 00 06 Nee ve dog, off Nee Wes S OTALL-I.KAt L#TtQATLA1 CtASWWATICK 'DID Wee . .. . . ........... 0 IN 5 A a30 9 u t$ FM M a it 19 -0 9 0 0 0000 0 00 0 0 41see 0 0 0 0 0 0 0 1 0 00 0of 0 0 0 4 *79 g 9 'Moo =o 4 - U ~4 it IS 4 ts If 3 10'.'1 a a U 1% :6 IT A A S L a -1 -J f.- M A-A --I A P. r I T. I -'~ -,y 7 1 -A PC 'IC LV A Determin4don of wan4dium In c4st Irons and A the aid of f.plikesylaminewsloic add. V, 41"'J'Aaw A. a. Ikkill P-1 henj &IV ruic acid was successfully used &4 an indicatot in -phenanthtoline in dctg. V in cast irons and slag I udwalor is ornful I ve enough for t be detec t mm of 11, ~ Z. KA 00 06 00 9 V 1, M I, V S V4 V 4; Aj .1 a a -~-oo a with 0 ICIIIII. hAwn- red of The I, V. 11, h W W -.~W W ii, I** i 00 00 00 -00 I I L A &(TALLOGWAL LIT146IL49 CLASSIPKATICN 00 8 00 t -03 -1 .1, A., , I rlv or1w 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 Is 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 STHPIN, V.V. The Laboratory of Standard Specimens puts nev spectrum analysis standards on the market. Izv. AN SSSR.Ser.fiz.19 no.2:178-179 Mr-AP 155. (KLRA 9:1) 1.1-aboratoriya standartnyl,-h obraztsov pri Urallskom institute metallov. (Tartu--Spectrum ^nalysis--Congressas) STXPD1, V.T.; SHAYEVA, Te.V. Gravimetric analysis of tungsten in concentrates arA In steel alloys. Zav.lab. 21 no.2:149-151 155. (mLRA 8:6) 1. Ural'skiv institut chernykh metallov. (Tungsten) (Metallurgical analysis) STICPDJ. Va. Production of new standard specimens and spectral standards. zav. lab. 21 no.3:381-382 155. (NLRA 1,3:6) 1. Nachallnik Isboratorli standartnykh obrastsov. (Spectrum analysis) Category: USSR/Analy-tical Chemistry - General Questions. G-1 Abs Jour: Referat Zhur-Khimiya., No 9., 1957, 30949 Author Stepin V. V. Inst Urals-Tn-sfi-t-ute of Ferrous Metals Title New Standard Specimens and Spectral Standards Orig Pub: Zavod. laboratoriya, 1956, 22, No 11., 1391-1393 Abstract: A review of the work, during 1955, of the TAboratory of Standard Specimens of the Urals Institute of Ferrous Metals, relating to provision of new standard specimens for checking chemical, po- tentiometric and photocolorl tric methods of analysis, and of standards for spectral analyses. In addition to descriptions of new series of standards, there are reported the results of their study from the standpoint of the effect on magnitude of error in analysis of "third elements" and of the structure of alloys. Card 1/1 -25- 66558 SOV/81-199-15-53184 Translation from: Referativnyy zhurnal. Khimiya, 1959, Nr 15, P 130 (USSR) AUTHORS: Stepin, V.V., Pliss, A.M., Silayeva, Ye.V. TITLE: Methods for Determining Admixtures in Vanadium Metal. Communication 1. PERIODICAL: Byul. nauchno-tekhn. inform. Urallskiy n.-I. in-t chern. metallcv, 1958, Nr 4, PP 103-109 ABSTRACT: A photometric method has been developed for determining P in vanadium metal in the form of a blue phosphorus-molybdenum complex with preliminary separation of V on a H-cationite filter. For increasing the sensitivity of the method extraction of the blue complex by butyl alcohol has been applied. The method permits the determination of small quantities of P with an error of *~' 0.0005%. A photometric method has also been developed for determining Si In vanadium metal in the form of a blue silicon-molyb- denum complex with preliminary separation of V on a H-cationite filter. It has been established that for the preparation of the blue conplex it is more expedient to apply r,,ohr's salt as a reducing agent; the error of determination is � 0.0075%. The gravimetric method for determining Si in Card 1/2 vanadium metal which is based on the separation of a gel of the silicic W 66558 SOVAI-59-15-531821 Methods for Determining Admixtures in Vanadium Metal. Communication 1. acid In it :juiruric, ,cj,j joitAtion Ii.-in boon wtdij iijora procInti. Tfit) priotomettrIc f"Ortfilyl for dr.-termilntng fo, In thr.- Corm of a blue arq#,.,n1c-molybdenum complex with its ;relimlnar-I separation by distillation has been made more precise. With the aim of increasing the sensitivity of the method, extraction by a mixture of butyl alcohol and ethylacetate has been applied. The method permits the determination of As writh an error of t 0.0002%. Authors' sumnary. Card 212 T Hcri_; Stepi n, V, Ponosnv V ~ I.. SOV/32-24-8-7/45 7T1 V, a I ~ky e V~~ %, 1 11, 1 Tho Separation of Trace Amounts of Bismuth, Cobalt, Nickel, It-on, tind Coppor Using lonites (Otdeleniyo malykh kolic~iestv vismuta, svintsa, kribalta, n1kolyn, l'ottroret, zheleza i medi s pomoshchlyu ionitov) PERIODICAL: Zavodskaya Laboratoriya, 1958, Vol. 24, Ur 8, PP. 934-938 (USSR) ABSTRACT: In this paper-chromatographic methods are described for sepa- rating the above metals in the analysis of nickel and nickel alloys. The separation is based upon the difference in the stability of the complex compounds which these elements form in concentrated acid solutions. In 8n hyd1rochloric acid these complexes are adsorbed onto the anionite, and with sub- sequent elution with 4-0.5n hydrochloric acid the less stable complexes of cobalt, copper, and iron are destroyed and com- pletely desorbed. Lead is desorbed with a 0.02n hyd:f-achloric acid solution, and bismuth with a 2n sulfuric acid solution. To separate out phosphate ions "vofatit P" and anionite e SeDaration of Trace Amounts of Bismuth, SOV/32-24-8-7/43 ~obajt. Nickel, Phosphorus, Iron, and Copper Using Ionites type: AN-2F ' and TK were used. The latter were used in the Cl- form, and the cationites were used in the H'~' form. An analytical procedure is given which employs data obtained by N Aellson ani Krause (Ref 4) in their investigations on the degree of adsorption of lead, and which can be us43d for the det,n!rmination of iron according to the ion exchange method of D j, Ryabchikov and V,Ye. Bukhtiarov (Ref 9). The separation of the iron and copper fractions in the method ju.-;t referred to was not successful, and the probable cause of this failure was the variable quality of the anionite used. Also mentioned are the attempts of .1ur and Kraus (Ref 5) to selectively elute nickel, manganese, cobalt, copper, iron, and others, in this order, from the anionite. There are 5 figures, 6 tables, and 12 references, 10 of which are Sovir-t- A I A T I ON: Ural i,, institut chernyk'-, riotallov (Ural Institute for FL-rrous Metals) Card 2/2 SOV/32-24-IO-66/70 A71 T;~MR: Ste;in' V. 7., TITLE: On the Issue c I- tandard Samples and Spectral S,;andards (0 vypuske otandartnykh obrazt-,~,v i spektralInykh etalonzv) PERIODICAL: Zavodskaya Laboratoriya, 1058, 71o1 24, Nr 10, pp '2014-129A (USSR.) ABSTRACT; In the laot two years the laboratcry of the insti-ute mentioned under Association has considerably extended the nomenclature of the standard sampies and standards. The following standard samples ,%rere issued: Carbon steels with 0,022,d- 5, 0,033,d- P 0, 12~-Q` C, 0, 64;0 C, I 05'/"o C, alloyed steels with 0,46% C, O;i7% 1 , 1 11 i'~ Cr, 0, 1 O~. Cu , 0, 1 7;.' c, 0, 68~4. Mn, 0 ~ 105el- P, 0, 115% 3 ' Si. 23' 0,13' C and 0 0,`4% si, 0,42% Lin, 3 ;0 24,6% Cr, 0,22% Ili, 1 , , , 7 'A 1 9,080 Mn, 0,57-" S; 11% Cu and 0,275 0,18%. C, ~io ~) 0 70- 5 ~ i , ; 0,11% Cu, 4-~fo Ni. and 12, 0/,"jo' Cr, 0, 16%; C, 1,25'% 'Mni 0,72% Ni, 2 0 3:'~~ Cr , 13,13% --'.i and 0,12lic' C-~; C,38% C, 0,4%1 11,11n, 2,27% si, Q 2; 0, 18io IN and O,Mf Ma. A number of othEr standard Cr, oamrles are also given with,)ut mentioning their compositions. By the ~,nd of 1958 the iss-,,e of steel samples of the following composition is Planned: 0,20-4 C, 0,40;~ Mn, 0,32'i~~ S4; O,IB% '~ai' Card 1/2 0,43~'- Illo, 'N ard 0,757'0' V- Some data on the w,,-rking program SOV/3 2-24 -10-606/70 On th,~ issue -,f Standard SamPles and Spectral Standards of thi3 laboratory are given, and the is3ue of a nimber -f spe~-,*Iral standards with bc-ron, 75PC~ ferro5ilfcon, ::Iiicomanganese, cast iron ("processed" with magnesium), tungst,;n str-~;ctural s t c,- 71 and -?.romium;--nickel steel is mi-ant:.cned. ASSOCIATION: Labratori~,,-t ur~-11 Scli~~n' i('f- Card 2, 2 /2) AUTHORS; Petukhova-, N. I., Kurbatova, V- 1.1 SOV/'42-25,7-13/50 Stepin; V. V.,. Ponosov, V. I, TITLE: News in Brief (Korotk4-ye soobshcheniya) PERIODICAL: Zavodskaya laboratoriya, 1959, Vol 25., Nr 7, P 806 (USSR) ABSTRACT: 9~ 1. Petukhova, V. 1. Kurbatova, V. V. Stepin ant[ V. I. Ponosov describe a method for the colorimetric determination of tantalum in crystalline silicium; in the absence of titani- um, iron molybdenum and tungsten. Ta is separated from Ti, Fe and Ylo by precipitation of the latter with phenylarsonic acid. The separation of Ta from W takes place by means of a precipi- tation of --opperon. The final determination of Ta is carried out colc-~imetrically according to the pyTogallol reaction. V, I. Kurbatova (Uraltskiy institut chernykh metallo- - Ural Institute for Iron Metals) suggests a method for the determina.- tion of aliminLIM in manganese ores. The method is based upon an electrometric and compensation-free titration of Al with a solution of sodium fluoride (or ammonium fluoride) in a mixture of acetate buffer,, Within the sphere of PH 3-5 well reducible results were ashieved. V~ V. Stepin and V, I, Ponosov ( 'Ural'.- Card 1/2 skiy institut cherriykh metallov - Ural Institute for Iron NPWS in Bvief SOV132-25 -'1 -13/50 Metals) describe a methcd for aeparating small amounts of lead from molybdenum by means of a weakly alkaline anion exchanger M Lead is adsorbed from a 1.5 - 2.5 n salt solution, while molybdenum rema4na in the solution, The method can be applied to the analyeis -.f ferromolybdenum, Lead is determined acc~rd- Ing to the d"Athizon method. The granulation of the anion ex- ,~~hanger is found to be 0.39 * 0-45 mm; the rate cl' flow of the solution 4 .0 - ', .2 ml./min. There are 2 Sor_~O referenees. ASSOCIATION. Ural'.akiy ins'r-2.ttr; shernykh metallov (Ural Institute for Ferr-us Mletal 9) Card 2/2 VflfJ111Y Vavil'Yovich; )'ILAYEVA, Yalizavota VnBlllyovnaj PLISS, Anaotaoiya M1khfjylo-nvj; KURBATOVA, Vora Ivanovna; KRYLICHKOVA, Lidiya Yerkurlyevna; PONOSOV, Vladimir 11lich; DYMOV, A.M., doktor khim. nauk, prof., red.; FEDO;iOV, A.A., st. nauchn. sotr., red.: TFACTE!;K0. N.S.p inzh., red.; DOBRZHANSKIY, A.V.j st. imbp.red.; LEVIT, Ye.I., red.izd- va; ISLIZITIYEVA, P.G... tekhn. red. [Analysis of ferrous metals, alloys and manganese ores] Ana- liz chernykh metallov, splavov i margantsevykh rud. (By] V.V. Stepin i dr. Moskvaj Metallurgizdat, 1964, 498 p, (MIRA 17:3) 1. TSentrallnyy nauchno-isoledovatellskiy institut chernoy metallurgii (for Dymov, Fedorov, Tkachenko, Dobrzhanskiy). Slill.'1AER", "Fedor Xikhaylovich; %Fas-iliy - - -, -------- . - "A tL- - -- . -,~L', Li u , ~, , , . . - . S .- ed . (Ion exchange chromatography in the analysis of metals] lonoolnemnyi khromatograficheskil analiz metallov. Mo- skva$ Votrillurglia, 1965. 295 p. (MIRA IS.-4) L 5872'0-65 PIT(M)/E-'/IP(t)/EVIP'(b)/EWA(h) Peb JD 'AH5016M BOOK EXPLOITATICK S/ /7 Shemyakin, Fedor Mikhaylovi.ch; Stepint Vasilly Vasilevich 13 f/ Ion-exchange chrcmatographic analysis of metals (Iono-obmannyy khromatograt'ichs- skiy analiz matallov) Tzd-wo "Metallurgiya% 1965. 295 P., Mus.,, appehd, Errata slip inserted* 4832 copies printed. Editort I* Fe Kharlamov; Editor of the publishing houeet 0a M. Kamayevaj Tecr ical editort Le Ve Dobuzhinskaya TOPIC TAGS: chromatographic metals analysial ion exchange chromatography PURPOSE AND COVERAGE: ThiB book waa intended for specialists in analytic-chemical central and shop laboratories, for engineers in the metallurgical and Machine- building industries, and for personnel in scientific-resoarch institutes slid higher educational institutions. The book is presented as a laboratory marual for metallurgical plantse Basic theoretical positions In ion-exchange chromatcgraphy are presented, sorbents used am listed,, and their selection and standardization describtd,, well *&.the apparatus used, the techniquej and the application are as Card 213 .L 58720-65 "5016971 of ion-ioxchangs chromatography in metals analysis. The Introduction was ;rit*ta,n* by Professor A. Mo Pymov, Doctor of Chemical Sciancea, TABIZ CF CCNTENTS: Foreword 7 Cho Is Brief presentation of the theory of chroaatographic analysis M 11 Ch. 2. Sokbents used, their selection and standardization 116 Ch. ). Apparatus and equipment used In chromatography. TaahnRps - - 154 Cho 4. Application of ion-exchange chromatography in metals analysis - - 166- Ch. 5, Preparation of ion-exchange reavahts-and standard solutions,, sorption# and desorption - - 224 Ch. 6, Methods of analyzing 2!K! mazzals and alloys with the application or Ion exchange 235 Cho 7, Methods of analyzing ferrous-dotal &1~qys with the application of Ion exchange - - 271 Appendix 289 Carcl 2/3 L 5872C~-65 AU5016871 SUB CCDE: UK OrHERt 111 Card 3/3" SUBMIrTED: 29Jan65 DATS ACQt 03Jun65 YR IMF SOV: 168 STEFIN, Va~iiliy Vasillyevich; SILAYEVA, Yelizaveta. Vasillyevna; KURBATOVA, Vera Ivanovna; KHANOVA, Tarra a Filaretovna,- h9tBASH, Tatlyana Llvovna; FONOSOV, Vladimir Illich [Analysis of nonferrous metals and alloys] Analiz tavetnykh metallov i splavov. Moskva, Metallurglia, 1965. 187 p. (MIRA 180) L 61049-~ Z4TW/M(m)/W(t)/ZdF(-b) --LIP(c)- ACCESSION NR: AT504249 116VIRN"100010001009310P9 5- AUTHORSt Stepin, V, V,j Ponosolrj Vo Lj Mellchekovaj Z Y TITLEz Investigation' and development of methods for the determination of Zn in heat-resistant and magnesium alloys and of Pb,, Zn,, and Bi in metallic vanadium with the application of ion-exchange chromatogrUhy < SOURUE4. AN SSSR. Institut fizicheskoy h-himilMo, emaya tekhnolof~qa (Ion exchange technology), Moscow, lzd-vo Naukaj 965, 93-95 1 74 I TOPIC TAGS: zinc,'linc alloy, lead *~Zismuth'2 lanadium ') ~~~siup allp;!,, ion s anion excWan~q resiny exchanger, ion exchange resin, analy f, ~5.* ABSTRACT: This work was undertaken to develop f ast, simple, and reliable methods (using ion-exchange chromatography) for the determination of Zn in high-temperatule and magnesium alloys as well as for the determination of Zn, Pb, and Di in metallic vanadium. Methods for the determination of Zn in high-temperature alloys in the presence of Feo Mn, Si, Cr, 14o, V, Cu, Ti, Bi, Co, Alj, ai-A Ni, and in magnesium alloys using a strongly basic anion-exchangs resin AV-17 have been developed, The experimental error is 10% for an initial concentration of Zn 10-3 - 10-4% and 2-5% for an initial concentration of Zn - 0.2 to 1,2% respectively, i Card L- 63049-65- ACCESSION NRt AT50142h9 1. method for the determination of trace amounts of Fb, Zn, and Bi in metallic vanadium is developed* This method is based on the ion-excnange properties Of the anion-exchango resin (saturated with chloride ions)a The error in the T4 0-3 dot-efffiMation is 10% for an initial concentration of elements equal to 2 x 1 2 x lo-49 Orige arts hass 1 equation, ASSOCIATIONs none SUBMITTEDt 26Feb05 NO REF SM 005 FXL t 00 OTHER: 000 SUB CODE: r C f Card Z/Z STEPRIJ V.V. Stan6ard samplea and sy-ecimums, as it means of improving the Qualit,-- of analysis. Zav. lab. 31 no.8:915-916 165. (MIRA 18:9--) STPWO, Ye.K. Rodeuts in the lower Omur Valley. Izv. Irk.gos. protivochum. tnst. 10:122-131 152. (MIRA 10:12) (AMUR VALL&Y-RODENIA) I . I-: SOV/120-59--5-38/46 AUTHORS: Bakulin, Ye. A. and Stepin, Ye, V. TITLE: A Source for the Isotopic Analysis of Chlorine PERIODICAL: Pribory i tekhnika eksperimenta, 1959, Nr 5, Pri 138-1-39 (USSR) ABSTRACT: A description is given of' an ion swirce for tho meamure- ment of the isotopic composition of chlorine based on the phenomenon of surface ionization. The ion source was developed for the analysis of small quantities of chlorine in chlorine-containing specimens. In order to increase the number of analysed specimens without releasing the vacuum, the source was made up of four independent evaporators and ionizers fixed on a drum (Fig 1,2). The device is shown in Fig 1 in which 1 is the evaporator, 2 is the drum, 3 is an insulator, 4 is a tungsten wire, 5,6 are sleeves, 7 is a bronze plate, 8 is a glass holder, 9 is a centring washer. The evaporators were made of tantalum foil, 0.15 mm thick and in the form of narrow "boats". The ionizers were in the form of tungsten wires 0.15 mm in diameter and placed above the boats with the aid of special sleeves. Cardl/3 The sagging of the wires on heating was prevented by SOV/~20-59-5-38/46 A Sotirce J*or the Isotopic Analysis of Chlorine flexible brorwn plaftim. The spactmanx could b-i changed by rotating the glass support. Tho stilt wnn deposited in the form of a solution of 47thyj alcohol. The use of' othyl jilcohol i.-# covivonlent since it wets tantalum and the salt is deposited in is uniform layer. The wire could be heated up to 2500*C and since evaporation of the salt from the boat due to thermal radiation from the wire was small, the evaporator had to be heated independently. The evaporator was heated with a current of 2 to 3 A. Fig 2 shows the disposition of the drum, the wire of the evaporator and the accelera- ting electrode. In this figure I is the evaporator, 2 is the drum, 4 is the tungsten wire and 10 the accelerating electrode. The source can be used to study solid specimens containing 10-7 g of chlorine. Since the source is based on surface ionization, a simple mass spectrum is obtained which makes the isotopic analysis of chlorine much easier. The source can also be used for other electro-negative elements which show the effect Card2/3 of surface ionization. There are 2 figures and 3 Soviet L-~ SOV/120-59-5-38/46 A Sotirce for the Iflotopic Atinlysis of Chloi-ino ASSOC Wrr ON: Fi v. I It o- t v It Im i chosk I y I itst i ttit AN SSSR ( 11hy.4 i co-- tit chil I cik I 111-4 L I Lii til . A c . S, - , 11S'~slt ) SUBMITTED: July 29, 1959 Card 3/3 ;%cczz-'1Gu Nru AvIto4l:r6o AU211OR: Bakulin, 'Yo. A.; Stepin, Ye. V. TITIZ: Separation of hydrogen isotopes in aqueous solutions of bydrocbloric acid. SOURCE; Zhurnal fizicheskoy khImij, v. 38, no. 6, 1964, 1655-1656 TOPIC TAGS; heavy water, deuterium, isotope separation, electrical transport, transference cell, electrmigration, isotope enricbment ABSTRACT: This work describes the construction of a transference cell (Fig. I) and presents the results on the separation of hydrogen isotopes in qqueous eolu- tions or hydrochloric acid by the ionic mobility method. The 50 ca-1 cathode com- partment (1) was filled with 11C1 of the desired Soncentration, containing --V12 % deuterium. The anode compartment (2) was "l cm. -in volume and was filled with CuC12 electrolyte. The formation of a boundary between HC1 and CuC12 was done In .the central part of the column, consisting of a tube (3), 2.mm in Ala ter and -8 cm long. To improve the formation of a boundary this tube was filled with 60 - 70 microa quartz sand. Since hydrogen ions will be different in mobilities, then deuterium earicbment will occur in the boundary region* However,, the isotope Card 1/4 ,AccEssioN NR: Ap4o4176o iexchazige takes place in aqueous solutions aa follows: H*+ HDO w-- etf[20 ~~since deuterium enrichmentoccurs In the bwwAary region,, this equation AU be ;shifted to the left,, toward the Increased concentration of deuterium in water* The experimental conditions are such that the boundary between HM and CuC12 Is ;stationary with respect to the Instrument. Thererore, solvent flow takes place frm the cathode cacqxLrtment through the boundary into the anod compartment. This' ~solvent, however, is enriched with heavy hydrogen at the bouadaa7. When the CCU- icentration of RM varies from 3.2 N to 10-3 N the shift of the isotopic cogip"44-4- :of deuteriun was o.16 % and o.28 % respectively. it is postulated that this :method may be used for the study of the isotopic hydrogen exchan In acid solu- tions. "The authors express their gratitude to Academician B. P. KOUStantinov for his continual interest in this work and bin valuable discussions of the Ixesults." OrU. art* has: I figure. ASSOC=ON: rAningradskiy fiziko -tekhnicheskiy institut (rmingrad imutute of Cord_ ACCK.'3STGN NE: AP4041:160 Yr,yaic6 and Toc"010") SMUTPEM: I, 19.Jun63 SUB'CODE: '-.NP DATE ACQ: 00 FAVCL: 01 NO W SOV: 003 01MR: 000 3/4 HI(I ENCLOSVAY 01 Fig. 1 Construction of transference caU Card 4/4 I , . , t 4 , I . ~ ~ :,., . . I I I ~ . I ) . : . , . , - , : , , ? . 4 , - , ~,, , - , I -,.-I ';; ~ - -, r c ~ I I . . . . I -,:. ,'- I . 11 '~ , - --t , , ; -- I L 2496-66- FliT(1)/F-TC/EPF(n)-2/E4G(m)/EPA(w)-2 IJP(C) AT ACCESSION Nitt AP5020729 UR/0057/05/033/006/1419/1422 45 _~' AUTWOR: Dakulin, Ye. A.; Stopinj Ye. V.1 Shcherbininal V, V. PC AV,/, TITLE: Investigation of the electric double layer In a plasma _